ML16364A068

From kanterella
Revision as of 01:52, 19 May 2018 by StriderTol (talk | contribs) (Created page by program invented by StriderTol)
Jump to navigation Jump to search
Radiological Survey and Dose Assessment Report for the Western New York Nuclear Service Center and Off-Site Areas in Follow Up to Aerial Gamma Radiation Survey, Rev. 1, Appendix G: Data Validation Report, Coa 405245
ML16364A068
Person / Time
Site: West Valley Demonstration Project, P00M-032
Issue date: 12/14/2016
From:
State of NY, Energy Research & Development Authority
To:
Office of Nuclear Material Safety and Safeguards, Office of Nuclear Reactor Regulation
Shared Package
ML17006A156 List:
References
Download: ML16364A068 (616)
v • d • e


Text

Data Validation Report 405245 1%1#11 II Laboratories uLc :ai WrBmoor :rrlf The GEIL Gll'Oll.lilj> lllNfC PO Box 30712 Ctmlestori. SC 29417 2:il4Q Smge Road Charleston, SC 29407 p $43.555.8171 F 843.766.117$ October 03, 2016 Ms. Laurie Losey MJW Technical Services 15 Hazelwood Drive Suite 112 . Buffalo, New York 14228 Re: Soil Radioisotopes Work Order: 405245

Dear Ms. Losey:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on December 21, 2015. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4422. Purchase Order: GELP15-0894 Chain of Custody: NYSERDA-20 Enclosures

  • Sincerely, Jake Crook Project Manager I nm1 I llU 1111 n m llliU II gel.com MJW Technical Services Soil Radioisotopes SDG: 405245 Table of Contents Case Narrative .................. , ................................................................... 1 Chain of Custody and Supporting Documentation ..................... : ......... 5 Data Review Qualifier Definitions ....................................................... 6 Radiological Analysis ..................................................................... ; ..... 9 Case Narrative ............................................................................ 10 Sample Data Summary .................................. ........................... :16 Quality Control Summary ............ ............................................ .49 Gamma Spectroscopy Raw Data ................................................ 55 Continuing Calibration ........ : .................................. .454 Background and Efficiency Data ..................................... .458 RAD Standards Traceability ............................................. 531 Runlogs ............................................................................. 54 7 . Gas Flow Raw Data .................................................................. 549 Continuing Calibration Data ...... * ....................................... 559 Background and Efficiency Data ...... .-............................... 564 RAD Standards Traceability ............................................. 605 ..................................................................... ..... 613

. Case Narrative Page 1of614 Page 2of614 October 03, 2016 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary Case Narrative for MJW Technical Services SDG: 405245 Sample Receipt The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on December 21, 2015 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification The laboratory received the following samples: ID Client ID 405245001 HO.l.l 405245002 HO.l.2 405245003 H0.1.5 405245004 HO.l.6 405245005 H0.2.l 405245006 H0.2.2 405245007 H0.3.l 405245008 H0.3.2 405245009 H0.4.l 405245010 H0.4.2 405245011 H0.5.l 405245012 H0.5.2 405245013 REACH7.l.l 405245014 REACH7.l.2 405245015 REACH2 l.l. l 405245016 REACH21.l.2 Case Narrative Sample analyses were conducted using methodology as outlined in GEL Laboratories, LLC (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package.

Page 3of614 Data Package The enclosed data package contains the following sections: General Narrative, Chain of Custody and Supporting Documentation, and data from the following fractions: Radiochemistry. Jake Crook Project Manager List of current GEL Certifications as of 03* October 2016 State Certification Alaska UST-0110 Arkansas 88-0651 CLIA 42D0904046 California 2940 Colorado SC00012 Connecticut PH-0169 Delaware SC00012 DoD ELAP/ ISO 17025 A2LA 2567.01 Florida NELAP £87156 Foreign Soils Permit P330-15-00283,P330-15-00253 Georgia SC00012 Georgia SDWA 967 Hawaii SC00012 Idaho Chemistry SC00012 Idaho Radiochemistry SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky SDW A 90129 Kentucky Wastewater 90129 Louisiana NELAP 03046 (AI33904) Louisiana SDW A LA160006 Maryland 270 Massachusetts M-SC012* Michigan 9976 Mississippi SC00012 Nebraska NE-OS-26-13 Nevada SC000122016-1 New Hampshire NELAP 205415 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R-158 Oklahoma 9904 Pennsylvania NELAP 68-00485 S.Carolina Radchem 10120002 South Carolina Chemistry 10120001 Tennessee TN 02934 TexasNELAP T104704235-16-ll UtahNELAP SC000122016-20 Vermont VT87156 Virginia NELAP 460202 Washington C780 West Virginia 997404 Page 4of614 Page 5of614 Chain of Custody and Supporting Documentation Data Review Qualifier . . Definitions Page 6of614 Page 7of614 Data Review Qualifier Definitions Qualifier Explanation

  • A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound < Result is less than value reported > Result is greater than value reported RPD of sample and duplicate evaluated using +/-RL. Concentrations* are <5X the RL A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank B Metals-Either presence of analyte detected in the associated blank, or MDL/IDL < sample value < PQL BD Results are either below the MDC or tracer recovery is low C Analyte.has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample d 5-day BOD-The 2:1 depletion requirement was not met for this sample E Organics-Concentration of the target analyte exceeds the instrument calibration range E Metals-%difference of sample and SD is >10%. Sample concentration must meet flagging criteria H Analytical holding time was exceeded h Preparation or preservation holding time was exceeded J Value is estimated N Metals-The Matrix spike sample recovery is not within specified control limits N Organics-Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC). Quantitation is based on nearest internal standard response factor N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the reporting limit UI Gamma Spectroscopy-Uncertain identification X Consult Case Narrative, Data Summary package, .or Project Manager concerning this qualifier Y QC Samples were not spiked with this Z Paint Filter Test-Particulates passed through the filter, however no free liquids were observed.

P Organics-The concentrations between the primary and confirmation columns/detectors is >40% difference. For HPLC, the difference is >70%. U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD. Page 8of614 Radiological Analysis . Page 9 of614 Case Narrative Page 10 of 614 Radiochemistry Technical Case Nar.rative MJW Technical Services (MJWC) SDG #: 405245 Product: Gamma with Ingrowth Analytical Method: DOE HASL 300, 4.5.2.3/Ga-Ol-R Analytical Procedure: GL-RAD-A-013 REV# 25 Analytical Batch: 1596387 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 20 ,_Preparation Batch: 1596281 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405245001 405245002 405245003 405245004 405245005 405245006 405245007 405245008 405245009 405245010 405245011 405245012 405245013 405245014. 405245015 405245016 1203621685 1203621686 1203621687 Client Sample Identification H0.1.1 H0.1.2 H0.1.5 H0.1.6 H0.2.1 H0.2.2 H0.3.1 H0.3.2 H0.4.1 H0.4.2 H0.5.1 H0.5.2 REACH7.1.1 REACH7.l.2 REACH21.1.1 REACH21.1.2 Method Blank (MB) 40524500l(H0.1.1) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information Page 11 of 614 Samples 405245 001, 002, 003, 004, 005, 006, 007, 008, 009, 010, Oil, 012, 013, 014, 015, 016, and 1203621686 (duplicate) were logged out of the holding period. Samples were analyzed as soon as possible. Reporting result. Qualifier Information Qualifier Reason Analyte Sample Client Sample UI Data rejected due to high Bismuth-212 405245013 REACH7.l.I counting uncertainty. Protactiniurn-231 405245003 H0.1.5 405245007 H0.3.1 UI Data rejected due to high Bismuth-212 405245005 H0.2.1 peak-width. Protactiniurn-231 405245013 REACH7.l.I 405245015 REACH21.l.I Tin-126 405245005 H0.2.1. UI Data rejected due to Protactinium-231 405245009 H0.4.1 interference. 405245012 H0.5.2 405245016 REACH21.l.2 Tin-126 405245002 :Ho.1.2 405245003 H0.1.5 405245004 H0.1.6 405245006 H0.2.2 405245007 H0.3.1 405245008 H0.3.2 405245010 H0.4.2 405245012 : H0.5.2 405245013 REACH7.1.1 405245014 REACH7.l.2 405245016 REACH2 l .1.2 1203621686 HO. 1.1 ( 40524500 IDUP) UI Data rejected due to low . Actinium-227 405245011 H0.5.1 abundance. 405245013 REACH7.l.I Page 12 of 614 Antimony-125 Bismuth-212 Cesium-137 Europium-154 Radium-228 Tin-126 UI Data rejected due to no Cesium-137 valid peak. Product: GFPC, Gross A/B, solid Analytical Method: EPA 900.0/SW846 9310/SM 7110B Modified. Analytical Procedure: GL-RAD-A-OOIB REV# 17 Analytical Batch: 1597819 Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596281 405245012 H0.5.2 405245002 H0.1.2 405245003 H0.1.5 405245004 H0.1.6 405245006 H0.2.2 405245007 H0.3.1

  • 405245008 H0.3.2 405245009 H0.4.1 405245010 H0.4.2 405245011 H0.5.1 405245014 REACH7.1.2 405245015 REACH21.1.1 405245016 REACH21.1.2 405245013 REACH7.l.1 405245015 REACH21.1.1 405245003 H0.1.5 405245009 H0.4.1 405245015 REACH21.1.1 405245016 REACH21.l.2 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405245001 405245002 405245003 405245004 405245005-405245006 Page 13of614 Client Sample Identification H0.1.1 H0.1.2 H0.1.5 H0.1.6 H0.2.1 H0.2.2 405245007 405245008 405245009 405245010 405245011 405245012 405245013 405245014 405245015 405245016 1203625471 1203625472 1203625473 1203625474 1203625475 H0.3.1 H0.3.2 H0.4.1 H0.4.2 H0.5.1 . H0.5.2 REACH7.l.1 REACH7.1.2 REACH21.l.1 REACH21.l.2 Method Blank (MB) 405245003(HO. l .5) Sample Duplicate (DUP) 405245003(HO. l .5) Matrix Spike (MS) 405245003(HO. l .5) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) _The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Misq:llaneous Information section. Gross Alpha/Beta Preparation Information High hygroscopic salt content in evaporated samples can cause the sample mass to fluctuate due to moisture absorption. To minimize this interference, the salts are converted to oxides by heating the sample under a flame until a dull red color is obtained. The conversion to oxides stabilizes the sample weight and ensures that proper alpha/beta efficiencies are assigned for each sample. Volatile radioisotopes of carbon, hydrogen, technetium, polonium and cesium may be lost during sample heating. Recounts Sample 1203625474 (HO. l.5MSD) was recounted due to high recovery. The recount is reported. Miscellaneous Information 1. Samples405245001,405245002,405245003,405245004,405245005,405245006,405245007, 405245008,405245009,405245010,405245011,405245012,405245013,405245014,405245015,405245016, 1203625472, 1203625473, and 1203625474 were received within holding but analyzed out of holding. 1. Reporting results Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. Page 14 of 614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for MJWCOOl MJW Technical Services Client SDG: 405245 GEL Work Order: 405245 The Qualifiers in this report are defined as follows:
  • A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a Tracer compound H Analytical holding time was exceeded U Analyte was analyzed for, but not detected above the Le. UI Gamma Spectroscopy--Uncertain identification h Preparation or preservation holding tim*e was exceeded ReviewN alidation GEL requires all analyticai data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: Date: 03 OCT 2016 Name: Theresa Austin Title: Group Leader Page 15of614 Sample Data Summary Page 16 of 614 Company: Address: Contact: Project: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Eosey Soil Radioisotopes Certificate of Analysis Report Date: Client Sample ID: H0.1.1 405245001 Soil 15-DEC-15 21-DEC-15 <;lient 15.8% Project: MJWC00115 MJWCOOl Sample ID: Matrix: Client ID: Collect Date: Receive Date: Collector: Moisture: October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date' Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actinium-227 HUh -0.102 +/-0.238 0.400 0.183 +/-0.242 pCi/g MXRl 10/03/16 0432 1596387 1 Antimony-125 HUh 0.0136 +/-0.0951 0.192 0.0855 +/-0.0953 pCi/g Bismuth-212 HUh 0.431 +/-0.522 1.12 0.500 +/-0.558 pCi/g Bismuth-214 Hh 0.916 +/-0.168 0.114 0.0498 +/-0.172 pCi/g Cesium-137 Hh 0.117 +/-0.0893 0.0608 0.0261 +/-0.0894 0.100 pCi/g Cobalt-60 HUh 0.00955 +/-0.0372 0.0825 0.0343 pCi/g Europium-154 HUh 0.0399 +/-0.107 0.238 0.101 +/-0.108 pCi/g Lead-212 Hh 0.732 +/-0.122 0.0956 0.0442 +/-0.128 pCi/g Lead-214 Hh 0.954 +/-0.186 0.106 . 0.047 +/-0.190 pCi/g Potassium-40 Hh 12.4 +/-1.49 0.597 0.235 +/-1.62 pCi/g Protactinium-231 HUho 0.158 +/-0.424 0.863 0.397 +/-0.432 pCi/g Radium-226 Hh 0.916 +/-0.168 0.114 0.0498 +/-0.172 pCi/g Radium-228 Hh 0.724 +/-0.282 0.219 0.0915 +/-0.284 pCi/g Thallium-208 Hh 0.291 +/-0.0707 0.0589 0.0257 +/-0.0718 pCi/g Tin-126 HUh 0.0412 +/-0.193 0.141 0.0665 +/-0.193 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 8.85 +/-3.18 3.98 1.74 +/-3.62 4.00 pCi/g JXC9 09/26/16 1358 1597819 2 Beta Hh 20.5 +/-2.69 2.73 1.27 +/-3.93 10.0 pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOl 09/08/16 1343 1596i81 The following Analytical Methods were performed Method Description DOE HASL 300, 4.5.2.3/Ga-Ol-R 2 EPA 900.0/SW846 9310/SM 71 lOB Modified Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Page 17 of 614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Certificate of Analysis Report Date: Client Sample ID: HO.I.I Project: MJWC00115 Sample ID: 405245001 Client ID: MJWCOOI October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 18 of 614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: H0.1.2 Sample ID: 405245002 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 21-DEC-15 Collector: Client Moisture: 15.5% Certificate of Analysis Project: Client ID: Report Date: MJWCOOl 15 MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty *MDC Le TPU RL Units PF DF Analyst. Date Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actinium-227 HUh -0.00153 +/-0.182 0.337 0.154 +/-0.182 pCi/g MXRI 10/03/16 0433 1596387 1 Antimony-125 HUh 0.0263 +/-0.0863 0.177 0.0799 +/-0.0871 pCi/g Bismuth-212 HUih 0.00 +/-0.636 0.938 0.422 +/-0.674 pCi/g Bismuth-214 Hh
  • 0.922 +/-0.158 0.110 0.049 +/-0.163 pCi/g Cesium-137 Hh 0.193 +/-0.0585 0.0546 0.0238 +/-0.0591 0.100 pCi/g Cobalt-60 HUh -0.0313 +/-0.0364 0.0599 0.0242 +/-0.0391 pCi/g Europium-154 HUh -0.00507 +/-0.0893 0.181 0.0751 +/-0.0893 pCi/g Lead-212 Hh 0.710 +/-0.101 0.0796 0.0368 +/-0.108 pCi/g Lead-214 Hh 0.973 +/-0.183 0.106 0.0481 +/-0.188 pCi/g Potassium-40 Hh 11.5 +/-1.36 0.472 0.183 +/-1.48 pCi!g Protactinium-231 HUh -0.0503 +/-0.371 0.668 0.304 +/-0.372 pCi/g Radium-226 Hh 0.922 +/-0.158 0.110 0.049 +/-0.163 pCi/g Radium-228 Hh 0.715 +/-0.222 0.204 0.0874 +/-0.225 pCi/g Thallium-208 Hh 0.227 +/-0.0578 0.053 0.0234 +/-0.0586 pCi/g Tin-126 HUih 0.00 +/-0.0706 0.0657 0.0306 +/-0.0721 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 9.14 +/-3.27 3.91 1.69 +/-3.79 4.00 pCi/g JXC9 09/26/16 1359 1597819 2 Beta Hh 15.2 +/-2.34 2.50 1.16 +/-3.17 10.0 pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOI 09/08/16 1343 1596281 The following Analytical Methods were performed Method Description DOE HASL 300, 4.5.2.3/Ga-01-R 2 EPA 900.0/SW846 9310/SM 711 OB Modified Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Page 19of614 GEL LABO RA TORIES LLC . 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Certificate of Analysis Report Date: Client Sample ID: H0.1.2 Project: MJWCOOI 15 Sample ID: 405245002 Client ID: MJWCOOI October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 20of614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com. Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: H0.1.5 Sample ID: 405245003 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 21-DEC-15 Collector: Client *Moisture: 16.8% Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU
  • RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actinium-227 HUh -0.0247 +/-0.225 0.406 0.184 +/-0.225 pCi/g MXRl 10/03/16 0433 1596387 Antimony-125 HUh -0.0427 +/-0.104 0.172 0.0754 +/-0.106 pCi/g Bismuth-212 HUih 0.00 1.31 0.595 +/-0.742 pCi/g Bismuth-214 Hh 0.494 +/-0.202 0.106 0.0454 +/-0.206 pCi/g Hh 0.0702 +/-0.0581 0.0664 0.0288 +/-0.0584 0.100 pCi/g Cobalt-60 HUh 0.0242 +/-0.0344 0.0845 0.0348 +/-0.0362 pCi/g Europium-154 HUh -0.024 +/-0.124 0.242 0.101 +/-0.125 pCi/g Lead-212 Hh 0.686 +/-0.132 0.108 0.0501 +/-0.145 pCi/g Lead-214 Hh 0.961 +/-0.188 0.338 0.163 +/-0.207 pCi/g Potassium-40 Hh 10.3 +/-1.49 0.665 0.264 +/-1.73 pCi/g Protactinium-231 HU!h . 0.00 +/-0.665 0.776 0.350 +/-0.675 pCi/g Radium-226 Hh 0.494 +/-0.202 0.106 0.0454 +/-0.206 pCi/g Radium-228 HUih 0.00 +/-0.341 0.468 0.216 +/-0.417 pCi/g Thallium-208 Hh 0.291 +/-0.0831 0.0544 0.0233 +/-0.0868 pCi/g Tin-126 HU!h 0.00 +/-0.140 0.0943 0.0432 +/-0.141 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 14.2 +/-3.88 3.89 1.65 +/-4.82 4.00 pCi/g JXC9 09/26/16 1359 1597819 2 Beta Hh 16.4 +/-2.82 3.45 1.63 +/-3.64 10.0 pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOI 09/08/16 1343 1596281 The following Analytical Methods were performed Method Description
  • DOE HASL 300, 4.5.2.3/Ga-Ol-R 2 EPA 900.0/SW846 9310/SM 71108 Modified Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Page 21of614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Certificate of Analysis Report Date: Client Sample ID: H0.1.5 Project: MJWCOOl 15 Sample ID: 405245003 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty' are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 22of614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwoocl Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: H0.1.6 Sample ID: 405245004 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 21-DEC-15 Collector: Client Moisture: 14.9% Certificate of Analysis Project: Client ID: Report Date: MJWC00115 MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actinium-227 HUh 0.0199 +/-0.205 0.409 0.188 +/-0.205 pCi/g MXRl 10/03/16 0434 1596387 1 Antimony-125 HUh -0.0875 +/-0.0936 0.160 0.0703 +/-0.102 pCi/g Bismuth-212 HU!h 0.00 +/-0.967 1.23 0.559 +/-1.08 pCi/g Bismuth-214 Hh 0.897 +/-0.193 0.0954 0.0408 +/-0.196 pCi/g Cesium-137 Hh 0.256 +/-0.0754 0.0559 0.0239 +/-0.0762 0.100 pCi/g Cobalt-60 HUh 0.0043 +/-0.031 0.0671 0.0271 +/-0.031 pCi/g Europium-154 HUh -0.0493 +/-0.134 0.246 0.106 +/-0.136 pCi/g Lead-212 Hh 0.700 +/-0.1 l l 0.0876 0.0404 +/-0.117 pCi/g Lead-214 Hh 0.854 +/-0.189 0.305 0.147 +/-0.192 pCi/g Potassium-40 Hh l 1.6 +/-1.39 0.476 0.179 +/-1.51 pCi/g Protactinium-231 HUh 0.0641 +/-0.422 0.815 0.375 +/-0.423 pCi/g Radium-226 Hh 0.897 +/-0.193 0.0954 0.0408 +/-0.196 pCi/g Radium-228 Hh 0.871 +/-0.253 0.213 0.090 +/-0.257 pCi/g Thallium-208 Hh 0.193 +/-0.062 0.0592 0.0261 +/-0.0626 pCi/g Tin-126 HU!h 0.00 +/-0.114 0.104 0.0487 +/-0.114 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 13.7 +/-4.00 3.97 1.64 +/-4.82 4.00 pCi/g JXC9 09/26/16 1359 1597819 2 Beta Hh 13.0 +/-2.56 2.95 1.36 +/-3.16 10.0 pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOI 09/08/16 1343 1596281 The following Analytical Methods were performed Method Description DOE HASL 300, 4.5.2.3/Ga-Ol-R 2 EPA 900.0/SW846 9310/SM 71 lOB Modified Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Page 23of614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: $oil Radioisotopes Certificate of Analysis Client Sample ID: H0.1.6 Project: Sample ID: 405245004 Client ID: Parameter Qualifier Result Uncertainty MDC Le TPU RL Units Surrogate/Tracer Recovery Test Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level '(1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 24of614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Report Date: MJWC00115 MJWCOOI October 3, 2016 PF DF Analyst Date Time Batch Mtd. Batch ID Recovery% . Acceptable Limits \

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: H0.2.1 Sample ID: 405245005 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 21-DEC-15 Collector: Client Moisture: 20.8% Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actinium-227 HUh 0.000117 +/-0.214 0.401 0.186 +/-0.214 pCi/g MXRI 10/03/16 0434 1596387 1 Antimony-125 HUh 0.0422 +/-0.105 0.197 0.0907 +/-0.107 pCi/g Bismuth-212 HU!h 0.00 +/-0.967 0.826 0.372 +/-0.971 pCi/g Bismuth-214 'Hh 0.990 +/-0.180 0.120 0.0548 +/-0.185 pCi/g Cesiurri-137 Hh 0.107 +/-0.0573 0.0483 0:0211 +/-0.0574 0.100 pCi/g Cobalt-60 HUh 0.0126 +/-0.0406 0.0799 0.0353 +/-0.041 pCi/g Europium-154 HUh -0.0362 +/-0.120 0.214 0.0946 +/-0.121 pCi/g Lead-212 Hh 1.22 +/-0.127 0.0976 0.0458 +/-0.142 pCi/g Lead-214 Hh 1.02 +/-0.179 0.122 0.0564 +/-0.184 pCi/g Potassium-40 Hh 18.2 +/-1.49 0.610 0.263 +/-1.76 pCi/g Protactinium-231 Hh 0.472 +/-0.482 0.913 0.428 +/-0.536 pCi/g Radium"226 Hh 0.990 +/-0.180 0.120 0.0548 +/-0.185 pCi/g Radium-228 Hh 1.11 +/-0.340 0.188 0.0814 +/-0.345 pCi/g Thallium-208 Hh 0.341 +/-0.0925 0.0546 0.0245 +/-0.0937 pCi/g Tin-126 HU!h 0.00 +l-0.199 0.148 0.070 +/-0.200 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 14.8 +/-4.05 3.90 1.62 +/-4.97 4.00 pCi/g JXC9 1359 1597819 2 Beta Hh 21.5 +/-2.77 2.51 1.15 +/-4.19 10.0 pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep JXOl 09/08/16 1343 1596281 The following Analytical Methods were performed Method Description DOE HASL 300, 4.5.2.3/Ga-01-R 2 EPA 900.0/SW846 9310/SM 71 lOB Modified Surrogate/Tracer Recovery Test . Batch ID Recovery% Acceptable Limits Page 25of614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: H0.2.1 Sample ID: 405245005 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 26of614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: H0.2.2 Sample ID: 405245006 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 21-DEC-15 Collector: Client Moisture: 18.6% Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU *RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actinium-227 HUh 0.105 +/-0.242 0.479 0.222 +/-0.247 pCi/g MXRl 10/03/16 0434 1596387 1 Antimony-125 HUh 0.0228 +/-0.0901 0.181 0.0802 +/-0.0907 pCi/g Bismuth-212 HUih 0.00 +/-0.952 1.46 0.677 +/-1.12 pCi/g Bismuth-214 Hh 0.979 +/-0.218 0.134 0.0599 +/-0.222 pCi/g Cesium-137 Hh 0.222 +/-0.0656 0.0703 0.031 +/-0.0663 0.100 pCi/g Cobalt-60 HUh -0.0182 +/-0.0494 0.0908 0.0388 +/-0.0501 pCi/g Europium-154 HUh 0.0588 +/-0.106 0.236 0.100 +/-0.109 pCi/g Lead-212 Hh 1.12 +/-0.129 0.0991 0.046 +/-0.142 pCi/g Lead-214 Hh 1.35 +/-0.217 0.381 0.185 +/-0.224 pCi/g Potassium-40 Hh 19.8 +/-1.84 0.625 0.253 +/-2.10 pCi/g Protactinium-231 HUh 0.127 +/-0.495 0.957 0.444 +/-0.499 pCi/g Radium-226 Hh 0.979 +/-0.218 0.134 0.0599 +/-0.222 pCi/g Radium-228 Hh 1.02 +/-0.375 0.269 0.118 +/-0.378 pCi/g Thallium-208 Hh 0.455 +/-0.104 0.0555 0.024 +/-0.106 pCi/g Tin-126 HUlh 0.00 +/-0.120 0.140 0.0667 +/-0.121 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 19.1 +/-4.61 3.88 1.60 +/-6.05 4.00 pCi/g JXC9 09/26/16 1359 1597819 2 Beta Hh 25.6 +/-3.03 2.71 1.25 +/-4.72 10.0 pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOl 09/08/16 1343 1596281 The following Analytical Methods were performed Method Description DOE HASL 300, 4.5.2.3/Ga-Ol-R 2 EPA 900.0/SW846 9310/SM 71108 Modified Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Page 27of614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Certificate of Analysis Report Date: Client Sample ID: H0.2.2. Project: MJWC00115 Sample ID: 405245006 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 28 of 614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: H0.3.1 Sample ID: 405245007 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 21-DEC-15 Collector: Client Moisture: 14.9% Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 3, 2016 Parameter Qualifier Result Uncertainty MDC* Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actinium-227 HUh -0.0737 +/-0.237 0.374 0.170 +/-0.240 pCi/g MXRl 10/03/16 0435 1596387 1 Antimony-125 HUh -0.0843 +/-0.100 0.177 0.0791 +/-0.107 pCi/g Bismuth-212 HUlh 0.00 +/-0.961 1.27 0.584 +/-1.27 pCi/g Bismuth-214 Hh 0.727 +/-0.187 0.121 0.0537 +/-0.189 pCi/g Cesium-137 Hh 0.174 +/-0.0812 0.0757 0.034 +/-0.0816 0.100 pCi/g Cobalt-60 HUh -0.0108 +/-0.0399 0.0721 0.0299 +/-0.0402 pCi/g Europium-154 HUh 0.0494 +/-0.112 0.217 0.0924 +/-0.114 pCi/g Lead-212 Hh 0.722 +/-0.137 0.113 0.0531 +/-0.142 pCi/g Lead-214 Hh 0.880 +/-0.190 0.313 0.151 +/-0.193 pCi/g. Potassium-40 Hh 13.2 +/-1.53 0.626 0.257 +/-1.68 pCi/g Protactinium-231 HU!h 0.00 +/-0.837 0.756 0.345 +/-0.848 pCi/g Radium-226 Hh 0.727 +/-0.187 0.121 0.0537 +/-0.189 pCi/g Radium-228 Hh 1.14 +/-0.340 0.199 0.0837 +/-0.345 pCi/g Thallium-208 Hh 0.324 +/-0.0784 0.061 0.0271 +/-0.0796 pCi/g Tin-126 HU!h 0.00 +/-0.108 0.124 0.0586 +/-0.109 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid Dry Weight Corrected" Alpha Hh 16.6 +/-4.43 3.85 1.55 +/-5.51 -4.00 pCi/g JXC9 09/26/16 1359 1597819 2 Beta Hh 13.6 +/-2.37 2.29 1.04 +/-3.24 10.0 pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOl 09/08/16 1343 1596281 The following Analytical Methods were performed Method Description DOE HASL 300, 4.5.2.3/Ga-01-R 2 EPA 900.0/SW846 9310/SM 71 lOB Modified Surrogate/Tracer Recovery Test Batch ID Recovery%

  • Acceptable Limits Page 29 of 614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Certificate of Analysis Report Date: Client Sample ID: H0.3.1 Project: MJWCOOl 15 Sample ID: 405245007 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 30 of 614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty GEL LABORATORIES LLC. 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: H0.3.2 Sample ID:
  • 405245008 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 21-DEC-15 Collector: Client Moisture: 14.2% Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOI October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL *Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actinium-227 HUh -0.0292 +/-0.185 0.335 0.153 +/-0.186 pCi/g MXRI 10/03/16 0435 1596387 1 Antimony-125 HUh -0.0494 +/-0.0834 0.155 0.0695 +/-0.0864 pCi/g Bismuth-212 HU!h 0.00 +/-0.809 1.08 0.495 +/-0.968 pCi/g Bismuth-214 Hh 0.643 +/-0.145 0.0909 0.0399 +/-0.154 pCi/g Cesium-137 Hh 0.203 +/-0.068 0.049 0.0213 +/-0.0698 0.100 pCi/g Cobalt-60 HUh -0.0216 +/-0.0292 0.0518 0.0206 +/-0.0308 pCi/g Europium-154 HUh 0.0524 +/-0.0866 0.185 0.0787 +/-0.0899 pCi/g Lead-212 Hh 0.780 +/-0.105 0.0714 0.0327 +/-0.123 pCi/g Lead-214 Hh 0.953 +/-0.159 0.273 0.132 +/-0.177 pCi/g Potassium-40 Hh 12.2 +/-1.27 0.371 0.137 +/-1.67 pCi/g Protactinium-231 HUh 0.242 +/-0.351 0.694 0.319 +/-0.371 pCi/g Radium-226 Hh 0.643 +/-0.145 0.0909 0.0399 +/-0.154 pCi/g Radium-228 Hh 0.987 +/-0.244 0.162 0.0675 +/-0.281 pCi/g Thallium-208 Hh 0.249 +/-0.0653 0.0542 0.0242 +/-0.0684 pCi/g Tin-126 HU!h 0.00 +/-0.109 0.0923 0.0432 +/-0.111 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 15.2 +/-3.99 3.96 1.69 +/-5.05 4.00 pCi/g JXC9 09/26/16 1359 1597819 2 Beta Hh 17.4. +/-2.89 3.53 1.67 +/-3.83 10.0 pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOl 09/08/16 1343 1596281 The following Analytical Methods were performed Method Description DOE HASL 300, 4.5.2.3/Ga-Ol-R 2 EPA 900.0/SW846 9310/SM 71 lOB Modified Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Page 31of614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Certificate of Analysis Report Date: Client Sample ID: H0.3.2 Project: MJWC00115 Sample ID: 405245008 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Fador DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectabli;; Concentration Page 32of614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty GEL LABO RA TORIES LLC 2040 SavagE!l Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: H0.4.1 Sample ID: 405245009 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 21-DEC-15 Collector: Client Moisture: 22.2% Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth Dry Weight Corrected" Actinium-227 HUh -0.0177 +/-0.225 0.433 0.199 +/-0.225 pCi/g MXRl 10/03/16 0436 1596387 1 Antimony-125 HUh 0.0747 +/-0.102 0.214 0.097 +/-0.108 pCi/g Bismuth-212 HUih 0.00 +/-0.543 1.23 0.556 +/-0.659 pCi/g Bismuth-214 Hh 0.655 +/-0.176 0.115 0.0503 +/-0.178 pCi/g Cesium-137 Hh 0.286 +/-0.0876 0.0632 0.0274 +/-0.0884 0.100 pCi/g Cobalt-60 HUh 0.0109. +/-0.0331 0.0748 0.0307 +/-0.0335 pCi/g Europium-154 HUh 0.0837 +/-0.102 0.241 0.102 +/-0.109 pCi/g Lead-212 Hh 0.776 +/-0.172 0.125 0.0587 +/-0.177 pCi/g Lead-214 Hh 0.936 +/-0.186 0.307 0.148 +/-0.190 pCi/g Potassium-40 Hh 12.1 +/-1.51 0.636 0.257 +/-1.63 pCi/g Protactinium-231 HU!h 0.00 +/-0.679 0.805 0.367 +/-0.712 pCi/g Radium-226 Hh 0.655 +/-0.176 0.115 0.0503 +/-0.178 pCi/g Radium-228 HU!h 0.00 +/-0.370 0.595 0.280 +/-0.502 pCi/g Thallium-208 Hh 0.312 +/-0.0922 0.0593 0.0259 +/-0.0932 pCi/g Tin-126 HUh 0.0457 +/-0.155 0.173 0.0822 +/-0.156 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 11.9 +/-3.56 3.98 1.71 +/-4.26 4.00 pCi/g JXC9 09/26/16 1359 1597819 2 Beta Hh 18.3 +/-2.39 2.07 0.945 +/-3.63 10.0 pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOl 09/08/16 1343 1596281 The following Analytical Methods were performed Method Description DOE HASL 300, 4.5.2.3/Ga-Ol-R 2 EPA 900.0/SW846 9310/SM 71 lOB Modified Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Page 33 of 614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Losey Project: Soil Radioisotopes Certificate of Analysis Report Date: Client Sample ID: H0.4.l Project: MJWC00115 Sample ID: 405245009 Client ID: MJWCOOl October 3, 2016 *Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (l.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 34of614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: H0.4.2 Sample ID: 405245010 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 21-DEC-15 Collector: Client Moisture: 17.6% Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst
  • Date Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actinium-227 HUh -0.0539 +/-0.242 0.461 0.211 +/-0.243 pCi/g MXRl 10/03/16 0436 1596387 1 Antimony-125 HUh 0.0919 +/-0.0994 0.220 0.098 +/-0.108 pCi/g Bismuth-212 HUih 0.00 +/-0.676 1.50 0.685 +/-0.819 pCi/g Bismuth-214
  • Hh 0.796 +/-0.197 0.136 0.0596 +/-0.200 pCi/g Cesium-137" Hh 0.330 +/-0.0895 0.0763 0.0332 +/-0.0906 0.100 pCi/g Cobalt-60 HUh 0.019 +/-0.0543 0.115 0.0491 +/-0.055 pCi/g Europium-154 HUh 0.0648 +/-0.164 0.340 0.148 +/-0.166 pCi/g Lead-212 Hh 0.972 +/-0.138 0.0934 0.0427 +/-0.147 pCi/g Lead-214 Hh 1.02 +/-0.195 0.355 0.171 +/-0.200 pCi/g Potassium-40 Hh 12.4 +/-1.62 0.672 0.261 +/-1.75 pCi/g Protactinium-231 HUh 0.404 +/-0.542 1.03 0.473 +/-0.578 pCi/g Radium-226 Hh 0.796 +/-0.197 0.136 0.0596 +/-0.200 pCi/g Radium-228 Hh 0.899 +/-0.413 0.352 0.155 +/-0.416 pCi/g Thallium-208 Hh 0.209 +/-0.0971 0.072 0.0316 +/-0.0975 pCi/g Tin-126 HUih 0.00 +/-0.124 0.105 0.0496 +/-0.124 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 13.7 +/-3.63 4.00 1.75 +/-4.51 4.00 pCi/g JXC9 09126116 1359 1597819 2 Beta Hh 14.5 +/-2.54 3.02 1.42 +/-3.30 10.0 pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOI 09/08/16 1343 1596281 The following Analytical Methods were performed Method Description DOE HASL 300, 4.5.2.3/Ga-01-R 2 EPA 900.0/SW846 9310/SM 71 IOB Modified Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Page 35of614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: 'Soil Radioisotopes Certificate of Client Sample ID: H0.4.2 Project: Sample ID: 405245010 Client ID: Parameter Qualifier Result Uncertainty MDC Le TPU RL Units Surrogate/Tracer Recovery Test Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 36of614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Report Date: MJWC00115 MJWCOOI October 3, 2016 PF DF Analyst Date Time Batch Mtd. Batch ID Recovery% Acceptable Limits GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: H0.5.1 Sample ID: 405245011 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 21-DEC-15 Collector: Client
  • Moisture: 21.9% Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actinium-227 HUlh 0.00 +/-0.265 0.559 0.259 +/-0.296 pCi/g MXRl 10/03/16 0445 1596387 Antimony-125 HUh 0.0977 +/-0.121 0.254 0.115 +/-0.129 pCi/g Bismuth-212 HU!h 0.00 +/-1.07 1.57 0.716 +/-1.26 pCi/g Bismuth-214 Hh 0.813 +/-0.225 0.157 0.0696 +/-0.228 pCi/g Cesium-137 Hh 0.340 +/-0.113 0.096 0.0429 +/-0.114 0.100 pCi/g Cobal.t-60 HUh 0.0173 +/-0.0471 0.102 0.0429 +/-0.0478 pCi/g Europium-154 HUh -0.112 +/-0.149 0.247 0.102 +/-0.158 pCi/g Lead-212 Hh 1.05 +/-0.144 0.109 0.0503 +/-0.155 pCi/g Lead-214 Hh 0.894 +/-0.226 0.362 0.174 +/-0.229 pCi/g Potassium-40 Hh 12.6 +/-1.80 0.851 0.352 +/-1.92 pCi/g Protactinium-231 HUh 0.00969 +/-0.518 0.995* 0.456 +/-0.518 pCi/g Radium-226 Hh 0.813 +/-0.225 0.157 0.0696 +/-0.228 pCi/g Radium-228 Hh 1.14 +/-0.292 0.253 0.106 +/-0.298 pCi/g Thallium-208 Hh 0.331 +/-0.104 0.0704 0.0307 +/-0.105 pCi/g Tin-126 HUh .0.0211 +/-0.204 0.183 0.0866 +(-0.205 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 13.0 +/-3.87 3.88 1.60 +/-4.56 4.00 pCi/g JXC9 09/26/16 1359 1597819 2 Beta Hh 17.3 +/-2.90 3.38 1.58 +/-3.66 10.0 pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOI 09/08116 1343 1596281 The following Analytical Methods were performed Method Description DOE HASL 300, 4.5.2.3/Ga-01-R 2 EPA 900.0/SW846 9310/SM 71 IOB Modified Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Page 37of614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Certificate of Analysis Report Date: Client Sample ID: H0.5.1 Project: MJWCOOl 15 Sample ID: 405245011 Client ID: MJWCOOI 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Notes:* The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 38 of 614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes -Client Sample ID: H0.5.2 Sample ID: 405245012 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 21-DEC-15 Collector: Client Moisture: 19.7% Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 3, 2016 *Parameter Qualifier Result Uncertainty MDC *LC TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actinium-227 HUh -0.0295 +/-0.236 0.428 0.196 +/-0.237 pCi/g MXRl 10/03/16 0446 1596387 1 Antimony-125 HU!h 0.00 +/-0.181 0.202 0.0903 +/-0.231 pCi/g Bismuth-212 Hh 2.06 +/-0.633 0.768 0.326 +/-0.641 pCi/g Bismuth-214 Hh 0.777 +/-0.182 0.130 0.0574 +/-0.185 pCi/g Cesium-137 Hh 0.789 +/-0.104 0.0656 0.0285 +/-0.110 0.100 pCi/g Cobalt-60 HUh -0.00627 +/-0.0384 0.0771 0.0317 +/-0,0385 pCi/g Europium-154 fjUh -0.0502 +/-0.115 0.216 0.0895 +/-0.117 pCi/g Lead-212 Hh 1.05 +/-0.134 0.107 0.0497 +/-0.145 pCi/g Lead-214 Hh 1.00 +/-0.167 0.333 0.161 +/-0.172 pCi/g Potassium-40 Hh 13.9 +/-1.66 0.725 0.300 +/-1.81 pCi/g Protactinium-231 HU!h 0.00 +/-0.598 0.674 0.301 +/-0.629 pCi/g Radium-226 Hh 0.777 +/-0.182 0.130 0.0574 +/-0.185 pCi/g Radium-228 Hh 0.981 +/-0:360 0.179 0.0715 +/-0.364 pCi/g Thallium-208 Hh 0.320 +/-0.0776 0.068 0.0302 +/-0.0788 pCi/g Tin-126 HU!h 0.00 +/-0.123 0.128 9.0596 +/-0.124 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 12.2 +/-3.35 3.58 1.55 +/-4.15 4.00 pCi/g JXC9 09126116 1404 1597819 2 Beta Hh 17.1 +/-2.59 3.06 1.45 +/-3.65 10.0 pCi/g The following Prep Methods were performed *Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOl 09/08/16 1343 1596281 The following Analytical Methods were performed Method Description DOE HASL 300, 4.5.2.3/Ga-Ol-R 2 EPA 900.0/SW846 9310/SM 71 lOB Modified Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Page 39of614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Certificate of Analysis Report Date: Client Sample ID: H0.5.2 Project: MJWCOOl 15 Sample ID: 405245012 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are*defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 40 of 614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: REACH7.l.l Sample ID: 405245013 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 21-DEC-15 Collector: Client Moisture: 25.4% Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actinium-227 HU!h 0.00 +/-0.250 0.516 0.241 +/-0.281 pCi/g MXRI 10/03/16 0446 1596387 1 Antimony-125 HUh 0.0536 +/-0.115 0.227 0.104 +/-0.118 pCi/g Bismuth-212 HU!h 0.00 +/-1.28 1.04 0.462 +/-1.29 pCi/g Bismuth-214 Hh 0.815 +/-0.183 0.137 0.0612 +/-0.187 pCi/g Cesium-137 HU!h 0.00 +/-0.0534 0.116 0.054 +/-0.0759 0.100 pCi/g Cobalt-60 HUh -0.00756 +/-0.0409 0.078 0.0324 +/-0.041 pCi/g Europium-154 HUh -0.0163 +/-0.0781 0.156 0.0604 +/-0.0785 pCi/g Lead-212 Hh 1.18 . H-0.137 0.0966 0.0447 +/-0.151 pCi/g Lead-214 Hh 0.864 +/-0.174 0.144 0.0661 +/-0.177 pCi/g Potassium-40 Hh 13.6 +/-1.56 0.606 0.243 +/-1.71 pCi/g Protactinium-231 HUlh 0.00 +/-1.21 0.689 0.310 +/-1.28 pCi/g Radium-226 Hh 0.815 .+/-0.183 0.137 0.0612 +/-0.187 pCi/g Radium-228 Hh 1.08 +/-0.327 0.253 0.109 +/-0.332 pCi/g Thallium-208 Hh 0.284 +/-0.111 0.0641 0.0283 +/-0.112 pCi/g Tin-126 HU!h 0.00 +/-0.128 0.159 0.0756 +/-0.129 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 11.9 +/-3.37 3.93 1.74 +/-4.09 4.00 pCi/g JXC9 09/26/16 1359 1597819 2 Beta Hh 18.7 +/-2.48 2.50 1.17 +/-3.63 10.0 pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil \rep GL-RAD-A-021 JXOI 09/08/16 1343 1596281 The following Analytical Methods were performed Method Description DOE HASL 300, 4.5.2.3/Ga-01-R 2 EPA 900.0/SW846 9310/SM 71 IOB Modified Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Page 41of614 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: REACH7.l.I Sample ID: 405245013 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl .. October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 42of614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: REACH7.l.2 Sample ID: 405245014 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 21-DEC-15 Collector: Client Moisture: 15.3% Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU, RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actinium-227 HUh -0.108 +/-0.182 0.342 0.157 +/-0.189 pCi/g MXRI 10/03/16 0447 1596387 1 Antimony-125 HUh -0.0465 +/-0.0854 0.156 0.0698 +/-0.088 pCi/g Bismuth-212 HU!h 0.00 +/-0.944 1.14 0.526 +/-1.05 pCi/g Bismuth-214 Hh 0.792 +/-0.152 0.0918 0.0402 +/-0.155 pCi/g Cesium-137 Hh 0.151 +/-0.0607 0.0521 0.0228 +/-0.061 0.100 pCi/g Cobalt-60 HUh -0.00814 +/-0.0382 0.0732 0.0314 +/-0.0384 pCi/g Europium-154 HUh 0.048 +/-0.099 0.208 0.0904 +/-0.101 pCi/g Lead-212 Hh 0.950 +/-0.112 0.0726 0.0334 +/-0.123 pCi/g Lead-214 Hh 1.00 +/-0.134 0.282 0.136 +/-0.140 pCi/g Potassium-40 Hh 13.3 +/-1.43 0.581 0.243 +/-1.59 pCi/g Protactinium-231 HUh 0.304 +/-0.623 0.712 0.328 +/-0.626 pCi/g Radium-226 Hh 0.792 +/-0.152 0.0918 0.0402 +/-0.155 pCi/g Radium-228 Hh 0.718 +/-0.248 0.169 0.071 +/-0.250 pCi/g Thallium-208 Hh 0.337 +/-0.0722 0.0522 0.0232 +/-0.0736 pCi/g Tin-126 HU!h 0.00 +/-0.118 0.0986 0.0465 +/-0.11°9 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 11.8 +/-3.72 3.99 1.67 +/-4.37 4.00 pCi/g JXC9 09/26/16 1404 1597819 2 Beta Hh 17.2 +/-2.55 2.45 1.12 +/-3.58 10.0 pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOI 09/08/16 1343 1596281 The following Analytical Methods were performed Method Description DOE HASL 300, 4.5.2.3/Ga-01-R 2 EPA 900.0/SW846 9310/SM 71 lOB Modified Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Page 43of614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: REACH? .1.2 Sample ID: 405245014 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result UncertainJy MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd.
  • Surrogate/Tracer Recovery Test Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 44of614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: REACH21.1.l Sample ID: 405245015 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 21-DEC-15 Collector: Client Moisture: 29.6% Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date -Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actinium-227 HUh -0.0146 ' +/-0.280 0.475 0.219 +/-0.280 pCi/g MXRl 10/03/16 0447 1596387 Antimony-125 HUh 0.0611 +/-0.125 0.245 0.112 +/-0.128 pCi/g Bismuth-212 HU!h 0.00 +/-0.928 1.44 0.663 +/-1.21 pCi/g Bismuth-214 Hh 1.04 +/-0.217 0.162 0.0735 +/-0.222 pCi/g Cesium-137 Hh 0.302 +/-0.130 0.0861 0.0387 +/-0.130 0.100 pCi/g Cobalt-60 HUh -0.00192 +/-0.0484 0.0937 0.0399 +/-0.0484 pCi/g Europium-154 HUih 0.00 +/-0.177 0.280 0.122 +/-0.190 pCi/g Lead-212 Hh 1.17 +/-0.150 0.114 0.0533 +/-0.163 pCi/g Lead-214 Hh 1.08 +/-0.231 0.140 0.0637 +/-0.235 pCi/g Potassium-40 Hh 17.6 +/-1.82 0.632 0.253 +/-2.05 pCi/g Protactinium-231 HU!h 0.00 +/-1.43 0.883 0.404 +/-1.47 pCi/g Radium-226 Hh 1.04 +/-0.217 0.162 0.0735 +/-0.222 pCi/g Radium-228 Hh 1.24 +/-0.325 0.284 0.124 +/-0.331 pCi/g Thallium-208 Hh 0.419 +/-0.106 0.0645 0.0283 +/-0.108 pCi/g Tin-126 HU!h 0.00 +/-0.136 0.194 0.0928 +/-0.145 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 11.7 +/-3.49 3.88 1.67 +/-4.19 4.00 pCi/g JXC9 09/26/16 1359 1597819 2 Beta Hh 20.l +/-2.60 2.55 1.19 +/-3.83 10.0 pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOl 09/08/16 1343 1596281 The following Analytical Methods were performed Method
  • Description DOE HASL 300, 4.5.2.3/Ga-01-R 2 EPA 900.0/SW846 9310/SM 71 IOB Modified Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Page 45of614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Certificate of Analysis Report Date: Client Sample ID: REACH21.l.1 Project: MJWCOOI 15 Sample ID: 405245015 Client ID: MJWCOOI October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Notes:. The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 46 of 614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: REACH21.l.2 Sample ID: 405245016 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 21-DEC-15 Collector: Client Moisture: 21.6% Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOI October 3, 2016 Parameter Qualifier* Result Uncertainty MDC Le TPU RL Units
  • PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gamma with Ingrowth "Dry Weight Corrected" Actinium-227 HUh -0.00748 +/-0.285 0.526 0.236 +/-0.285 pCi/g MXRI 10/03/16 0448 1596387 I Antimony-125 HUh 0.00945 +/-0.151 0.304 0.135 +/-0.151 pCi/g Bismuth-212 HUih 0.00 +/-1.15 1.78 0.790 +/-1.23 pCi/g Bismuth-214 Hh 0.959 +/-0.234 0.178 0.0762 +/-0.238 pCi/g Cesium-137 HU!h 0.0908 +/-0.0871 0.094 0.0397 +/-0.0872 0.100 pCi/g Cobalt-60 HUh 0.0216 +/-0.0616 0.140 0.0574 +/-0.0624 pCi/g Europium-154 HUh -0.0358 +/-0.183 0.365 0.149 +/-0.184 pCi/g Lead-212 Hh 1.19 +/-0.160 0.107 0.0482 +/-0.172 pCi/g Lead-214 Hh 1.17 +/-0.221 0.141 0.0607 +/-0.226 pCi/g Potassium-40 Hh 16.0 +/-2.26 1.02 0.393 +/-2.41 pCi/g Protactinium-231 HUlh 0.00 +/-0.806 0.997 0.444 +/-0.840 pCi/g Radium-226 Hh 0.959 +/-0.234 0.178 0.0762 +/-0.238 pCi/g Radium-228 Hh 1.14 +/-0.437 0.362 0.150 +/-0.441 pCi/g Thallium-208 Hh 0.379 +/-0.121 0.110 0.0483 +/-0.122 pCi/g Tin-126 HUih 0.00 +/-0.143 0.133 0.0615 +/-0.144 pCi/g Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 16.8 +/-4.38 3.90 1.60 +!-5.50 4.00 pCi/g JXC9 09/26/16 1400 1597819 2 Beta Hh 22.6 +/-2.94 2.81 1.30 +/-4.35 10.0 pCi/g The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 JXOI 09/08/16 1343 1596281 The following Analytical Methods were performed Method Description DOE HASL 300, 4.5.2.3/Ga-Ol-R 2 EPA 900.0/SW846 9310/SM 71 lOB Modified Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Page 47of614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey
  • Project: Soil Radioisotopes Client Sample ID: REACH21.l.2 Sample ID: 405245016 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 3, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery* Test Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level . MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 48 of 614 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits Page 49of614 Quality Control Summary '

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Report Date: October 3, 2016 Client: MJW Technical Services Page 1 of 5 15 Hazelwood Drive Suite 112 Buffalo, New York Contact: Ms. Laurie Losey Workorder: 405245 Parmname NOM Qua) QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596387 QC1203621686 405245001 DUP Actinium-227 HUh -0.102 HU 0.140 pCi/g 0 NIAMXRl 1010311605:34 Uncert: +l-0.238 +l-0.160 TPU: +l-0.242 +l-O.F3 Antimony-125 HUh 0.0136 HU 0.0587 pCi/g 0 NIA Uncert: +l-0.0951 +l-0.0791 TPU: +l-0.0953 +l-0.0835 Bismuth-212 HUh 0.431 H 1.05 pCi/g 5.91 (0%-100%) Uncert: +l-0.522 +l-0.674 TPU: +l-0.558 +l-0.677 Bismuth-214 Hh 0.916 H 0.759 pCilg 18.7. (0%-20%) Uncert: +l-0.168 +l-0.147 TPU: +l-0.172 +l-0.151 Cesium-137 Hh 0.117 H 0.0935 pCi/g 22.6 (0%-100%) Uncert: +l-0.0893 +l-0.0546 TPU: +l-0.0894 +l-0.0547 Cobalt-60 HUh 0.00955 HU -0.0229 pCilg 0 NIA Uncert: +l-0.0372 +l-0.034 TPU: +l-0.0374 +l-0.0356 Europium-154 HUh 0.0399 HU -0.00679 pCilg 0 NIA Uncert: +l-0.107 +l-0.0882 TPU: +l-0.108 +l-0.0883 Lead-212 Hh 0.732 H 0.866 pCilg 16.7 (0%-20%) Uncert: +l-0.122 +l-0.106 TPU: +l-0.128 +l-0.116 Lead-214 Hh 0.954 H 0.946 pCilg .832 (0%-20%) Uncert: +l-0.186 +l-0.157 TPU: +l-0.190 +l-0.162 Potassium-40 Hh 12.4 H 12.9 pCi/g 3.79 (0%-20%) Uncert: +l-1.49 +l-1.33 TPU: +l-1.62 +l-1.49 Protactinium-231 HUh 0.158 HU 0.234 pCi/g 0 NIA Un cert: +l-0.424 +l-0.417 TPU: +l-0.432 +l-0.420 Ra,dium-226 Hh 0.916 H 0.759 pCilg 18.7 (0%-20%) *uncert: +l-0.168 +l-0.147 TPU: +l-0.172 +l-0.151 Radium-228 Hh 0.724 H 1.03 pCilg 34.6 (0%-100%) Uncert: +l-0.282 +l-0.278 TPU: +l-0.284 +l-0.283 Thallium-208 Hh 0.291 H 0.202 pCilg 36.1 (0%-100%) Uncert: +l-0.0707 +l-0.0675 Page 50 of 614 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summarl:'. Workorder: 405245 Page 2 of 5 Parm name NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596387 TPU: +/-0.0718 +/-0.0681 Tin-126 HUh 0.0412 HUI 0.00 pCi/g 33.9 NIA Uncert: +/-0.193 +/-0.0737 TPU: +/-0.193 +/-0.075 QC1203621687 LCS Americium-241 489 564 pCi/g 115 (75%-125%) MXRl 10/03/16 04:53 Un cert: +/-9.29 TPU: +/-42.6 Actinium-227 u -0.947 pCi/g Uncert: +/-3.68 TPU: +/-3.70 Antimony-125 u 0.0977 pCi/g Uncert: +/-1.62 TPU: +/-1.62 Bismuth-212 u 0.990 pCi/g Uncert: +l-7AO TPU: +/-7.42 Bismuth-214 u -0.43 pCi/g Uncert: +/-0.957 TPU: +/-0.976 Cesium-137 179. 192 pCi/g 107 (75%-125%) Uncert: +/-3.33 TPU: +/-8.89 Cobalt-60 162 159 pCi/g 98.6 (75%-125%) Uncert: +/-3.49 TPU: +/-6.82 Europium-154 u -0.581 pCi/g Uncert: +/-0.887 TPU: +/c0.925 Lead-212 0.726 pCi/g Uncert: +/-0.707 TPU: +/-0.780 Lead-214 u 0.150 pCi/g Uncert: +/-1.01 TPU: +/-1.01 Potassium-40 u -1.8 pCi/g Uncert: +/-2.12 TPU: +/-2.27 u 0.967 pCi/g Un cert: +/-6.53 TPU: +/-6.54 Radium-226 u -0.43 pCi/g Uncert: +/-0.957 TPU: +/-0.976 Radium-228 u -1.06 pCi/g Un cert: +/-3.32 Page 51of614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summar:y Workorder: 405245 Page 3 of 5 Parmname NOM Sam(!le Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596387 TPU: +/-3.35 Thallium-208 u -0.254 pCi/g Uncert: +/-0.492 TPU: +/-0.505 Tin-126 38.9 pCi/g Uncert: +/-2.11 TPU: +/-3.21 QC1203621685 MB Actinium-227 u -0.00882 pCilg MXRl l 0/03/16 04:48 Uncert: +/-0.125 TPU: +/-0.125 Antimony-125 u 0,00683 pCi/g Uncert: +/-0.048 TPU: +/-0.0481 Bismuth-212 u -0.159 pCi/g Uncert: +/-0.245 TPU: +/-0.255 Bismuth-214 u 0.0396 pCi/g Uncert: +/-0.0524 TPU: +/-0.0554 Cesium-137 u -0.00704 pCi/g* Uncert: +/-0.0222 TPU: +/-0.0224 Cobalt-60 u -0.00884 pCi/g Uncert: +/-0.0211 TPU: +/-0.0214 Europium-154 u -0.0279 pCi/g Uncert: +/-O.OS54 TPU: +/-0.0568 Lead-212 u -0.0119 pCi/g Uncert: +/-0.0271 TPU: +/-0.0277 Lead-214 u -0.0541 pCi/g Uncert: +/-0.0482 TPU: +/-0.0541 Potassium-40 u 0.0791 pCi/g Uncert: +/-0.264 TPU: +/-0.266 Protactinium-231 u -0.0237 pCi/g Un cert: +/-0.198 TPU: +/-0.199 Radium-226 u 0.0396 pCi/g Uncert: +/-0.0524 TPU: +/-0.0554 Radium-228 u -0.0548 pCi/g Un cert: .+/-0.0902 Page 52of614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Workorder: 405245 QC Summarl'.: Page 4 of 5 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596387 TPU: +/-0.0936 Thallium-208 u 0.00473 pCi/g Uncert: +/-0.0242 TPU: +/-0.0243 Tin-126 u 0.0148 pCi/g* Uncert: +/-0.0326 TPU: +/-0.0332 Rad Gas Flow Batch 1597819 ' QC1203625472 405245003 DUP Alpha Hh 14.2 H 7.98 pCi/g 56.l (0%-100%) JXC9 09/26/1613 :58 Uncert: +/-3.88 +/-2.96 TPU: +/-4.82 +/-3.35 Beta Hh 16.4 H 17.2 pCi/g 4.55 . (0%-20%) Uncert: +/-2.82 +/-2.14 TPU: +/-3.64 +/-3.20

  • QCI203625475 LCS Alpha 1-10 121 pCi/g 110 (75%-125%) JXC9 09/26/1613:58 Uncert: +/-11.0 TPU: +/-25.7 Beta 399 453 pCi/g 113 (75%-125%) Uncert: +/-15.7 TPU: +/-64.9 QC1203625471 MB Alpha u -1.11 pCi/g JXC9 09/26/1613:58 Uncert: +/-1.30 TPU: +/-1.30 Beta u -2.22 pCi/g Uncert: +/-2.56 TPU: +/-2.56 QC1203625473 405245003 MS Alpha 121 Hh 14.2 H 159 pCi/g 120 (75%-125%) JXC9 09/26/1613:58 Uncert: +/-3.88 +/-17.9 TPU: +/-4.82 +/-34.3 Beta: 440 Hh 16.4 H 477 pCi/g 105 (75%-125%) Uncert: +/-2.82 +/-17.3 TPU: +/-3.64 +/-62.4 QC1203625474 405245003 MSD Alpha 118 Hh 14.2 H 144 pCi/g 9.84 110 (0%-20%) JXC9 09/27/1610:14 Uncert: +/-3.88 +/-16.3 TPU: +/-4.82 +/-34.7 Beta 427 Hh 16.4 H 436 pCi/g 8.92 98.4 (0%-20%) Uncert: +/-2.82 +/-16.1 TPU: +/-3.64 +/-63.1 Notes: Page 53 of 614 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 405245 Parmname NOM Sample Qual QC Units RPD% REC% TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). The Qualifiers in this report are defined as follows: ** < > BD FA H J K L M M NIA NI ND NJ Q Analyte is a Tracer compound Result is less than value reported Result is greater than value reported Results are either below the MDC or tracer recovery is low Failed analysis. Analytical holding time was exceeded Value is estimated Analyte present. Re.Ported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD REMP Result> MDC/CL and< RDL RPD or %Recovery limits do not apply. See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the Le. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Page 5 of 5 Range Anlst R u UI UJ UL x y Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. . Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Other specific qualifiers were required to properly define the results. Consult case narrative. A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. h Preparation or preservation holding time was exceeded Date Time NIA indii:ates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable. **Indicates analyte is a surrogate/tracer compound. A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/-the RL is used to evaluate the DUP result. For PS, PSD, and .SDILT results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 54of614 Page 55 of 614 Gamma Spectroscopy
  • Raw Data*

Effective 3/25/2010 Revision 1 Effective March 2010 Radiochemistry Batch Checklist 30-Sep-2016 Batch# lf"'lt,:J"f t Product: LSo/..J/A'l'J"W....oato: td(.:sjr. Criteria: Yes No Comments Sample Solids are less than or equal to 100 ma for GAB. dJ. Samples have been blank corrected (If required), Blank correction renorted Included llf renulredl. A.Ii.-If activity less than lox MDA/MDC, error Is less than or equal to 1SO% of sample activity. If greater than 10* MDA/ MDC, error Is 40% or less, / If below the MDA/ MDC "rror Is nk-.. . Instrument source check Is within limits. / ITnst*untnnt bL-n rheck Is within u ...... ., Method RDL/ LLD has been met. / If duplicate activities are: / Less than 5* MDA/ MOC, then RPD Is 1000/o or less, If greater 5* MDA/ MDC, then RPD 200/o or less, If below the MDA/ MDC, the RPD Is 00/o, Or meets the client's reaulred RER acceptance criteria. Tracer yield Is 15-125%

  • Carrier yield 25-1250/o, (Or meets the client's contract acceptance criteria}. "'Ii. ' Method blank Is less than the RDL/ LLD. ./ llH r*-nlnc .,,. o;o1" actiVltvl Sample was run within hold time, ./ v* I ft SamPle was correctlv Preserved If reaulred. -Smears Taken for Radioactive batches. Method Spike and LCS are within 75-1250/a / lrn* --ets the .. uent'c c-->-act ""'C""**nc" crlt.,rlal-No blank spaces on data forms. / All line outs Initialed and dated. '**-------*--Aux data Is correct. J4-CllentSneclal renulrements nane has been checked. / Raw Data and/ or snectrum are Included and orooerlv statused. / MS, LCS, and Duplicate RPD/RER values uploaded to UMS and / .,., .... _ veri""" .... /If .. /VIA. a ** _ .. --*-*-" *-*-r * ., .. v Batch Data Exceotlon RePorts CDERl comoleted If aPPllcable. ./ Do.1 (J /("/,.'7..lsd '( Batch Data Exception Reports (DER) second reviewed. / Dlsnosltlon verified to be comnleted. ' l11.t1nun* Cnr .. *ctlon C"..,Dl"*"d If renulred jll(,,, Review sample historical results If available Ai11: (If REMP, results above MDC have been verified bv historical results. recount or re-analvsls, l . . ' . /D-5-16 Secondary Rovlow Performed __ -'"' __________ _ to/r Page 56of614 GL*CHL-RAD-013 Rev 1 Page 1of1 -

GEL Laboratories LLC Form GEL-DER DER Report No.: 1563681 Revision No.: 1 DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: Type: 03-0CT-16 Radiochemistry Specifications Process. Instrument Type: Test I Method: Matrix Type: Client Code: GAMMA SPECTROMETER DOE HASL 300, 4.5.2.3/Ga-01-R Solid MJWC Batch ID: Sample Numbers: 1596387 See Below Potentially affected work order(s)(SDG):405245 Application Issues: Sample Analyzed out of Holding Sample Logged out of Holding Specification and Requirements DER Disposition: Exception

Description:

Samples 405245 001, 002, 003, 004, 005, 006, 007, 008, 009, 010, 011, Samples were analyzed as soon as possible. Reportfng result. 012, 013, 014, 015, 016, and 1203621686 (duplicate) were logged out of the holding period. . Originator's Name: Data Validator/Group Leader: Bryan Williams 03-0CT-16 Michael Hilton 03-0CT-16 Page 57of614 Gamma Spec Queue Sheet Batch #:1596387 Analyst: MXRl First Client DueDate:l0/04/2016 Internal Due Date: 09130/2016 Gamma LCS Isotope: Mixed Gamma Initials: K ,,S-Prep Date: __ I Container JD 405245001-1 HO.I.I 405245002-1 H0.1.2 4052450\i.i-i Ii0.1.5 405245004-1 H0.1.6 405245005-1 H0.2.1 405245006-1 H0.2.2 405245007-1 H0.3.1 .lf!;;:?.15(108-1 H0.3.2 405245009-1 H0.4.1 405245010-1 H0.4.2 405245011-1 H0.5.1 405245012-1 H0.5.2 405245013-1 REACH7.l.1 405245014-1 REACH7.l.2 405245015-1 REACH21.l.1 405245016-1 REACH21.1.2 1203621685-1 MB 1203621686-1 DUP H0.1.1(4052 45001) 1203621687-1 LCS GEL Laboratories LLC, Radiochemistry Division LCS Code: Expiration Date: I..'(! 1 ! ?..'l Vol: rv'l l-'t / 11...)l.<e Library: SQ\.A b Type SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE

  • SAi\IPLE SAMPLE SAl\<lPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP LCS Hazard Code Client Matrix MJWCOOl sorL MJWCOOl SOIL MJWCOOI SOIL MJWCOOl SOIL MJWCOOI SOIL MJWCOOl SOIL MJWCOOI sorL MJWCOOl SOIL MJWCOOl SOIL MJWCOOI SOIL MJWCOOl SOIL MJWCOOI SOIL MJWCOOI SOIL MJWCOOI SOIL MJWCOOl SOIL MJWCOOI SOIL QC ACCOUNT SOIL QC ACCOUNT SOIL QC ACCOUNT SOIL Balance wtt;cy Al" Geometry (I/ ) Detector Collect Date 15-DEC-15 10:14:00 Rt I r.Al'-J I 155.344 g I I I 15-DEC-15 10:19:00{\f ! 146.202 g 51 15-DEC-15 10:18:00 flJI I 139.591 g I ' 15-DEC-1510:2l:OOfi_.f ! 145.276 g I 7 15-DEC-15 I 1:42:00(L.l2t I 117.771 g IS I I 15-DEC-1511:46:00f2_f I 116.68 g I 'Li..t I 15-DEC-15 12:17:00 UZ i 126.52 g I I 15-DEC-15 12:20:00 1.f 153.247 g 301 15-DEC-15 12:31:00' 1 j-139.ll9 g 15-DEC-15 12:35:00 142.421 g 15-DEC-15 12:53:00 134.661 g <g 15-DEC-15 12:56:00 (l..,_f I 132.296 g °i 15-DEC-15 11:04:01\'21 136.095 g. I \q I 15-DEC-15 11:08:00fi{ 154.135 g I -z.o I I 15-DEC-15 14:02:00\11.f 120.577 g I l q--15-DEC-15 l4:06:ooyi,f 125.408 g ! '3cl q/rz .. l!v (U ll:)b", :SL!'1 Lj'{ 15-DEC-15 l0:14:01f).i 1r;i;-3fYI SI qlrz..(I"" 14 I lit; I H* I -09/16/2016 Sealing Date/Time (if Applicable) q 11-z,[! y, -I !

VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:33:13.97 ********************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245001.CNF;l Background file : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM01.CNF;402 Background date : Z-OCT-2016 10:59:55. Sample date : 15-DEC-2015 10:14:00 Acquisition date : 3-0CT-2016 04:32:47. Sample ID : R405245001 Sample quantity : 1.55344E+02 GRAM Detector name : GAMOl Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.34 0.0% Energy tolerance : 1.50000 keV Analyst Initials : MXRl Abundance limit : 75.00000 Sensitivity : 3.00000 Batch ID : 1596387 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 .32 33 34 6 6 0 1 1 1 4 4 4 0 0 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 3 3 0 0 0 0 Page 59of614 Energy 35.53* 38.03* 63. 56* 72. 27 74.77 77.18* 87.59 90.15 92.71* 129.33 139.79 185.74* 238.62*

241.75* 254.14 271.21 278.31 295.40* 329.40 338.67*

351.92* 425.92 510.85* 566.17* 583.28* 609.34* 641. 93 662.94 768.52 772.75 795.17 821. 93 855.23 860.24 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 50 15 27 29 102 160 40 33 70 30 32 69 250 66 37 52 32 141 23 55 200 29 20 28 100 163 23 36 30 24 14 12 10 22 Bkgnd FWHM Channel Left Pw

  • Cts/Sec %Err 18 53 139 63 117 104 184 108 135 141 89 92 70 99 53 98 51 63 62 49 46. 90 45 39 13 15 84 33 9 8 3 6 20 5 2.02 1. 52 1.11 1. 32 1. 31 1. 32 1. 78 1.22 1. 75 0. 96 2.42 1. 06 1.12 1. 80 3.92 2.34 3.46 1. 30 1. 95 1.15 1.13 7.93 1. 95 2.42 1. 04 1. 73 14.10 1. 41 2.15 2.15 1. 67 0.88 5.47 0.57 71. 76 76.76 127.81 145.24 150.24 155.04 175.87 181.00 186.12 259.34 280.26 372 .15 477.91 484.15 508.94 543.07 557. 27* 591.45 659.43 677.98 704.46 852.45 1022.27 1132.89 1167.09 1219.20 1284.37 1326.39 1537.49 1545.95 1590.77 1644.27 1710.85 1720.88 68 68 123 143 143 143 171 171 171 255 275 367 472 472 504 537 552 585 649 672 699 835 1016 1125 1163 1213 1254 1318 1532 1532 . 1587 1640 1700 .1715 17 l.38E-02 28.2 17 4.24E-03106.8 10 7. 4*9E-03 87. 3 16 8.00E-03 39.3 16 2.82E-02 21.l 16 4.45E-02 14.4 22 1.llE-02 66.5 22 9.25E-03 54.0 22 1. 95E-02 36. 7 10 8.30E-03 76.4 9 8.77E-03 56.9 11 1.91E-02 31.8 19 6.95E-02 8:5 19 1.84E-02 35.8 11 1.04E-02 40.8 16 1.44E-02 45.1 11 8.90E-03 47.0 12 3.92E-02 14.2 14 6.35E-03 76.5 10 1.53E-02 28.2 12 5.55E-02 9.9 30 8.06E-03 97.2 13 5.58E-03 85.4 13 7.89E-03 50.6 10 2.77E-02 12.4 12 4.52E-02 9.3 37 6.52E-03126.2 15 1.00E-02 38.8 23 8.28E-03 27.6 23 6.81E-03 33.8 7 3.77E-03 35.4 9 3.25E-03 49.3 14 2.70E-03104.5 10 6.06E..:.03 28.8 Fit 2.53E+OO 3.30E+OO 1. 66E+OO 2.26E+OO 7.45E-01 Peak Search Report (continued) Page : 2 Sample ID : R405245001 Acquisition date 3-0CT-2016 04:32:47 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 911.34* 55 14 1. 31 1823.04 1815 13 1.52E-02 19.9 36 0 935.69 19 8 0.85 1871.72 1866 14 5.40E-03 41.1 37 0 941.67 11 4, 2.38 1883.67 1880 7 3.17E-03 40.3 38 0 950.88 15 8 2.93 1902.08 1896 12 4.12E-03 47.6 39 4 964.42 24 14 2.47 1929.15 1923 20 6.65E-03 34.9 7.58E-01 40 4 969. 26 32 3 2.26 1938.84 1923 20 8.82E-03 21. 6 41 0 1003.09 8 2 0.53 2006.48 2003 6 2.35E-03 41. 4 42 0 1023. 96 13 7 4.35 2048.20 2041 13 3.47E-03 50.7 43 0 1043.93 10 16 0.98 2088.12 2079 13 2.75E-03 89.8 44 0 1120.13* 33 5 1. 47 2240.47 2235 11 9.13E-03 22.5 45 0 1156.54 16 14 7.72 2313.26 2302 18 4. 31E-03 61.1 46 0 1178.64 5 9 0.52 2357.44 2350 9 1.25E-03128.1 47 0 1199. 54 17 6 1.13 2399.23 2395 11* 4.70E-03 36.5 48 0 1295.19 9 0 0.63 2590.44 2586 8 2.50E-03 33.3 49 0 1355.94 5 .6 0.62 27'11. 90 2708 8 1. 28E-03104. 5 50 0 1460.73* 275 0 1. 81 2921.37 2916 12 7.63E-02 6.1 51 0 1764.31* 20 0 1. 99 3528.22 3522 13 5.68E-03 24.0 Flag: "*" = Peak area was modified by background subtraction Page 60of614 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 05:33:16 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245001.CNF;l PEAK.Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 15-DEC-2015 10:14:00 R405245001 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 04:32:47 155.34 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMAl 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Page 61of614 Nuclide PB-214 PB-214 PB-214 PB-214 TL-208 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 277.37 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 HG-203 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 279.20 74.66 74.82 74.82 351.06 CAN 0 01:00:00.34 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : R405245001 Acquisition date 3-0CT-2016 04:32:47 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error* Status K-40 1460.82 10.66* 9.709E-01 1.241E+Ol 1. 241E+Ol 12.21 OK CD-109 88.03 3.70* 4.607E+OO 4 .115E-01 6.389E-01 477.37 OK SN-126 64.28 9.60 2.329E+OO 7.734E-01 7.734E-01 174.58 OK 86.94 ' 8. 90 4.607E+OO 1. 711E-01 1. 711E-01 477.37 OK 87.57 37.00* 4.607E+OO 4 .115E-02 4 .115E-02 477.37 OK BA-137M 661.66 89.90* l.880E+OO 1. 091E-01 1.112E-01 77.55 OK CS-137 661.66 85.10* l.880E+OO 1.153E-01 l.174E-01 77.55 OK HG-203 70.83 3.69 3.267E+OO 1.516E+OO l .181E+02 78.53 OK 72. 87 6.19 3.267E+OO 9.035E-01 7.042E+Ol 78.53 OK 279.20 81.56* 3.932E+OO 3.130E-02 2.440E+OO 168.78 OK TL-208 277.37 6.60 3.944E+OO Line Not Found <<INT Reject 583.19 85.00* 2.089E+00 2.910E-01 2.910E-01 24.81 OK 860.56 12.50 1.520E+OO 5.705E-01 5.705E-01 57.62 OK PB-212 74.82 10.28 3.518E+OO 1.134E+OO 1.134E+OO 68.06 OK 77 .11 17.10 3.748E+OO 1.577E+OO l.577E+OO 28.80 OK 238.63 43.60* 4.455E+00 7.320E-01 7.320E-01 16.98 OK 300.09 3.30 3.690E+OO Line Not Found Absent BI-214 609.32 45.49* 2.015E+OO 9.153E-01 9.156E-01 18.67 OK 1120.29 14.92 1. 2'23E+OO 8.690E-01 8.693E-01 45.06 OK' 1764.49 15.30 8 .117E-01 7.525E-01 7.527E-01 48.04 OK PB-214 74.82 5.80 3.522E+00 Line Not Found <<INT Reject 77 .11 9.70 3.748E+OO 2.781E+00 2.781E+OO 28.80 OK ' 87.09 3.41 4.572E+OO Line Not Found <<INT Reject 242.00 7.25 4.406E+OO Line Not Found <<INT Reject 295.22 18.42 3.740E+OO 1.138E+OO l.139E+00 28.50 OK 351.93 35.60* 3.216E+OO 9.533E-01 9.536E-01 19.86 OK RN-222 609.32 45.49* 2.015E+OO 9.153E-01 9.156E-01 18.67 OK 1120. 29 14.92 1.223E+OO 8.690E-01 8.693E-01 45.06 OK 1764.49 15.30 8 .117E-01 7.525E-01 7.527E-01 48.04 OK RA-224 240.99 4.10* 4.410E+OO 6. 071E-02 6.071E-022621.68 OK RA-226* 609.32 45.49* 2.015E+OO 9.153E-01 9.156E-01 18.67 OK 1120.29 14.92 1. 223E+OO 8.690E-01 8.693E-01 45.06 OK 1764.49 15.30 8 .117E-01 7.525E-01 7.527E-01 48.04 OK AC-228 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11. 27 3.325E+OO 8.066E-01 8.066E-01 56.41 OK 794.95 4.25 1. 621E+OO . 9.890E-01 9.890E-01 70.78 OK 835.71 1. 61 1.557E+OO Line Not Found Absent 911.20 25.80* 1. 451E+OO 7.237E-01 7.237E-01 39.75 OK 968. 97 15.80 l.379E+OO 7.144E-01 7.144E-01 43.19 OK RA-228. 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11. 27 3.325E+OO 8.066E-01 8.066E-01 56.41 OK 794.95 4.25 1.621E+OO 9.890E-01 9.890E-01 70.78 OK 835.71 1. 61 1.557E+OO Line Not Found Absent 911.20 25.80* l.451E+00 7.237E-01 7.237E-01 39.75 OK 968. 97 15.80 1.379E+OO 7.144E-01 7.144E-01 43.19 OK TH-228 74.82 10.28 3.518E+00 1.134E+OO 1.134E+OO 68.06 OK 77 .11 17.10 3.748E+OO 1.577E+OO 1.577E+OO 28.80 OK 238.63 43.60* 4.455E+OO 7.320E-01 7.320E-01 16.98 OK 300.09 3.30 3.690E+OO Line Not Found Absent Page 62of614 Nuclide Line Activity Report (continued) Page : 3 Sample ID : R405245001 Acquisition date 3-0CT-2016 04:32:47 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Ef f pCi/GRAM pCi/GRAM %Error Status TH-230 609.32 45.49* 2.015E+OO 9.153E-01 9.153E-01 18.67 OK 1120.29 14.92 1.223E+OO 8.690E-01 8.690E-01 45.06 OK 1764.49 15.30 8. ll 7E-01 7.525E-01 7.525E-01 48.04 OK TH-232 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11. 27 3.325E+OO 8.066E-01 8.066E-01 56.41 OK 835.71 1. 61 1.557E+OO ,-----Line Not Found Absent 911.20 25.80* 1.451E+00 7.237E-01 7.237E-01 39.75 OK 968. 97 15.80 1.379E+OO 7.144E-01 7.144E-01 43.19 OK TH-234 63.29 3.70* 2.329E+OO 2.007E+OO 2.007E+OO 174.58 OK 92.59 4.23 4. 941E+OO 2.080E+OO 2.080E+OO 73.37 OK U-234 609.32 45.49* 2.015E+OO 9.153E-01 9.153E-01 18.67 OK 1120.29 14.92 1.223E+OO 8.690E-01 8.690E-01 45.06 OK 1764.49 15.30 8. ll 7E-01 7.525E-01 7.525E-01 48.04 OK U-235 89. 96 3.47 4.782E+OO 1.248E+OO 1.248E+OO 108.08 OK 93.35 5.60 4.941E+OO 1. 571E+00 1. 571E+OO 73.37 OK 143.76 10. 96* 5.868E+OO Line Not Found Absent 163.33 5.08 5.647E+OO Line Not Found Absent 185. 72 57.20 5.296E+OO 1.318E-01 1.318E-01 63.51 OK 205.31 5.01 4.973E+OO Line Not Found Absent U-238 63.29 3.70* 2.329E+OO 2.007E+OO 2.007E+OO 174.58 OK 92.59 4.23 4.941E+OO 2.080E+OO 2.080E+OO 73.37 OK AM-243 43.53 5.90 3.822E-01 Line Not Foµnd Absent 74.66 67.20* 3.518E+OO l.735E-01 l.735E-01 68.06 OK ANH-511 511. 00 100.00* 2.335E+OO 4.520E-02 4.520E-02 170.89 OK Flag: "*" = Keyline Page 63of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:33:18.15 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245001.CNF;l *
  • Acquisition date 3-0CT-2016 04:32:47 Sensitivity : 3.000 *
  • Detector ID GAMOl Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.34 Half life ratio : ***** *
  • Sample date 15-DEC-2015 10:14:00 Analyst initials: MXRl *
  • Sample ID R405245001 Sample Quantity 1.5534E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SQLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 20-JUL-2016 07:03:55 Eff. Geometry : CAN *
  • Eff. File , : DKA100: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert* Nuclide (pCi/GRAM . ( 1 . 96-sigma ) K-40 1.241E+Ol 1.485E+OO CD-109 6.389E-01 2.989E+OO SN-126 4 .115E-02 1.925E-01 BA-137M 1.112E-01 8.449E-02 CS-137 1.174E-01 8.925E-02 HG-203 2.440E+OO 4.035E+OO TL-208 2.910E-01 7.074E-02 PB-212 7.320E-01 l.218E-01 BI-214 9.156E-01 l.675E-01 PB-214 9.536E-01 1.856E-01 RN-222 9.156E-01 1.675E-01 RA-224 6.071E-02 1.560E+OO RA-226 9.156E-01 l.675E-01 AC-228 7.237E-01 2.819E-01 RA-228 7.237E-01 2.819E-01 TH-228 7.320E-01 l.218E-01 TH-230 9.153E-01 1.675E-01 TH-232 7.237E-01 2.819E-01 TH-234 2.007E+OO 3.433E+OO U-234 9.153E-01 1.675E-01 U-235 6.146E-02 2.016E-01 U-238 2.007E+OO 3.433E+OO AM-243 1. 735E-01 l.157E-01 ANH-511 4.520E-02 7.570E-02 Non-Identified Nuclides ----Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 .Page 64of614 Key-Line Activity (pCi/GRAM -8.557E+OO l.076E-02 0.000E+OO l.877E-02 -5.998E-02 O.OOOE+OO K.L. Cnt Uncert (1. 96-sigma) i.141E+Ol 4.437E-02 l.960E+41 3.142E-02 3.698E-01 1.273E+04 MDA (pCi/GRAM 5. 972E-01 2.179E+OO 1.413E-01 5. 7 51E-02 6.075E-02 3. 721E+OO 5.889E-02 9.555E-02 l.144E-01 1.059E-01 l.144E-01 1.024E+OO l.144E-01 2.186E-01 2.186E-01 9.555E-02 l.144E-01 2.186E-01 2.705E+OO 1.144E-01 3.940E-01 2.705E+OO 9.277E-02 5.480E-;-02 MDA (pCi/GRAM 2.009E+Ol 9.633E-02 O.OOOE+OO 8.039E-02 6.989E-01 O.OOOE+OO NOT IDENT. NOT IDENT*. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 3.347E+02 O.OOOE+OO SHORT HLIF MN-54 4 .*997E-02 5 .188E-02 l.219E-01 NOT IDENT. C0-56 -3.808E-01 5.580E-01 8.829E-01 NOT IDENT. MN-56 O.OOOE+OO 1.465E+41 O.OOOE+OO SHORT HLIF C0-57 -8.520E-03 4.598E-02 9.151E-02 NOT IDENT. C0-58 -1.159E-01 4.179E-01 7.980E-01 NOT IDENT. FE-59 2.891E+OO 4.883E+OO 1.115E+Ol NOT IDENT. C0-60 9.548E-03 3.719E-02 8.249E-02 NOT IDENT. ZN-65 -5. 723E-02 2.065E-01 3. 251E-01 NOT IDENT. GE-68 -1.773E+OO 2.462E+OO 4.024E+OO NOT IDENT. AS-73 -3.901E+OO 1. lllE+Ol 2.039E+Ol NOT IDENT. AS-74 O.OOOE+OO 3.856E+03 0.000E+OO SHORT HLIF SE-75 2.424E-02 1.808E-01 3.635E-01 FAIL ABUN BR-77 O.OOOE+OO 2.791E+36 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 4.402E+02 O.OOOE+OO SHORT HLIF RB-83 -2.286E-01 5.753E-01 1.071E+OO NOT IDENT. KR-85 4.749E+OO 7.057E+OO 1.384E+Ol NOT IDENT. SR-85 4.652E-01 6.922E-01 1.357E+OO NOT IDENT. RB-86 O.OOOE+OO 2.288E+o4 O.OOOE+OO SHORT HLIF Y-88 3.844E-03 1. 981E-01 4.519E-01 NOT IDENT. Y-91 -3.010E+02 5.713E+02 9.044E+02 NOT IDENT. NB-94 1.152E-02 3.216E-02 6.552E-02 NOT IDENT. NB-95 -6.143E-02 8.671E-01 1.476E+OO NOT IDENT. NB-95M -1.172E+OO 2.336E+OO 3.904E+OO NOT IDENT. ZR-95 6.073E-02 1.405E+OO 2.732E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.462E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.116E+41 O.OOOE+OO SHORT HLIF RH-101 -2.873E-02 3. 728E-02 6.281E-02 NOT I DENT .. RH-102 4.733E-02 5.899E-02 1.287E-01 NOT IDENT. RU-103 -2.341E+o0 4.452E+OO 8.145E+OO FAIL A:BUN RH-106 2.108E-01 5.440E-01 1.107E+OO NOT IDENT. RU-106 2.108E-01 5.440E-01 1.107E+00 NOT IDENT. AG-108M -1. lllE-02 3.098E-02 5. ll 7E-02 NOT IDENT. AG-llOM -1.017E-02 1.149E-01 2.170E-01 NOT IDENT. SN-113 -1.704E-01 2.177E-01 3.876E-01 NOT IDENT. CD-115 O.OOOE+OO 3.178E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 7.081E+04 O.OOOE+OO SHORT HLIF TE-123M 5.353E-02 l.277E-01 2.608E-01 NOT IDENT. SB-124 -2.806E-01 1. 762E+OO 3.778E+OO NOT IDENT. SB-125 1.360E-02 1.915E-01 NOT IDENT. TE-125M -8.139E+Ol 2.827E+02 5.029E+02 NOT IDENT. I-126 O.OOOE+OO 5.223E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 7.821E+05 O.OOOE+OO SHORT HLIF SB-lZ\7 O.OOOE+OO 6.827E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.373E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.395E+41 O.OOOE+OO .SHORT HLIF TE-132 O.OOOE+OO 7.772E+25 O.OOOE+OO SHORT HLIF BA-133 1.544E-02 3.948E-02 7.466E-02 NOT IDENT. I-133 O.OOOE+OO 1. 786E+41 O.OOOE+OO SHORT HLIF CS-134 6.433E-02 4.462E-02 1. 045E-01 FAIL ABUN CS-135 -4.598E-02 1.464E-01 2.495E-01 NOT IDENT. I-135 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.591E+05 O.OOOE+OO SHORT HLIF CE-139 5.839E-03 9.319E-02 l.877E-01 NOT IDENT. BA-140 O.OOOE+OO 9.365E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.859E+05 O.OOOE+OO SHORT HLIF CE-141 1.070E+Ol 2.123E+Ol 4.359E+Ol NOT IDENT. O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -2.255E-01 3.973E-01 6.811E-01 NOT IDENT. PM-144 -2.252E-03 5.565E-02 1.073E-01 NOT IDENT. PR-144 -1. 786E-01 4.819E+OO 9.292E+OO NOT IDENT. PM-146 2.629E-02 4.461E-02 9.325E-02 NOT IDENT. ND-147 O.OOOE+OO 1.805E+07 O.OOOE+OO SHORT HLIF PM-147 -2.500E+02 7. 7"23E+02 1. 526E+03 NOT IDENT. PM-149 0.000E+OO 5.091E+39 O.OOOE+OO SHORT HLIF EU-150 8.498E-03 2. 721E-02 5.000E-02 FAIL ABUN EU-152 2.762E-02 9.267E-02 1.873E-01 FAIL ABUN GD-153 l.030E-01 1.995E-01 3.559E-01 NOT IDENT. EU-154 3.988E-02 l.069E-01 2.380E-01 NOT IDENT. EU-155 9.628E-02 1.181E-01 2. 311E-01 FAIL ABUN TB-160 -4.843E-01 1. 748E+OO 3.239E+OO FAIL ABUN H0-166M -1.687E-02 5.919E-02 l.096E-01 FAIL ABUN TM-171 -3.152E+OO 2.764E+Ol 5.201E+Ol NOT IDENT. HF-172 -2.829E-03 2.553E-01 4.620E-01 FAIL ABUN LU-172 7.992E-02 7.174E-02 1.705E-01 FAIL ABUN LU-176 2.388E-03 2. 271E-02 4.538E-02 FAIL ABUN Page 65of614 HF-181 -1.701E+OO 4.052E+OO 7.487E+OO NOT IDENT. TA-182 -3.106E-01 7.780E-01 1.503E+OO FAIL ABUN RE-183 -l.380E+OO 3.550E+OO 6.466E+OO NOT IDENT. RE-184 7.641E+OO .. 2 .158E+Ol 4.670E+Ol NOT IDENT. W-188 -6.523E+Ol l.250E+02 2.055E+02 FAIL ABUN IR-192 -2.993E-02 3.752E-01 7.403E-01 FAIL ABUN BI-207 2.439E-02 4.992E-02 1.052E-01 FAIL ABUN PB-210 3.137E+OO 4.274E+OO 8.895E+OO NOT IDENT. BI-211 0.000E+OO 5 .112E-01 8.325E-01 FAIL ABUN PB-211 6.629E-01 1.239E+OO FAIL ABUN BI-212 4.306E-01 5.224E-01 1.115E+OO NOT IDENT. RN-219 1. 820E-01 3.694E-01 7.656E-01 FAIL ABUN RA-223 -1. 887E-01 6.476E-01 1. 096E+OO FAIL ABUN AC-227 -1.022E-01 2.375E-01 3.995E-01 NOT IDENT. TH-227 -l.022E-01 2.375E-01 3.995E-01 NOT IDENT. TH-229 -8.025E-02 4.318E-01 8.451E-01 FAIL ABUN PA-231 1. 57 5E-01 4.244E-01 8.625E-01 NOT IDENT. TH-231 -1. 887E-01 6.476E-01 1. 096E+OO FAIL ABUN PA-233 8.381E-03 5.640E-02 1.130E-01 NOT IDENT. PA-234 -l.257E-01 2.781E-01 3.692E-01 NOT IDENT. PA-234M -2.831E+OO 4 .115E+OO 6.676E+00 NOT IDENT. NP-237 8.381E-03 5.640E-02 1.130E-01 NOT IDENT. NP-238 O.OOOE+OO 5.616E+40 O.OOOE+OO SHORT HLIF NP-239 1.660E-01 2.657E-01 5.102E-01 FAIL ABUN PU-239 4.823E+02 7.218E+02 6.857E+02 FAIL ABUN AM-241 6.847E-02 1.857E-01 3.349E-01 NOT IDENT. CM-243 -7. 309E-'02 1. 096E-01 l.888E-01 FAIL ABUN BK-247 6.953E-03 6.668E-02' 1.334E-01 NOT IDENT. CM-247 3. 252E-0"2 3.365E-02 7.315E-02 FAIL ABUN CF-249 6.152E-03 3.612E-02 7.241E-02 FAIL ABUN CF-251 -2.702E-02 l.088E-01 2.123E-01 NOT I DENT'. Page 66 of 614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:33:14.82 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82" 266 10.66* 9.709E-01 l.241E+Ol 1.241E+Ol 12.21 CD-109 88.03 52 3.70* 4.607E+OO 1.461E+OO 2.268E+OO 132.92 SN-126 64.28 36 9.60 2.329E+OO 7.734E-01 7.734E-01 174.58 86.94 52 8.90 4.607E+OO 6.073E-01 6.073E-01 132.92 87.57 52 37.00* 4.607E+OO 1. 461E-01 l.461E-Ol 132.92 BA-137M 661.66 38 89.90* 1.880E+OO 1.091E-01 l .112E-01 77.55 CS-137 661. 66 38 85.10* 1.880E+OO l.153E-01 1.174E-01 77.55 HG-203 70.83 38 3.69 3.267E+OO 1.516E+OO l .181E+02. 78.53 72. 87 38 6.19 3.267E+OO 9.035E-01 7.042E+Ol 78.53 279.20 37 81. 56* 3.932E+OO 5.589E-02 4.356E+OO 93.98 TL-208 277.37 37 6.60 3.932E+OO 6.907E-01 6.907E-01 93.98 583.19 107 85.00* 2.089E+00 2.910E-01 2.910E-01 24.81 860.56 22 12.50 l.520E+OO 5.705E-01 5.705E-01 57.62 BI-211 72.87 38 1. 23 3.267E+OO 4.547E+OO 4.547E+OO 78.53 351.06 226 12.92* 3.216E+OO 2.627E+OO 2.627E+00 19.86 PB-212 74.82 133 10.28 3.518E+OO 1. 776E+.oo 1. 776E+OO 42.21 77 .11 209 17.10 3.748E+00 1.577E+OO 1.577E+OO 28.80 238.63 294 43.60* 4.455E+OO 7.320E-01 7.320E-01 16'. 98 300.09 ------3.30 3.690E+OO ------Line Not Found ------BI-214 609.32 174 45.49* 2.015E+00 9.153E-01 9.156E-01 18. 67 1120.29 33 14.92 1.223E+OO 8.690E-01 8.693E-01 45.06 1764.49 19 15.30 8. ll 7E-01 7.525E-01 7.527E-01 48.04 PB-214 74.82 133 5.80 3.518E+OO 3.148E+OO 3.150E+OO 42.21 77 .11 209 9.70 3.748E+OO 2.781E+OO 2.781E+OO 28.80 87.09 52 3.41 4.607E+OO l.585E+00 1.585E+OO 132. 92 242.00 78 7.25 4.410E+OO l.173E+OO 1.173E+OO 71. 59 295.22 162 18.42 3.740E+OO l.138E+00 l.139E+00 28.50 351. 93 226 35.60* 3.216E+OO 9.533E-01 9.536E-01 19.86 RN-222 609.32 174 45.49* 2.015E+OO 9.153E-01 9.156E-01 18. 67 1120.29 33 14.92 1.223E+OO 8.690E-01 8.693E-01 45.06 1764.49 19 15.30 8. ll 7E-01 7.525E-01 7.527E-01 48.04 RA-224 240.99 78 4.10* 4.410E+OO 2.074E+OO 2.074E+OO 71. 59 RA-226 609.32 174 45.49* 2.015E+OO 9.153E-01 9.156E-01 18.67 1120.29 33 14.92 1.223E+OO 8.690E-01 8.693E-01 45.06 1764.49 19 15.30 8 .117E-01 7.525E-01 7.527E-01 48.04 AC-228 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 63 11. 27 3.325E+00 8.066E-01 8.066E-01 56.41 794.95 14 4.25 1.621E+OO 9.890E-01 9.890E-01 70.78 835.71 ------1. 61 l.557E+00 ------Line Not Found ------911. 20 56 25.80* 1.451E+OO 7.237E-01 7.237E-01 39.75 968. 97 32 15.80 1.379E+OO 7.144E-01 7.144E-01 43.19 RA-228 105.21 ------1.10 5.519E+00 ------Line Not Found ------338.32 63 11. 27 3.325E+OO 8.066E-01 8.066E-01 56.41 794.95 14 4.25 1.621E+OO 9.890E-01 9.89.0E-01 70.78 835.71 ------1. 61 1.557E+OO ------Line Not Found* ------911. 20 56 25.80* 1.451E+OO 7.237E-01 7.237E-01 39.75 968. 97 32 15.80 l.379E+OO 7.144E-01 7.144E-01 43.19 Page 67of614 Nuclide Line Activity Report (continued) Page : 2 Sample ID : R405245001 Acquisition date 3-0CT-20i6 04:32:47 Nuclide Type: -Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-228 . 74. 82 133 10.28 3.518E+OO 1. 776E+OO 1. 776E+OO 42.21 77 .11 209 17.10 3.748E+OO 1.577E+OO l.577E+OO 28.80 238.63 294 43.60* 4.455E+OO 7.320E-01 7.320E-01 16.98 300.09 ------3.30 3.690E+OO ------Line Not Found ------TH-230 609.32 174 45.49* 2.015E+OO 9.153E-01 9.153E-01 18.67 1120.29 33 14.92 l.223E+OO 8.690E-01 8.690E-01 45.06 1764.49 19 15.30 8 .117E-01 7.525E-01 7.525E-01 48.04 TH-232 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 63 11. 27 3.325E+OO 8.066E-01 8.066E-01 56.41 835. 71 ------1. 61 1.557E+OO ------Line Not Found ------911.20 56 25.80* 1.451E+OO 7.237E-01 7.237E-01 39.75 968. 97 32 15.80 1.379E+OO 7.144E-01 7 .14.4E-01 43.19 TH-234 63.29 36 3.70* 2.329E+OO 2.007E+OO 2;007E+00 174.58 92.59 90 4.23 4.941E+OO 2.080E+OO 2.080E+OO 73.37 U-234 609.32 174 45.49* 2.015E+OO 9.153E-01 9.153E-01 18.67 1120.29 33 14.92 l.223E+00 8.690E-01 8.690E-01 45.06 1764.49 19 15.30 8. ll 7E-01 7.525E-Ol* 7.525E-01 48.04 U-235 89. 96 43 3.47 4.782E+00 l.248E+OO 1.248E+OO 108.08 93.35 '90 5.60 4.941E+OO 1. 571E+OO 1. 571E+'OO 73.37 143.76 ------10. 96* 5.868E+00 ------Line Not Found ------163.33 ------5.08 5.647E+OO ------Line Not Found ------185.72 83 57.20 5.296E+OO l.318E-01 l.318E-01 63.51 205.31 ------5.01 4.973E+00 ------Line Not Found ------U-238 63.29 36 3.70* ,2. 329E+OO 2.007E+OO 2.007E+OO 174.58 92.59 90 4.23 4.941E+00 2.080E+OO 2.080E+OO 73.37 AM-243 43.53 ------5.90 3.822E-01 ------Line Not Found ------74.66 133 67.20* 3.518E+OO 2.717E-01 2.718E-01 42.21 ANH-511 511. 00 22 100.00* 2.335E+OO 4.520E-02 4.520E-02 170.89 Flag: "*" Key line Page 68of614 Summary of Nuclide Activity Sample ID : R405245001 Acquisition date Page : 3 3-0CT-2016 04:32:47 Total number of lines in spectrum 51 Number of unidentified lines 16 Number of lines tentatively identified by NID 35 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-2311 U-234 U-235 U-238 AM-:-243 ANH-511 Hlife 1.25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 46.59D 1.41E+10Y 7.04E+08Y l.41E+l0Y 1600. ODY 1600. ODY 1600. ODY l.41E+l0Y 1600. DOY 1.41E+10Y l.41E+l0Y l.41E+l0Y 7.54E+04Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 55 1. 00 1. 02 1. 02 77.9 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand *Total Activity Uncorrected pCi/GRAM l.241E+Ol l.461E+OO 1.461E-01 1.091E-01 l.153E-01 5.589E-02 2.910E-01 2.627E+OO 7.320E-01 9.153E-01 9.533E-01 9.153E-01 2.074E+OO 9.153E-01 7.237E-01 7.237E-01 7.320E-01 9.153E-01 7.237E-01 2.007E+OO 9.153E-01 l.318E-01 2.007E+OO 2.717E-01 4.520E-02 3.291E+Ol 3.291E+Ol Decay Corr pCi/GRAM 1.241E+Ol 2.268E+OO 1.461E-01 1.112E-01 l.174E-01 4.356E+OO 2.910E-01 2.627E+OO 7.320E-01 9.156E-01 9.536E-01 9.156E-01 2.074E+OO 9.156E-01 7.237E-01 7.237E-01 7.320E-01 9.153E-01 7.237E-01 2.007E+OO 9.153E-01 1.318E-01 2.007E+OO 2.718E-01 .4.520E-02 3.803E+Ol 3.803E+Ol 68.63% Decay Corr 2-Sigma Error 0.152E+Ol 3.014E+OO l.942E-01 0.862E-01 0.911E-01 4.094E+00 0.722E-01 0.522E+OO 1.243E-01 1.710E-01 1. 894E-01 1.710E-01 1. 485E+OO l.710E-01 2.877E-01 2.877E-01 1.243E-01 l.709E-01 2.877E-01 3.503E+OO 1.709E-01 0.837E-01 3.503E+OO l.147E-01 7. 725E-02 2-Sigma %Error 12.21 132.92 132.92 77.55 77.55 93.98 24.81 19.86 16.98 18.67 19.86 18.67 71. 59 18.67 39.75 39.75 16.98 18. 67 -39.75 174.58 18.67 63.51 174.58 42.21 170.89 Flags: "K" Keyline not found "E" = Manually edited Manually accepted "A" = Nuclide specific abn. limit Page 69of614 Flags K Unidentified Energy Lines Page : 4 Sample ID : R405245001 Acquisition date : 3-0CT-2016 04:32:47 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 6 35.53 69 25 2.02 71. 76 68 17 1.38E-02 56.3 4.36E-02 6 38.03 21 74 1. 52 76.76 68 17 4.24E-03 **** 1.08E-01 0 129.33 37 176 0.96 259.34 255 10 8.30E-03 **** 5.91E+OO T 0 139.79 39 111 2.42 280.26 275 9 8.77E-03 **** 5.89E+OO T 0 254.14 44 61' 3.92 508.94 504 11 l.04E-02 81. 6 4.24E+OO T 0 271.21 60 114 2.34 543.07 537 16 1. 44E-02 90.3 4.02E+OO T 0 329.40 26 71 1. 95 659.43 649 14 6.35E-03 **** 3.41E+OO T 0 425.92 32 100 7.93 852.45 835 30 8.06E-03 **** 2.73E+OO T 0 566.17 31 42 2.42 1132. 89 1125 13 7.89E-03 **** 2.14E+OO 0 641. 93 25 89 14.10 1284.37 1254 37 6.52E-03 **** 1.93E+OO 3 768.52 31 10 2.15 1537.49 1532 23 8.28E-03 55.2 1. 67E+OO 3 772.75 25 8 2.15 1545.95 1532 23 6.81E-03 67.7 1.66E+OO T 0 821. 93 12 7 0.88 1644.27 1640 9 3.25E-03 98.5 1.58E+OO 0 855.23 10 21 5.47 1710.85 1700 14 2.70E-03 **** 1.53E+00 0 935.69 20 8 0.85 1871.72 1866 14 5.40E-03 82.1 1. 42E+OO 0 941. 67 12 4 2.38 1883.67 1880 7 3.17E-03 80.6 1. 41E+OO 0 950.88 15 8 2.93 1902.08 1896 12 4.12E-03 95.2 1. 40E+OO 4 964.42 24 14 2.47 1929.15 1923 20 6.65E-03 69.8 1.38E+OO T 0 1003.09 9 2 0.53 2006.48 2003 6 2.35E-03 82.8 1. 34E+OO T 0 1023. 96 13 7 4.35 2048.20 2041 13 3.47E-03 **** l.32E+OO 0 1043.93 10 16 0.98 2088.12 2079 13 2.75E-03 **** 1.30E+OO 0 1156.54 15 13 7.72 2313.26 2302 18. 4. 31E-03 **** 1.19E+OO 0 1178.64 4 8 0.52 2357.44 2350 9 1. 25E-03 **** 1. l 7E+OO .T 0 1199. 54 17 6 1.13 2399.23 2395 11 4.70E-03 73.0 1.15E+OO 0 1295.19 9 0 0.63 2590.44 2586 8 2.50E-03 66.7 1.08E+OO 0 1355.94 4 6 0.62 2711. 90 2708 8 1.28E-03 **** 1.04E+OO Flags: "T" = Tentatively associated Page 70of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:33:31.62 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 . * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245001.CNF;l *
  • Acquisition date 3-0CT-2016 04:32:47 Sensitivity : 3.000 *
  • Detector ID GAMOl Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.34 Half life ratio : ***** *
  • Sample date 15-DEC-2015 10:14:00 Nuclide Library : SOLID *
  • Sample ID R405245001 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.5534E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 20-JUL-2016 07:03:55 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9 * ******************************************************************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 HG-203 TL-208 PB-212 BI-214 . PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.349E-01 1.026E+OO 6.653E-02 2. 471E-02 2.610E-02 1. 693E+00 2.565E-02 4.423E-02 4.984E-02 4. 696E-02 4.984E-02 4.742E-01 4.984E-02 9.148E-02 9.148E-02 4.423E-02 4.983E-02 9.148E-02 l.269E+00 4.983E-02 1.862E-01 1.269E+OO 4.338E-02 2.450E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 71of614 Le (pCi/GRAM 8.857E+OO 4.069E-02 O.OOOE+OO 3.190E-02 2.986E-01 0.000E+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM.:...171 HF-172 LU-172 LU-176 HF-181 Page 72of614 5.275E-02 3.814E-01 O.OOOE+OO 4.282E-02 3.250E-01 4. 672E+OO 3.428E-02 l.380E-01 l.667E+OO 9.492E+OO O.OOOE+OO 1.663E-01 O.OOOE+OO 0.000E+OO 4.665E-01 6.212E+OO 6.093E-01 O.OOOE+OO 1.692E-01 3.812E+02 2.901E-02 6.424E-01 1.805E+OO 1.192E+.00 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.935E-02 5.722E-02 3.524E+OO 4.947E-01 4.947E-01 2.278E-02 9.458E-02 1. 729E-01 O.OOOE+OO O.OOOE+OO l.225E-01 1.414E+OO 8.548E-02 2.357E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.369E-02 O.OOOE+OO 4.595E-02 1. 141E-01 O.OOOE+OO O.OOOE+OO 8.710E-02 O.OOOE+OO O.OOOE+OO 2.053E+Ol O.OOOE+OO 3.188E-01 4.709E-02 4.080E+OO 4.215E-02 O.OOOE+OO 7 .114E+02 O.OOOE+OO .2.285E-02 8. 551E-02 1. 1.006E-01 1.088E-01 1.373E+OO 4.781E-02 2.421E+Ol 2.169E-01 7.391E-02 2.067E-02 3. 331E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HL'IF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDEN'J'. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 73of614 6.243E-01 3.013E+OO 1. 965E+Ol 9.451E+Ol 3.334E-01 4.551E-02 4.160E+OO 4.000E-01 5.565E-Ol 4.997E-01 3.468E-01 4.985E-01 1.826E-01 1.826E-01 3.922E-01 .3. 965E-01 4.985E-01 5.151E-02 l.451E-01 2.7.48E+OO 5.151E-02 O.OOOE+OO 2.399E-01 3.242E+02 1. 569E-01 8. 811E-02 6 .112E-02 3.328E-02 3.271E-02 9.879E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:33:38.60 ******************"*************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE*.GAMMA]R405245001.CNF;l *
  • Acquisition date 3-0CT-2016 04:32:47 Sensitivity : 3.000 *
  • Detector ID GAMOl Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.34 Half life ratio : ***** *
  • Sample date 15-DEC-2015 10:14:00 Nuclide Library : SOLID *
  • Sample ID R405245001 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.5534E+02 GRAM *
  • Quantity Err(%) : 1.2875E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date' 20-JUL-2016 07:03:55 Eff. Geometry : 'CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM K-40 CD-109 SN-126 BA-137M CS-137 HG-203 TL-208 PB-212 BI-214 PB-214 . RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 1.241E+Ol 6.389E-:--01 4 .115E-02 1.112E-01 1.174E-01 2.438E+OO 2.910E-01 7.320E-01 9.156E-01 9.536E-01 9.156E.:..01 6.071E-02 9.156E-01 7.237E-01 7.237E-01 7.320E-01 9.153E-01 7.237E-Ol* 2.007E+OO 9.153E-01 6.146E-02 2.007E+OO 1.735E-01 4.520E-02 Act Error ( 1. 96-sigma) 1.620E+OO 2. 996E+OO 1.930E-01 8.462E-02 8.940E-02 4.042E+OO 7.182E-02 l.278E-01 1. 721E-01 1. 898E-01 1. 721E-01 1. 565E+OO 1. 721E-01 2.844E-01 2.844E-01 l.278E-01 1.720E-01 2.844E-01 3.462E+OO 1.720E-01 2.016E-01 *3.462E+OO 1.169E-01 7.572E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 74of614 Key-Line Activity (pCi/GRAM -8.557E+00 1.076E-02 -1.000E+41 1.877E-02 -5.998E-02 7.902E+03 K.L Act error (1. 96-sigma) 1.141E+Ol 4.437E-02 3.718E+41 3.144E-02 3.698E-01 l.273E+04 TPU ( 1. 96-sigma) 1. 620E+OO 2. 996E+OO 1.930E-01 8.462E-02 8.940E-02 4.042E+OO 7.182E-02 1. 278E-01 l.721E-01 1.898E-01 1.721E-01 1.565E+OO 1. 721E-01 2.844E-01 2.844E-01 1.278E-01 1. 720E-01 2.844E-01 3.462E+OO 1.720E-01 2.016E-01 3.462E+OO 1.169E-01 7. 572E-02 TPU (1.96-sigma) 1.205E+Ol. 4.463E-02 O.OOOE+OO 3.256E-02 3.708E-01 l.322E+04 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 -l.912E+02 3.348E+02 3.457E+02 SHORT HLIF MN-54 4.997E-02 5.192E-02 5.660E-02 NOT IDENT. C0-56 -3.808E-01 5.840E-01 NOT IDENT: MN-56 -1.000E+41 1.466E+41 O.OOOE+OO SHORT HLIF C0-57 -8.520E-03 4.598E-02 4.614E-02 NOT IDENT. C0-58 -l.159E-01 4.179E-01 4.212E-01 NOT IDENT. FE-59 2.891E+OO 4.888E+OO 5.058E+OO NOT IDENT. C0-60 9.548E-03 3. 719E-02 3.744E-02 NOT IDENT. ZN-65 -5.723E-02 2.065E-01 2.081E-01 NOT IDENT. GE-68 -1.773E+OO 2.463E+OO 2.589E+OO NOT IDENT. AS-73 -3.901E+OO l .114E+Ol l.127E+Ol NOT IDENT. AS-74 3.920E+Ol 3.856E+03 3.856E+03 SHORT HLIF SE-75 2.424E-02 l.808E-01 l.811E-01 FAIL ABUN BR-77 l.i577E+37 1.417E+38 O.OOOE+OO SHORT HLIF SR-82 3.704E+02 4.405E+02 4. 711E+02 SHORT HLIF RB-83 -2.286E-01 5.762E-01 5.853E-01 NOT IDENT. KR-85 4.749E+OO 7.060E+OO 7.377E+OO NOT IDENT. SR-85 4.652E-01 6.925E-01 7.235E-01 NOT IDENT. RB-86 -l.832E+04 2.290E+04 2.434E+04 SHORT HLIF Y-88 3.844E-03 l.981E-01 l.981E-01 NOT IDENT. Y-91 -3.010E+02 5.714E+02 5.873E+02 NOT IDENT. NB-94 l.152E-02 3.216E-02 3.258E-02 NOT IDENT. NB-95 -6.143E-02 8.671E-01 8.675E-01 NOT IDENT. NB-95M , -1.172E+OO 2.338E+OO 2.397E+00 NOT IDENT. ZR-95 6.073E-02 l.405E+OO 1.405E+OO NOT IDENT. NB-97 l.000E+41 4.943E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 6.925E+41 O.OOOE+OO SHORT HLIF M0-99 -4.521E+30 2.462E+31 O.OOOE+OO SHORT HLIF TC-99M 1. OOOE+41 1.120E+41 O.OOOE+OO SHORT HLIF RH-101 -2.873E-02 3.764E-02 3.980E-02 NOT IDENT. RH-102 4.733E-02 5.912E-02 6.285E-02 NOT IDENT. RU-103 -2.341E+OO 4.453E+OO 4.576E+00 FAIL ABUN RH-106 2.108E-01 5.442E-01 5.524E-01 NOT IDENT. RU-106 2.108E-01 5.442E-01 5.524E-01 NOT IDENT. AG-108M -1. lllE-02 3.098E-02 3.138E-02 NOT IDENT. AG-llOM -1.017E-02 1.149E-01 l.150E-01 NOT IDENT. SN-113 -1. 704E-01 2.178E-01 2.310E-01 NOT IDENT. co-*115 1.691E+38 3.192E+38 O.OOOE+OO SHORT HLIF SN-ll 7M 2.606E+04 7.087E+04 7 .184E+o4 SHORT HLIF TE-123M 5.353E-02 1.277E-01 1.300E-01 NOT IDENT. SB-124 -2.806E-01 1. 762E+OO 1. 767E+OO NOT IDENT. SB-125 1.360E-02 9.508E-02 9.527E-02 NOT IDENT. TE-125M -8.139E+Ol 2.827E+02 2. 851E+02 NOT IDENT. I-126 3.430E+05 5.243E+05 5.466E+05 SHORT HLIF SB-126 -3.363E+05 7.845E+05 7.990E+05 SHORT HLIF SB-127 -2.602E+21 7.669E+21 O.OOOE+OO SHORT HLIF I-131 l.166E+08 2.373E+09 2.373E+09 SHORT HLIF I-132 -1.000E+41 1.810E+42 O.OOOE+OO SHORT HLIF TE-132 -3.613E+25 7.904E+25 O.OOOE+OO SHORT HLIF BA-133 1.544E-02 3.948E-02 4.009E-02 NOT IDENT. I-133 -1.000E+41 2.512E+41 O.OOOE+OO SHORT. HLIF CS-134 6.433E-02 4.471E-02 5.329E-02 . FAIL ABUN CS-135 -4.598E-02 l.465E-01 1.479E-01 NOT IDENT. I-135 -l.000E+41 7.555E+41 0.000Et00 SHORT HLIF CS-136 3.188E+05 2.614E+05 2.983E+05 SHORT HLIF CE-139 5.839E-03 9.319E-02 9.323E-02 NOT IDENT. BA-140 2.159E+05 9.366E+05 9.416E+05 SHORT HLIF LA-140 -3.831E+05 2.865E+05 3.345E+05 SHORT HLIF CE-141 1.070E+Ol 2.123E+Ol 2.177E+Ol NOT IDENT. CE-143 1. OOOE+41 2.827E+41 O.OOOE+OO SHORT HLIF CE-144 -2.255E-01 3.975E-01 4.103E-01 NOT IDENT. PM-144 -2.252E-03 5.565E-02 5.566E-02 NOT IDENT. PR-144 -1. 786E-01 4.819E+OO 4*. 819E+OO NOT IDENT. PM-146 2.629E-02 4.465E-02 4.620E-02 NOT IDENT. ND-147 -3.831E+05 1. 805E+07 1.805E+07 SHORT HLIF PM-147 -2.500E+02 7. 724E+.02 7.806E+02 NOT IDENT. PM-149 -3.924E+39 5.161E+39 O.OOOE+OO SHORT HLIF EU-150 8.498E-03 2.721E-02 2.748E-02 FAIL ABUN EU-152 2.762E-02 9. 2 68E.:..02 9.352E-02 FAIL ABUN GD-153 1. OTOE-01 1.996E-01 2.049E-01 NOT IDENT. EU-154 3.988E-02 l.069E-01 l.084E-01 NOT IDENT. EU-155 9.628E-02 1.183E-01 l.260E-01 FAIL ABUN TB-160 -4.843E-01 1.748E+OO 1. 762E+OO FAIL ABUN H0-166M -1.687E-02 5.920E-02 5. 969E-02 FAIL ABUN TM-171 -3.152E+OO 2.764E+Ol 2.768E+Ol NOT IDENT. HF-172 -2.829E-03 2.553E-:-01 FAIL ABUN LU-172 7.992E-02 7.219E-02 8.068E-02 FAIL ABUN LU-176 2.388E-03 2.271E-02 2.274E-02 FAIL ABUN Page 75of614 HF-181 -1. 7 OlE+OO 4.053E+OO 4.125E+OO NOT IDENT. TA-182 -3.106E-01 7. 781E-01 7.906E-01 FAIL ABUN RE-183 -1. 38 OE+OO 3.556E+OO 3.610E+OO NOT IDENT. RE-184 7.641E+OO 2.166E+Ol 2.193E+Ol NOT IDENT. W-188 -6.523E+Ol l.252E+02 l.286E+02 FAIL ABUN IR-192 -2.993E-02 3.752E-01 3.754E-01 FAIL ABUN BI-207 2.439E-02 4.993E-02 5 .113E-02 FAIL ABUN PB-210 3.137E+OO 4.283E+OO 4.510E+OO NOT IDENT. BI-211 2.627E+OO 5.245E-01 l.295E+OO FAIL ABUN PB-211 -2.608E-01 6.630E-01 6.734E-01 FAIL ABUN BI-212 4.306E-01 5.228E-01 5.577E-01 NOT IDENT. RN-219 l.820E-01 3.701E-01 3:791E-01 FAIL ABUN RA-223 -l.887E-01 6.477E-01 6.533E-01 FAIL ABUN AC-227 -1.022E-01 2.379E-01 2.423E-01 NOT IDENT. TH-227 -l.022E-01 2.379E-01 2.423E-01 NOT IDENT. TH-229. -8.025E-02 4.318E-01 4.333E-01 FAIL ABUN PA-231 1. 575E-01 4.258E-01 4.317E-01 NOT IDENT. TH-231 -1.887E-01 6.477E-01 6.533E-01 FAIL ABUN PA-233 8.381E-03 5.640E-02 5.653E-02 NOT IDENT. PA-234 -1.257E-01 3 .131E-01 3.182E-01 NOT IDENT. PA-234M -2.831E+OO 4. ll 7E+OO 4.310E+OO NOT IDENT. NP-237 8.381E-03 5.640E-02 5.653E-02 NOT IDENT. NP-238 2.873E+40 5.617E+40 O.OOOE+OO SHORT HLIF NP-239 1.660E-01 2.661E-01 2.764E-01 FAIL ABUN PU-239 4.823E+02 7.221E+02 7. 541E+02 FAIL ABUN AM-241 6.847E-02 1.858E-01 l.883E-01 NOT IDENT. CM-243 -7.309E-02 1.098E-01 l.147E-01 FAIL ABUN BK-247 6 ."953E-03 6.669E-02 6.677E-02 NOT IDENT. CM-247 3.252E-02 3.409E-02 3. 711E-02 FAIL ABUN CF-249 6.152E-03 3.612E-02 3.623E-02 FAIL ABUN CF-251 -2.702E-02 1. 088E-01 1.095E-01 NOT IDENT. Page 76of614
  • GEL* Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 52.3803 87.09 86.2328 136.47* 70.8579 45.60 57.9401 87.57 86.2721 140.51 0.0000 46.54 44.0913 88.03 86.3097 143.76 80.3896 49.72 0.0000 88.34 86.3352 144.24 76.3449 51. 35 73.5669 88.47 86.3455 145.44 75.5609 51. 87 74.7847 89. 96 86.4668 152.43 80.1932 52.39 63.1416 1093.63 86.5215 153.25 0.0000 52.97 71.3792 91.11 0.0000 323.87 84.5615 53.44 69.0801 92.59 86.6780 156.02 0.0000 54.07 59.7606 93.35 86.7382 158.56 0.0000 57.36 0.0000 94.56 86.8341 159.00 69.4100 57.53 68.2535 94.65 86.8411 162.33 54.1047 57.98 71.8227 94.67 86.8427 162.66 0.0000 59.27 64.4652 94.87 65.2458 163.33 54.1406 59.32 64.4691 97.43 62 .12 65 165.86 54.2297 59.54 64.4860 98.43 67.5000 176.31 58.9252 60. 96 69.3205 98.44 67.5008 176.60 0.0000 61.17 67.7616 99.53 74.9367 177.52 65.0398 62.93 76.9797 100. 11 90.9531 181.07 0.0000 63.29 77. 0116 102.03 68.9447 181.52 69 .1137 63.58 77.0371 103.18 82.5697' 184.41 60.0914 64.28 77.0986 103.37 82.5835 143.76 60.1392 66.73 74.5357 105.21 65.4304 193.51 59.5450 67.24 80.9254 105.31 65.4360 197.03 50.0159 125.81 8'4 .1399 106.12 63.0099 198.01 57.0687 67.75 84.1458 106.47 86.5099 201.83 48.3958 69.67 70.0042 109.28 81.7598 203.43 '50.2020 70.83 79.6499 111. 00 78.1550 205.31 56.4277 72. 81 69.4418 111. 76 0.0000 210.85 60.1426 72. 87 69.4463 114. 06 69.6454 215.65 47.8883 74.66 69.5768 116. 30 0.0000 222 .11 58.7376 74.82 69.5883 116.74 67.3039 227.09 53. 5413 74.97 69.5992 119.76 66.2164 227.38 58.9048 77 .11 69.7529 121.12 66.7041 228.16 0.0000 78.74 75.4905 121. 22 70.0449 228.18 52.6795 79. '69 70.7395 121. 78 75.0810 116.74 52.6795 80.12 62.7279 122.06 75.0975 235.69 61. 8532 80.19 0.0000 122. 92 80.1577 235. 96 59.1727 80.57 59.5378* '123.07 80.1670 238.63 52.0728 81. 00 70.8322 265.00 66.0021 238.98 0.0000 81. 07 70.8371 125.81 79.0816 240.99 52.1365 81. 75 88.2035 127.23 87.9638 242.00 52.1637 83.79 80.7124 127.91 72.9221 244.70 36.4749 84.00 80.7292 129.30 70.4819 252.40 0.0000 85.43 92.1588 131.20 73.1036 252.80 42.5029 86.55 86.1884 133.02 80.7754 254.15 0.0000 86.79 86.2079 133.52 87.1186 256.23 46.1990 86.94 86.2203 136.00 65.7744 2 60. 90 0.0000 Page 77of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 36.3851 355.39 0.0000 584.27 15.3522 264.80 38.2069 356.01 22.7300 595.83 0.0000 2 65. 00 38.2103 364.49 0.0000 427.87 21. 594 7 2 68. 22 45.1041 366.42 0. 0000* 602.52 0.0000 269.46 32.8228 372.51 22.8794 604.72 13.8988 270.03 32.8315 375.05 24.8109 607.14 21. 6349 271. 23 32.8506 377.52 31.5209 609.32 15.4633 273.65 0.0000 356.01 20.1079 610.33 15.4675 276.40 27.4432 388.16 26.8544 614.28 13.9362 277.37 34.3193 388.63 0.0000 618.01 21. 7015 277.60 34.3231 391.69 34.5740 620.36 23.7843 278.00 34.3300 264.66 28.9087 621. 93 18.6218 279.20 34.3491 401.81 24.1013 630.19 0.0000 279.54 34.3544 402.40 20.2493 631. 2 9 12.4468 279.70 38.4803 404.85 31.8492 633.25 12.4536 280.46 42.6184 410.95 29.9865 634.78 0.0000 283.69 33.0447 413. 71 23.2388 635.95 12.4629 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 49.6066 423.72 0.0000 645.85 15.6207 285.90 0.0000 427.09 21. 4056 657.76 12.5371 287.50 45.9768 427.87 21.4119 657.90 0.0000 290.67 55.2527 433.94 27.7978 661.66 12.5503 293.27 0.0000 439.40 22.4768 664.57 0.0000 351. 93 36.9116 453.88 21. 6079 666.33 *o. 0000 295. 96 36.9238 463.37 15.7660 666.50 0.0000 879.38 38.8162 468.07 16.7780 667.71 0.0000 299.98 33.2922 473.00 0.0000 677.62 17.8550 300.09 41.6171 475.06 17.8066 685.70 0.0000 300.13 41. 6180 *476.78 16. 8271 695.00 0.0000 301.36 37.0142 477.60 28.7127 696 . .49 17.9428 302.85 44.4463 482.18 27.7653 696.51 17.9428 256.23 34.2863 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.9470 306.78 33.3933 497.08 19.9292 697.49 14.7804 308.46* 35.2748 505.52 10.4912 702.65 15.8569 311. 90 33.4688 507.63 0.0000 706.68 19.0481 316.51 28.8783 511. 00 24.0222 711. 68 19.0730 319.41 0.0000 514.00 16.5309 720.70 0.0000 320.08 0.0000 514.00 16.5309 721. 93 0.0000 321.04 38.0823 520.40 20.0781 722.78 14.8761 323.87 39.2502 520.69 0.0000 722.91 14.8767 325.23 35.0647 522.65 0.0000 '723.31 14.87,78 328.76 0.0000 527.90 0.0000 724.19 17.0072 333.37 37.5317 528.26 15.0958 727.33 14.8932 333.97 32.3795 529.59 19.1291 733.00 13.8490 334.37 39.4254 529.87 0.0000 735.93 8.5286 338.28 36.6688 531.02 0.0000 333.97 17.0638 338.32 36.6696 537.26 0.0000 739.50 0.0000 311. 90 26.8208 546.56 0.0000 747.24 8.5527 340.48 26.8208 552.55 19.2644 748.06 9.6237 340.55 0.0000 563.25 15.2576 752.31 8.5632 344.28 32.0472 569.33 24.4561 753.82 0.0000 345.93 27.3533 946.00 19. 8713 756.73 13.9305 351. 06 ' 20.7942 569.70 19.8729 756.80 13. 9305 351. 93 20.8014 583.19 15.3473 884.68 6.4407 Page 78of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81. 16.1090 1274.44 13.5601 1620.50 5.6484 766.42 20.9449 1001.03 8.4830 1621. 92 4.7079 766.84 19.3359 1002.74 11. 314 7 1678.03 0.0000 772.60 0.0000 1004.73 6.7915 1690.97 3.8030 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 102*5. 87 0.0000 1764.49 2.8810 778.90 8.0801 1028.54 0.0000 1063.66 2.8832 783.70 0.0000 1037.84 17.0911 1771.35 2.8835 785.37 17.2643 1038.76 0.0000 1791.20 0.0000 792.07 8.1055 631.29 15.4083 1808.65 1. 9319 794.95 4 .*3258 1048.07 0.0000 1810.72 0.0000 795.86 9.7354 1049.04 11. 4185 1836.06 2.9083 810.06 11. 9382 1050.41 17.1326 810.29 11. 9390 1063.66 9 .1608 344.28 10.8541 1077.00 0.0000 810.76 8.6839 1077.34 14.9255 815.77 0.0000 1085.87 8.0499 1048.07 0.0000 1093.63 4.6068 832.01 7.6357 1099.45 4.6120 834.85 5.4576 1112. 07 15.0238 835. 71 10.9176 1112. 84 13.8701 836.80 0.0000 1115. 54 13.8770 846.75 0.0000 1120.29 10.4172 846.77 22.3274 1120. 55 10. 4180 856.80 0.0000 1221.41 8.6829 860.56 4.9406 1129.67 10.4355 871. 09 14.3060 1131. 51 0.0000 873 .. 19 12 .1109 1147.95 0.0000 875.33 0.0000 1173.23 19.6342 879.38 13.2300 1177.95 8.4223 880.51 9.9247 1189.05 11.4274 883.24 12.1378 1204.77 15.5139 884.68 16.5564 1221.41 11.4932 8 8 9. 2 8. 13. 2588 1231.02 9.7411 894.76 12.1682 1235.36 0.0000 898.04 5.5349 1238.28 16.8465 900.72 7.7534 1260.41 0.0000 903.28 6.6494 1271.87 8.9178 911. 20 8.8812 1274.44 7 .1372 912.08 6.6621 1274.54 8.0299 923.98 0.0000 1291.59 2.8633 926.50 15.5928 1298.22 0.0000 929 .11 11.1438 1312 .11 0.0000 937.49 8. 3728 1332.49 6.3062 944 .13 0.0000 1362.66 0.0000 946.00 8.9469 1365.19 3.6228 949.00 5.0358 1368.63 0.0000 667.71 0.0000 1384.29 3.6338 962.31 15.1496 1408.01 2.7356 964.08 11. 2260 1457.56 0.0000 966 .17 11. 2309 1460.82 4.5972 911.20 11. 2370 1489.16 5.5404 968.97 11.2370 1505.03 2.7768 983.53 0.0000 1584.12 6.5557 984.45 0.0000 1596.21 0.0000 Page 79of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:34:11.05 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245002.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM05.CNF;477 Background date : Z-OCT-2016 11:00:07. Sample date 15-DEC-2015 10:19:00 Acquisition date : 3-0CT-2016 04:33:24. Sample ID R405245002 Sample quantity 1. 46202E+o2* GRAM Detector n.ame GAM05 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.55 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596387 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 0 2 0 3 2 4 2 5 0 6 3 7 3 8 3 9 0 10 0 11 0 12 0 13 0 14 . 0 15 0 16 5 17 5 18 0 19 0 20 0 21 0 22 3 23 3 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 2 32 2 33 2 34 0 Page 80of614 Energy 46.06* 63.37* 73.11* 76.75* 83.35* 86.66* 89.41 92.33* 111.16 128.56 131.48 146.79 153.57 185.50* 208.78 238.33* 241.49 264.00 278.10 294.96* 313.44 338.21* 341. 71 344.69 351. 82* 462.45 540.47 583.26* 609.29* 648.28* 661. 44 664.89 668.19 727.84 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 73 41 3*2 328 40 109 74 125 11 43 25 19 .13 85 65 294 115 25 22 172 15 76 33 17 247 30 13 95 201 8 73 19 19 14 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 179 187 94 89 102 86 101 115 112 87 114 66 76 90 102 64 79 85 79 50 54 25 21 26 72 36 12 13 24 36. 15 10 7 20 0.97 1.14 0.85 0.91 1.10 0.91 1. 05 1.18 0.97 0.99 1. 31 1. 47 0.56 1. 41 1. 36 0.98 1. 82 3.49 1.29 1. 09 1. 34 1. 30 1. 66 1. 37 1.18 3.31 3.44 1.18 1. 34 6.05 1. 62 1. 74 1. 87 1. 43 93.95 128.53 148.00 155.27 168.46 175.09 180.58 186.42 224.05 258.83 264.67 295.26 308.80 372.63 419.16 478.20 484.53 529.51 557. 71 591.39 628.33 677.84 684.83 .690.80 705.04 926.15 1082.09 1167. 60 1219.63 1297.57 1330.77 1337.35 1456.57 88 123 145 145 166 172 172 172 223 256 263 294 307 369 415 474 474 523 552 587 623 673 673 689 698 920 1075 1163 1214 1287 1318 1318 1318 1449 . 11 2.04E-02 38.9 8 1.13E-02 62. 8 22 8.86E-03 52.7 22 9.llE-02 7.1 6 1.lOE-02 44.6 22 3.03E-02 16.3 22 2.04E-02 24.5 22 3.48E-02 17.9 7 3.0lE-03164.1 7.1.21E-02 38.5 9 6.87E-03 80.6 6 5.28E-03 71.4 6 3.60E-03109.7 9 2.36E-02 23.9 12 1.81E-02 33.1 16 8.17E-02 7.3 16 3 .19E-02 21. 2 13 6.81E-03 79.9 11 6.lOE-03 82.5 8 4.78E-02 10.6 12 4.17E-03101.3 16 2.llE-02 16.7 16 9.25E-03 30.9 6 4.75E-03 51.9 13 6.87E-02 9.6 13 8.24E-03 45.5 10 3.49E-03 59.7 11 2.65E-02 13.0 12 5.58E-02 8.7 18 2.30E-03177.0 26 2.03E-02 15.5 26 5.14E-03 46.9 26 5.18E-03 48.5 10 3.83E-03 66.4 Fit 1.15E+Ol 1.34E+OO 9.23E-01 1.74E+OO 1.22E+OO Peak Search Report (continued) Page : 2 Sample ID : R405245002 Acquisition date 3-0CT-2016 04:33:24 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 767.88* 24 18 2.31 1536.62 1532 9 6.78E-03 38.2 36 0 772. 02 11 17 0.63 1544.87 1540 9 3.06E-03 75.2 37 0 795.23 11 17 1. 01 1591.27 1587 7 3.03E-03 70.3 38 0 803.94* 17 5 3.39 1608.68 1604 10 4.75E-03 37.9 39 0 910. 96* 67 12 1. 24 1822.58 1816 11 l.85E-02 15.8 40 0 934.03 18 10 1. 56 1868.69 1861 13 5.13E-03 41. 8 41 0 949.79 20 4 3.57 1900 .19 1893 15 5.60E-03 30.6 42 0 964.36 22 6 1. 88 1929.33 1924 11 5.97E-03 30.2 43 0 969 .11 51 14 1. 34 1938.81 1934 13 1.41E-02 20.4 44 0 1028.78 9 5 1. 47 2058.08 2054 7 2.42E-03 55.3 45 0 1120.17* 36 13 0.79 2240.75 2235 11 l.OlE-02 26.3 46 4 1148. 31 10 4 1. 72 2296.99 2295 19 2. 71E-03 35.5 1.80E+OO 47 4 1151. 32 17 9 1. 87 2303.00 2295 19 4.65E-03 43.0 48 0 1245.48 8 9 1. 32 2491.22 2485 10 2.16E-03 83.5 49 0 1309.85 8 0 1. 50 2619.88 2617 6 2.22E-03 35.4 50 0 1461.03* 308 7 2.10 2922.04 2915 14 8.57E-02 6.0 51 0 1495.95 9 3 4.27 2991. 85 2983 14 2.40E-03 57.1 52 0 1509.22 13 0 1.16 3018.38 3012 12 3.61E-03 27.7 53 0 1765.09 36 9 2.02 3529.82 3520 17 9.86E-03 25.2 Flag: "*" = Peak area was modified by background subtraction Page 81of614 VMS Nuclide Identification Report V3.1 Generated 05:34:13 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245002.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 15-DEC-2015 10:19:00 R405245002 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 04:33:24 146.20 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMAS 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Page 82of614 Nuclide PB-214 PB-214 PB-214 PB-214 PB-214 TL-208 PB-214 Line 242.00 87.09 87.09 87.09 87.09 2'77.37 351. 93 Detector geometry: Elapsed real time: CAN 0 01:00:00.55 . 10.00 Half life ratio Systematic Error Efficiencies at : 0.00 % : Peak Energy Interfered Nuclide RA-224 TH.-22 9 SN-126 SN-126 CD-1'09 HG-203 BI-211 Line 240.99 85.43 86.94 87.57 88.03 279.20 351.06 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : R405245002 Acquisition date 3-0CT-2016 04:33:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.244E+00 1.149E+Ol 1.149E+Ol 12.06 OK CD-109 88.03 3.70* 8.914E+OO 1.044E+OO 1.621E+OO 68. 96 OK SN-126 64.28 9.60 9 .112E+00 3.030E-01 3.030E-01 125.65 OK 86.94 8.90 8.914E+00 4.341E-Ol 4.341E-01 68. 96 OK 87.57 37.00* 8.914E+OO l.044E-01 1.044E-01 68. 96 OK BA-137M 661. 66 89.90* 2. 417E+00 1. 793E-01 1.827E-01 30.91 OK CS-137 661. 66 85.10* 2.417E+00 1.895E-01 l.930E-01 30.91 OK CE-141 i45.44 48.29* 7.727E+00 3.106E-02 1.597E+Ol 142.79 OK HG-203 70.83 3.69 9.006E+OO Line Not Found Absent 72.87 6.19 8.988E+OO 3. 696E-01 2.881E+Ol 105.40 OK 279.20 81.56* 4.912E+OO l.330E-02 1.037E+OO 394.12 OK TL-208 277.37 6.60 4.923E+OO Line Not Found <<INT Reject 583.19 85.00* 2.673E+OO 2.269E-01 2.269E.:....01 26.01 OK 860.56 12.50 1. 959E+OO Line Not Found Absent PB-210 46.54 4.25* 9.664E+OO 1.193E+OO 1.223E+OO 77.76 OK PB-212 74.82 10.28 8.977E+OO Line Not Found Absent 77 .11 17.10 8. 967E+00 1.375E+00 l.375E+00 14.17 OK 238.63 43.60* 5.564E+OO 7.lOlE-01 7.lOlE-01 14.56 OK 300.09 '3.30 4.613E+OO Line Not Found Absent BI-214 609.32 45.49* 2. 581E+OO 9.214E-01 9.217E-01 17.45 OK 1120.29 14.92 1. 57 6E+OO 7.846E-01 7.849E-01 52.53 OK 1764.49 15.30 1. 032E+00 1.089E+OO 1.090E+OO 50.43 OK PB-214 74.82 5.80 8.977E+OO Line Not Found Absent 77 .11 9.70 8.967E+OO 2.424E+OO 2.425E+OO 14.17 OK 87.09 3.41 8.912E+OO Line Not Found <<INT Reject 242.00 7.25 5.497E+OO Line Not Found <<INT Reject 295.22 18.42 4.680E+OO 1.148E+OO 1.148E+OO 21.11 OK 351. 93 35.60* 4.042E+OO 9. 731E-0*1 9.734E-01 19. 21 OK RN-222 609.32 45.49* 2.581E+OO 9.214E-01 9.217E-01 17.45 OK 1120.29 14.92 l.576E+00 7.846E-01 7.849E-01 52.53 OK 1764.49 15.30 1.032E+OO 1.089E+OO 1.090E+OO 50.43 OK RA-224 240.99 4.10* 5.506E+OO 9.455E-01 9.455E-01 141.15 OK RA-226 609.32 45.49* 2.581E+OO 9.214E-01 9.217E-01 17.45 OK 1120.29 14.92 1.576E+OO 7.846E-01 7.849E-01 52.53 OK 1764.49 15.30 1.032E+OO 1.089E+OO 1.090E+OO 50.43 OK AC-228 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27 4.177E+OO 9.167E-01 9.167E-01 33.46 OK 794.95 4.25 2.087E+OO 6. 44'4E-Ol 6.444E-01 140.58 OK 835.71 1. 61 2.005E+OO Line Not Found Absent 911. 20 25.80* 1. 871E+OO 7.147E-01 7.147E-01 31. 63 OK 968. 97 15.80 1.778E+OO 9.305E-01 9.305E-01 40.78 OK RA-228 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27 4.177E+OO 9.167E-01 9.167E-01 33.46 OK 794.95 4.25 2.087E+00 6.444E-01 6.444E-01 140.58 OK '835.71 1. 61 2.005E+OO Line Not Found Absent 911.20 25.80* 1.871E+OO 7.147E-01 7.147E-01 31. 63 OK 968. 97 15.80 1.778E+OO 9.305E-01 9.305E-01 40.78 OK TH-228 74.82 10.28 8.977E+OO Line Not Found Absent 77 .11 17.10 8. 967E+OO 1.375E+OO 1.375E+OO 14.17 OK Page 83of614 Nuclide Line Activity Report (continued) Page : 3 Sample ID : R405245002 Acquisition date 3-0CT-2016 04:33:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 238.63 43.60* 5.564E+OO 7.lOlE-01 7.lOlE-01 14.56 OK 300.09 3.30 4.613E+OO Line Not Found Absent TH-229 85.43 14.70 8.914E+OO 2.628E-01 2.629E-01 68. 96 OK 88.47 24.00 8.895E+OO 2.188E-01 2.188E-01 48.98 OK 193.51 4.41* 6. 511E+OO Line Not Found Absent 210.85 2.80 6 .116E+OO Line Not Found Ab.sent TH-230 609.32 45.49* 2.581E+OO 9.214E-01 9.214E-01 17.45 OK 1120.29 14.92 1.576E+OO 7.846E-01 7.846E-01 52.53 OK 1764.49 15.30 1.032E+OO 1.089E+00 1.089E+OO 50.43 OK TH-232 105.21 1.10 8.704E+OO Line Not Found . Absent 338.32 11. 27 4.177E+OO 9.167E-01 9.167E-01 33.46 OK 835.71 1. 61 2.005E+OO Line Not Found Absent 911. 20 25.80* 1. 871E+OO 7.147E-01 7.147E-01 31.63 OK 968.97 15.80 1. 778E+OO 9.305E-01 9.305E-01 40.78 OK TH-234 63.29 3.70* 9 .112E+OO 7.863E-01 7.863E-01 125.65 OK 92.59 4.23 8.870E+00 2 .115E+OO 2 .115E+OO 35.86 OK U-234 609.32 45.49* 2.581E+OO 9.214E-01 9.214E-01 17.45 OK 1120.29 14.92 1.576E+OO 7.846E-01 7.846E-01 52.53 OK 1764.49 15:30 1.032E+OO 1.089E+OO 1. 089E+00 50.43 OK U-235 89.96 3.47 8.895E+OO 1.513E+OO 1.513E+OO 48.98 OK 93.35 5.60 8.870E+OO 1.598E+OO 1.598E+OO 35.86 OK 143.76 10. 96* 7.808E+OO Line Not Found Absent 163 .*33 5.08 7.279E+00 Line Not Found Absent 185.72 57.20 6.705E+OO 1.325E-01 1.325E-01 47.81 OK 205.31 5.01 6.238E+OO Line Not Found Absent U-238 63. 29 3.70* 9 .112E+OO 7.863E-01 7.863E-01 125.65 OK 92.59 4.23 8.870E+OO 2.115E+OO 2 .115E+OO 35.86 OK BK-247 84.00. 40.00 8.934E+OO 7.103E-02 7.106E-02 89.14 OK .102.03 7.00 8.754E+OO Line Not Found Absent 106.47 11. 00 8.683E+OO Line Not Found Absent 119. 76 4.00 8.417E+OO Line Not Found Absent 123.68 1. 00 8.326E+OO Line Not Found Absent 265.00 30.00* 5.126E+OO 9.246E-02 9.249E-02 159.89 OK Flag: "*" = Keyline Page 84of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:34:14.52. *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245002.CNF;l *
  • Acquisition date 3-0CT-2016 04:33:24 Sensitivity : 3.000 *
  • Detector ID GAM05 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 Ol:OOi00.55 Half life ratio :* ***** *
  • Sample date 15-DEC-2015 10:19:00 Analyst initials: MXRl *
  • Sample ID R405245002 Sample Quantity 1.4620E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20 .
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.149E+Ol 1.358E+OO CD-109 1. 621E+OO 1. 096E+OO SN-126 l.044E-01 7.057E-02 BA-137M 1.827E-01 5.535E-02 CS-137 1.930E-01 5.847E-02 CE-141 1.597E+Ol 2.234E+Ol HG-203 1. 037E+OO 4.005E+OO TL-208 2.269E-01 5.783E-02 PB-210 1.223E+OO 9.322E-01 PB-212 7.lOlE-01 1.013E-01 BI-214 9.217E-01 1. 576E-01 PB-214 9.734E-01 1.833E-01 RN-222 9.217E-01 1. 576E-01 RA-224 9.455E-01 l.308E+00 RA-226 9.217E-01 1.576E-01 AC-228 7.147E-01 2.216E-01 RA-228 7.147E-01 2.216E-01 TH-228 7.lOlE-01 1. 013E-01 TH-229 4. lllE-02 3.446E-01 TH-230 9.214E-01 1.576E-01 TH-232 7.147E-01 2.216E-01 TH-234 7.863E-01 9.682E-01 U-234 9.214E-01 1. 576E-01 U-235 l.240E-01 1.242E-01 U-238 7.863E-01 9.682E-01 BK-247 9.249E-02 l.449E-01 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 85of614 Key-Line Activity (pc;i/GRAM -1. 411E+OO -2.963E-03 O.OOOE+OO 8.253E-03 K.L. Cnt Uncert (1. 96-sigma) 9.423E+OO 3.606E-02 l.960E+41 2.517E-02 MDA (pCi/GRAM 4.719E-01 1.021E+OO 6.573E-02 5.173E-02 5.464E-02 2.785E+Ol 3.225E+OO 5.302E-02 5.315E-01 7.956E-02 *1.lOlE-01 l.063E-01 1.lOlE-01 8.535E-01 1.lOlE-01 2. 041E-01 2. 041E-01 7.956E-02 6.583E-01 1.lOlE-01. 2.041E-01 7.165E-01 1.lOlE-01 2.557E-01 7.165E-01 1.007E-01 MDA (pCi/GRAM .1.829E+Ol 7.261E-02 O.OOOE+OO 6.048E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 -4.709E-02 2.838E-01 5.338E-01 FAIL ABUN V-48 O.OOOE+OO 8 .167E+03* O.OOOE+OO SHORT HLIF CR-51 0.000E+OO 2.845E+02 O.OOOE+OO SHORT HLIF MN-54 9.319E-03 5.275E-02 l.043E-01 NOT IDENT. C0-56 -3. 511E-01 4.574E-Ol 7.780E-01 NOT IDENT. MN-56 O.OOOE+OO l.309E+41 O.OOOE+OO SHORT HLIF C0-57 -9.265E-04 2.980E-02 5.812E-02 NOT IDENT. C0-58 -2.103E-02 4.699E-01 8.991E-01 NOT IDENT. FE-59 1.073E+OO 5.855E+OO l.194E+Ol NOT IDENT. C0-60 -3.131E-02 3.643E-02 5.990E-02 NOT IDENT. ZN-65 6.694E-02 l.490E-01 2.946E-01 NOT IDENT. GE-68 -7.621E-03 1.609E+OO 3.360E+OO NOT IDENT. AS-73 4.056E-01 1.515E+OO 3.142E+OO NOT IDENT. AS-74 O.OOOE+OO 2.953E+03 O.OOOE+OO SHORT HLIF SE-75 2.563E-01 4.015E-01 3.170E-01 FAIL ABUN BR-77 O.OOOE+OO 2.320E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.606E+02 O.OOOE+OO SHORT HLIF RB-83 1. 979E-01 5.532E-01 1.129E+OO NOT IDENT. KR-85 -1.875E+Ol 7.82.4E+00 1.118E+Ol NOT IDENT. SR-85 -1.840E+OO 7.674E-01 1. 096E+OO NOT IDENT. RB-86 O.OOOE+OO 1.593E+04 O.OOOE+OO SHORT HLIF Y-88

  • 5.782E-02 2.032E-01 4.597E-01 NOT IDENT. Y-91 -2.666E+02 4.379E+02 7.817E+02 NOT IDENT. NB-94 -9.042E-03 2.805E:._02 5.125E-02 NOT IDENT. NB-95 7.622E-01 6.564E-01 l.411E+OO NOT IDENT. NB-95M 7.419E-01 1.945E+OO 3.462E+OO NOT IDENT. ZR-95 6.262E-02 9.712E-01 l.943E+00 NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 8.795E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.755E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 9.488E+40 O.OOOE+OO SHORT HLIF RH-101 0.000E+OO 4.289E-02 4. 301E-02 FAIL*ABUN RH-102 -4.160E-03 4.497E-02 8.803E-02 FAIL ABUN RU-103 -5.818E-01 4.125E+OO 8.023E+00 FAIL ABUN RH-106 -l.935E-01 4.723E-01 8.602E-01 NOT IDENT. RU-106 -1.935E-01 4.723E-01 8.602E-01 NOT IDENT. AG-108M -1.399E-02 2.051E-02 3.758E-02 NOT IDENT. AG-llOM 8.388E-02 6.297E-02 l.612E-01 NOT IDENT. SN-113 -1.557E-01 1.655E-01 2.955E-01 NOT IDENT. CD-115 O.OOOE+OO 3.101E+38 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 5.224E+04 O . .OOOE+OO SHORT HLIF TE-123M 6.150E-02 9.954E-02 1. 986E-01 NOT IDENT. SB-124 -1.718E-01 l.418E+OO 3.004E+00 NOT IDENT. SB-125 2.633E-02 8.626E-02 1. 768E-01 FAIL ABUN TE-125M 7.225E+Ol 1. 7 62E+02 3.326E+02 NOT IDENT. I-126 O.OOOE+OO 7.508E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 6. 691E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.093E+21 0.000E+OO SHORT HLIF I-131 O.OOOE+OO 2.263E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 9.504E+40 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 7.028E+25 O.OOOE+OO SHORT HLIF BA-133 -7.818E-03 3.522E-02 6.190E-02 NOT IDENT. I-133 O.OOOE+OO l.045E+41 O.OOOE+OO SHORT HLIF CS-134 4.192E-02 5.775E-02 1.004E-01 FAIL ABUN CS-135 -1. 671E-01 1. 384E-01 l.941E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.082E+05 O.OOOE+OO SHORT HLIF CE-139 3.877E-04 7.825E-02 1. 492E-01 NOT IDENT. BA-140 O.OOOE+OO 7.973E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.499E+05 O.OOOE+OO SHORT HLIF CE-143. O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CE-144 -1.407E-01 2.639E-01 4.465E-01 NOT IDENT. PM-144 3.701E-02 5. 401E-02 l .112E-01 NOT IDENT. PR-144 3.217E+00 4.676E+OO 9.627E+OO NOT IDENT. PM-146 6.202E-03 3.326E-02 6.803E-02 NOT IDENT. ND-147 O.OOOE+OO 1.714E+07 O.OOOE+OO SHORT*HLIF PM-147 -1.225E+02 5.215E+02 9.998E+02 NOT IDENT. PM-149 O.OOOE+OO 4.149E+39 O.OOOE+OO SHORT HLIF EU-150 l .118E-02 2.301E-02 4.140E-02 FAIL ABUN EU-152 9.243E-02 9.408E-02 l.516E-01 FAIL ABUN GD-153 -4.378E-02 1. ll 7E-01 l.975E-01 NOT IDENT. EU-154 -5.066E-03 8.925E-02 1. 805E-01 NOT IDENT. EU-155 4. 441E-02 6.377E-02 1.326E-01 FAIL ABUN TB-160 -3.327E-01 1.189E+OO 2.217E+OO FAIL ABUN H0-166M -3.863E-02 4. 996E-02 8.524E-02 FAIL ABUN TM-171 -2.645E-01 3.651E+OO 7.408E+OO NOT IDENT. HF-172 4.258E-02 l.671E-01 3.086E-01 FAIL ABUN LU-172 l.530E-02 6.221E-02 1.316E-01 FAIL ABUN Page 86of614 LU-176 -2.269E-02 2.089E-02 3.267E-02 FAIL ABUN HF-181 2.349E+OO 3.237E+OO 6.934E+OO FAIL ABUN TA-182 . 2.945E-01 8.486E-01 1.745E+OO FAIL ABUN RE-183 2.481E-Ol 6.553E-01 l.368E+OO NOT IDENT. RE-184 1.006E+Ol 2.336E+Ol 4.790E+Ol NOT IDENT. W-188 -1.339E+Ol 9.683E+Ol 1.599E+02 FAIL ABUN IR-192 -4.173E-02 3.623E-01 6. 02 6E-01 FAIL ABUN BI-207 l.538E-02 3.974E-02 8.564E-02 FAIL ABUN BI-211 O.OOOE+OO 5.049E-01 7.797E-01 FAIL ABUN PB-211 -5.500E-02 5.704E-01 1.119E+OO NOT IDENT. BI-212 4.886E-01 6.363E-01 9.377E-01 FAIL ABUN RN-219 2.169E-01 2.862E-01 6.214E-01 NOT IDENT. RA-223 -4.078E-02 4.470E-01 8 .131E-01 FAIL ABUN AC"-227 -1.525E-03 l.819E-01 3.371E-01 NOT IDENT. TH-227 -l.525E-03 1.819E-01 3. 371E-01 NOT IDENT. PA-231 -5.029E-02 3. 714E-01 6.675E-01 NOT IDENT. TH-231 -4.078E-02 4.470E-01 8.131E-01 FAIL ABUN PA-233 1. 599E-02 5.078E-02 9.639E-02 *FAIL ABUN PA-234 -9.473E-02 2.512E-01 3.841E-01 FAIL ABUN PA-234M -2:454E+OO 4.278E+OO 7.935E+OO FAIL ABUN NP-237 1.599E-02 5. 078K-02 9.639E-02 FAIL ABUN NP-238 O.OOOE+OO 3.610E+40 O.OOOE+OO SHORT HLIF NP-239 -8.720E-03 l.552E-01 3.024E-01 FAIL ABUN PU-239 O.OOOE+OO 3.905E+02 4.657E+02 FAIL ABUN AM-241 -l.774E-02 3.884E-02 7.085E-02 NOT IDENT. AM-243 O.OOOE+OO 3 .132E-02 7 .135E-02 NOT IDENT. CM-243 * -4.978E-02 5.846E-02 1. 073E-01 FAIL ABUN CM-247 4.474E-04 2.807E-02 5.604E-02 FAIL ABUN CF-249 1.129E-03 3.052E-02 6. lllE-02 NOT*IDENT. CF-251 2.295E-02 7.908E-02 1.553E-01 NOT IDENT. ANH-511 -1.800E-02 4.236E-02 9.021E-02 NOT IDENT. Page 87of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:34:12.01 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 297 10.66* l.244E+OO 1.149E+Ol 1.149E+Ol 12.06 CD-109 88.03 135 3.70* 8.914E+OO 2.102E+OO 3.263E+OO 32.57 SN-126 64.28 52 9.60 9 .112E+OO 3.030E-01 3.030E-01 125.65 86.94 135 8.90 8.914E+OO 8. 739E.:._01 8.739E-01 32.57 87.57 135 37.00* 8.914E+OO 2.102E-01 2.102E-01 32.57 BA-137M 661. 66 76 89.90* 2.417E+OO 1. 793E-01 1.827E-01 30.91 CS-137 661. 66 76 85.10* 2.417E+OO l.895E-01 l.930E-01 30.91 CE-141 145.44 23 48.29* 7. 727E+OO 3.106E-02 1.597E+Ol 142.79 HG-203 70.83 ------3.69 9.006E+OO ------Line Not Found ------72.87 40 6.19 8.988E+OO 3.696E-01 2.881E+Ol 105.40 279.20 25 81.56* 4.912E+OO 3.166E-02 2.468E+OO 164.91 TL-208 277.37 25 6.60 4.912E+OO 3.913E-01 3.913E-01 164.91 583.19 100 85.00* 2.673E+00 2.269E-01 2.269E-01 26.01 860.56 ------12.50 1.959E+OO ------Line Not Found ------PB-210 46.54 95 4.25* 9.664E+00 1.193E+OO 1.223E+OO 77.76 BI-211 72.87 40 1.'23 8.988E+OO 1.860E+OO 1.860E+OO 105'.40 351.06 273 12.92* 4.042E+OO 2. 681E+OO 2. 681E+OO 19.21 PB-212 74.82 ------10.28 8.977E+OO ------Line Not Found ------77 .11 411 17.10 8. 967E+OO 1. 37 5E+OO l.375E+OO 14.17 238.63 335 43.60* 5.564E+OO 7. lOlE-01 7 .16rn-01 14.56 300.09 ------3.30 4.613E+OO ------Line Not Found ------BI-214 609.32 211 45.49* 2.581E+OO 9.214E-01 9.217E-01 17.45 1120.29 36 14.92 1. 576E+OO 7.846E-01 7.849E-01 52.53 1764.49 33 15.30 1.032E+OO 1.089E+OO 1.090E+OO 50.43 PB-214 74.82 ------5.80 8.977E+OO ------Line Not Found ------77 .11 411 9.70 8. 967E+OO 2.424E+OO 2.425E+00 14.17 87.09 135 3.41 8.914E+OO 2.281E+OO 2.282E+OO 32.57 242.00 131 7.25 5.506E+OO 1.683E+OO 1.683E+00 42.48 295.22 193 18.42 4.680E+OO 1.148E+OO 1.148E+OO 21.11 351. 93 273 35.60* 4.042E+OO 9. 731E-01 9.734E-01 19. 21 RN-222 609.32 211 45.49* 2.581E+OO 9.214E-01 9.217E-01 17.45 1120.29 36 14.92 1. 576E+00 7.846E-01 7.849E-01 52.53 1764.49 33 15.30 1.032E+OO 1. 089E+OO 1.090E+OO 50.43 RA-224 240.99 131 4.10* 5.506E+OO 2.975E+OO 2.975E+OO 42.48 RA-226 609.32 211 45.49* 2.581E+OO 9.214E-01 9.217E-01 17.45 1120.29 36 14.92 1. 576E+00 7.846E-01 7.849E-01 52.53 1764.49 33 15.30 1.032E+OO 1.089E+OO l.090E+OO 50.43 AC-228 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 84 11. 27 4.177E+OO 9.167E-01 9.167E-01 33.46 794.95 11 4.25 2.087E+OO 6.444E-01 6.444E-01 140.58 835.71 ------1. 61 2.005E+OO ------Line Not Found ------911.20 67 25.80* 1.871E+OO 7.147E-01 7.147E-01 31. 63 968. 97 51 15.80 l.778E+OO 9.305E-01 9.305E-01 40.78 RA-228 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 84 11. 27 4.177E+OO 9.167E-01 9.167E-01 33.46 794.95 11 4.25 2.087E+OO 6.444E-01 6.444E-01 140.58 835. 71 ------1. 61 2.005E+OO ------Line Not Found ------Page 88of614 Nuclide Line Activity Report (continued) Page : 2 Sample ID : R405245002 Acquisition date 3-0CT-2016 04:33:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 911. 20 67 25.80* 1.871E+OO 7.147E-01 7.147E-01 31. 63 968. 97 51 15.80 1. 778E+OO 9.305E-01 9.305E-01 40.78 TH-228 74.82 ------10.28 8.977E+OO ------Line Not Found ------77 .11 411 17.10 8. 967E+OO 1. 375E+OO 1.375E+OO 14.17 238.63 335 43.60* 5.564E+OO 7.lOlE-01 7. lOlE-01 14.56 300.09 ------3.30 4.613E+OO ------Line Not Found ------TH-229 85.43 135 14.70 8.914E+OO 5.291E-01 5. 2 91E-01* 32.57 88.47 91 24.00 8 .. 895E+OO 2.188E-01 2.188E-01 48.98 193.51 ------4.41* 6. 511E+OO ------Line Not Found ------210.85 ------2.80 6 .116E+OO ------Line Not Found ------TH-230 609.32 211 45.49* 2.581E+OO 9.214E-01
  • 9. 214E-01 17.45 1120.29 36 14.92 1. 57 6E+OO 7.846E-01 7.846E-01 52.53 1764.49 33 *15.30 1.032E+OO 1. 089E+OO l.089E+00 50.43 TH-232 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 84 -11. 27 4.177E+OO 9.167E-01 9.167E-01 33.46 835.71 ------1. 61 2.005E+OO ------Line Not Found ------911.20 67 25.80* 1. 871E+OO 7.147E-01 7.147E-01 31. 63 968. 97 51 15.80 1.778E+OO 9.305E-01 9.305E-01 40.78 TH-234 63.29 52 3.70* 9 .112E+OO 7.863E-01 7.863E-01 125.65 92.59 155 4.23 8.870E+OO 2 .115E+OO 2 .115E+OO 35.86 U-234 609.32 211 45.49* 2.581E+OO 9.214E-01 9.214E-01 17.45 1120.29 36 14.92 1.576E+OO 7.846E-01 7.846E-01 52.53 1764.49 33 15.30 1.032E+OO 1. 089E+OO 1. 089E+OO 50.43 U-235 89. 96 91 3.47 8.895E+00 1.513E+OO l.513E+00 48.98 93.35 155 5.60 8.870E+OO 1.598E+OO l.598E+OO 35.86 143.76 ------10. 96* 7.808E+OO ------Line Not Found ------163.33 ------5.08 7.279E+OO ------Line Not Found ------185.72 99 57.20 6.705E+OO 1.325E-01 l.325E-01 47.81 205.31 ------5.01 6.238E+OO ------Line Not Found ------U-238 63.29 52 3.70* 9 .112E+OO 7.863E-01 -7. 863E-01 125.65 92.59 155 4.23 8.870E+OO 2 .115E+OO 2 .115E+OO 35.86 BK-247 84.00 49 40.00 8.934E+00 7.103E-02 7.106E-02 89.14 102.03 ------7.00 8.754E+OO ------Line Not Found ------106.47 ------11. 00 8.683E+OO ------Line Not Found ------119.76 ------4.00 8.417E+OO ------Line Not Found ------123.68 ------1. 00 8.326E+OO ------Line Not Found ------265.00 28 30.00* 5.126E+OO 9.246E-02 9.249E-02 159.89 Flag: "*"* Key line Page 89of614 Summary of Nuclide Activity Sample ID : R405245002 Acquisition date Page : 3 3-0CT-2016 04:33:24 Total number of lines in spectrum 53 Number of unidentified lines 11 Number of lines tentatively identified by NID 42 79.25% Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 CE-141 HG-203 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 TH-234 U-234 U-235 U-238 BK-247 Hlif e 1. 25E+0'9Y 461.40D 2.30E+05Y 30.08Y 30.08Y 32.51D 46.59D l.41E+10Y 22.20Y 7.04E+08Y 1. 41E+10Y 1600. OOY 1600. OOY 1600. OOY l . .41E+10Y 1600.00Y 1. 4lE+lOY 1.41E+10Y 1. 41E+10Y 7340.00Y 7.54E+04Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 1380.00Y Decay 1. 00 1. 55 1. 00 1. 02 1. 02 514. 77.9 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.149E+Ol 2.102E+OO 2.102E-01 1. 793E-01 l.895E-01 3.106E-02 3.166E-02 2.269E-01 1.193E+OO 2.681E+OO 7.lOlE-01 9.214E-01 9. 731E-01 9.214E-01 2.975E+OO 9.214E-01 7.147E-01 7.147E-01 7. lOlE-01 2.188E-01 9.214E-01 7.147E-01 7.863E-01 9.214E-01 1.325E-01 7.863E-01 9.246E-02 3.247E+Ol 3.247E+Ol Flags: "K" "E" Keyline not found Manually edited Page 90of614 Decay Corr pCi/GRAM 1.149E+Ol 3.263E+OO 2.102E-01 1. 827E-01
  • 1.930E-01 l.597E+Ol 2.468E+OO 2.269E-01 1.223E+00 2.681E+OO 7.lOlE-01 9.217E-01 9.734E-01 9.217E-01 2.975E+00 9.217E-01 7.147E-01 7.147E-01 7. lOlE-01 2.188E-01 9.214E-01 7.147E-01 7.863E-01 9.214E-01 1.325E-01 7.863E-01 9.249E-02 5.204E+Ol 5.204E+Ol Decay Corr 2-Sigma Error 0.139E+Ol 1.063E+OO 0.685E-01 0.565E-01 0.597E-01 2.280E+Ol 4.069E+OO 0.590E-01 0. 951E+OO 0.515E+OO 1.034E-01 1.608E-01 l.870E-01 1.608E-01 l.264E+00 1.608E-01 2.261E-01 2.261E-01 1.034E-01 1. 072E-01 1.608E-01 2.261E-01 9.879E-01 1.608E-01 0.634E-01 9 .*87 9E-01 14.79E-02 Manually accepted 2-Sigma %Error Flags 12.06 32.57 32.57 30.91 30.91 142.79 164.91 26. 01 77.76 19.21 14.56 17.45 19.21 17.45 42.48 17.45 31. 63 31. 63 14.56 48.98 K 17.45 31. 63 125.65 17.45 47.81 K 125.65 159.89 "M" "A" Nuclide specific abn. limit Unidentified Energy Lines Page : 4 Sample ID : R405245002 Acquisition date : 3-0CT-2016 04:33:24 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 111.16 13 136 0.97 224.05 223 7 3.0lE-03 **** 8.60E+00 T 0 128.56 52 104 0.99 258.83 256 7 l.21E-02 77.0 8.21E+OO T 0 131. 48 30 137 1. 31 264 .* 67 263 9 6.87E-03 **** 8.13E+OO T 0 153.57 15 90 0.56 308.80 307 6 3.60E-03 **** 7.54E+OO T 0 208.78 75 118 1. 36 419.16 415 12 1. 81E-02 66.3 6.16E+OO 0 313.44 17 60 1. 34 628.33 623 12 4.17E-03 **** 4.45E+OO 3 341. 71 37 24 1. 66 684.83 673 16 9.25E-03 61. 9 4.14E+OO T 0 344.69 19 29 1. 37 690.80 689 6 4.75E-03 **** 4. llE+OO T 0 462.45 32 39 3.31 926.15 920 13 8.24E-03 91. 0 3.22E+OO T 0 540.47 13 13 3.44 1082.09 1075 10 3.49E-03 **** 2.84E+OO 0 648.28 9 38 6.05 1297.57 1287 18 2.30E-03 **** 2.46E+OO 2 664.89 19 10 1. 74 1330.77 1318 26 5.14E-03 93.7 2.41E+OO T 2 668.19 19 8 1. 87 1337.35 1318 26 5.18E-03 97.0 2.40E+00 T 0. 727.84 14 21 1. 43 1456.57 1449 10 3.83E-03 **** 2.24E+OO T 0 767.88 25 18 2.31 1536.62 1532 9 6.78E-03 76.3 2.15E+00 T 0 772. 02 11 17 0.63 1544.87 1540 9 3.06E-03 **** 2.14E+OO T 0 803.94 17 5 3.39 1608.68 1604 10 4.75E-03 75.7 2.07E+OO 0 934.03 19 10 1. 56 1868.69 1861 13 5.13E-03 83.7 1. 83E+OO o. 949.79 20 4 3.57 1900.19 1893 15 5.60E-03 61. 2 1. 81E+OO T 0 964. 36 22 6 1. 88 1929.33 1924 11 5.97E-03 60.4 l.79E+OO T 0 1028.78 9 5
  • l. 47 2058.08 2054 7 2.42E-03 **** 1. 69E+OO T 4 1148. 31 10 4 1. 72 2296 ."99 2295 19 2.71E-03 71.1 l.54E+00 T 4 1151.32 16 9 1. 87 2303.00 2295 19 4.65E-03 86.0 1.54E+OO 0 1245.48 8 9 1. 32 2491. 22 2485 10 2.16E-03 **** 1.44E+OO 0 1309.85 8 0 1. 50 2619.88 2617 6 2.22E-03 70.7 1.38E+OO 0 1495.95 8 3 4.. 27 2991. 85 2983 14 2.40E-03 **** 1.22E+OO 0 1509.22 12 0 1.16 3018.38 3012 12 3. 61E-03 55.5 1. 21E+OO Flags: "T"* = Tentatively associated Page 91of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:34:30.40 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245002.CNF;l *
  • Acquisition date 3-0CT-2016 04:33:24 Sensitivity 3.000 *
  • Detector ID GAM05 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.55 Half li£e ratio : ***** *
  • Sample date 15-DEC-2015 10:19:00 Nuclide Library : SOLID **
  • Sample ID R405245002 Analyst initials: MXRl *
  • Number 1596387 Sample Quantity : 1.4620E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 * * . Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20 * ******************************************************************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer. to Certificate of Analysis. Identified Nuclides \_ Nuclide K-40 CD-109 SN-126 BA-137M CS-137 CE-141 HG-203 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 TH-234 U-234 U-235 U-238 BK-247 Le (pCi/GRAM 1.833E-01 4.757E-01 3.062E-02 2:253E-02 2.380E-02 1.292E+Ol l.471E+OO 2.338E-02 2.470E-01 3.679E-02 4.900E-02 4. 814E-02 4.900E-02 3.947E-01 4.900E-02 8.742E-02 8.742E-02 3.679E-02 3.038E-01 4.899E-02 8.742E-02 3.362E-01 4.899E-02 l.193E-01 3.362E-01 4.563E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 92of614 Le (pCi/GRAM 8.159E+OO 3.015E-02 O.OOOE+OO 2.332E-02 2.252E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM'--14 6 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 93of614 O.OOOE+OO 0.000E+OO 4.541E-02 3.397E-01 O.OOOE+OO 2.689E-02 3.889E-01 5.227E+OO 2.421E-02 l.272E-01 1.397E+OO 1.475E+OO O.OOOE+OO 1.454E-01 O.OOOE+OO O.OOOE+OO 5.076E-01 5.003E+OO 4.906E-01 O.OOOE+OO l.824E-01 3.324E+02 2.254E-02 6.269E-01 1.607E+OO 8.289E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 1.995E-02 3.814E-02 3.557E+OO 3.815E-01 3.815E-01 1.645E-02 6.919E-02 1.303E-01 O.OOOE+OO O.OOOE+OO 9.285E-02 1.107E+OO 7.986E-02 1.554E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.790E-02 O.OOOE+OO 4.501E-02 8.812E-02 O.OOOE+OO O.OOOE+OO 6.909E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.066E-01 5.022E-02 4.349E+00 3.030E-02 O.OOOE+OO 4. 61'9E+02 O.OOOE+OO 1. 890E-02 6.897E-02 9.203E-02 7.510E-02 6.180E-02 9.064E-01 3.687E-02 3.481E+OO l.437E-01 5.648E-02 l.463E-02 SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT; SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN . NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 AM-243 CM-243 CM-247 CF.-'-249 CF-251 ANH-511 94of614 3.125E+OO 7.679E-01 6.415E-01 2.092E+Ol 7.299E+Ol 2.704E-01 3.701E-02 3.763E-01 5.066E-01 4.215E-01 2.807E-01 3.648E-01 l.540E-01 1.540E-01 3.044E-01 3.648E-01 4.401E-02 1:597E-01 3.484E+OO 4.401E-02 O.OOOE+OO 1.403E-01 2.187E+02 3.317E-02 3.446E-02 4.952E-02 2.527E-02 2.763E-02 7.153E-02 4. 272E-02 FAIL. ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT I DENT .. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:34:36.69 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245002.CNF;l * *Acquisition date 3-0CT-2016 04:33:24 Sensitivity : 3.000 *
  • Detector ID *GAM05 Energy tolerance: 1. 500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.55 Half life ratio : ***** *
  • Sample date 15-DEC-2015 10:19:00 Nuclide Library : SOLID *
  • Sample ID R40524'5002 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : l.4620E+02 GRAM *
  • Quantity Err(%) : 1.3680E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* *
  • CALIBRATION INFORMATION * * * *
  • Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *.
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
  • Combined Activity-MDA Report NOTE: Not all Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1.96-sigma) (1. 96-sigma) K-40 1.149E+Ol 1. 484E+00 1. 484E+OO CD-109 1. 621E+OO 1.122E+OO 1.122E+OO SN-126 1.044E-01 7.208E-02 7.208E-02 BA-137M l.827E-01 5.590E-02 5.590E-02 CS-137 l.930E-01 5.905E-02 5.905E-02 CE-141 1.597E+Ol 2.235E+Ol 2.235E+Ol HG-203 1.037E+OO 4.008E+00 4.008E+OO TL-208 2.269E-01 5.863E-02 5.863E-02 PB-210 1.223E+OO 9.391E-01 9.391E-01 PB-212 7.lOlE-01 1.081E-01 1. 081E-01 BI-214 9.217E-01 1.62,SE-01 1.625E-01 PB-214 9.734E-01 1.877E-01 l.877E-01 RN-222 9.217E-01 1.625E-01 1.625E-01 RA-224 9.455E-01 1.316E+OO 1.316E+OO RA-226 9.217E-01 1. 625E-0'1 l.625E-01 AC-228 7.147E-01 2.246E-01 2.246E-01 RA-228 7.147E-01 2.246E-01 2.246E-01 TH-228 7.lOlE-01 1. 081E-01 1.081E-01 TH-229 4 .111E-02 3.446E-01 3.446E-01 TH-230 9.214E-01 1.625E-01 l.625E-01 TH-232 7.147E-01 2.246E-01 2.246E-01 TH-234 7.863E-01 9.837E-01 9.837E-01 U-234 9.214E-01 1.625E-01 1.625E-01 U-235 1.240E-01 l.244E-01 l.244E-01 U-238 7.863E-01 9.B37E-01 9.837E-01 BK-247 9.249E-02 1.461E-01 1.461E-01 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 9.6-sigma) BE-7 -1. 411E+OO 9.423E+OO 9.444E+OO NOT IDENT. NA-22 -2.963E-03 3.606E-02 3.608E-02 NOT IDENT. NA-24 l.OOOE+41 5.443E+42 O.OOOE+OO SHORT HLIF AL-26 8.253E-03 2.518E-02 2.545E-02 NOT IDENT. Page 95 of 614 SC-46 -4.709E-02 2.838E-01 2.846E-01 FAIL ABUN V-48 -4.551E+03 8.169E+03 8.422E+03 SHORT HLIF CR-51 -5.622E+Ol 2.845E+02 2.856E+02 SHORT HLIF MN-54 9.319E-03 5.275E-02 5.292E-02 NOT IDENT. C0-56 -3. 511E-01 4.576E-01 4.842E-01 NOT IDENT. MN-56 -l.OOOE+41 1.309E+41 O.OOOE+OO SHORT HLIF C0-57 -9.265E-04 2.980E-02 2.980E-02 NOT IDENT. C0-58 -2.103E-02 4.699E-01 4.700E-01 NOT IDENT. FE-59 1.073E+OO 5.855E+OO 5.875E+OO NOT IDENT. .C0-60 -3 .131E-02 3.645E-02 3.909E-02 NOT IDENT. ZN-65 6.694E-02 1.490E-01 l.520E-01 NOT IDENT. GE-68 -7.621E-03 1.609E+OO l.609E+OO NOT IDENT. AS-73 4.056E-01 1. 517E+OO 1.528E+OO NOT IDENT. AS-74 9.519E+02 2.954E+03 2.985E+03 SHORT HLIF SE-7.5 2.563E-01 4.017E-01 4.180E-01 FAIL ABUN BR-77 1.625E+37 1.374E+38 O.OOOE+OO SHORT HLIF SR-82 -3.095E+02 5.608E+02 5.779E+02 SHORT HLIF RB-83 1. 97 9E-01 5.539E-01 5.610E-01 *NOT IDENT. KR-85 -1.875E+Ol 7.861E+OO l.154E+Ol NOT IDENT. SR-85 -1.840E+OO 7.711E-01 l.132E+OO NOT IDENT. RB-86 -7.136E+03 l.593E+04 l.625E+04 SHORT HLIF Y-88 5.782E-02 2.033E-01 2.049E-01 NOT IDENT. Y-91 -2.666E+02 4.380E+02 4.542E+02 NOT IDENT. NB-94 -9.042E-03 2.806E-02 2.835E-02 NOT IDENT. NB-95 7.622E-01 6.572E-01 7.416E-01 NOT IDENT. NB-95M .7.419E-01 1. 946E+OO 1. 975E+OO NOT IDENT. ZR-95 6.262E-02 9.712E-01 9. 717E-01 NOT IDENT. NB-97 1.000E+41 2.458E+41 O.OOOE+OO SHORT HLIF ZR-97 -1. OOOE+41 8.805E+40 O.OOOE+OO SHORT HLIF M0-99 1. 533E+31 2.757E+31 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 9.539E+40 O.OOOE+OO SHORT HLIF RH-101 5.686E-02 4.410E-02 5.lOlE-02 FAIL ABUN RH-102 -4.160E-03 4.497E-02 4.501E-02 FAIL ABUN RU-103 -5.818E-01 4.125E+00 4.134E+00 FAIL ABUN RH-106 -l.935E-01 4.725E-01 4.805E-01 NOT IDENT. RU-106 -1.935E:...01 4.725E-01 4.805E-01 NOT IDENT. AG-108M -1.399E-02 2.052E-02 2.147E-02 NOT IDENT. AG-llOM 8.388E-02 6.312E-02 7.358E-02 NOT IDENT. SN-113 -1.557E-01 1.656E-01 1. 799E-01 NOT IDENT. CD-115 -1.006E+38 3.106E+38 O.OOOE+OO SHORT HLIF SN-ll 7M 6.616E+04 5.280E+04 6.064E+04 SHORT HLIF TE-123M 6.150E-02 9.957E-02 l.034E-01 NOT IDENT. SB-124 -1.718E-01 1.418E+OO 1.421E+OO NOT IDENT. SB-125 2.633E-02 8.626E-02 8.708E-02 FAIL ABUN TE-125M 7.225E+Ol l.763E+02 l.792E+02 NOT IDENT. I-126 8.173E+05 7.586E+05 8.434E+05 SHORT HLIF SB-126 1.225E+05 6.694E+05 6. 717E+05 SHORT HLIF SB-127 -2. 770E+21
  • 7.138E+21 O.OOOE+OO SHORT HLIF I-131 -l.462E+09 2.264E+09 2.358E+09 SHORT HLIF I-132 l.000E+41 1.807E+42 O.OOOE+OO SHORT HLIF TE-132 6.523E+25 7.490E+25 O.OOOE+OO SHORT HLIF BA-133 -7.818E-03 3.522E-02 3.540E-02 NOT IDENT. I-133 1.000E+41 2.052E+41 O.OOOE+OO SHORT HLIF CS-134 4.192E-02 5.778E-02 6.079E-02 FAIL ABUN CS-135 -1.671E-01 1. 389E-01 1. 580E-01 NOT IDENT. I-135 1.000E+41 1.356E+42 O.OOOE+OO SHORT HLIF CS-136 -l.060E+05 2.085E+05 2.140E+05 SHORT HLIF CE-139 3.877E-04 7.825E-02 7.825E-02 NOT IDENT. BA-140 -6.390E+05 7.977E+05 8.481E+05 SHORT HLIF LA-140 -2. 496E+05 2. 501E+05 2.743E+05 SHORT HLIF CE-143 1.000E+41 2.433E+41 O.OOOE+OO SHORT HLIF CE-144 -1.407E-01 2.640E-01 2.715E-01 NOT IDENT. PM-144 3.701E-02 5.406E-02 5.657E-02 NOT IDENT. PR-144 3.217E+00 4.678E+OO 4.898E+OO NOT IDENT. PM-146 6.202E-03 3.326E-02 3.338E-02 NOT IDENT. ND-147 l.512E+06 1.714E+07 1. 716E+07 SHORT HLIF PM-147 -l.225E+02 5.215E+02 5.244E+02 NOT IDENT. PM-149 l.879E+39 4.169E+39 O.OOOE+OO SHORT HLIF EU-150 l .118E-02 2.301E-02 2.356E-02 FAIL ABUN EU-152 9.243E-02 9.422E-02 l.030E-01 FAIL ABUN GD-153 -4.378E-02 l.117E-01 l.135E-01 NOT IDENT. EU-154 -5. 0.66E-03 8.925E-02 8.928E-02 NOT IDENT. EU-155 4.441E-02 6.384E-02 6.691E-02 FAIL ABUN TB-160 -3.327E-01 1.189E+OO l.198E+OO FAIL ABUN H0-166M -3.863E-02 5.00lE-02 5.295E-02 FAIL ABUN TM-171 -2.645E-01 3.651E+OO 3.653E+OO NOT IDENT. HF-172 4.258E-02 1. 672E-01 l.683E-01 FAIL ABUN LU-172 1.530E-02 6.223E-02 6.261E-02 FAIL ABUN Page 96of614 LU-176 -2.269E-02 2.091E-02 2.328E-02 FAIL ABUN HF-181 2.349E+OO 3.239E+OO 3.407E+OO FAIL ABUN TA-182 2.945E-01 8.486E-01 8.590E-01 FAIL ABUN RE-183 2.481E-01 6.564E-01 6.659E-01 NOT IDENT. RE-184 1.006E+Ol 2.348E+Ol 2. 391E+Ol NOT IDENT. W-188 -l.339E+Ol 9.685E+Ol 9.703E+Ol FAIL ABUN IR-192 -4.173E-02 3.623E-01 3.628E-01 FAIL ABUN BI-207 1.538E-02 3.974E-02 4.034E-02 FAIL ABUN BI-211 2.681E+OO 5.190E-01 l.315E+OO FAIL ABUN PB-211 -5.500E-02 5.704E-01 5.709E-01 NOT IDENT. BI-212 4.886E-01 6.368E-01 6.738E-01 FAIL ABUN RN-219 2.169E-01 2.875E-01 3.036E-01 NOT IDENT. RA-223 -4.078E-02 4.470E-01 4.473E-01 FAIL ABUN AC-227 -l.525E-03 1.819E-01 l.819E-01 NOT IDENT. TH-227 -l.525E-03 1.819E-01 l.819E-01 NOT IDENT. PA-231 -5.029E-02 3.716E-01 3.723E-01 NOT IDENT. TH-231 -4.078E-02 4.470E-01 4.473E-01 FAIL ABUN PA-233 1.599E-02 5.079E-02 5.130E-02 FAIL ABUN. PA-234 -9.473E-02 2.736E-01 2.769E-01 FAIL ABUN PA-234M -2.454E+OO 4.280E+OO 4.420E+OO FAIL ABUN NP-237 1.599E-02 5.079E-02 5.130E-02 FAIL ABUN NP-238 5.448E+39 3.610E+40 O.OOOE+OO SHORT HLIF NP-239 -8.720E-03 1.552E-01 1.553E-01 FAIL ABUN PU-239 5.178E+02 3.912E+02 4.556E+02 FAIL ABUN AM-241 -1. 77 4E-02 3.886E-02 3. 967E-02 NOT IDENT. AM-243 1.508E-01 3.265E-02 7.541E-02 NOT IDENT. CM-243 -4.978E-02 5.864E-02 6.279E-02 FAIL ABUN CM-247 4.474E'-04 2.807E-02 2.807E-02 FAIL ABUN CF-249 l.129E-03 3.052E-02 3.052E-02 NOT IDENT. CF-251 2.295E-02 7.913E-02 7.980E-02 NOT IDENT. ANH-511 -l.800E-02 4.237E-02 4.314E-02 NOT I DENT .. Page 97of614
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 55.2632 87.09 62.0565 136.47 58.3932 "45.60 58.0361 87.57 62.1304 140.51 0.0000 46.54 58.2461 88.03 62.2005 143.76 40.4132 49. 72 0.0000 88:34 62.2474 144.24 46.0365 51. 35 79.0527 88.47 62. 2673 145.44 55.3566 51. 87 72.8633 89. 96 62.4927 152.43 50.6713 52.39 72.9973 1093.63 62.5951 153.25 0.0000 52.97 65.9902 91.11 0.0000 323.87 57.1705 53.44 62.9130 92. 59 62. 8863 156.02 0.0000 54.07 76.6183 93.35 62.9990 158.56 0.0000 57.36 0.0000 94. 56 63.1774 159.00 55.5908 57.53 65.4059 94.65 63.1909 162.33 50.8026 57.98 67 .1199 94.67 63.1936 162.66 0.0000 59.27 77.9597 94.87 63.2227 163.33 53.9349 59.32 77. 9725 97.43 67 .1961 165.86 52.1035 59.54 83.4464 98.43 44.1975 176.31 58 .1166 60. 96 71. 8511 98.44 44.1984 176.60 0.0000 61.17 76.8010 99.53 60.5833 177.52 40.5455 62. 93 77.2259 100 .11 64.2836 181.07 0.0000 63.29 77.3122 102.03 42.7354 181.52 44.6152 63.58 75.7349 103.18 56.5167 184.41 48.9994 64.28 83.5974 103.37 65.6592 143.76 47.3373 66.73 84.7722 105.21 52.1881 193.51 45.7256 67.24 96. 5537 105.31 48.5363 197.03 52.3556 125.81 90.8453 106.12 52.2903 198.01 44.9352 67.75 92.5308 106.47 64.2642 201.83 50.5414 69.67 67.0648 109.28 59.1060 203.43 42.0272 70.83 78.5029 111. 00 65.4974 205.31 46.0924 72.81 74.4326 111.76 0.0000 210.85 38.0820 72.87 74.4454 114. 06 52.2300 215.65 33.9361 74.66 74.8160 116. 30 0.0000 222 .11 47.4518 74.82 74.8489 116.74 56.2637 227.09 36.6386 74.97 74.8798 119.76 58.4873 227.38 33.3192 77.11 75.3168 121.12 53.9137 228.16 0.0000 78.74 75.6458 121. 22 53.9241 228.18 40.0221 79.69 75.8358 121. 78 57.7706 116.74 40.0221 80.12 75.9211 122.06 52 .1168 235.69 47.8587 80.19 0.0000 122.92 52.2033 235. 96 47.8744 80.57 76.0104 123.07 56.0161 238.63 50.6497 81. 00 76.0956 265.00 62.7350 238.98 0.0000 81. 07 76.1097 125.81 55.9910 240.99 50.7884 81. 75 51. 9841 127.23 57.4162 242.00 50.8482 83.79 74.9009 127.91 49.8243 244.70 31. 7367 84.00 60.9985 129.30 49.9529 252.40 0.0000 85.43 61.2185 131. 20 50.1282 252.80 17.1577 86. 55 61. 9740 133.02 63.1910 254.15 0.0000 86. 79 62.0107 133.52 63.2478 256.23 37.8904 86.94 62.0339 136.00 51.8620 260.90 0.0000 . Page 98of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 31.2863 355.39 0.0000 584.27 18. 7271 264.80 31.2913 356.01 31.5979 595.83 0.0000 265.00 31. 2979 364.49 0.0000 427.87 18.8995 268.22 58.9343 366.42 0.0000 602.52 0.0000 269.46 36.1058' 372. 51 40.1506 604.72 13.4588 270.03 32. 6313 375.05 26.5378 607.14 23.9590 271.23 49.0085 377.52 30.8796 609.32 21. 9884 273.65 0.0000 356.01 25.0021 610.33 22.0009 276.40 36.3688 388.16 29.4131 614.28 16.5363 .277. 37 36.4057 388.63 0.0000 618.01 16.0671 277.60 36.4142 391;69 31.2305 620. 36 22.1208 278.00 36.4294 264.66 20.0927 621.93 26.1650 279.20 36.4748 401. 81 19.2361 630.19 0.0000 279.54 29.8174 402.40 27.9922 631.29 13.1476 279.70 29.8220 404.85 32.4269 633.25 15.1862 280.46 34.5581 410.95 25.5337 634.78 0.0000 283.69 29.5502 413. 71 28.2337 635.95 19.2636 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 27.2339 423. 72 0.0000 645.85 13.2486 285.90 0.0000 427.09 23.1689 657.76 10.7670 287.50 35.5966 427.87 24. 9654 657.90 0.0000 290.67 39.6779 433.94 25.0759 661.66 15.4120 293.27 0.0000 439.40 21. 5781 664.57 0.0000 351.93 41. 8498 453.88 19.9832 666.33 0.0000 295.96 55.8411 463.37 20.1147 666.50 0.0000 879.38 47.9858 468.07 23 .1144 667.71 0.0000 299.98 46.8505 473.00 0.0000 677. 62 10.3581 300.09 46.8552 475.06 22.1177 685.70 0.0000 300.13 46.8576 476.78 21. 2209 695.00 0.0000 301.36 38.4932 477.60 24.9247 696.49 19.8643 302.85 34.9349 482.18 18.5193 696. 51 19.8651 256.23 30.1636 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 23.0107 306.78 43. 5311 497.08 22.4409 697.49 24.0585 308.46 25. 8372 505.52 35.7247 702.65 22.0220 311. 90 31.5923 507.63 0.0000 706.68 26.2675 316.51 27.6610 511. 00 38.6794 711.68 21. 0645 319.41 0.0000 514.00 68.9989 720.70 0.0000 320.08 0.0000 514.00 68.9989 721. 93 0.0000 321. 04 20.8329 520.40 21. 8264 722.78 22.2347 323.87 27.0307 520.69 0.0000 722. 91 22.2365 325.23 27.0643 522.65 0.0000 723.31 22.2407 328.76 0.0000 527.90 0.0000 724 .19 19.0715 333.37 -28.0898 528.26 20.0259 727.33 11.1413 333.97 28.1051 529.59 15.2702 733.00 17.0228 334.37 26.4609 529.87 0.0000 735.93 21. 3078 338.28 23.2342 531.02 0.0000 333.97 22.3885 338.32 23.2348 537.26 0.0000 739.50 0.0000 311. 90 23.2792 546.56 0.0000 747.24 19.2773 340.48 23.2792 552.55 14.5154 748.06 16.0706 340.55 0.0000 563.25 21.4235 752.31 22.5432 344.28 12.5125 569.33 18.5678 753.82 0.0000 345.93 30.0732 946.00 18.5702 756.73 10.7564 351.06 31. 0456 569.70 20.5266 756.80 10.7568 351.93 31. 0689 583.19 18.7163 884.68 19.4253 Page 99of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 8.1006 1274. 4*4 14.2202 1620.50 0.0000 766.42 9.7233 1001.03 21. 3669 1621.92 2.1299 766.84 11. 3459 1002.74 18.7076 1678.03 0.0000 772.60 o.o*ooo 1004.73 10.6974 1690.97 3.2463 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 6.5999 778.90 13.0371 1028.54 0.0000 1063.66 1. 7 621 783.70 0.0000 1037.84 7.2153 1771. 35 6.6097 785.37 19.6121 1038.76 0.0000 1791.20 0.0000 792.07 19.6699 631. 29 18.0933 1808.65 2.2211 15.3182 1048.07 0.0000 1810.72 0.0000 795.86 1'8.0610 1049.04 15.3928 1836.06 3.3510 810.06 15.4190 1050.41 9.9647 810.29 14.3187 1063.66 10.0097 344.28 14.3198 1077.00 0.0000 810.76 14.3219 1077.34 8.2282 815.77 0.0000 1085.87 13.7531 1048.07 0.0000 1093.63 10 .1118 832.01 12.2282 1099.45 14.7363 834.85 13.3560 1112. 07 18.4973 835.71 11.1340 1112.84 17.5759 836.80 0.0000 1115. 54 8.8887 846.75 0.0000 1120. 29 15.7642 846.77 21.2521 1120.55 15.7663' 856.80 0.0000 1221.41 14.8418 '860.56 17.9987 1129. 67 8.3716 871.09 20.3350 1131.51 0.0000 873.19 10.1763 1147.95 0.0000 875.33 0.0000 1173.23 14.1467 879.38 9.0680 1177.95 12.2787 880.51 11. 3403 1189.05 15.1650 883.24 4.5410 1204.77 17.1431 884.68 2.2718 1221.41 14.3582 889.28 11. 3802 1231.02 21.1205 894.76 15. 9665 1235.36 0.0000 898.04 11. 4197 1238.28 14.2940 900. 72 14.8609 1260.41 0.0000 903.28 11. 4429 1271.87 7.7734 911. 20 12.0526' 1274.44 8.7517 912.08 15.5012 1274.54 8.7517 923.98 0.0000 1291.59 5.8634 926.50 11. 5466 1298.22 0.0000 929 .11 6.9348 1312 .11 0.0000 937.49 10.4355 1332.49 12.8524 944.13 0.0000 1362. 66 0.0000 946.00 12.2141 1365.19 3.9907 949.00 8.1519 1368.63 0.0000 667.71 0.0000 1384.29 5.0143 962.31 12.6400 1408.01 2.0186 964.08 11. 2430 1457.56 0.0000 966.17 0.0000 1460.82 4.0935 911. 20 8.4475 1489.16 1. 6494 968.97 8.4475 1505.03 4. 9682 983.53 0.0000 1584.12 9.4982 984.45 0.0000 1596.21 0.0000 Page VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:35:09.55 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * *****t************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245003.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM06.CNF;499 Background date : Z-OCT-2016 11:00:12. Sample date 15-DEC-2015 10:18:00 Acquisition date : 3-0CT-2016 04:33:45. Sample ID R405245003 Sample quantity 1.39591E+02 GRAM Detector name : GAM06 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: *o 01:00:00.57 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596387 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 6 6 6 6 0 0 0 0 0 0 0 0 4 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 101of614 Energy 62.98* 74.90* 77.22 84.07* 86.98 89.88 92.92* 106.95 128.44 140.14* 185.44* 209.34 238.58* 242.01* 270.78* 278.23 '286.81 288.75 295.09* 300.58 328.96 351.98 432.88 446.86 452.84 467.87 470.69 504.73 511. 24* 583.29* 609.34* 645.09 661.59 681.05 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 51 98 153 37 84 51 110 73 19 6 40 48 221 44 11 25 15 17 85 17 35 194 16 11 13 10 15 6 25 99 88 16 22 5 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 113 1. 41 107 1. 09 92 1. 24 7 9 1. 68 95 1. 61 65 1.14 89 1.71 83 4.40 77 1. 24 77 1. 00 138 1.18 72 . 0.86 78 1. 02 63 1. 27 69 1.14 28 1. 80 28 1.24 44 1. 82 40 1. 23 39 1. 70 23 3.36 52 1.19 23 1.79 19 0.92 29 0.69 19 1.15 16 0.66 17 0.87 31 1. 88 20 1.42 50 1. 52 16 1. 58 .17 2.52 10 0.49 125.68 149.49 154.12 167.81 173.64 179.42 185.49 213.55 256.49 279.88 370.39 418.16 476.61 483.47 540.97 555.84 573.00 576.87 589.55 600.52 657.24 703.27 864.97 892.92 904.88 934.91 940.54 1008.59 1021. 62 1165. 65 1217.73 1289.20 1322.20 1361.10 120 144 144 164 164 164 164 208 254 276 366 413 473 481 535 552 552 552 585 597 653 698 859 889 898 929 937 1004 1015 1159 1212 1281 1316 1356 10 l.41E-02 42.5 20 2.73E-02 20.0 2.23E+00 20 4.25E-02 14.0 30 1.02E-02 46.7 1.lOE+OO 30 2.32E-02 25.0 30 1.43E-02 30.4 30 3.05E-02 20.2 12 2.02E-02 27.8 7 5.21E-03 80.5 7 1.54E-03272.5 11 1.lOE-02 60.7 10 1.32E-02 36.4 8 6.14E-02 9.8 8 1. 21E-02 37. 2 10 3.12E-03145.4 30 6.94E-03 40.4 2.82E+OO 30 4.29E-03 60.8 30 4.84E-03 78.4 8 2.37E-02 17.4 8 4.67E-03 68.3 9 9.80E-03 29.5 10 5.40E-02 10.0 9 4.44E-03 60.8 8 3.0lE-03 77.2 10 3.70E-03 81.1 8 2.81E-03 82.2 8 4.04E-03 54.6 7 1.65E-03119.4 16 7.04E-03 63.9 15 2.76E-02 14.6 15 2.43E-02 20.8 12 4.36E-03 59.l 10 5.98E-03 42.2 8 1.51E-03108.9 Peak Search Report (continued) Page : 2 Sample ID : R405245003 Acquisition date 3-0CT-2016 04:33:45 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 729.59 52 22 . 6. 44 1458.15 1447 23 1.45E-02 27.5 36 0 768.42 19 9 1.17 1535.80 1530 11 5.20E-03 40.8 37 0 786.45 5 10 0.79 1571.86 1565 8 1. 41E-03116. 8 38 0 806.09 10 7 1. 01 1611.13 1608 6 2.88E-03 51.2 39 0 911.01* 38 27 1.12 1820.93 1814 15 1. 05E-02 34 .1 40 0 969. 52 29 12 1. 47 1937.94 1932 13 8. 09E-03 31. 3 41 5 997.79 8 2 2.08 1994.47 1993 15 2.28E-03 28.6 2.55E+OO 42 5 1000.55 25 6 1. 79 2000.00 1993 15 6.84E-03 25.7 43 0 1009.10 14 5 3.89 2017.09 2011 11 3.82E-03 42.5 44 0 1018.37 9 6 0.79 2035.63 2028 10 2.61E-03 55.8 45 0 1120.79* 21 25 0.65 2240.47 2231 16 5.92E-03 59.3 46 0 1200.89 9 14 1. 04 2400.69 2392 12 2. 51E-03 91.2 47 0 1210.55 11 2 1.13 2420.01 2416 8 3.04E-03 37.6 48 0 1239.01* 14 15 0.86 2476.94 2466 15 4.00E-03 65.0 49 0 1459.87* 213 7 2.48 2918.77 2912 14 5.93E-02 7.4 50 0 1762.91 28 0 1. 46 3525.14 3517 14 7.78E-03 18.9 Flag: "*" = Peak area was modified by background subtraction Page 102 of 614 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 05:35:11 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245003.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 15-DEC-2015 10:18:00 R405245003 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 04:33:45 139.59 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA6 0 01:00:00-.00 1.50 keV No Empirical 75.00 Interference Report Interfering Page 103of614 Nuclide PB-214 PB-214 PB-214 PB-214 TL-208 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 277.37 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Sys.tematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 HG-203 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 . 88. 03 279.20 74.66 74.82 74.82 351.06 CAN 0 01:00:00.57 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : R405245003 Acquisition date 3-0CT-2016 04:33:45 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.005E+OO 1.027E+Ol 1.027E+Ol 14.84 OK CD-109 88.03 3.70* 5.183E+OO 2.151E+OO 3.340E+OO 66.31 OK SN-126 64.28 9 .*60 2.597E+OO 1.343E+OO 1.343E+OO 85.08 OK 86.94 8.90 5.183E+OO 8.944E-01 8.944E-01 66.31 OK 87.57 37. 00*. 5.183E+OO 2 .15rn.:...01 2.151E-01 66.31 OK BA-137M 661.66 89.90* 2.028E+OO 6.523E-02 6.645E-02 84.47 OK CS-137 661.66 85.10* 2.028E+OO 6.891E-02 7.020E-02 84.47 OK HG-203 70.83 3.69 3.616E+OO Line Not Found Absent 72.87 6.19 3.859E+OO Line Not Found Absent 279.20 81. 56* 3.949E+OO 2.241E-02 1. 747E+OO 168.54 OK TL-208 277.37 6.60 3.958E+OO Line Not Found <<INT Reject 583.19 85.00* 2.243E+OO 2. 911E-01 2. 911E-01 29.14 OK 860.56 12.50 1.624E+OO Line Not Found Absent BI-211 72. 87 1. 23 3.859E+OO Line Not Found Absent 351.06 12.92* 3.303E+OO 6.575E-01 6.575E-01 132.62 OK PB-212 74.82 10.28 4.088E+OO l.120E+00 1.120E+OO 55.88 OK 77 .11 17.10 4.336E+OO 1.344E+OO 1.344E+OO 27. 96 OK 238.63 43.60* 4.430E+OO 6.858E-01 6.858E-01 19.59 OK 300.09' 3.30 3. 724E+OO 8.057E-01 8.057E-01 '136. 60 OK BI-214 609.32 45.49* 2.166E+OO 4.937E-01 4.938E-01 41. 69 OK 1120.29 14.92 1. 27 9E+OO 5.890E-01 5.892E-01 118. 70 OK 1764.49 15.30 8.592E-01 Line Not Found Absent PB-214 74.82 5.80 4.080E+OO Line Not Found * <<INT Reject 77 .11 9.70 4.336E+OO 2.368E+OO 2.369E+OO 27. 96 OK 87.09 3.41 5.190E+OO Line Not Found <<INT Reject 242.00 7.25 4.384E+OO Line Not Found <<INT Reject 295.22 18.42 3.777E+OO 7.220E-01 7.223E-01 34.84 OK 351. 93 35.60* 3.304E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.166E+OO 4.937E-01 4.938E-01 41.69 OK 1120.29 14.92 1.279E+00 5.890E-01 5.892E-01 118.70 OK 1764.49 15.30 8.592E-01 Line Not Found Absent RA-224 240.99 4.10* 4.384E+OO 1.740E-01 1. 740E-01 671.36 OK RA-226 609.32 45.49* 2.166E+OO 4. 937E-01 4.938E-01 41. 69 OK 1120.29 14.92 l.279E+OO 5.890E-01 5.892E-01. 118.70 OK 1}64.49 15.30 8.592E-01 Line Not Found Absent TH-228 74.82 10.28 4.088E+00 1.120E+OO i.120E+o*o 55.88 OK 77 .11 17.10 4.336E+OO 1.344E+OO 1.344E+OO 27. 96 OK 238.63 43.60* 4.430E+OO 6.858E-01 6.858E-01 19.59 OK 300.09 3.30 3. 724E+OO 8.057E-01 8.057E-01 136.60 OK TH-229 85.43 14.70 4.963E+OO 3.260E-01 3.260E-01 93.48 OK 88.47 24.00 5.374E+OO 2.567E-01 2.567E-01 60.87 OK 193.51 4.41* 5.130E+OO -----Line Not Found Absent 210.85 -2. 80 4.841E+OO Line Not Found Absent TH-230 609.32 45.49* 2.166E+OO 4.937E-01 4.937E-01 41. 69 OK 1120.29 14.92 l.279E+OO 5.890E-01 5.890E-01 118.70 OK 1764.49 15.30 8.592E-01 Line Not Found Absent PA-231 283.69 1. 70 3.891E+OO Line Not Found Absent 301.36 5.35* 3. 724E+00 4.970E-01 4.970E-01 136.60 OK TH-234 63.29 3.70* 2.597E+OO 3.485E+OO 3.485E+OO 85.08 OK Page 104 of 614 Nuclide Line Activity Report (continued) Page : 3 Sample ID : R405245003 Acquisition date 3-0CT-2016 04:33:45 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 92.59 4.23 5.549E+OO 3.009E+OO 3.009E+OO 40.48 OK U-234 609.32 45.49* 2.166E+OO 4.937E-01 4.937E-01 41. 69 OK 1120.29 14.92 l.279E+OO 5.890E-01 5.890E-01 118.70 OK 1764.49 15.30 8.592E-01 Line Not Found Absent U-235 89. 96 3.47 5.374E+OO 1. 776E+OO 1. 776E+OO 60.87 OK 93.35 5.60 5.549E+OO 2.273E+OO 2.273E+OO 40.48 OK 143.76 10.96* 5.990E+OO Line Not Found Absent 163.33 5.08 5.669E+OO Line Not Found Absent 185.72 57.20 5.272E+OO 8. 051E-02 8.051E-02 121.47 OK 205.31. 5.01 4.931E+OO Line Not Found Absent U-238 63.29 3.70* 2.597E+00 3.485E+OO 3.485E+OO 85.08 OK 92.59 4.23 5.549E+OO 3.009E+OO 3.009E+OO 40.48 OK AM-243 43.53 5.90 3.924E-01 Line Not Found Absent 74.66 67.20* 4.088E+OO 1.714E-01 l.714E-01 55.88 OK ANH-511 511. 00 100.00* 2.486E+OO 5. 751E-02 5.751E-02 127.71 OK Flag: "*" = Keyline Page 105of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:35:12.67 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245003.CNF;l *
  • Acquisition date 3-0CT-2016 04:33:45 Sensitivity : 3.000 *
  • Detector ID GAM06 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • real time: 0 01:00:00.57 Half life ratio : ***** *
  • Sample date 15-DEC-2015 10:18:00 Analyst initials: MXRl *
  • Sample ID R405245003 Sample Quantity 1.3959E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 8-MAR-2016 07:26:53 Eff, Geometry : CAN * '* Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4
  • Combined Activity-MDA Report Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.027E+Ol l.493E+OO CD-109 3.340E+OO 2.171E+OO SN-126 2.151E-01 l.398E-01 BA-137M 6.645E-02 5.501E-02 CS-137 7.020E-02 5.811E-02 HG-203 1. 747E+OO 2.885E+OO TL-208 2. 911E-01 8. 313E-02 BI-211 6.575E-01 8.545E-01 PB-212 6.858E-01 1.316E-01 BI-214 4.938E-01 2.017E-01 PB-214 9.610E-01 1.883E-01 RN-222 4.938E-01 2.017E-01 RA-224 1.740E-01 1.145E+OO RA-226 4.938E-01 . 2. 017E-01 TH-228 6.858E-01 l.316E-01 TH-229 1.472E-01 4. llOE-01 TH-230 4.937E-01 2.017E-01 PA-231 4.970E-01 6.653E-01 TH-234 3.485E+00 2.905E+OO U-234 4.937E-01 2.017E-01 U-235 1.603E-03 l.646E-01 U-238 3.485E+OO 2.905E+OO AM-243 1.714E-01 9.387E-02 ANH-511 5.751E-02 7.198E-02 Non-Identified Nuclides Nuclide BE-7 f'.)"A-22 NA-24 AL-26 SC-46 V-48 Page 106of614 Key-Line Activity (pCi/GRAM 6.326E+OO -9. 7 51E-03 O.OOOE+OO 2.281E-02 1. 761E-01 O.OOOE+OO K.L. Cnt Uncert ( 1 . 96-sigma ) 1.109E+Ol 5.054E-02 1. 960E+41 2.366E-02 3.709E-01 1.079E+04 MDA (pCi/GRAM 6. 651E-01 1.455E+OO 9.425E-02 6.282E-02 6.637E-02 3.567E+OO 5.440E-02 3.490E-01 1.080E-01 1.058E-01 3.381E-01 1.058E-01 1.218E+OO 1.058E-01 1. 080E-01 7.976E-01 1. 058E-01 7.758E-01 2.068E+OO 1.058E-01 3. lllE-01 2.068E+OO 8.083E-02 4.657E-02 MDA (pCi/GRAM 2.339E+Ol 9.832E-02 O.OOOE+OO 7.339E-02 7.775E-01 O.OOOE+OO )' NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 3. ll 7E+02 O.OOOE+OO SHORT HLIF MN-54 7.700E-03 6.068E-02 l.201E-01 NOT IDENT. C0-56 -l.667E-01 3.752E-01 6.673E-01 FAIL ABUN MN-56 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-57 -2.167E-02 4.134E-02 7.501E-02 NOT IDENT. C0-58 -3.004E-01 4.309E-01 7.139E-01 NOT IDENT. FE-59 -1. 371E+OO 7.038E+OO l.365E+Ol NOT IDENT. C0-60 2.424E-02 3.444E-02 8.452E-02 NOT IDENT . ZN-65 2.748E-02 . 1. 942E-01 3.586E-01 NOT IDENT. GE-68 8.989E-02 2.510E+OO 5.104E+OO NOT IDENT. AS-73 2.816E+OO 9.446E+OO l.939E+Ol NOT IDENT. AS-74 O.OOOE+OO 4 .151E+o3 O.OOOE+OO SHORT HLIF SE-75 -2.556E-01 2.099E-01 3.195E-01 FAIL ABUN BR-77 O.OOOE+OO 3.014E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.088E+02 O.OOOE+OO SHORT HLIF RB-83 -3.816E-02 6.165E-01 l.200E+OO NOT IDENT. KR-85 2.045E+OO 6.060E+OO l.254E+Ol NOT IDENT. SR-85 2.000E-01 5.944E-01 l.230E+00 NOT IDENT. RB-86 O.OOOE+OO 2.415E+04 O.OOOE+OO SHORT HLIF Y-88 -5.704E-02 2.030E-01 4.042E-01 NOT IDENT. Y-91 2.784E+02 5.049E+02 l.003E+03 NOT IDENT. NB-94 9.614E-03 3.493E-02 6.909E-02 NOT I DENT .. NB-95 -l.514E-01 8.974E-01 l.473E+OO NOT IDENT. NB-95M 8.180E-01 2.071E+OO 3.724E+OO NOT I DENT. ZR-95 -7.747E-01 l.453E+OO 2.531E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.375E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.671E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO L 960E+41 O.OOOE+OO SHORT HLIF RH-101 3.330E-02 5.253E-02 5.145E-02 FAIL ABUN RH-102 -3.298E-02 4.741E-02 8.179E-02 NOT IDENT. RU-103 -2.737E+OO 4.585E+OO 8.290E+OO FAIL ABUN RH-106 -3.395E-01 4.155E-01 6. 967E-01 NOT IDENT. RU-106 -3.395E-'-01 4.155E-01 6.967E-01 NOT IDENT. AG-108M 3. 585E-02 . 4.273E-02 5.028E-02 FAIL ABUN AG-llOM -4.974E-02 l.025E-01 l.777E-01 NOT IDENT. SN-113 -1.454E-01 2.128E-01 3.877E-01 NOT IDENT. CD-115 O.OOOE+OO 3.021E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 6.502E+04 O.OOOE+OO SHORT HLIF TE-123M 7.576E-03 l.195E-01 2.254E-01 NOT IDENT. SB-124 1. 706E+OO 1.559E+OO 4.705E+OO FAIL ABUN SB-125 -4.269E-02 1.040E-01 1. 724E-01 NOT IDENT. TE-125M 2.581E+Ol 2.245E+02 4.068E+02 NOT IDENT. I-126 O.OOOE+OO 5.520E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 6.504E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 4. 811E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.523E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 8.575E+25 O.OOOE+OO SHORT HLIF BA-133 -3. 913E-02 3.962E-02 5.934E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 2.231E-03 5.876E-02 l .113E-01 NOT IDENT. CS-135 5.092E-02 l.476E-01 2. 611E-01 NOT IDENT. I-135 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-136 0.000E+OO 2.159E+05 O.OOOE+OO SHORT HLIF CE-139. -3. 726E-02 l.054E-01 1.897E-01 NOT IDENT. BA-140 O.OOOE+OO 6.849E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.487E+05 O.OOOE+OO SHORT HLIF CE-141 -1.205E+Ol l.903E+Ol 3.363E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 628E+41 O.OOOE+OO SHORT HLIF CE-144 -9.951E-02 2.986E-01 5.499E-01 NOT IDENT. PM-144 -2.843E-02 5.865E-02 l.038E-01 NOT IDENT. PR-144 -2.461E+OO 5.076E+OO 8.982E+OO NOT IDENT. PM-146 4.736E-02 7. 531E-02 7. 401E-02 FAIL ABUN ND-147 O.OOOE+OO l.805E+07 O.OOOE+OO SHORT HLIF PM-147 3.770E+02 6.933E+02 l.399E+03 NOT IDENT. PM-149 O.OOOE+OO 6.437E+39 O.OOOE+OO SHORT HLIF EU-150 -l.892E-02 2.198E-02 3.974E-02 FAIL ABUN EU-152 3.678E-02 9.054E-02 1. 876E-01 NOT'IDENT. GD-153 -l.816E-02 l.482E-01 2.634E-01 NOT IDENT. EU-154 -2.399E-02 1.243E-01 2.419E-01 NOT IDENT. EU-155 9.186E-02 9.604E-02 1.994E-01 FAIL ABUN TB-160 -9.759E-02 1.687E+OO 3.246E+OO FAIL ABUN H0-166M 3.261E-03 4.365E_:02 8.908E-02 FAIL ABUN TM-171 l.586E+Ol 2.286E+Ol 4.875E+Ol NOT IDENT. HF-172 -l.668E-02 2.209E-01 3.857E-01 FAIL ABUN LU-172 -6.278E-02 8.847E-02 l.566E-01 FAIL ABUN LU-176 7.675E-04 l.957E-02 4.006E-02 FAIL ABUN Page 107of614 HF-181 5.413E-01 3.180E+OO 6.570E+OO NOT IDENT. TA-182 l.037E-01 8.225E-01 l.716E+00 FAIL ABUN RE-183 -1.582E+OO 2.568E+OO 4.875E+OO NOT IDENT. RE-184 -1.580E+Ol 2.332E+Ol 5.229E+Ol NOT IDENT. W-188 1.246E+02 1. 700E+02 FAIL ABUN IR-192 6.990E-03 3.687E-01 7.479E-01 FAIL ABUN BI-207 1. 211E-02 4.769E-02 l.015E-01 FAIL ABUN PB-210 -1.820E-01 4.564E+OO 9 .112E+OO NOT IDENT. PB-211 -7.835E-02 6.041E-01 1.185E+OO NOT IDENT. BI-212 1. 049E+OO 5.620E-01 1.307E+00 FAIL ABUN RN-219 l.052E-01 3.519E-01 7.246E-01 FAIL ABUN RA-223 -7.988E-02 5.172E-01 9.806E-01 FAIL ABUN AC-227 -2.469E-02 2.246E-01 4.056E-01 FAIL ABUN TH-227 -2.469E-02 2.246E-01 4.056E-01 FAIL ABUN AC-228 0.000E+OO 3.414E-01 4.681E-01 FAIL ABUN RA-228 O.OOOE+OO 3.414E-01 4.681E-01 FAIL ABUN TH-231 -7.988E-02 5.172E-01 9.806E-01 FAIL ABUN TH-232 O.OOOE+OO 3.414E-01 4.681E-01 FAIL ABUN PA-233 2.989E-04 5.079E-02 1.028E-01 FAIL ABUN PA-234 -4.292E-02 2.281E-01 4.654E-01 NOT IDENT. PA-234M 0.000E+OO 5.549E+OO 1.098E+Ol FAIL ABUN NP-237 2.989E-04 5.079E-02 1.028E-01 FAIL ABUN NP-238 O.OOOE+OO 4.590E+40 O.OOOE+OO SHORT HLIF NP-239 -1.120E-01 2.165E-01 3.943E-01 FAIL ABUN PU-239 3.032E+02 4.784E+02 5.827E+02 FAIL ABUN AM-241 4.912E-02 1.253E-01 -2.458E-01 NOT IDENT. CM-243 l.578E-02 8.653E-02 1. 588E-01 FAIL ABUN BK-247 -1.130E-01 7.617E-02 1.103E-01 FAIL ABUN . CM-247 -1.105E-02 3.367E-02 6.410E-02 FAIL ABUN CF-249 2.750E-02 3.845E-02 8.138E-02 NOT IDENT. CF-251 3.097E-02 l.102E-01 2.109E-01 FAIL ABUN Page 108of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:35:10.38 Nuclide Line Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM * %Error K-40 1460*.82 205 10.66* 1.005E+OO 1.027E+Ol 1.027E+Ol 14.84 CD-109 88.03 100 3.70* 5.183E+OO 2.817E+OO 4.373E+OO 49.97 SN-126 64.28 62 9.60 2.597E+OO 1.343E+OO 1.343E+OO 85.08 86.94 100 8.90 5.183E+OO 1.171E+OO 1.171E+OO 49.97 87.57 100 37.00* 5.183E+OO 2.817E-01 2.817E-01 49.97 BA-137M 661. 66 22 89.90* 2.028E+OO 6.523E-02 6.645E-02 84.47 CS-137 661. 66 22 85.10* 2.028E+OO 6.891E-02 7.020E-02 84.47 HG-203 70.83 ------3.69 3.616E+OO ------Line Not Found ------72.87 ------6.19 3.859E+OO ------Line Not FOl,\nd ------279.20 28 81.56* 3.949E+OO 4.597E-02 3.583E+OO 80.80 TL-208 277. 37 28 6.60 3.949E+OO 5. 681E-01 5. 681E-01 80.80 583.19 103 85.00* 2.243E+OO 2. 911E-01 2. 911E-01 29.14 860.56 ------12.50 1. 624E+OO ------Line Not Found ------BI-211 72.87 ------1. 23 3.859E+OO ------Line Not Found ------351.06 210 12.92* 3.303E+OO 2.647E+OO *2. 64 7E+OO 19.99 PB-212 74.82 119 10.28 4.088E+OO 1. 528E+00 1.528E+OO 39.92 77 .11 185 17.10 4.336E+OO 1.344E+OO 1.344E+OO 27. 96 238.63 246 43.60* 4.430E+OO 6.858E-01 6.858E-01 19.59 300.09 18 3.30 3. 724E+OO 8.057E-01 8.057E-01 136.60 BI-214 609.32 90 45.49* 2.166E+OO 4.937E-01 4.938E-01 41. 69 1120.29 21 14.92 1. 279E+OO 5.890E-01 5.892E-01 118.70 1764.49 ------15.30 8.592E-01 ------Line Not Found ------PB-214 74.82 119 5.80 4.088E+OO 2.708E+OO 2.709E+OO 39.92 77 .11 185 9.70 4.336E+OO. 2.368E+OO 2.369E+OO 27. 96 87.09 100 3.41 5.183E+OO 3.056E+OO 3.057E+OO 49.97 242.00 48 7.25 4.384E+OO 8.204E-01 8.207E-01 74.45 295.22 93 18.42 3.777E+OO 7.220E-01 7.223E-01 34.84 351. 93 210 35.60* 3.303E+OO 9.606E-01 9.610E-01 19.99 RN-222 609.32 90 45.49* 2.166E+OO 4.937E-01 4.938E-01 41.69 1120.29 21 14.92 1.279E+OO 5.890E-01 5.892E-01 118.70 1764.49 ------15.30 8.592E-01 ------Line Not Found ------RA-224 240.99 48 4.10* 4.384E+OO 1.451E+OO 1.451E+OO 74.45 RA-226 609.32 90 45. 49*. 2.166E+OO 4.937E-01 4.938E-01 41. 69 1120. 29 21 14.92 1.279E+OO 5.890E-01 5.892E-01 118.70 1764.49 ------15.30 8.592E-01 ------Line Not Found ------TH-228 74.82 119 10.28 4.088E+OO 1. 528E+OO 1.528E+OO 39.92 77 .11 185 17.10 .4.336E+OO 1.344E+OO 1.344E+OO 27. 96 238.63 246 43.60* 4.430E+OO 6.858E-01 6.858E-01 19.59 300.09 18 3.30 3. 724E+OO 8.057E-01 8.057E-01 136.60 TH-229 85.43 44 14.70 4. 963E+OO 3.260E-01 3.260E-'--01 93. 48 . 88.47 62 24.00 5.374E+OO 2.567E-01 2.567E-01 60.87 193.51 ------4.41* 5 .130E+OO ------Line Not Found ------210.85 ------2.80 4. 841E+OO ------Line Not Found ------TH-230 609.32 90 45.49* 2.166E+OO 4.937E-01 4.937E-01 41. 69 1120.29 21 14.92 1.279E+OO 5.890E-01 5.890E-01 118. 70 1764.49 ------15.30 8.592E-01 ------Line Not Found ------PA-231 283.69 ------1. 70 3. 891E+OO ------Line Not Found ------Page 109of614 Nuclide Line Activity Report (continued) Sample ID : R405245003 Acquisition date Page : 2 3-0CT-2016 04:33:45 Nuclide Type: Nuclide TH-234 U-234 U-235 U-238 AM-243 ANH-511 Energy 301.36 63. 29 92.59 609.32 1120. 29 1764.49 89. 96 93.35 143.76 163.33 185. 72 205.31 92.59 43.53 74.66 511. 00 Flag: "*" -Keyline Page 110of614 Area 18 62 131 90 21 62 131 45 62 131 119 27 %Abn 5.35* 3.70* 4.23 45.49* 14.92 15.30 3.47 5.60 10. 96* 5.08 57.20 5.01 3.70* 4.23 5.90 67.20* 100.00* %Eff 3. 724E+OO 2.597E+OO 5.549E+OO 2.166E+OO 1.279E+OO 8.592E-01 5.374E+OO 5.549E+OO 5.990E+OO 5.669E+OO 5. 272E+OO 4.931E+OO 2.597E+OO 5.549E+OO 3.924E-01 4.088E+00 2.486E+OO Uncorrected Decay Corr pCi/GRAM pCi/GRAM 4.970E-01 4.970E-01 3.485E+OO 3.485E+OO 3.009E+OO 3.009E+OO 4.937E-01 4.937E-01 5.890E-01 5.890E-01 ------Line Not Found 1.776E+OO 1.776E+OO 2.273E+OO 2.273E+OO, ------Line Not Found ------Line Not Found 8.051E-02 8.051E-02 ------Line Not Found 3.485E+OO 3.485E+OO 3.009E+00 3.009E+OO ------Line Not Found 2.337E-01 5.751E-02 5.751E-02 2-Sigma , %Error 136.60 85.08 40.48 41. 69 118.70 60.87 40.48 121. 4 7 85.08 40.48 39.92 127. 71 Summary of Nuclide Activity Sample ID : R405245003 Acquisition date Page : 3 3-0CT-2016 04:33:45 Total number of lines in spectrum 50 Number of unidentified lines 14 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-229 TH-230 PA-231 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 46.59D 1.41E+l0Y 7.04E+08Y l.41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+l0Y 1600. OOY 1.41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 1. 55 1. 00 1. 02 1. 02 77.9 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.027E+Ol 2.817E+OO 2.817E-01 6.523E-02 6.891E-02 4.597E-02 2. 911E-01 2.647E+OO 6.858E-01 4.937E-01 9.606E-01 4.937E-01 1.451E+OO 4.937E-01 6.858E-01 2.567E-01 4.937E-01 4.970E-01 3.485E+00 4.937E-01 8. 051E-02 3.485E+OO 2.337E-01 5.751E-02 3.083E+Ol 3.083E+Ol Decay Corr pCi/GRAM 1.027E+Ol 4.373E+OO 2.817E-01 6.645E-02 7.020E-02 3.583E+OO 2. 911E-01 2.647E+OO 6.858E-01 4.938E-01 9.610E-01 4.938E-01 1. 451E+OO 4.938E-01 6.858E-01 2.567E-01 4.937E-01 4.970E-01 3.485E+OO 4.937E-01 8. 051E-02 3.485E+OO 2.337E-01 5.751E-02 3.593E+Ol 3.593E+Ol 72. 00% Decay Corr 2-Sigma Error 0.152E+Ol 2.185E+OO l.408E-01 5.613E-02 5.930E-02 2.895E+OO 0.848E-01 0.529E+OO l.343E-01 2.059E-01 l.921E-01 2.059E-01 1.080E+OO 2.059E-01 *1.343E-01 1. 563E-01 2.058E-01 6.789E-01 2. 965E+OO 2.058E-01 9.779E-02 2. 965E+OO 0.933E-01 7.345E-02 "M" Manually accepted 2-Sigma %Error 14.84 49.97 49.97 84.47 84.47 80.80 29.14 19.99 19.59 41. 69 19.99 41. 69 74.45 41. 69 19.59 60.87 41. 69 136.60 85.08 41. 69 121.47 85.08 39.92 127.71 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 111 of 614 Flags K K Unidentified Energy Lines Page : 4 Sample ID : R405245003 Acquisition date : 3-0CT-2016 04:33:45 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 106.95 86 99 4.40 213.55 208 12 2.02E-02 55.7 6.05E+OO T 0 128.44 22 90 1. 24 256.49 254 7 5.21E-03 **** 6.15E+OO T 0 140.14 6 90 1. 00 279.88 276 7 l.54E-03 **** 6.04E+OO T 0 209.34 54 81 0.86 418.16 413 10 l.32E-02 72.9 4.87E+OO 0 270.78 12 76 1.14 540.97 535 10 3.12E-03 **** 4.03E+OO T 4 286.Bl 17 31 1.24 573.00 552 30 4.29E-03 **** 3.86E+OO T 4 288.75 19 48 1. 82 576.87 552 30 4.84E-03 **** 3.84E+OO 0 328. 96 38 25 3.36 657.24 653 9 9.80E-03 59.1 3.48E+OO T 0 432.88 17 24 1. 79 864.97 859 9 4.44E-03 **** 2.82E+OO T 0 446.86 11 20 0.92 892.92 889 8 3.0lE-03 **** 2.76E+OO 0 452.84 14 30 0.69 904.88 898 10 3.70E-03 **** 2.73E+OO T 0 467.87 11 20 1.15 934.91 929 8 2.81E-03 **** 2.66E+OO T 0 470.69 15 17 0.66 940.54 937 8 4.04E-03 **** 2.65E+00 0 504.73 6 18 0.87 1008.59 1004 7 1. 65E-03 **** 2. 5rn*+oo T 0 645.09 16 17 1.58 1289.20 1281 12 4.36E-03 **** 2.07E+OO T 0 681.05 6 10 0.49 1361.10 1356 8 1. 51E-03 **** 1.98E+OO 0 729.59 53 22 6.44 .1458.15 1447 23 1.45E-02 55.0 l.87E+00 0 768.42 19 9 1.17 1535.80 1530 11 5.20E-03 81. 6 1.79E+OO 0 786.45 5 10 0.79 1571. 86 1565 8 1.41E-03 **** 1.76E+OO T 0 806.09 10 7 1. 01 1611.13 1608 6 2.88E-03 **** 1. 72E+OO 0 911. 01 38 27 1.12 1820.93 1814 15 1. 05E-02 68.3 1. 54E+OO T 0 969.52 29 12 1. 47 1937.94 1932 13 8.09E-03 62.7 l.46E+OO T 5 997.79 8 2 2.08 1994.47 1993 15 2.28E-03 57.2 1. 42E+OO 5 1000.55 24 6 1. 79 2000.00 1993 15 6.84E-03 51. 5 1. 42E+OO T. 0 1009.10 14 5 3.89 2017.09 2011 11 3.82E-03 85.1 1.41E+OO 0 1018.37 9 6 0.79 2035.63 2028 10 2. 61E-03 **** 1. 40E+00 0 1200.89 9 14 1. 04 2400.69 2392 12 2.51E-03 **** l.20E+00 0 1210.55 11 2 1.13 2420.01 2416 8 3.04E-03 75.2 1.19E+00 0 1239.01 14 15 0.86 2476.94 2466 15 4.00E-03 **** 1.17E+OO T 0 1762.91 26 0 1. 46 3525.14 3517 14 7.78E-03 37.8 8. 6.0E-01 Flags: "T" = Tentatively associated Page 112of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:35:27.99 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245003.CNF;l *
  • Acquisition date 3-0CT-2016 04:33:45 Sensitivity : 3.000 *
  • Detector ID GAM06 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.57 Half life ratio : ***** *
  • Sample date 15-DEC-2015 10:18:00 Nuclide Library : SOLID *
  • Sample ID R405245003 Analyst initials: MXRl * ** Batch Number 1596387 Sample Quantity : l.3959E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;14
  • Combined Critical Level Report NOTE: Not "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-229 TH-230 PA-231 TH-234 U-234 U-235 U-238 AM-243 ANH-511 .Le (pCi/GRAM 2.644E-01 6.661E-01 4. 315E-02. 2. 727E-02 2.881E-02 1. 601E+OO 2.331E-02 1.570E-01 5.0lOE-02 4.536E-02 1.627E-01 4.536E-02 5.670E-01 4.536E-02 5.0lOE-02 3.653E-01 4.535E-02 3.501E-01 9.550E-01 4.535E-02 1.440E-01 9.550E-01 3.759E-02 .2.029E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 113 of 614 Le (pCi/GRAM l.046E+Ol 4 .119E-02 O.OOOE+OO 2.806E-02 3.361E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT.HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M . I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 114of614 5.158E-02 2.716E-01 O.OOOE+OO 3.446E-02 2.808E-01 5.872E+OO 3.481E-02 l.534E-01 2.189E+OO 8.992E+OO O.OOOE+OO l.428E-01 O.OOOE+OO O.OOOE+OO 5.292E-01 5.539E+OO 5.432E-01 O.OOOE+OO l.432E-01 4.258E+02 3. 071E-02 6.382E-01 1.700E+OO 1.087E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.357E-02 3.359E-02 3.578E+OO 2.878E-01 2.878E-01 2.221E-02 7.446E-02 l.718E-01 O.OOOE+OO O.OOOE+OO 1.041E-01 1. 851E+OO 7.544E-02 1.874E+02 O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.578E-02 O.OOOE+OO 4.917E-02 1.190E-01 O.OOOE+OO O.OOOE+OO 8.747E-02 O.OOOE+OO O.OOOE+OO 1.546E+Ol O.OOOE+OO 2.520E-01 4.520E-02 3.912E+00 3.235E-02 O.OOOE+OO 6.459E+02 1.756E-02 8.507E-02 l.210E-01 l.013E-01 9.293E-02 1.368E+OO 3.737E-02 2.256E+Ol 1. 781E-01 6.631E-02 l.784E-02 2.858E+OO NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT' IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN. FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 AC-228 RA-228 TH-231 TH-232 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 115 of 614 7. 227E.:...01 2.224E+OO 2.231E+Ol 7.602E+Ol 3.344E-01 4.329E-02 4.254E+OO 5.258E-01 5.946E-01 3.244E-01 4.368E-01 1.839E-01 l.839E-01 2.157E-01 2.157E-01 4.368E-01 2.157E-01 4.603E-02 1.916E-01 4.876E+OO 4.603E-02 O.OOOE+OO l.815E-01 2. 717E+02 1. 128E-01 7.313E-02 4.903E-02 2.857E-02 3.700E-02 9.737E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:35:34.02 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245003.CNF;l *
  • Acquisition date 3-0CT-2016 04:33:45 Sensitivity : 3.000 *
  • Detector ID GAM06 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.57 Half life ratio : ***** *
  • Sample date 15-DEC-2015 10:18:00 Nuclide Library : SOLID *
  • Sample ID R405245003 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity 1.3959E+02 GRAM *
  • Quantity Err(%) 1. 4328E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * * ** CALIBRATION INFORMATION *
  • Eff. Cal. date 8-MAR-2016 07:26:53 Eff. 'Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;14
  • Combined Activity-MDA Report NOTE: Not all Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1 . 96-sigma) K-40 1.027E+Ol 1. 730E+00 1.730E+OO CD-109 3.340E+OO 2.201E+00 2.201E+OO SN-126 2 .151E-01 l.413E-01 1.413E-01 BA-137M 6.645E-02 5.528E-02 5.528E-02 CS-137 7.020E-02 5.840E-02 5.B40E-02 HG-203 1. 747E+OO 2.904E+OO 2.904E+OO TL-208 2. 911E-01 8.680E-02 8.680E-02 BI-211 6. 57*5E-01 8.953E-01 8.953E-01 PB-212 6.858E-01 1.454E-01 1.454E-01 BI-214 4.938E-01 2.061E-01 2.061E-01 PB-214 9.610E-01 2.070E-01 2.070E-01 RN-222 4.938E-01 2.061E-01 2.061E-01 RA-224 1. 740E-01 1.157E+OO l.157E+OO RA-226 4.938E-01 2.061E-01 2.061E-01 TH-228 6.858E-01 1.454E-01 l.454E-01 TH-229 1.472E-01 4 .112E-01 4 .112E-01 TH-230 4.937E-01 2.060E-01 2.060E-01 PA-231 4.970E-01 6.750E-01 6.750E-01 TH-234 3.485E+OO 3.009E+OO 3.009E+00 U-234 4.937E-01 2.060E-01 2.060E-01 U-235 l.603E-03 1. 646E-01 1.646E-01 U-238 3.485E+OO 3.009E+OO 3.009E+OO AM-243 l.714E-01 9.526E-02 9.526E-02 ANH-511 5. 751E-02 7.215E-02 7.215E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 6.326E+OO 1. llOE+Ol l.146E+Ol NOT IDENT. NA-22 -9 .'7 51E-03 5.054E-02 5.073E-02 NOT IDENT. NA-24 -l.OOOE+41 4.031E+41 O.OOOE+OO SHORT HLIF AL-26 2.281E-02 2. 372E-02 2.585E-02 NOT IDENT. SC-46 l.761E-01 3. 715E-01 3.799E-01 FAIL ABUN V-48 -6.421E+03 l.083E+04 l.121E+04 SHORT HLIF Page 116 of 614 CR-51 3.219E+Ol* 3 .117E+02 3 .121E+02 SHORT HLIF MN-54 7.700E-03 6.069E-02
  • 6.079E-02 NOT IDENT. C0-56 -1.667E-01 3.757E-01 3.832E-01 FAIL ABUN MN-56 -1.000E+41 2.201E+41 O.OOOE+OO SHORT HLIF C0-57 -2.167E-02 4.137E-02 4.251E-02 NOT IDENT. C0-58 -3.004E-01 4.321E-01 4.528E-01 NOT IDENT. FE-59 -1. 371E+OO 7.043E+OO 7.070E+OO NOT IDENT. C0-60 2.424E-02 3.449E-02 3.618E-02 NOT IDENT. ZN-65 2.748E-02 l.943E-01 1.947E-01 NOT IDENT. GE-68 8.989E-02 2.510E+OO 2. 511E+OO NOT IDENT. AS-73 2.816E+OO 9.464E+OO 9.548E+OO NOT IDENT. AS-74 -6.140E+02 4.152E+03 4.161E+03 SHORT HLIF SE-75 -2.556E-01 2 .113E-01 2.407E-01 FAIL ABUN BR-77 1.570E+37 1.327E+38 0.000E+OO SHORT HLIF SR-82 9.702E+OO 5.088E+02 5.088E+02 SHORT HLIF RB-83 -3.816E-02 6.165E-01 6.167E-01 NOT IDENT. KR-85 2.045E+OO 6.063E+OO 6.133E+OO NOT IDENT. SR-85 2.000E-01 5.947E-01 6.015E-01 NOT IDENT. RB-86 -1.102E+03 2.415E+04 2.416E+04 SHORT HLIF Y-88 -5.704E-02 2. 031E-01 2.047E-01 NOT IDENT. Y-91 2.784E+02 5.055E+02 5.209E+02 NOT IDENT. NB-94 9.614E-03 3.494E-02 3.521E-02 NOT IDENT. NB-95 -l.514E-01 8.975E-01 9. OOlE-01 NOT IDENT. NB-95M 8.lBOE-01 2.073E+OO 2.106E+OO NOT IDENT. ZR-95 -7.747E-01 1. 455E+OO 1.497E+OO NOT IDENT. NB-97 -1.000E+41 6.173E+41 O.OOOE+OO SHORT HLIF ZR-97 -1.000E+41 1.378E+41 O.OOOE+OO SHORT HLIF M0-99 -1. 288E+31 2.675E+31 O.OOOE+OO SHORT HLIF TC-99M l.000E+41 5.342E+41 O.OOOE+OO SHORT HLIF RH-101 3.330E-02 5.291E-02 5.500E-02 FAIL ABUN RH-102 -3.298E-02 4.755E-02 4.982E-02 NOT IDENT. RU-103 -2.737E+OO 4.591E+OO 4.754E+OO FAIL ABUN RH-106 -3.395E-01 4.168E-01 4.440E-01 NOT IDENT. RU-106 -3.395E-01 4.168E-01 4.440E-01 NOT IDENT. AG-108M 3.585E-02 4.284E-02 4.579E-02 FAIL ABUN AG-llOM -4.974E-02 1.027E-01 1.051E-01 NOT IDENT. SN-113 -l.454E-01 2. lJlE-01 2.230E-01 NOT IDENT. CD-115 l.092E+38 3.028E+38 O.OOOE+OO SHORT HLIF SN-117M -2.850E+04 6.512E+04 6.638E+04 SHORT HLIF TE-123M 7.576E-03 1.195E-01 1.196E-01 NOT IDENT. SB-124 1.706E+OO 1.564E+OO 1. 743E+OO FAIL ABUN SB-125 -4.269E-02 1.041E-01 1.058E-01. NOT IDENT. TE-125M 2.581E+Ol 2.246E+02 2.249E+02 NOT IDENT. I-126 l.280E+05 5.523E+05 5. 5.53E+05 SHORT HLIF SB-126 -3.968E+05 6.553E+05 6.793E+05 SHORT HLIF SB-127 2.858E+21 6.157E+21 O.OOOE+OO SHORT HLIF I-131 -2.666E+09 2.535E+09 2.805E+09 SHORT HLIF I-132 l.000E+41 4.574E+43 O.OOOE+OO SHORT HLIF TE-132 4.515E+25 8.766E+25 O.OOOE+OO SHORT HLIF BA-133 -3.913E-02 3.978E-02 4.351E-02 NOT IDENT. I-133 -l.000E+41 2.908E+41 O.OOOE+OO SHORT HLIF CS-134 2. 231E-03 5.876E-02 5.877E-02 NOT IDENT. CS-135 5.092E-02 l.477E-01 l.494E-01 NOT IDENT. I-135 -1.000E+41 1. 2 63E+42 O.OOOE+OO SHORT HLIF CS-136 -1.030E+05 2.168E+05 2.217E+05 SHORT HLIF CE-139 -3. 726E-02 1.057E-01 l.070E-01 NOT IDENT. BA-140 3.026E+05 6.854E+05 6.989E+05 SHORT HLIF LA-140 5. 651E+03 2.487E+05 2.487E+05 SHORT HLIF CE-141 -1.205E+Ol 1.905E+Ol 1. 981E+Ol NOT IDENT. CE-143 1.000E+41 1.633E+41 O.OOOE+OO SHORT HLIF CE-144 -9. 951E-02 2.987E-01 3.021E-01 NOT IDENT. PM-144 -2.843E-02 5.872E-02 6.0lOE-02 NOT IDENT. PR-144 -2. 461E+OO 5.080E+OO 5.200E+OO NOT IDENT. PM-146 4.736E-02 7.547E-02 7.844E-02 FAIL ABUN ND-147 -9.058E+06 1.807E+07 1.853E+07 SHORT HLIF PM-147 3.770E+02. 6.938E+02 7.143E+02 NOT IDENT. PM-149 5.401E+39 6.557E+39 O.OOOE+OO SHORT HLIF EU-150 -1.892E-02 2.205E-02 2.364E-02 FAIL ABUN EU-152 3.678E-02 9.061E-02 9.212E-02 NOT IDENT'. GD-153 -1.816E_.:02 1.482E-01 1.484E-01 NOT IDENT. EU-154 -2.399E-02 1.244E-01 1.248E-01 NOT IDENT. EU-155 9.186E-02 9.637E-02 1.049E-01 FAIL ABUN TB-160 -9.759E-02 '1. 687E+OO 1.688E+OO FAIL ABUN H0-166M 3.261E-03 4.365E-02 4.368E-02 FAIL ABUN TM-171 1.586E+Ol 2.291E+Ol 2.400E+Ol NOT IDENT. HF-172 -1.668E-02 2.209E-01 2.211E-01 FAIL ABUN LU-172 -6.278E-02 8.933E-02 9.370E-02 FAIL ABUN LU-176 7.675E-04 l.957E-02 1.958E-02 FAIL ABUN Page 117 of614 HF-181 5.413E-01 3.180E+OO 3.190E+OO NOT IDENT. TA-182 1.037E-01 8.226E-01 8.239E-01 FAIL ABUN RE'-183 -1.582E+OO 2.579E+00 2.676E+OO NOT IDENT ., RE-184 1.580E+Ol 2.368E+Ol 2.473E+Ol NOT IDENT. W-188 -3.657E+Ol 1. 247E+02 l.257E+02 FAIL ABUN IR-192 6.990E-03 3.687E-01 3.687E-01 FAIL ABUN BI-207 l.211E-02 4.773E-02 4.804E-02 FAIL ABUN PB-210 -1.820E-01 4.564E+OO 4.564E+OO NOT IDENT. PB-211 -7.835E-02 6.041E-01 6.051E-01 NOT IDENT. BI-212 l.049E+OO 5. 711E-01 7.415E-01 FAIL ABUN RN-219 l.052E-01 3.522E-01 3.554E-01 FAIL ABUN RA-223 -7.988E-02 5.173E-01 5.186E-01 FAIL ABUN AC-227 -2.469E-02 2.246E-01 2.249E-01 FAIL ABUN TH-227 -2.469E-02 2.246E-01 2.249E-01 FAIL ABUN AC-228 5.102E-01 3 .. 478E-01 4.170E-01 FAIL ABUN RA-228 5.1028-01 3.478E-01 4.170E-01 FAIL ABUN TH-231 -7.988E-02 5.173E-01 5;186E-01 FAIL ABUN TH-232 5.102E-01 3.478E-01 4.170E-01 FAIL ABUN PA-233 2.989E-04 5.079E-02 5.079E-02 FAIL ABUN PA-234 .-4. 2 92E-02 2.334E-01 2.342E-01 NOT IDENT. PA-234M 1.lOOE+Ol 5.789E+OO 7.623E+OO FAIL ABUN NP-237 2.989E-04 5.079E-02 5.079E-02 FAIL ABUN NP-238 -2.239E+40 4.601E+40 O.OOOE+OO SHORT HLIF NP-239 -1.120E-01 2.168E-01 2.226E-01 FAIL ABUN PU-239 3.032E+02 4.789E+02 4.980E+02 FAIL ABUN AM-241 4.912E-02 l.254E-01 1.273E-01 NOT IDENT. CM-243 1.578E-02 8.654E-02 8.684E-02 FAIL ABUN BK-247 -1.130E-01 '8. 002E-02 9.487E-02 FAIL ABUN CM-247 -1.105E-02 3.373E-02 3.410E-02 FAIL ABUN CF-249 2.750E-02 3.857E-02 4. 051E-02 NOT IDENT. CF-251 3.097E-02 1.103E-01 1. lllE-01 FAIL ABUN Page 118of614
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 51.0306 87.09 39.3807 136.47 52.7247 45. 60 50.5219 87.57 39.4204 140.51 0.0000 46.54 60.9815 88.03 39.4583 143.76 47.3463 49.72 0.0000 88.34 39.4838 144.24 43.1684 51. 35 53.1770 88.47 39.4945 145.44 55.9017 51. 87 48.0209 89.96 39.6163 152.43 50.0766 52.39 39.3505 1093.63 39.6718 153.25 0.0000 52. 97 43.7973 91.11 0.0000 323.87 50.2029 53.44 49.1205 92.59 39.8291 156.02 0.0000 54.07 50.0892 93.35 39.8900 158.56 0.0000 57.36 0.0000 94.56 39.9865 159.00 47.3133 57.53 43.4838 94.65 39. 99.37 162.33 46.4493 57.98 47.0919 . 94. 67 39.9953 162.66 0.0000 59.27 28.5337 94.87 40.0111 163.33 36.7771 59.32 34.4828 97.43 45.4017 165.86 54.2686 59.54 34.5034 98.43 49.3887 176.31 39. 6112 60.96 48.3706 98.44 49.3899 176.60 0.0000 61.17 48.3978 99.53 50.7959 177.52 42.9782 62.93 48.6234 100 .11 46.9409 181.07 0.0000 63.29 48.6691 102.03 30.0995 181.52 59. 0714 63.58 48.7059 103.18 41. 9681 184.41 48.9099 64.28 55.4205 103.37 41. 9831 143.76 48.9891 66.73 58.1924 105.21 43.4431 193.51 33.7189 67.24 63.7296 105.31 43. 4511 197.03 36.1177 125.81 61.0653 106.12 43.5159 198.01 38.4191 67.75 61. 07 61 106.47 43.5438 201.83 35.1858 69.67 54.9550 109.28 43.7664 203.43 35. 2511 70.83 67.3569 111. 00 55.8744 205.31 33.4279 72.81 67.6769 111. 76 0.0000 210.85 38.2253 72. 87 59. 0718 114. 06 45.1418 215.65 39.1989 74.66 59.3213 116. 30 0.0000 222 .11 35.9932 74.82 59.3433 116.74 55.4297 227.09 49.0258 74.97 59.3643 119.76 56.7285 227.38 42.0353 77 .11 59.6577 121.12 38.5824 228.16 0.0000 78.74 59.8789 121. 22 38.5888 228.18 36.2278 79.69 60.0063 121. 78 44.7234 116.74 36.2278 80.12 60.0640 122.06 52.8795 235.69 29.8390* 80.19 0.0000 122.92 44.8083 235. 96 34.5603 80.57 60.1240 123.07 50.9312 238.63 55.1333 81. 00 37.6135 265.00 54.0416 238.98 0.0000 81. 07 37.6193 125.81 50.4787 240.99 61.5826 81. 75 37.6755 127.23 50.5948 242.00 37.9355 83.79 39.1048 127.91 41. 0681 244.70 22.1897 84.00 39.1224 129.30 47.3336 252.40 0.0000 85.43 39.2426 131.20 44.0365 252.80 26.3633 86.55 39.3359 133.02 54.8584 254.15 0.0000 86.79 39.3555 133.52 46.6143 256.23 33.6659 86. 94 39.3681 136.00 54.0733 2 60. 90 0.0000 Page 119of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 44.8487 355.39 0.0000 584.27 12.0610 264.80 47.2789 356.01 28.8052 595.83 0.0000 265.00 47.2873 364.49 0.0000 427.87 28.3771 268.22 29.1885 366.42 0.0000 602.52 0.0000 269.46 35.3110 372.51 19.4407 604. 72 24.3730 270.03 35.3296 375.05 28.3294 607.14 21. 3521 271.23 35.3694 377.52 16.8507 609.32 12.2144 273.65 0.0000 356.01 18.7095 610.33 12.2207 276.40 31.0451 388.16 23.2356 614.28 13.7752 277.37 25.7578 388.63 0.0000 618.01 11.2448 277.60 25.7629 391. 69 29.5645 620.36 8.1875 278.00 25.7726 264.66 12. 6211 621.93 15.3632 279.20 25.8008 401.81 20.7511 630.19 0.0000 279.54 25.8084 402.40 27.0776 631. 29 13.3756 279.70 25.8123 404.85" 22.6028 633.25 11. 3281 280.46 25.8302 410.95 26.3285 634.78 0.0000 283.69 25.9059 413.71 21.8296 635.95 9.2805 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 25.9456 423. 72 0.0000 645.85 6.2163 285.90 0.0000 427.09 16.5187 657.76 23.4421 287.50 25.9943 427.87 22.0361 657.90 0.0000 290.67 29.7913 433.94 17.9754 661.66 14.6124 293.27 0.0000 439.40 25.9019 664.57 0.0000 351. 93 26.1718 453.88 22.4067 '666.33 0.0000 295. 96 34.9180 463.37 25.3570 666.50 0.0000 879.38 24.9988 468.07 8.4767 667. 71 0.0000 299.98 29.2001 473.00 0.0000 677.62 12.6172 300.09 29.2030 475.06 21. 2819 685.70 0.0000 300 .13 29.2037 476.78 20.8309 695.00 0.0000 301.36 28.8174 477.60 17.0519 696.49 21. 2085 302.85 28.8539 482.18 13.2990 696.51 21. 2085 256.23 26.3820 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 14. 8511 306.78 21.8180 497.08 20.1246 697.49 16.9743 308.46 21. 0088 505.52 31.7794 702.65 18.0763 311. 90 24.4410 507.63 0.0000 706.68 18.1088 316.51 23.6888 511. 00 15.4567 711. 68 8.5404 319.41 0.0000 514.00 15.4831 720.70 0.0000 320.08 0.0000 514.00 15.4831 721.93 0.0000 321. 04 23. 7771 520.40 19.4238 722.78 8.0453 323.87 24.5133 520.69 0.0000 722.91 9.6552 325.23 19.1721 522.65 0.0000 723.31 9.6566 328.76 0.0000 527.90 0.0000 724 .19 6.4402 333.37 24.4441 528.26 11.7061 727. 33 9.6735 333.97 30.8914 529.59 15.6191 733.00 9. 6969 334.37 32.6184 529.87 0.0000 735.93 6.4727 338.28 26.6917 531.02 0.0000 333.97 9.7156 338.32 28.4151 537.26 0.0000 739.50 0.0000 311.90 60.3756 546.56 0.0000 747.24 14.0918 340.48 60.3756 552.55 16.8049 748.06 13.0122 340.55 0.0000 563.25 10.9355 752.31 17.3802 344.28 25.9521 569.33 8.9762 753.82 0.0000 345.93 34.6476 946.00 8.9769 756.73 18. 5011 351.06 26.9579 569.70 8.9777 756.80 18. 5011 351.93 26.9755 583.19 12.0547 884.68 9.8240 Page 120of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 16.3855 1274:44 9.9907 1620.50 6.3270 766.42 13 .1118 1001.03 12.2528 1621. 92 2.1097 766.84 13 .1143 1002.74 7.1516 1678.03 0.0000 772.60 0.0000 1004.73 0.0000 1690.97 0.0000 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 1.7396 778.90 8.7861 1028.54 0.0000 1063.66 1.0885 783.70 0.0000 1037.84 9.0424 1771.35 2.1776 785.37 8.2587 1038.76 0.0000 1791.20 0.0000 792.07 18.7701 631.29 11. 7876 1808.65 0.0000 794.95 13.2646 1048.07 0.0000 1810.72 0.0000 795.86 18.7985 1049.04 10.8896 1836.06 3.3091 810.06 12.0098 1050.41 10.8940 810.29 13.3457 1063.66 8.2b51 344.28 12.2345 1077.00 0.0000 810.76 10. 0111 1077.34 11. 9026 815.77 0.0000 1085.87 9 .17 97 1048.07 0.0000 1093.63 17.4832 832.01 8. 9727. 1099.45 14.7490 834.85 11. 2280 1112. 07 9.5179 835.71 7.8622 1112.84 13.5754 836.80 0.0000 1115. 54 10.3749 846.75 0.0000 1120.29 9.2767 I 846.77 10.1514 1120.55 9.2773 856.80 0.0000 1221.41 9.2798 860.56 7.9368 1129. 67 12.0939 871.09 17.0740 1131. 51 0.0000 873.19 7.9741 1147.95 0.0000 875.33 0.0000 1173.23 12.2502 879.38 10.2759 1177.95 10.3796 880.51 7.9958 1189.05 5. 6796 883.24 5.7170 1204.77 5.7052 884.68 13.7280 1221.41 8.5979 889.28 9.1673 1231. 02 15.3262 894.76 10.3337 1235.36 0.0000 898.04 8.0470 1238.28 13.4369 900.72 8.0547 1260.41 0.0000 903.28 5.7587 1271.87 8. 7182 911. 20 6.9302 1274.44 10.6630 912.08 6.9324 1274.54 10.6630 923.98 0.0000 1291.59 4.8691 926.50 3.4839 1298.22. 0.0000 929 .11 6.9744 1312 .11 0.0000 937.49 11. 6581 1332.49 2.9531 944.13 0.0000 1362.66 0.0000 946.00 8.7695 1365.19 0.0000 949.00 7.0229 1368.63 0.0000 667. 71 0.0000 1384.29 6.9825 962.31 10.5824 1408.01 6.0209 964. 08 9.8831 1457.56 0.0000 966 .17 15.5418 1460.82 5.0824 911.20 14.1421 1489.16 4.0935 968. 97 14.1421 1505.03 7.1906 983.53 0.0000 1584.12 4.1841 984.45 0.0000 1596. 21 0.0000 Page 121 of 614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:36:05.24 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245004.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM07.CNF;484 Backgro"und date : 2"-0CT-2016 11:00:17. Sample date 15-DEC-2015 10:21:00 Acquisition date : 3-0CT-2016 04:34:09. Sample ID R405245004 Sample quantity 1.45276E+02 GRAM Detector name : GAM07 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.46 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596387 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 1 1 1 0 0 0 3 3 0 0 0 0 0 0 0 0 0 0 0 2 2 0 0 0 0 0 0 0 0 0 0 Page 122 of 614 Energy 63.61* 74.93* 77.17 87.15 89.87 92.65* 116.85 186.16* 209.35 238.56* 241.72 247.43 295.43* 328.25 338.10* 351.90* 438.68 455.84 466.46 510.87* 515.00 563.50 583.01* 586.48 609.15* 633.57 661.26 720.50 728 .18 763.76 769.14 794.40 807.64 829.21 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 23 115 170 60 35 62 32 37 33 256 89 22 112 24 56 192 27 42 23 58 9 18 72 18 172 13 85 19 26 15 19 18 25 5 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 142 104 99 104 105 107 65 72 72 59 56 27 52 36 55 66 22 41 24 23 18 19 15 5 31 21 18 13 26 16 25 5 31 10 1.13 1.15 1. 20 1.16 1.16 1.17 1. 57 1.12 1. 45 1.23 1. 38 1. 46 1. 21 1. 73 1.12 0.97 1. 94 7.79 4.06 1. 90 0.52 3.14 1. 83 1. 92 1. 66 3.57 1. 31 1. 72 *1.68 1. 42 2.22 1. 37 8.72 1. 37 127.70 150.34 154.82 174.79 180.21 185.79 234.16 372.75 419.12 477.53 483.86 495.27 591.25 656.88 676.57 704.16 877.69 912.00 933.22 1022.04 1030.29 1127. 27 1166.29 1173.22 1218.56 1267.38 1322.75 1441.22 1456.58 1527. 72 1538.48 1589.00 1615.47 1658.60 124 143 143 164 164 164 230 369 414 472 472 493 586 651 671 698 871 902 926 1015 1027 1121 1161 1161 1210 1259 1316 1434 1449 1523 1533 1585 1599 1650 9 19 19 28 28 28 8 8 9 17 17 6 9 9 12 12 11 20 12 13 8 11 16 16 18 14 14 13 15 9 11 9 25 *10 6.44E-03 98.8 3.20E-02 17.9 8.78E-01 4.73E-02 13.0 1.66E-02 31.6 1.71E+OO 9.81E-03 50.7 1. 72E-02 33 .1 8.78E-03 47.9 1. 02E-02 45. 9 9.17E-03 49.5 7.12E-02 8.1 1.23E+OO 2.48E-02 18.8 6.llE-03 43.0 3.lOE-02 15.2 6.67E-03 49.5 1.55E-02 30.1 5. 34E-02 11. 3 7.52E-03 38.7 1.17E-02 41.8 6.25E-03 50.1 1.62E-02 26.8 2.60E-03 82.0 4.91E-03 53.7 1.99E-02 16.4 2.0lE+OO 4.99E-03 36.9 4.79E-02 10.9 3.61E-03 79.8 2.37E-02 15.0 5.31E-03 45.1 7. 29E-*03 46. 8 4.20E-03 53.9 5.14E-03 57.0 5.llE-03 31.3 6.86E-03 64.2 1.39E-03126.5 Peak Search Report (continued) Page : 2 Sample ID : R405245004 Acquisition date 3-0CT-2016 04:34:09 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 8 83 .. 39 14 10 1. 54 1766.94 1760 13 3.95E-03 52.5 36 0 910.90* . 72 7 1. 04 1821. 96 1815 14 1. 99E-02 14.8 37 0 964. 36 17 16 2.34 1928.87 1921 13 4.73E-03 54.3 38 0 969.06* 32 8 1. 06 1938.28 1934 9 8.93E-03 25.3 *39 0 1043.01. 13 4 1. 73 2086.15 2081 9 3.53E-03 41. 0 40 0 1069.53 7 7 1. 42 2139.19 2132 10 1.85E-03 86.1 41 0 1120.09 41 14 2.07 2240.30 2232 14 l.13E-02 25.1 42 0 1152. 22 6 11 1. 02 2304.55 2299 7 1.53E-03106.6 43 0 1162.76 26 4 0.82 2325.62 2317 17 7.22E-03 26.7 44 0 1168. 69 9 4 0.80 2337.47 2333 7 2.36E-03 50.1 45 0 1195 .15 10 16 4.26 2390.39 2381 13 2.76E-03 89.5 46 0 1219.53 12 13 2.73 2439.16 2433 10 3.43E-03 60.7 47 0 1341.69 9 0 1. 38 2683.44 2676 12 2.50E-03 33.3 48 0 1460.29* 280 0 2.29 2920.64 2914 13 7.77E-02 6.1 49 0 1764.30* 15 6 2.56 3528.62 3522 12 4.lOE-03 44.9 Flag: "*" = Peak area was modified by background subtraction Page i23*of 614 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 05:36:07 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245004.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 15-DEC-2015 10:21:00 R405245004 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 04:34:09 145.28 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit. SOLID GAMMA7 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Page 124 of 614 Nuclide PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74:82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.46 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : R405245004 Acquisition date 3-0CT-2016 04:34:09 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn -%Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.122E+OO 1.162E+Ol 1.162E+Ol 12.17 OK KR-85 514.00 0.43* 2.617E+OO 4.529E+OO 4.774E+OO 163.95 OK SR-85 514.00 96. 00* 2.617E+OO 2.048E-02 4.683E-01 163.95 OK CD-109 88.03 3.70* 5.740E+OO l.019E+OO l.582E+OO 113. 65 OK SN-126 64.28 9.60 3.539E+OO 4.456E-01 4.456E-01 197.70 OK 86.94 8.90 5.740E+OO 4.237E-01 4.237E-01 113. 65 OK 87.57 37.00* 5.740E+OO 1.019E-01 L 019E-01 113. 65 OK BA-137M 661. 66 89.90* 2 .139E+OO 2.382E-01 2.426E-01 30.02 OK CS-137 661. 66 85.10* 2.139E+OO 2.516E-01 2.563E-01 30.02 OK TL-208 277.37 6.60 4.377E+OO Line Not Found Absent 583.19 85.00* 2.366E+OO l.934E-01 1.934E-01 32.74 OK 860.56 12.50 1.736E+OO Line Not Found Absent BI-211 72.87 1. 23 4.591E+OO Line Not Found Absent 351. 06 12.92* 3.592E+OO 3. 851E-02 3.851E-022293.92 OK PB-212 74.82 10.28 4. 7 91E+OO 1.034E+OO 1.034E+OO 53.90 OK 77 .11 17.10 4.995E+OO 1.283E+OO 1.283E+OO 26. 03 OK 238.63 43.60* 4.931E+OO 6.998E-01 6.998E-01 16 .24 OK 300. 09, 3.30 4.103E+OO -----Line Not Found -Absent BI-214' 609.32 45.49* 2.284E+OO 8.971E-01 '8.974E-01 21. 88 OK 1120.29 14.92 1.406E+OO 9.903E-01 9.907E-01 50.10 OK 1764.49 15.30 9.423E-01 4. 996E-01 4.998E-01 89.81 OK PB-214 74.82 5.80 4. 781E+OO -----Line Not Found <<INT Reject 77 .11 9.70 4.995E+OO 2.262E+OO 2.263E+OO 26.03 OK 87 . .09 3.41 5.736E+OO Line Not Found <<INT Reject 242.00 7.25 4.877E+OO Line Not Found <<INT Reject 295.22 18.42 4.157E+OO 8.398E-01 8.400E-01 30.50 OK 351. 93 35.60* 3.592E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.284E+OO 8.971E-01 8.974E-01 21. 88 OK 1120.29 14.92 1.406E+OO 9.903E-01 9.907E-01 50.10 OK 1764.49 15.30 9.423E-01 4. 996E-01 4.998E-01 . 89. 81 OK RA-224 240.99 4.10* 4.882E+OO 1.137E+OO 1.137E+OO 95.45 OK RA-226 609.32 45.49* 2.284E+OO 8.971E-01 8.974E-01 21. 88 OK 1120.29 14.92 1.406E+OO 9.903E-01 9.907E-01 50.10 OK 1764.49 15.30 9.423E-01 4. 996E-01 4.998E-01 89.81. OK AC-228 105.21 1.10 6.488E+OO -Line Not Found Absent 338.32 11. 27 3.715E+OO 7.607E-01 7.607E-01 60.29 OK 794.95 4.25 1.850E+OO 1.234E+OO 1.234E+OO 62.59 OK 835. 71 1. 61 1.777E+OO Line Not Found Absent 911. 20 25.80* 1.660E+OO 8. 711E-01 8. 711E-01 29.66 OK 968. 97 15.80 1.580E+OO 6.660E-01 6 .. 660E-01 50.59 OK RA-228 105.21 1.10 6.488E+OO Line Not Found Absent 338.32 11. 27 3.715E+OO 7.607E-01 7.607E-01 60.29 OK 794.95 4.25 1.850E+OO 1.234E+OO 1.234E+OO 62. 59 OK 835.71 1. 61 1.777E+OO Line Not Found Absent 911.20 25.80* 1.660E+OO 8.711E-01 8. 711E-01 29.66 OK 968. 97 15.80 1.580E+OO 6.660E-01 6.660E-01 50.59 OK TH-228 74.82 10.28 4.791E+OO 1.034E+OO 1.034E+OO 53.90 OK 77 .11 17.10 4.995E+OO 1.283E+OO 1.283E+OO 26.03 OK 238.63 43.60* 4. 931E+OO 6.998E-01 6.998E-01 16.24 OK Page 125of614 Nuclide Line Activity Report (continued) Page : 3 Sample ID : R405245004 Acquisition date 3-0CT-2016 04:34:09 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff* pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 4.103E+OO Line Not Found Absent TH-230 609.32 45.49* 2.284E+OO 8.971E-01 8.971E-01 21. 88 OK 1120.29 14.92 1.406E+OO 9.903E-01 9.904E-01 50.10 OK 1764.49 15.30 9.423E-01 4. 996E-01 4. 996E-01 89.81 OK TH-232 105.21 1.10 6.488E+OO Line Not Found Absent 338.32 11.27 3.715E+OO 7.607E-01 7.607E-01 60.29 OK 835.71 1. 61 1.777E+OO Line Not Found Absent 911.20 25.80* 1.660E+OO 8. 711E-01 8. 711E-01 29.66 OK 968.97 15.80 l.580E+OO 6.660E-01 6.660E-01 50.59 OK TH-234 63.29 3.70* 3.539E+00 1.156E+OO 1.156E+OO 197.70 OK 92.59 4.23 6.041E+OO 1.540E+OO 1.540E+OO 66.18 OK U-234 609.32 45.49* 2.284E+OO 8 .. 971E-01 8. 971E-01 21. 88 OK 1120.29 14.92 1.406E+OO 9.903E-01 9.903E-01 50.10 OK 1764.49 15.30 9.423E-01 4.996E-01 4. 996E-01 89.81 OK U-235 89. 96 3.47 5.897E+OO l.097E+OO 1.097E+OO 101.46 OK . 93. 35 5.60 6.041E+OO 1.163E+OO l.163E+OO 66.18 OK 143.76 10. 96* 6.563E+OO Line Not Found Absent 163.33 5.08 6.266E+OO Line Not Found Absent 185.72 57.20 5.849E+OO 6.586E-02 91. 82 OK 205.31 5.01 5.496E+OO Line Not Found Absent U-238 63.29 3.70* 3. 539E+OO 1.156E+OO 1.156E+OO 197.70 OK 92.59 4.23 6.041E+OO 1.540E+OO 1.540E+OO 66.18 OK AM-243 43.53 5.90 6.933E-01 Line Not Found' Absent 74.66 67.20* 4.791E+OO 1.582E-01 1.582E-01 53.90 OK ANH-511 511. 00 100.00* 2.634E+OO l.213E-01 1.213E-01 53.56 OK Flag: "*" = Keyline Page 126 of 614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:36:08.17 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245004.CNF;l *
  • Acquisition date 3-0CT-2016 04:34:09 Sensitivity : 3.000 *
  • Detector ID GAM07 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.46 Half life ratio : ***** *
  • Sample date 15-DEC-2015 10:21:00 Analyst initials: MXRl *
  • Sample ID R405245004 Sample Quantity 1.4528E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff .. cal. date 19-AUG-2016 11:09:59 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;15
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Nuclide K-40 KR-85 SR-85 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC--,228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Activity (pCi/GRAM 1.162E+Ol 4.774E+OO 4.683E-01 1. 5.82E+OO l.019E-01 2.426E-01 2.563E-01 1.934E-01 3. 851E-02 6.998E-01 8.974E-01 8.540E-01 8.974E-01 1.137E+OO 8.974E-01 8. 711E-01 . 8.711E-01 6.998E-01 8. 971E-01 8.711E-01 1.156E+OO 8. 971E-01 6.032E-02 l.156E+OO 1.582E-01 1. 213E-01 Cnt uncert (1. 96-sigma) l.386E+OO 7.670E+OO 7.524E-01 1. 762E+OO 1.135E-01 7 .138E-02 7.541E-02 6.204E-02 8.658E-01 1.113E-01 1.925E-01 1. 891E-01 1.925E-01 1.063E+OO 1.925E-01 2.532E-01 2.532E-01 1.113E-01 1.924E-01 2.532E-01 2.240E+OO 1.924E-01 1. 756E-01 2.240E+OO 8.358E-02 6.366E-02 Non-Identified Nuclides N1:J.Clide BE-7 NA-22 NA-24 AL-26 Page 127of614 Key-Line Activity (pCi/GRAM -3.991E+OO -2.205E-02 0.000E+OO l.237E-02 K.L. Cnt Uncert (1. 96-sigma) 9.372E+OO 5.428E-02 1. 960E+41 2.618E-02 MDA (pCi/GRAM 4.761E-01 1.337E+OO 1.311E-01 1.613E+OO 1.044E-01 5.290E-02 5.589E-02 5.923E-02 3.049E-01 8.756E-02 9.536E-02 3.045E-01 9.536E-02 9.389E-01 9:536E-02 2.132E-01 2.132E-01 8.756E-02 9.533E-02 2.132E-01 1.705E+OO 9.533E-02 3.296E-01 1. 705E+OO 6.844E-02 4. 901E-02 MDA (pCi/GRAM 1. 727E+Ol 9. 865E:...02 O.OOOE+OO 6.766E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 1. 249E-01 3.166E-01 6.590E-01 FAIL ABUN V-48 O.OOOE+OO 1.177E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.224E+02 O.OOOE+OO SHORT HLIF MN-54 -7.402E-03 6.152E-02 1.218E-01 NOT IDENT. C0-56 -1. 756E-01 3.769E-01 7.165E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E:l-41 O.OOOE+OO SHORT HLIF C0-57 -4.962E-03 4.000E-02 7. 401E-02 NOT IDENT. C0-58 2.247E-Ol 5.655E-01 1.056E+OO NOT IDENT. FE-59 2.504E+OO 5.739E+OO 1.234E+Ol NOT IDENT. C0-60 4.295E-03 3.097E-02 6.712E-02 NOT IDENT. ZN-65 8.316E-02 1.615E-01 3.244E-01 NOT IDENT. GE-68 l.137E-02 1.877E+OO 3.874E+OO NOT IDENT. AS-73 3.403E+OO 5.851E+OO 1. 211E+Ol NOT IDENT. AS-74 O.OOOE+OO 3.680E+03 O.OOOE+OO SHORT HLIF SE-75 9.329E-02 1.688E-01 3.532E-01 NOT IDENT. BR-77 O.OOOE+OO 2.548E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 4.673E+02 O.OOOE+OO SHORT HLIF RB-83 -2.952E-02 6.277E-01 1.200E+OO NOT IDENT. RB-'-86 O.OOOE+OO 1.662E+04 O.OOOE+OO SHORT HLIF Y-88 -2.056E-02 2.152E-01 4.630E-01 NOT IDENT. Y-91 -3.763E+02 4.578E+02 7.703E+02 NOT IDENT. NB-94 3.121E-02 3.079E-02 6.691E-02 NOT IDENT. NB-95 5. 723E-02 9. 964E-01 l.353E+00 NOT IDENT. NB-95M 1.085E+OO 1.897E+OO 3.636E+OO NOT IDENT. ZR-.95 7.605E-01 1. 119E+OO 2.448E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 0.000E+OO 1. 960E+41 0.000E+OO SHORT HLIF M0-99 O.OOOE+OO 2.29'3E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.614E+41 O.OOOE+OO SHORT HLIF RH-101 -1. 411E-02 3.00lE-02 5.338E-02 NOT IDENT. RH-102 2. 281E-03 5.350E-02 1.043E-01 NOT I DENT: RU-103 -3.220E+OO 3.985E+OO 6. 811E+OO FAIL ABUN RH-106 6.663E-03 4.076E-01 8.014E-01 NOT IDENT. RU-106 6.663E-03 4.076E-01 8.014E-01 NOT IDENT. AG-108M -5.691E-03 2.756E-02 4.660E-02 NOT IDENT. AG-llOM 1.352E-01 1.392E-01 2.063E-01 FAIL ABUN SN-113 -6.069E-02 2.162E-01. .4.070E-01 NOT IDENT. CD-115 0.000E+OO 3.574E+38 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 5.801E+04 O.OOOE+OO SHORT HLIF TE-123M 1.819E-02 2. 071E-01 NOT IDENT. SB-124 2.565E-01 1.471E+00 3.475E+OO NOT IDENT. SB-125 -8.754E-02 9.356E-02 1.600E-01 NOT IDENT. TE-125M -l.009E+02 2.323E+02 4. l 71E+02 NOT IDENT. I-126 O.OOOE+OO 6.028E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.145E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 5.746E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.360E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 7.789E+25 O.OOOE+OO SHORT HLIF BA-133 -1.835E-03 3.516E-02 6.234E-02' NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-134 8.024E-02 4.922E-02 1. 006E-01 FAIL ABUN CS-135 -6.629E-02 l.348E-01 2.538E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.329E+05 O.OOOE+OO SHORT HLIF CE-139 -l.868E-02 l.032E-01 1.849E-01 NOT IDENT. BA-140 O.OOOE+OO 8.358E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 1.621E+05 O.OOOE+OO SHORT HLIF CE-141 3.631E+OO 1. 772E+Ol 3.342E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.560E+41 O.OOOE+OO SHORT HLIF CE-144 -7. 396E-02 3.033E-01 5.508E-01 NOT IDENT. PM-144 -3.632E-03 5.263E-02 9.904E-02 NOT IDENT. PR-144 -3.297E-01 4.552E+OO 8.562E+OO NOT IDENT. PM-146 3.561E-02 4.560E-02 9.514E-02 FAIL ABUN ND-147 O.OOOE+OO 2.063E+07 O.OOOE+OO SHORT HLIF PM-147 -2.860E+Ol '7.157E+02 1;334E+03 NOT IDENT. PM-149 O.OOOE+OO 4.248E+39 O.OOOE+OO SHORT HLIF EU-150 4.386E-03 2.183E-02 4.027E-02 FAIL ABUN EU-152 l.257E-02 7.952E-02 1.597E-01 FAIL ABUN GD-153 -5.148E-02 1.718E-01 2.917E-01 NOT IDENT. EU-154 -4.926E-02 l.344E-01 2.460E-01 NOT IDENT. EU-155 8.929E-02 9.866E-02 l.986E-01 FAIL ABUN TB-160 -1.907E-01 1.315E+OO 2.391E+OO FAIL ABUN HO-i66M 2.470E-03 4.343E-02 8:644E-02 NOT IDENT. TM-171 8.058E-01 l.468E+Ol 2.914E+Ol NOT IDENT. HF-172 7.599E-02 1.991E-01 3.840E-01 FAIL ABUN LU-172 8. 966E-02 8.055E-02 1.843E-01 FAIL ABUN LU-176 -2 .181E-02 2.153E-02 3.792E-02 FAIL ABUN Page 128 of 614

' HF-181 5.003E-01 3.715E+OO 7. 323E+OO NOT IDENT. TA-182 6.708E-01 9.605E-01 l.918E+OO FAIL ABUN RE-183 -4.652E-01 2.065E+OO 3. 960E+OO NOT IDENT. RE-184 3.527E+OO 2 .116E+Ol 4.Sl7E+Ol NOT IDENT. W-188 -3.743E+OO 9.989E+Ol 1. 7 69E+02 FAIL ABUN IR-192 .:...4. 365E-02 3.891E-01 7.468E-01 FAIL ABUN HG-203 -4.933E-01 l.815E+OO 3.505E+OO NOT IDENT. BI-207 l.554E-02 *5.154E-02 9.743E-02 FAIL ABUN PB-210 8.024E-Ol 2.383E+OO 4.827E+OO NOT IDENT. PB-211 2.423E-01 5.761E-01 l.188E+OO NOT IDENT. BI-212 l.055E+OO 9.671E-01 l.226E+OO FAIL ABUN RN-219 2.732E-02 3.440E-01 6.784E-01 NOT IDENT. RA-223 -6.272E-02 5.220E-01 9.157E-01 FAIL ABUN AC-227 l.988E-02 2.049E-01 4.091E-01 NOT IDENT. TH-227 l.988E-02 2.049E-01 4. 091E-01 NOT IDENT. TH-229 -l.344E-01 4.lOlE-01 7.195E-01 FAIL ABUN PA-231 6.407E-02 4.219E-01 8.153E-01 NOT IDENT. TH-231 -6.272E-02 5.220E-01 9.157E-01 FAIL ABUN PA-233 l.337E-02 5.079E-02 l.033E-01 NOT IDENT . . PA-234 -8.799E-02 2.695E-01 5.155E-01 FAIL ABUN PA-234M 7. 491E-01 4.041E+OO 8.500E+OO NOT IDEN'i'. NP-237 l.337E-02 5.079E-02 l.033E-01 NOT IDENT. NP-238 O.OOOE+OO 5.552E+40 O.OOOE+OO SHORT HLIF NP-239 3. 721E-01 3.490E-01 4.168E-01 FAIL ABUN PU-239 l.602E+02 2.637E+02 5.179E+02 NOT IDENT. AM-241 l.874E-03 l.070E-01 1. 941E-01 NOT IDENT. CM-243 3.622E-03 9.231E-02 l.738E-01 NOT IDENT. BK-247 2:066E-02 6.238E-02 l.277E-01 'NOT IDENT. CM-247 -4.188E-03 3.124E-02 6. 013E-02 NOT IDENT. CF-249 -l.316E-03 3.146E-02 6.172E-02 NOT IDENT. CF-251 -5.224E-02 l.023E-01 1. 768E-01 NOT IDENT. Page 129of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:36:05.94 Nuclide Line Activity Report .Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 269 10.66* 1.122E+OO 1.162E+Ol 1.162E+Ol 12.17 KR-85 514.00 10 0.43* 2.617E+OO 4.529E+OO 4.774E+OO 163.95 SR-85 514.00 10 96. 00* 2.617E+OO 2.048E-02 4.683E-01 163.95 CD-109 88.03 74 3.70* 5.740E+OO 1. 793E+OO 2.784E+OO 63.24 SN-126 64.28 29 9.60 3.539E+OO 4.456E-01 4.456E-01 197.70 86.94 74 8.90 5.740E+OO 7.454E-01 7.454E-01 63.24 87.57 74 37.00* 5.740E+OO 1. 793E-01 1. 793E-01 63.24 BA-137M 661.66 89 89.90* 2.139E+OO 2.382E-01 2.426E-01 30.02 CS-137 661.66 89 85.10* 2.139E+00 2.516E-01 2.563E-01 30.02 TL-208 277.37 ------6.60 . 4.377E+00 ------Line Not Found ------583.19 75 85.00* 2.366E+OO l.934E-01 l.934E-01 32.74 860.56 ------12.50 1. 736E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 4.591E+OO ------Line Not Found ------351.06 211 12.92* 3.592E+00 2.352E+OO 2.352E+00 22.60 PB-212 74.82 144 10.28 4.791E+OO l.508E+00 l.508E+00 35.70 77 .11

  • 212 17.10 4.995E+00 l.283E+OO L283E+OO 26.03 238.63 291 43.60* 4. 931E+OO 6. 99_8E-01 6.998E-01 16.24 300.09 ------3.30 4.103E+00 ------Line Not Found ------BI-214 609.32 180 45.49* 2.284E+OO 8. 971E-01 8.974E-01 21. 88 1120.29 40 14.92 1. 406E+OO 9.903E-01 9.907E-01 50.10 1764.49 14 15. 3-0 9.423E-01 4.996E-01 4.998E-01 89.81 PB-214 74.82 144 5.80 4.791E+OO 2.673E+00 2.674E+OO 35.70 77 .11 212 9.70 4. 995E+OO 2.262E+OO 2.263E+OO 26.03 87.09 74 3.41 5.740E+OO 1. 946E+OO l.946E+OO 63.24 242.00 102 7.25 4.882E+OO 1.483E+OO 1.483E+OO 37.61 295.22 124 18.42 4.157E+OO 8.398E-01 8.400E-01 30.50 351.93 211 35.60* 3.592E+00 8.537E-01 8.540E-01 22.60 RN-222 609.32 180 45.49* 2.284E+OO 8. 971E-01 8.974E-01 21. 88 1120.29 40 14.92 1.406E+OO 9.903E-01 9.907E-01 50.10 1764.49 14 15.30 9.423E-01 4.996E-01 4.998E-01 89.81 RA-224 240.99 102 4.10* 4.882E+OO 2.622E+OO 2.622E+OO 37.61 RA-226 609.32 180 45.49* 2.284E+OO 8.971E-01 8.974E-01 21. 88 1120.29 40 14.92 1. 406E+OO 9.903E-01 9.907E-01 50.10 1764.49 14 15.30 9.423E-01 4. 996E-01
  • 4.998E-01 89.81 AC:...228 105.21 ------1.10 6.488E+OO ------Line Not Found ------338.32 62 11. 27 3.715E+OO 7.607E-01 7.607E-01 60.29 794.95 19 4.25 l.850E+00 l.234E+OO 1.234E+OO 62.59 835.71 ------1. 61 l.777E+00 ------Line Not Found ------911.20 72 25.80* 1.660E+OO 8. 711E-01 8. 711E-01 29.66 968. 97 32 15.80 1. 580E+OO 6.660E-01 6. 660E-Ol* 50.59 RA-228 105.21 ------1.10 6.488E+OO ------Line Not Found ------338.32 *62 11. 27 3.715E+OO 7.607E-01 7.607E-01 60.29 794.95 19 4.25 1.850E+OO 1.234E+OO 1.234E+00 62.59 835.71 ------i. 61 l.777E+00 ------Line Not Found ------911. 20 72 25.80* 1.660E+OO 8. 711E-01 8.711E-01 29.66 "968.97 32 15.80 1. 580E+OO 6.660E-01 6.660E-01 50.59 TH--228 74.82 144 10.28 4.791E+OO 1.508E+OO 1.508E+OO 35.70 Page 130 of 614 Nuclide Line Activity Report (continued) Page : 2 Sample ID : R405245004 Acquisition date 3-0CT-2016 04:34:09 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 77.11 212 17.10 4.995E+OO l.283E+OO l.283E+OO 26.03 238.63 291 43.60* 4.931E+OO 6.998E-01 6.998E-01 16.24 300.09 ------3.30 4.103E+OO ------Line Not Found ------TH-230 609.32 180 45.49* 2.284E+OO 8.971E-01 8.971E-01 21. 88 1120.29 40 14.92 1. 406E+OO 9.903E-01 9.904E-01 50.10 1764.49 14 15.30 9.423E-01 4. 996E-01 4.996E-01 89.81 TH-232 105.21 ------1.10 6.488E+OO ------Line Not Found ------338.32 62 11. 27 3. 715E+OO 7.607E-01 7.607E-01 60.29 835. 71 ------1. 61 l.777E+OO ------Line Not Found ------911. 20 72 25.80* l.660E+OO 8. 711E-01 8. 711E-01 29.66 968. 97 32 15.80 l.580E+OO 6.660E-01 6.660E-01 50.59 TH-234 63.29 29 3.70* 3.539E+OO l.156E+OO l.156E+OO 197.70 92.59 76 4.23 6.041E+OO l.540E+OO l.540E+OO 66.18 U-234 609.32 180 45.49* 2.284E+OO 8. 971E-01 8. 971E-01 21. 88 1120. 29 40 14.92 1. 406E+OO 9.903E-01 9.903E-01 50.10 1764.49 14 15.30 9.423E-01 4. 996E-01 4. 996E-01 89.81 U-235 89. 96 43 3.47 5.897E+OO l.097E+OO l.097E+OO 101.46 93.35 76 5.60 6.041E+OO l.163E+00 l.163E+00 66.18 143.76 ------10.96* 6."563E+OO ------Line Not Found ------163.33 -------5.08 6.266E+00 ------Line Not Found ------185.72 43 57.20 5.849E+OO 6.586E-02 6.586E-02 91. 82 205.31 ------5.01 5.496E+OO ------Line Not Found ------U-238 63.29 29 3.70* 3.539E+OO l.156E+OO l.156E+OO 197.70 92.59 76 4.23" 6.041E+OO l.540E+OO l.540E+OO 66.18 AM-243 43.53 ------5.90 6.933E-01 ------Line Not Found ------74.66 144 67.20* 4.791E+OO 2.307E-01 2.307E-01 35.70 ANH-511 511. 00 62 100.00* 2.634E+OO l.213E-01 l.213E-01 53.56 Flag: *" Key line Page 131of614 Page : 3 Summary of Nuclide Activity Sample ID : R4D5245DD4 Acquisition date 3-0CT-2Dl6 D4:34:D9 Total number of lines in spectrum 49 Number of unidentified lines 16 Number of lines tentatively identified by NID 33 Nuclide Type : Nuclide K-4D
  • KR-85 SR-85 CD-1D9 SN-126 BA-137M CS-137 TL-2D8 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC'-228 RA-228 TH-228 TH-23D TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+D9Y 1D.56Y 64.84D 461. 4DD 2.3DE+D5Y 30.08Y 3D.08Y 1.41E+lDY 7.04E+08Y 1. 41E+1DY 1600. ODY 16DD. ODY 1600. ODY 1.41E+1DY 1600. ODY 1. 41E+10Y 1. 41E+10Y 1.41E+10Y 7.54E+D4Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4,47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 05 22.9 1. 55 1. 00 1. 02 1. 02 1. OD 1. OD 1. 00 1. 00 1. 00 1. OD 1. OD 1. OD 1. 00 1. 00 1. DD 1. 00 1. OD 1. DD 1. 00 1. DD 1. DD 1. OD 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.162E+Ol 4.529E+OO 2.D48E-02 l.793E+OO 1. 793E-01 2.382E-01 2.516E-01 1.934E-01 2.352E+DO 6.998E-01 8. 971E-01 8.537E-01 8.971E-01 2.622E+OO 8. 971E-01 8. 711E-01 8. 711E-01 6.998E-01 8. 971E-01 8.711E-01 1.156E+OO 8. 971E'-01 6.S86E-02 l.156E+00 2.307E-01 1.213E-01 3.589E+Ol 3.589E+Ol Decay Corr pCi/GRAM l.162E+Ol 4.774E+OO 4.683E-01 2.784E+OO 1. 793E-01 2.426E-01 2.563E-01 1.934E-01 2.352E+OO 6.998E-01 8.974E-01 8.974E-01 2.622E+OO 8.974E-01 8. 711E-01 8.711E-01 6.998E-01 8.971E-01 8. 711E-01 1.156E+OO 8.971E-01 6.586E-02 1.156E+OO 2.307E-01 1. 213E-01 3.758E+Ol 3.758E+Ol 67.35% Decay Corr 2-Sigma Error 0.141E+Ol 7.827E+OO 7.678E-01 1. 760E+OO 1.134E-Dl D.728E-01 D.769E-01 0.633E-01 0.532E+DD 1.136E-Dl l.964E-01 l.930E-01 1. 964E-01 D.986E+OD 1. 964E-01 2.584E-01 2.584E-01 1.136E-01 1. 963E-01 2.584E-01 2.286E+OO 1. 963E-01 6.D47E-02 2.286E+OO D.824E-01 0.650E-01 "M" Manually accepted 2-Sigma %Error 12 .17 163.95 163.95 63.24 63.24 30.02 30.02 32.74 22.60 16.24 21. 88 22.60 21. 88 37.61 21. 88 29.66 29.66 16. 24 21. 88 29.66 197.70 21. 88 91. 82 197.70 35.70 53.56 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 132of614 Flags K Unidentified Energy Lines Page : 4 Sample ID : R405245004 Acquisition date : 3-0CT-2016 04:34:09 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 116. 85 38 79 1. 57 234.16 230 8 8.78E-03 95.7 6.67E+OO T 0 209.35 38 83 1. 45 419.12 414 9 9.17E-03 99.0 5.42E+00 0 247.43 25 31 1. 46 495.27 493 6 6.llE-03 86.0 4.79E+OO 0 328.25 27 40 1. 73 656.88 651 9 6.67E-03 99.0 3.81E+OO T 0 438.68 29 24 1. 94 877.69 871 11 7.52E-03 77.3 2.99E+OO T 0 455.84 45 44 7.79 912.00 902 20 1.17E-02 83.7 2.89E+OO 0 466.46 24 25 4.06 933.22 926 12 6.25E-03 **** 2.84E+OO 0 563.50 19 20 3.14 1127.27 1121 11 4.91E-03 **** 2.43E+OO T 2 586.48 19 5 1. 92 1173.22 1161 16 4.99E-03 73.9 2.35E+OO 0 633.57 14 22 3.57 1267.38 1259 14 3.61E-03 **** 2.21E+OO T 0 720.50 20 13 1. 72 1441.22 1434 13 5.31E-03 90.1 2.00E+OO T 0 728.18 27 27 1. 68 1456.58 1449 15 7.29E-03 93.5 1.98E+OO T 0 763.76 15 16 1. 42 1527.72 1523 9 4.20E-03 **** 1.91E+OO T 0 769.14 19 25 2.22 1538.48 1533 11 5.14E-03 **** 1.90E+OO 0 807.64 25 32 8.72 1615.47 1599 25 6.86E-03 **** 1. 83E+OO 0 829.21 5 10 1. 37 1658.60 1650 10 1.39E-03 **** 1. 79E+OO 0 883.39 14 10 1. 54 1766.94 1760 13 3.95E-03 **** 1.70E+OO T 0 964.36 17 16 2.34 1928.87 1921 13 4.73E-03 **** 1.59E+OO T 0 1043.01 13 4 1. 73 2086.15 2081 9 3.53E-03 82.0 1. 49E+OO 0 1069.53 7 7 1. 42 2139.19 2132 10 1.85E-03 **** 1.46E+OO 0 1152. 22 5 10 1. 02 2304.55 2299 7 1.53E-03 **** 1.37E+OO 0 . 1162. 76 26 4 0.82 2325.62 2317 17 7.22E-03 53.3 1. 36E+OO 0 1168. 69 8 3 0.80 2337.47 2333 7 2.36E-03 **** 1.36E+OO 0 1195 .15 10 16 4.26 2390.39 2381 13 2.76E-03 **** 1.33E+OO 0 1219.53 12 12 2.73 2439.16 2433 10 3.43E-03 **** 1. 31E+OO 0 1341.-69 9 0 1. 38 2683.44 2676 12 2.50E-03 66.7 1. 21E+OO Flags: "T" = Tentatively associated Page 133 of 614 VAX/VMS Nuclide Identification Report Generated 03-0CT-201.6 05: 36: 21. 45
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245004.CNF;l *
  • date 3-0CT-2016 04:34:09 Sensitivity 3.000 *
  • Detector ID GAM07 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.46 Half life ratio : ***** *
  • Sample date 15-DEC-2015 10:21:00 Nuclide Library : SOLID *
  • Sample ID R405245004 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.4528E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 19-AUG-2016 11:09:59 Eff. Geometry : CAN *
  • Eff. File : DKAlOO:' [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;15
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified.Nuclides Nuclide K-40 KR-85 SR-85 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM l.793E-01 O.OOOE+OO O.OOOE+OO 7.529E-01 4.871E-02 2.266E-02 2.394E-02 2.605E-02 l.369E-01 4.039E-02 4.079E-02 l.467E-01 4.079E-02 4.331E-01 4.079E-02 9.000E-02 9.000E-02 4.039E-02 4.077E-02 9.000E-02 7.946E-01 4.077E-02 l.546E-01 7.946E-01 3.189E-02. 2.178E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 134 of 614 Le (pCi/GRAM 7.515E+OO 4.242E-02 O.OOOE+OO 2.621E-02 2.822E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-ll3 CD-ll5 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-i26 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-14'9 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 135 of 614 O.OOOE+OO 0.000E+OO 5.324E-02 3.023E-01 O.OOOE+OO . 3. 428E-02 4.591E-01 5.334E+OO 2.713E-02 l.395E-01 l.617E+OO 5.628E+OO O.OOOE+OO l.618E-01 0.000E+OO O.OOOE+OO 5.352E-01 O.OOOE+OO 1. 794E-01 3.194E+02 2.995E-02 5.873E-01 1. 678E+OO l.062E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.477E-02* 4.547E-02 2.890E+OO 3.453E-01 3.453E-01 2.065E-02 9.019E-02 l.837E-01 O.OOOE+OO O.OOOE+OO 9.596E-02 l.301E+OO 7.028E-02 l.943E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2. 772E-02 O.OOOE+OO 4.440E-02 l.168E-01 O.OOOE+OO O.OOOE+OO 8.599E-02 O.OOOE+OO O.OOOE+OO l.551E+Ol O.OOOE+OO 2.550E-01 4.341E-02 3.752E+OO 4.336E-02 O.OOOE+OO 6.190E+02 O.OOOE+OO l.810E-02 7.210E-02 l.364E-01 l.060E-01 9.323E-02 9.662E-01 3. 668E-02* l.348E+Ol 1. 789E-01 8.162E-02 1. 704E-02 3.273E+OO SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. *NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT *IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF *NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 .CM-247 CF-249 CF-251 Page 136 of 614 8.415E-01 1.838E+OO 1.914E+Ol 8.058E+Ol 3.385E-01 1.593E+OO 4.214E-02 2.249E+OO 5.340E-01 5.594E-01 3.052E-01 4.107E-01 1.881E-01 1.881E-01 3.307E-01 3.745E-01 4.107E-01 4.689E-02 2.211E:...01 3.703E+OO 4.689E-02 O.OOOE+OO 1.944E-01 2.415E+02 9. OllE-02 8.129E-02 5.849E-02 2. 694E-02

  • 2.755E-02 8.136E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:36:27.42 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA *
  • *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245004.CNF;l *
  • Acquisition date 3-0CT-2016 04:34:09 Sensitivity : 3.000 *
  • Detector ID GAM07 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.46 Half life ratio : ***** *
  • Sample date 15-DEC-2015 10:21:00 Nuclide Library : SOLID *
  • Sample ID R405245004 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : l.4528E+02 GRAM *
  • Quantity Err(%) : l.3767E-03 % * *Wet.wt corr : 1.00000 : 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* *
  • CALIBRATION INFORMATION * * * *
  • Eff. Cp.l. date 19-AUG-2016 11:'09:59 Eff. Geometry : CAN *'
  • Eff .. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM K-40 KR-85 SR-85 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 *RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 1.162E+Ol 4.774E+OO 4.683E-01 1.582E+OO l.019E-01 2.426E-01 2.563E-01 1.934E-01 3. 851E-02 6.998E-01 8.974E-01 8.540E-01 8.974E-01 1.137E+OO 8.974E-01 8. 711E-01 8. 711E-01 6.998E-01 8.971E-01 8.711E-01 l.156E+OO 8.971E-01 6.032E-02 l.156E+OO l.582E-01 1. 213E-01 Act Error , (1. 96-sigma) 1.513E+OO 7.673E+OO 7.527E-01 1. 773E+OO l.141E-01 7.214E-02 7.621E-02 6.258E-02 8.773E-01 1.174E-01 1. 963E-01 l.924E-01 1.963E-01 1.070E+OO 1. 963E-01 2.571E-01 2.571E-01 l.174E-01 1. 962E-01 2.571E-01 2.255E+OO 1. 962E-01 1. 756E-01 2.255E+OO 8:465E-02 6.385E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 137of614 Key-Line Activity (pCi/GRAM -3.991E+OO -2.205E-02 -1. OOOE+41 l.237E-02 K.L Act error ( 1. 96-sigma) 9.373E+OO 5.429E-02 6.542E+41 2.620E-02 TPU ( 1. 96-sigma) 1. 513E+OO 7.673E+OO 7.527E-01 1.773E+OO 1.141E-01 7.214E-02 7.621E-02 6.258E-02 8.773E-01 1.174E-01 1. 963E-01 l.924E-01 1. 963E-01 1.070E+OO 1. 963E-01 -2. 571E-01 2.571E-01 l.174E-01 1. 962E-01 2.571E-01 2.255E+OO 1. 962E-01 1. 756E-01 2.255E+OO 8.465E-02 6.385E-02 TPU 9.544E+OO 5.519E-02 O.OOOE+OO 2.678E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 1. 249E-01 3.166E-01 3.216E-01 FAIL ABUN V-48 -2.022E+03 1.177E+04 1.181E+04 SHORT HLIF CR-51. -2.593E+02 3.226E+02 3. 431E+02 SHORT HLIF MN-:-54 -7.402E-03 6.152E-02 6.161E-02 NOT IDENT. C0-56 -1. 756E-01 3.770E-01 3.852E-01 NOT IDENT .. MN-56 -1.000E+41 2.125E+41 O.OOOE+OO SHORT HLIF C0-57 -4. 962E-03 4.00lE-02 4.007E-02 NOT IDENT. C0-58 2.247E-01 5.656E-01 5.746E-01 NOT IDENT. FE-59 2.504E+OO 5.742E+OO 5.852E+OO NOT IDENT. C0-60 4.295E-03 3.097E-02 3.103E-02 NOT IDENT. ZN-65 8.316E-02 1.615E-01 l.658E-01 NOT IDENT. GE-68 l .137E-02 1.877E+OO l.877E+OO NOT IDENT. AS-73 3.403E+OO 5.893E+OO 6.089E+00 NOT IDENT. AS-74 -3.071E+02 3.681E+03 3.683E+03 SHORT HLIF SE-75 9.329E-02 1.689E-01 l.741E-01 NOT IDENT. BR-77 l.601E+37 1.353E+38 O.OOOE+OO SHORT HLIF SR-82 -4.385E+02 4.678E+02 5.078E+02 SHORT HLIF RB-83 -2.952E-02 6.277E-01 6.279E-01 NOT IDENT. RB-86 8.078E+03 1.663E+04 1.702E+04 SHORT HLIF Y-88 -2.056E-02 2.152E-01 2.154E-01 NOT IDENT. Y-91 -3.763E+02 4.581E+o2 4.885E+02 NOT IDENT. NB-94 3.121E-02 3.082E-02 3.388E-02 NOT IDENT. NB-95 5. 723E-02 9. 964E-01 9. 967E-01 NOT IDENT. NB-95M 1.085E+OO 1.899E+OO 1. 961E+OO NOT IDENT. ZR-95 7.605E-01 1.119E+OO 1.171E+OO NOT IDENT. NB-97 -1.000E+41 5.085E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 2.773E+41 O.OOOE+OO SHORT HLIF M0-99 1.473E+31 2. 296E+3'1 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 1.617E+41 O.OOOE+OO SHORT HLIF RH-101 -1. 411E-02 3.012E-02 3.079E-02 NOT IDENT. RH-102 2.281E-03 5.350E-02 5. 351E-02 NOT IDENT. RU-103 -3.220E+OO 3.988E+OO 4.244E+OO FAIL ABUN RH-106 6.663E-03 4.076E-01 4.076E-01 NOT IDENT. RU-106 6.663E-03 4.076E-01 4.076E-01 NOT IDENT. AG-108M -5.691E-03 2.757E-02 2.768E-02 NOT IDENT. AG-llOM 1.352E-01 l.393E-01 1.521E-01 FAIL ABUN SN-113 -6.069E-02 2.162E-01 2.179E-01 NOT IDENT. CD-115 -7.180E+37 3.576E+38 O.OOOE+OO SHORT HLIF SN-ll 7M 1.842E+04 5.805E+04 5.864E+04 SHORT HLIF TE-123M l.819E-02 l.107E-01 l. llOE-01 NOT IDENT. SB-124 2.565E-01 1.472E+OO l.476E+OO NOT IDENT. SB-125 -8.754E-02 9.363E-02 1.016E-01 NOT IDENT. TE-125M -1.009E+02 2.324E+02 2.368E+02 NOT IDENT. I-126 -1. 596E+05 6.031E+05 6.074E+05 SHORT HLIF SB-126 l.296E+06 1.169E+06 l.307E+06 SHORT HLIF SB-127 -2.179E+21 6.448E+21 O.OOOE+OO SHORT HLIF I-131 l.575E+09 2.362E+09 2 .. 466E+09 SHORT HLIF I-132 -l.000E+41 1. 8 67E+42 O.OOOE+OO SHORT HLIF TE-132 -l.626E+25 7.816E+25 O.OOOE+OO SHORT HLIF BA-133 -1.835E-03 3.516E-02 3.517E-02 NOT IDENT. I-133 l.OOOE+41 2.934E+41 O.OOOE+OO SHORT HLIF CS-134 8.024E-02 4.934E-02 6. llBE-02 FAIL ABUN CS-135 -6.629E-02 1.349E-01 1.382E-01 NOT IDENT. I-135 1.000E+41 l.626E+42 O.OOOE+OO SHORT HLIF CS-136 -2.579E+04 2.330E+05 2.333E+05 SHORT HLIF CE-139 -1.868E-02 l.032E-01 l.036E-01 NOT IDENT. BA-140 4.870E+05 8. 361E+05 8.644E+05 SHORT HLIF LA-140 l.599E+05 l.622E+05 1. 775E+05 SHORT HLIF CE-141 3. 631E+OO 1.772E+Ol 1. 779E+Ol NOT IDENT. CE-143 1.000E+41 l.563E+41 O.OOOE+OO SHORT HLIF CE-144 -7. 396E-02 3.033E-01 3.052E-01 NOT IDENT. PM-144 -3.632E-03 5.263E-02 5.266E-02 NOT IDENT. PR-144 -3.297E-01 4.552E+OO 4.555E+OO NOT IDENT. PM-146 3.561E-02 4.567E-02 4. 841E-02 FAIL ABUN ND-147 -5.092E+06 2.063E+07 2.075E+07 SHORT HLIF PM-147 -2.860E+Ol 7.1S7E+02 7.158E+02 NOT IDENT. PM-149 -4 .118E+37 4.249E+39 O.OOOE+OO SHORT HLIF EU-150 4.386E-03 2.183E-02 2.192E-02 FAIL ABUN EU-152 1.257E-02 7.953E-02 7.973E-02 FAIL ABUN GD-153 -5.148E-02 1. 718E-01 1.734E-01 NOT IDENT. EU-154 -4.926E-02 1.345E-01 1. 363E-01 NOT IDENT. EU-155 8.929E-02 9.887E-02 l.067E-01 FAIL ABUN TB-160 -1.907E-01 1.315E+OO 1.318E+OO FAIL ABUN H0-166M 2.470E-03 4.343E-02 4.345E-02 NOT IDENT. TM-171 8.058E-01 1.468E+Ol 1.469E+Ol NOT IDENT. HF-172 7.599E-02 1.995E-01 2.024E-01 FAIL ABUN LU-172 8. 966E-02 8.106E-02 9.058E-02 FAIL ABUN LU-176 -2.181E-02 2.155E-02 2.369E-02 FAIL ABUN Page 138 of 614 HF-181 5.003E-01 3.715E+OO 3. 722E+OO NOT IDENT. TA-182 6.708E-01 9.608E-01 1.007E+OO FAIL ABUN RE-183 -4.652E-01 2.066E+00 2.076E+OO NOT IDENT. RE-184 3.527E+OO 2. ll 7E+Ol 2.123E+Ol NOT IDENT. W-188 -3.743E+OO 9.989E+Ol 9.990E+Ol FAIL ABUN IR-192 -4.365E-02 3. 891E-01 3. 896E-01 FAIL ABUN HG-203 -4. 933E-01 . 1.815E+OO 1.829E+OO NOT IDENT. BI-207 1.554E-02 5.154E-02 5. 202E-02* FAIL ABUN PB-210 8.024E-01 2.384E+OO 2.411E+OO NOT IDENT. PB-211 2.423E-01 5.762E-01 5.865E-01 NOT IDENT. BI-212 l.055E+OO 9.685E-01 1. 079E+OO FAIL ABUN RN-219 2.732E-02 3.440E-01 3.442E-01 NOT IDENT. RA-223 -6. 272E-02 5.220E-01 5.227E-01 FAIL ABUN AC-227 1.988E-02 2.049E-01 2. 051E-01 NOT IDENT. TH-227 1.988E-02 2.049E-01 2.051E-01 NOT IDENT. TH-229 -1.344E-01 4.102E-01 4.146E-01 FAIL ABUN PA-231 6.407E-02 4.221E-01 4.231E-01 NOT IDENT. TH-231 -6. 272E-02 5.220E-01 5.227E-01 FAIL ABUN PA-233 1.337E-02 5.079E-02 5 .115E-02 NOT IDENT. PA-234 -8.799E-02 2.877E-01 2.904E-01 FAIL ABUN PA-234M 7. 491E-01 4.041E+OO 4.055E+OO NOT IDENT. NP-237 1. 337E-02 5.079E-02 5.115E-02 NOT IDENT. NP-238 2.264E+40 5.552E+40 O.OOOE+OO SHORT HLIF NP-239 3. 721E-Oi 3.503E-01 3.884E-01 FAIL ABUN PU-239 1. 602E+02 2.638E+02 2.735E+02 NOT IDENT. AM-241 1. 874E-03 l.070E-01 l.070E-01 NOT IDENT. CM-243 3.622E-03 9. 231E-02 9.232E-02 NOT IDENT. BK-247 2.066E-02 6.252E_:_02 6. 321E-02 NOT IDENT. CM-247 -4.188E-03 3,125E-02 3 .130E-02 NOT IDENT. CF-249 -l.316E-03 3.146E-02 3.147E-02 NOT IDENT. CF-251 -5.224E-02 l.025E-01 l.052E-01 NOT IDENT. Page 139of614

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 44.7171 87.09 65.1390 136.47 60.2016 45.60 43.0673 87.57 65 .1967 140.51 0.0000 46.54 46.0591 88.03 65.2520 143.76 63.0877 49.72 0.0000 88.34 65.2889 144.24 70.0137 51. 35 51. 518 0 88.47 65.3045 145.44 51. 7312 51. 87 48.6675 89. 96 65.4819 152.43 52.1988 52.39 50.6823 1093.63 65.5623 153.25 *o.oooo 52.97 58.5665 91.11 0.0000 323.87 45.3407 53.44 45.9320 92.59 65.7917 156.02 0.0000 54.07 61. 6667 93.35 65.8802 . 158. 56 0.0000 57.36 0.0000 94.56 58.2118 159.00 50.2896 57.53 60.2219 94.65 58.2210 162.33 59.8886 57.98 60.2870 94.67 58.2231 162.66 *o. 0000 59.27 68.4044 94.87 58.2435 163.33 57.6095 59.32 68.4125 97.43 65.6365 165.86 63.6817 59.54 55.5522 98.43 55.7439 176.31 46.5577 60. 96 55.7381 98.44 55.7447 176.60 0.0000 61.17 58.4207 99.53 61.2179 177.52 54.9900 62.93 62. 9912 100 .11 64.5030 181.07 0.0000 63.29 63.0430 102.03 70.1039 181.52 52.8375 63.58 63.0847 103.18 69.1567 184.41 49.7954 64.28 63.1847 103.37 69.1787 143.76 42.2263 66.73 60.5054 105.21 57.4617 193.51 49.8862 67.24 60.5731 105.31 57.4710 197.03 47.6306 125.81 78.1475 106.12 74.9197 198.01 50.1252 67.75 78.1593 106.47 65.1842 201.83 54.0084 69.67 70.3654 109.28 67.6616 203.43 51.6393 70.83 67.8263 111. 00 .44.8656 205.31 55.8456 72.81 62.3194 111.76 0.0000 210.85 61.1171 72.87 62.3273 114.06 63.0390 215.65 62.2406 74.66 62.5577 116. 30 0.0000 222 .11 41.7577 74.82 62.5781 116.74 46.3698 227.09 54.5462 74.97 62.5977 119.76 *54_7149 227.38 52.0432 77 .11 62.8690 '121.12 50.0098 228.16 0.0000 78.74 63.0733 121. 22 56.6863 228.18 55.4431 79.69 62.1556 121.78 55.6210 116.74 55.4431 80.12 55.9870 122.06 55.6438 235.69 36.8018 80.19 0.0000 122.92 57.9430 235. 96 40.6189 80.57 62.2627 123.07 57.9557 238.63 47.5063 81. 00 62.3145 265.00 54.6607 238.98 0.0000 81. 07 62.3232 125.81 53. 7114 240.99 47.6095 81. 75 60.3249 127.23 66.1551 242.00 47.6533 83.79 64.7374 127.91 61.7304 244.70 25.5914 84.00 64.7634 129.30 50.6065 252.40 0.0000 85.43 64.9379 131.20 50.7424 252.80 44.6812 86.55 65.0737 133.02 56.5239 254.15 0.0000 86.79 65.1026 133.52 57.6948 256.23 42.2310 86.94 65.1210 136.00 65.8385 260.90 0.0000 Page 140 of 614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 31.2539 355.39 0.0000 584.27 18.0085 264.80 34.7314 356.01 22.3452 595.83 0.0000 265.00 34.7371 364.49 0.0000 427.87 18.1462 268.22 53*. 9902 366.42 0.0000 602.52 0.0000 269.46 43.5862 372.51 26.3622 604. 72 8.0209 270.03 37.5025 375.05 29.2359 607.14 11. 7770 271.23 39.2862 377.52 16.0589 609.32 11. 7891 273.65 0.0000 356.01 20.8685 610.33 11. 7 945 276.40 32.4420 388.16 23.7803 614.28 12.8896 277.37 36.8551 388.63 0.0000 618.01 13.9876 277.60 43.8843 391. 69 33.3679 620.36 18.3108 278.00 37.7527 264.66 22.0529 621.93 12.9346 279.20 37.7903 401. 81 25.9069 630.19 0.0000 279.54 38.6799 402.40 26.8766 631.29 15.1536 279.70 38.6844 404.85 21.1496 633.25 15.1667 280.46 27.2720 410.95 29.9152 634.78 0.0000 283.69 44.1040 413.71 26.0997 635.95 8.1348 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 32.6821 423.72 O.DOOO 645.85 17.4297 285.90 0.0000 427.09 23.3887 657.76 14.7827 287.50 36.2771 427.87 30.2249 657.90 0.0000 290.67 35.9253 433.94 23.4849 661. 66 12.0653 293.27 0.0000 439.40 26.5056 664.57 0.0000 35'1. 93 38.2811 453.88 23.7593. 666.33 0.0000 295. 96 30. 7322. 463.37 27.8690 666.50 0.0000 879.38 42.8457 468.07 11. 9756 667.71 0.0000 299.98 33.0630 473.00 0.0000 677.62 18.7729 300.09 33.0660 475.06 14.0259 685.70 0.0000 300.13 33.0675 476.78 26.0730 695.00 0.0000 301.36 39.3612 477.60 20.0651 696. 49 17.8079 302.85 43. 8849 . 482.18 22.1276 696. 51 17.8079 256.23 30.4895 *487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 18.9272 306.78 42.2218 497.08 19.2648 697.49 12.2479 308.46 29.6827 505.52 10.6942 702.65 12.2738 311. 90 28.8594 507.63 0.0000 706.68 21.2351 316.51 30.7696 511. 00 21. 4499 711. 68 10.0792 319.41 0.0000 514.00 0.0000 720.70 0.0000 320.08 0.0000 514.00 0.0000 721. 93 0.0000 321. 04 34.5063 520.40 23.6083 722.78 20.2485 323.87 27.2992 520.69 0.0000 722. 91 20.2'500 325.23 31.4250 522.65 0.0000 723. 31 20.2529 328.76 0.0000 .527.90 0.0000 724 .19 20.2603 333.37 28.8635 528.26 18.5508 727. 33 18.9328 333.97 23.3760 529.59 15.4694 733.00 6.7771 334.37 23.3828 529.87 0.0000 735.93 12.4390 338.28 25.7470 531.02 . 0. 0000 333.97 9.0521 338.32 25.7481 537.26 0.0000 739.50 0.0000 311. 90 33.1553 546.56 0.0000 747.24 14.7657 340.48 33.1553 552.55 20.8643 748.06 9.0895 340.55 0.0000 563.25 12.5845 752.31 17.0709 344.28. 26.7804 569.33 17.8806 753.82 0.0000 345.93 28.8457 946.00 17.8820 756.73 7.9801 351. 06 25.9805 569.70 16.8314 756.80 7.9804 351. 93 25.9959 583.19 17.9989 884.68 17.1478 Page 141of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 13.7280 1274.44 11.1427 1620.50 6.5175 766.42 13.7314 1001.03 10.2292 1621. 92 8.6924 766.84 13.7334 1002.74 9.3042 1678.03 0.0000 772.60 0.0000 1004.73 11.1720 1690.97 2.2039 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 2.2360 778.90 5.7485 1028.54 0.0000 1063.66 2.2384 783.70 0.0000 1037.84 15.0459 1771.35 3.3583 785.37 18.4401 1038.76 0.0000 1791.20 0.0000 792.07 8.6655 631.29 12.0688 1808.65 1.8039 794.95 10.4095 1048.07 0.0000 1810.72 0.0000 795.86 8.6777 1049.04 13.2096 1836.06 4.5332 810.06 13.9570 1050.41 13.2147 810.29 13.9580 1063.66 10.6135 344.28 10.4692 1077.00 0.0000 810.76 10.4703 1077.34 8.5627 815.77 0.0000 1085.87 9.5374 1048.07 0.0000 1093.63 8.6028 832.01 18.2882 1099.45 9.5752 834.85 17.6025 1112. 07 15.3750 835.71 22.0100 1112.84 9.2268 836.80 0.0000 1115. 54 7.6948 846.75 0.0000 1120.29 12.5208 8 4 6 .'77 14.1421 1120. 55 12. 5223' 856.80 0.0000 1221.41 10.7905 860.56 10.6578 1129. 67 13.5198 871. 09 12.4794 1131.51 0.0000 873.19 9.8123 1147.95 0.0000 875.33 0.0000 1173.23 11.1698 879.38 7.1516 1177.95 10. 7643 880.51 2.8617 1189.05 14.1337 883.24 6.2658 1204.77 15.7705 884.68 11.4633 1221.41 9.5039 889.28 8.3715 1231. 02 9.9243 894.76 5.3917 1235.36 0.0000 898.04 9.8959 1238.28 10.9376 900. 72 8.1038 1260.41 0.0000 903.28 9. 0118 1271.87 11. 0322 911.20 9.9395 1274.44 17.0612 912.08 9.9422 1274.54 17.0612 923.98 0.0000 1291.59 9.0714 926.50 8.1736 1298.22 0.0000 929 .11 10. 9072 1312 .11 0.0000 937.49 21.8745 1332.49 5.0909 944.13 0.0000 1362.66 0.0000 946.00 15.5370 1365.19 2.0525 949.00 10.9779 1368.63 0.0000 667. 71 0.0000 1384.29 1.0309 962. 31 7.3499 1408.01 7.2568 964. 08 7.3540 1457.56 0.0000 966 .17 11.0383 1460.82 3.1479 911. 20 10.3117 1489.16 3.1681 968. 97 10.3117 1505.03 8.4780 983.53 0.0000 1584.12 6.4680 984.45 0.0000 1596.21 0.0000 Page 142of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 11:26:27.27 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245005.CNF;l Background file .DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM18.CNF;511 Background date Z-OCT-2016 11:01:02. Sample date 15-DEC-2015 11:42:00 Acquisition date : 3-0CT-2016 04:34:32. Sample ID R405245005 Sample quantity : 1.17771E+02 GRAM Detector name : GAM18 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: O 01:00:00.96 0.0% Energy tolerance 2.00000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596387 Detector SN# Matrix Spike ID . . LCS ID . 1556 ******************************************************************************** Pk It 1 3 2 3. 3 0 4 0 5 0 6 0 7 0 8 0 9 3 10 3 11 0 12 0 13 0 14 0 15 0 16 0 17 0 18 . 2 19 2 20 0 21 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33. 0 34 0 Page 143of614 Energy 74.80 77.13* 86.33 92.50* 128.75 154.76 186.35*' 209.31 238.80* 241.82 270.21 295.46* 328.61 338.17* 403.36 448.14 463.21 471.91 511.51* 583.73* 609.70* 658.73 662. 16 666.37 678.58 703.87 .727.51 769.77 787.99 796.88* 861.40 911. 94* 970.68* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 115 229 115 143 33 22 134 46 546 153 66 214 15 110 294 11 16 51 26 21 169 255 12 48 26 11 35 59 31 22 15 40 125 48 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 185 143 253 298 184 119 167 126 97 128 99 117 68 78 81 45 48 20 23 83 68 63 12 37 16 16 48 43 44 45 27 27 40 61 1.18 0.96 3.69 1.19 1. 56 1. 39 1.29 1.19 1. 21 1. 72 2 .. 81 1. 44 0.69 1. 54 1. 53 2.79 1. 00 2.09 1.74 2.18 1. 55 1. 49 0.99 1. 38 1. 52 0.65 7.76 3. 5.9 2.05 4.55 1. 37 3.80 1. 81 2.03 150.40 155.05 173.43 185.77 258 .-19 310.19 373.31 419.19 478.12 484.17 540;89 591.36 657.60 676. 71 705.06 807.00 896.50 926. 62 944.00-1023.16 1167. 51 1219.41 1317.42 1324.27 1332.68 1357.09 1407.64 1454.89 1539.35 1575.79 1593.56 1722.53 1823.55 1940.99 147 147 167 179 254 306 366 415 473 473 535 585 654 669 699 800 887 921 921 1015 1159 1213 1314 1320 1329 1354 1396 1446 1532 1568 1587 1712 1814 193A 14 3.20E-02 21.3 5.71E-01 14 6.37E-02 10.9 11 3.21E-02 28.2 14 3.96E-02 27.9 10 9.16E-03 78.7 8 6.lOE-03 88.9 14 3.71E-02 23.1 11 1.29E-02 49.3 16 1.52E-01 5.3 2.61E+OO 16 4.25E-02 18.5 12 1. 82E-02 32. 8 13 5.95E-02 12.6 8 4.21E-03 96.8 12 3.06E-02 19.1 14 8.16E-02 8.9 9 3.06E-03114.0 12 4.44E-03 90.1 26 1.41E-02 24.6 2.17E+OO 26 7.28E-03 30.2 15 5.81E-03113.6 17 4.69E-02 13.9 14 7.lOE-02 9.3 6 3.33E-03 54.0 10 1.33E-02 27.3 9 7.25E-03 34.8 7 3.06E-03 67.2 18 9.62E-03 50.5 16 l.64E-02 28.3 17 8.58E-03 53.6 14 6.09E-03 70.4 11 4.16E-03 77.1 18 1. 12E-02 34. 2 20 3.48E-02 15.7 13 1.34E-02 38.9 Peak Search Report (continued) Page : 2 Sample ID : R405245005 Acquisition date 3-0CT-2016 04:34:32 Pk It Energy Area Bkgnd FWHM Channel Left. Pw Cts/Sec %Err Fit 35 0 1070.11 13 18 4.74 2139.75 2134 14 3.57E-03 74.8 36 0 1086.80 11 14 1. 84 2173.11 2163 12 3.06E-03 76.1 37 0 1095.35 18 37 4.46 2190.21 2181 18 5.08E-03 80.6 38 0 1122. 25* 46 79 0.95 2243.99 2234 24 1.27E-02 55.4 39 0 1190. 32 20 15 3.98 2380.06 2371 15 5.60E-03 47.4 40 0 1379.12 15 7 0.95 2757.54 2752 12 4.27E-03 45.5 41 0 1461.81* 615 5 2 .11 2922.86 2912 21 1. 71E-01 4.2 42 0 1621.98 *14 4 1. 35 3243.12 3236 14 4.00E-03 38.2 43 0 1657.60 14 0 0.81 3314.36 3306 15 3.89E-03 26.7 44 0 1766.28* 40 10 2.34 3531. 67 3520 19 l. lOE-02 25.9 Flag: "*" = Peak area was modified by background subtraction Page 144 of 614 VMS Nuclide Identification Report V3.1 Generated* 3-0CT-2016 11:26:29 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245005.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 15-DEC-2015 11:42:00 R405245005 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 04:34:32 117.77 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA18 0 01:00:00.00 2.00 keV No Linear 75.00 Interference Report Interfering Page 145 of 614 Nuclide PB-214 PB-214 PB-214 PB-214* PB-21'4 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 BI-211 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 72. 87 74.66 74.82 74.82 351. 06 CAN 0 01:00:00.96 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : R405245005 Acquisition date 3-0CT-2016 04:34:32 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 1. 911E+OO 1.818E+Ol 1.818E+Ol 8.34 OK CD-109 88.03 3.70* 6.049E+OO 2.361E+OO 3.665E+OO 85.80 OK SN-126 64.28 9.60 3.252E+OO Line Not Found Absent 86.94 8.90 6.049E+00 9.814E-01 9.814E-01 85.80 OK 87.57 37.00* 6.049E+OO 2.361E-01 2.361E-01 85.80 OK CS-135 268.22 16.00* 6.231E+00 4. 296E-Ol* 4. 296E-01 65.56 OK BA-137M 661.66 89.90* 3.370E+OO 9.933E-02 1.012E-01 54.66 OK CS-137 661. 66 85.10* 3.370E+OO 1.049E-01 l.069E-01 54.66 OK TL-208 277.37 6.60 6.127E+00 Line Not Found Absent 583.19 85.00* 3.675E+OO 3.408E-01 3.408E-01 27.70 OK 860.56 12.50 2.812E+OO 7.060E-01 7.060E-01 68.39 OK BI-212 727.33 6.67* 3.159E+00 1. 743E+OO 1.743E+OO 56.60 OK 785.37 1.10 2.998E+OO Line Not Found Absent 1620.50 1. 47 1. 756E+OO 3.347E+OO 3.347E+OO 76.30 OK PB-212 74.82 10.28 4.750E+OO 9.044E-01 9.044E-01 79.31 OK 77 .11 17.10 5.043E+OO 1. 836E+00 1. 836E+00 21. 82 OK 238.63 43.60* 6.720E+OO 1.224E+OO l.224E+OO 10.55 OK 300.09 3.30 5.819E+00 Line Not Found Absent BI-214 609. 32' 45.49* 3.566E+OO 9.898E-01 9. 901E-01' 18.56 OK 1120.29 14.92 2.334E+OO 8. OllE-01 8.014E-01 110. 72 OK 1764.49 15.30 1.632E+OO 9.475E-01 9.478E-01 51. 79 OK PB-214 74.82 5.80 4.752E+OO Line Not Found <<INT Reject 77 .11 9.70 5.043E+OO 3.237E+OO 3.238E+00 21. 82 OK 87.09 3.41 6.121E+OO Line Not Found <<INT Reject 242.00 7.25 6.668E+OO Line Not Found <<INT Reject 295.22 18.42 5.879E+00 1.287E+OO 1. 287E+OO 25.22 OK 351. 93 35.60* 5. 217E+OO 1. 021E+OO 1. 021E+OO 17.89 OK RN-219 271.23 10.80 6. 231E+OO 6.365E-01 6.365E-01 65.56 OK 401. 81 6.60* 4.750E+OO 2.249E-01 2.249E-01 228.00 OK RN-222 609.32 45.49* 3.566E+OO 9.898E-01 9. 901E-01 18.56 OK 1120: 29 14.92 2.334E+OO 8. OllE-01 8.014E-01 110. 72 OK 1764.49 15.30 1.632E+OO 9.475E-01 9.478E-01 51.79 OK RA-224 240.99 4.10* 6.670E+OO l.398E+00 1.398E+OO 105.46 OK RA-226 609.32 45.49* 3.566E+OO 9.898E-01* 9.901E-01 18.56 OK 1120.29 14.92 2.334E+OO 8. OllE-01 8.014E-01 110. 72 OK 1764.49 15.30 1.632E+OO 9.475E-01 9.478E-01 51.79 OK AC-228 105.21 1.10 7.385E+OO Line Not Found Absent 338.32 11. 27 5.367E+OO 1.177E+OO 1.177E+OO 38.14 OK 794.95 4.25 2. 968E+OO 7.373E-01 7.373E-01 154.20 OK 835.71 1. 61 2.872E+OO Line Not Found -----Absent 911.20 25.80* 2.703E+OO 1.107E+OO 1.107E+OO 31. 37 OK 968. 97 15.80 2.588E+OO 7.250E-01 7.250E-01 77.72 OK RA-228 105.21 1.10 7 .*385E+OO Line Not Found Absent 338.32 11. 27 5.367E+OO 1.177E+OO l.177E+OO 38.14 OK 794.95 4.25 2. 968E+OO 7.373E-01 7.373E-01 154.20 OK 835.71 1. 61 2.872E+OO Line Not Found Absent 911.20 25.80* 2.703E+OO 1.107E+OO 1.107E+OO 31. 37 OK 968. 97 15.80 2.588E+OO 7.250E-01 7.250E-01 77. 72 OK TH-228 74.82 10. 28* 4.750E+OO 9.044E-01 9.044E-01 79.31 OK Page 146 of 614 Nuclide Line Activity Report (continued) Page : 3 Sample ID : R405245005 Acquisition date 3-0CT-2016 04:34:32 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 77.11 17.10 5.043E+00 l.836E+OO l.836E+OO 21. 82 OK 238.63 43.60* 6.720E+00 1.224E+OO 1.224E+OO 10.55 OK 300.09 3.30 5.819E+OO Line Not Found Absent TH-230 609.32 45.49* 3.566E+OO 9.898E-01 9.898E-01 18.56 OK 1120.29 14.92 2.334E+OO 8. OllE-01 8. OllE-01 110. 72 OK 1764.49 15.30 1. 632E+00 9.475E-01 9.475E-01 51. 79 OK TH-232 105.21 1.10 7.385E+OO Line Not Found Absent 338.32 11. 27 5.367E+OO 1.177E+OO 1.177E+OO 38.14 OK 835. 71 1. 61 2. 872E+OO Line Not Found Absent 911. 20 25.80* 2.703E+OO l.107E+OO l.107E+OO 31. 37 OK 968. 97 15.80 2.588E+OO 7.250E-01 7.250E-01 77.72 OK U-234 609.32 45.49* 3.566E+00 9.898E-01 9.898E-01 18.56 OK 1120.29 14.92 2.334E+OO 8. OllE-01 8.0llE-01 110. 72 OK 1764.49 15.30 1.632E+OO 9.475E-01 9.475E-01 51. 79 OK AM-243 43.53 5.90 3.443E-01 Line Not Found Absent 74.66 67.20* 4.750E+00 1.384E-01 1.384E-01 79.31 OK CM-247 278.00 3.40 6 .118E+OO Line Not Found Absent 287.50 2.00 5.986E+OO Line Not Found Absent 402.40 72. 00* 4.750E+OO 2.062E-02 2.062E-02 228.00 OK ANH-511 511. 00 100.00* 4.026E+OO 3.296E-02 3. 296E-02 227.25 OK Flag: "*" = Keyline Page 147of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 11:26:30.08 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245005.CNF;l *
  • Acquisition date 3-0CT-2016 04:34:32 Sensitivity : 3.000 *
  • Detector ID GAM18 Energy tolera.nce: 2. 000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.96 Half life ratio : ***** *
  • Sample date 15-DEC-2015 11:42:00 Analyst initials: MXRl *
  • Sample ID R405245005 Sample Quantity 1.1777E+02 GRAM * *Batch Number 1596387 Wet Weight '0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25-JUN-2016 08: 25 :*19 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.818E+Ol 1.486E+OO CD-109 3.665E+OO 3.082E+OO SN-126 2. 361E-01 l.985E-01 CS-135 4.296E-01 2.760E-01 BA-137M 1.012E-01 5.420E-02 CS-137 1. 069E-01 5.725E-02 TL-208 3.408E-01 9.252E-02 BI-212 1. 743E+00 9.667E-01 PB-212 1.224E+OO 1.266E-01 BI-214 9.901E-01 1.801E-01 PB-214 1. 021E+OO 1. 791E-01 RN-219 2.249E-01 5.026E-01 RN-222 9.901E-01 1. 801E-01 RA-224 l.398E+OO 1.445E+OO RA-226 9. 901E-01 1.801E-01 AC-228 l.107E+OO 3.403E-01 RA-228 l.107E+OO 3.403E-01 TH-228 1.224E+OO 1.266E-01 TH-230 9.898E-01 1.800E-01
  • TH-232 1.107E+OO 3.403E-01 U-234 9.898E-01 1. 800E-01 AM-243 1.384E-01 1. 07 5E-01 CM-247 2.062E-02 4.607E-02 ANH-511 3.296E-02 7.340E-Q2 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 148of614 Key-Line Activity (pCi/GRAM -5.997E+OO 7.733E-03 O.OOOE+OO l.198E-02 -2.058E-02 0.000E+OO K.L. Cnt Uncert ( 1. 96-sigma) 1.174E+Ol 4.605E-02 1. 960E+41 2.599E-02 3.819E-01 l.003E+04 MDA (pCi/GRAM 6.103E-01 2.499E+00 1.477E-01 2.431E-01 4.569E-02 4.826E-02 5.459E-02 8.263E-01 9.756E-02 1.202E-01 1. 221E-01 6 .181E-01 l.202E-01 l.045E+OO l.202E-01 1. 87 6E-01 1. 87 6E-01 9.756E-02 1. 201E-01 1. 876E-01 1.201E-01 9.896E-02 5.673E-02 5.293E-02 MDA (pCi/GRAM 1. 965E+Ol 8.856E-02' O.OOOE+OO 5. 968E-02 6.906E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 3.808E+02 O.OOOE+OO SHORT HLIF MN-54 -2.032E-02 6.127E-02 1. 07 5E-01 -NOT IDENT. C0-56 2. 021E-02 4.432E-01 8.182E-01 NOT IDENT. MN-56 -O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF C0-57 -2.383E-02 4.694E-02 8.087E-02 NOT IDENT. C0-58 -8.559E-02 5.596E-01 l.009E+OO NOT IDENT. FE-59 -1.668E+OO 7.385E+OO 1.158E+Ol NOT IDENT. C0-60 l.261E-02 4.063E-02 7.994E-02 NOT IDENT. ZN-65 -5.153E-04 2.125E-01 3.441E-01 _NOT IDENT. GE-68 8.991E-01 2.875E+OO 4.478E+OO NOT IDENT. AS-73 6.839E+OO 1.105E+Ol 2.213E+Ol NOT IDENT. AS-74 O.OOOE+OO 4.518E+03 O.OOOE+OO SHORT HLIF SE-75' 8.365E-02 2.139E-01 3.732E-01 NOT IDENT. BR-77 O.OOOE+OO 2.850E+36 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 6.167E+02 O.OOOE+OO SHORT HLIF RB-83 5.939E-01 5.706E-01 1.203E+OO NOT IDENT. KR-85 O.OOOE+OO 7.919E+OO 1.647E+Ol NOT IDENT. SR-85 O.OOOE+OO 7.760E-01 1.614E+OO NOT IDENT. RB-86 O.OOOE+OO 2.655E+04 O.OOOE+OO SHORT HLIF Y-88 -*1. 346E-03 2.0lOE-01 4.077E-01 NOT IDENT. Y-91 -3.102E+Ol 4.913E+02 9.100E+02 NOT IDENT. NB-94 O.OOOE+OO 6.634E-02 6.172E-02 FAIL ABUN NB-95 3.984E-01 8.217E-01 1.440E+OO NOT IDENT. NB-95M -4.195E-Ol 2.467E+OO 4.070E+OO NOT IDENT. ZR-95 1.042E+OO 1.358E+OO 2. 731E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 059E+41' O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.822E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO' 2.585E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 4.825E-02 7.443E-02 5. 871E-02 FAIL ABUN RH-102 4.322E-03 6.135E-02 l.155E-01 NOT IDENT. RU-103 -2.988E+OO 5.328E+OO 9.492E+OO FAIL ABUN RH-106 1.282E-01 5. lllE-01 9.808E-01 NOT IDENT. RU-106 l.282E-01 5. lllE-01 9.808E-01 NOT IDENT. AG-108M 2.628E-02 2.835E-02 5.581E-02 NOT IDENT. AG-llOM 2.548E-02 9. 967E-02 1. 888E-01 FAIL ABUN SN-113 -6:546E-03 2.155E-01 3.898E-01 NOT IDENT. CD-115 O.OOOE+OO 3.166E+38 -o.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 7.632E+04 O.OOOE+OO SHORT HLIF TE-123M 6.066E-02 1. 285E-01
  • 2.342E-01 NOT IDENT. SB-124 3.184E-01 2 .137E+OO 4.319E+OO NOT IDENT. SB-125 4.221E-02 l.052E-01 1.970E-01 FAIL ABUN TE-125M 9.814E+Ol 2.540E+02 4.752E+02 NOT IDENT. I-126 O.OOOE+OO 6.594E+05 O.OOOE+OO SHORT HLIF SB-l26 O.OOOE+OO 9.603E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.086E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2. 711E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 6.822E+40 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 7.841E+25 O.OOOE+OO SHORT HLIF BA-133 1.302E-02 4.454E-02 7.527E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 4.795E-02 7.247E-02 1. 068E-01 FAIL ABUN I-135 O.OOOE+OO 1.654E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.103E+05 O.OOOE+OO SHORT HLIF CE-139 -l.645E-01 l .142E--01 1.732E-01 NOT IDENT. BA-140 -O.OOOE+OO 7.788E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.662E+05 O.OOOE+OO SHORT HLIF CE-141 -6.220E+OO 2.412E+Ol 4.166E+Ol NOT IDENT. CE-143 O.OOOE+OO 8.850E+40 O.OOOE+OO SHORT HLIF CE-144 -2.150E-01 3.878E-01 6.578E-01 NOT IDENT. PM-144 -2.227E-04 6. 791E-02 l.094E-01 NOT IDENT. PR-144 5.230E-02 5.884E+OO 9.499E+OO NOT IDENT. PM-146 2.906E-02 5.130E-02 9.568E-02 NOT IDENT. ND-147 O.OOOE+OO 1. 788E+07 O.OOOE+OO SHORT HLIF PM-147 -2.415E+02 7.751E+02 l.363E+03 NOT IDENT. PM-149 0. OOO'E+OO 4. 996E+39 O.OOOE+OO SHORT HLIF EU-150 2.422E-02 2.794E-02 5.022E-02 FAIL ABUN EU-152 -6.247E-02 9.576E-02 l.639E-01 FAIL ABUN GD-153 l.057E-01 1.915E-01 3.410E-01 NOT IDENT. EU-154 -3.618E-02 l.195E-01 2.138E-01 NOT IDENT. EU-155 5.827E-02 l.103E-01 2.088E-01 FAIL ABUN TB-160 1.042E+OO 1. 951E+OO 3.766E+OO FAIL ABUN _H0-166M 9.322E-03 5.583E-02 1.057E-01 FAIL ABUN TM-171 6.243E+OO 2. 951E'+Ol 5.753E+Ol NOT IDENT. HF-172 6.244E-03 2.448E-01 4.065E-01 FAIL ABUN LU-172 . 1. 004E-01 1. 587E-Ol -l.744E-01 FAIL ABUN LU-176 1. 384E-03 2.270E-02 4.225E-02 NOT IDENT. HF-181 -l.493E+OO 4.073E+OO 6.935E+00 NOT IDENT. Page 149 of 614 TA-182 1.305E-01 8.530E-01 1.627E+OO FAIL ABUN RE-183 -5.188E-01 3.440E+OO 6.498E+OO NOT IDENT. RE-184 -1.lOlE+Ol 3.165E+Ol 4.985E+Ol NOT IDENT. W-188 -8.881E+Ol 1.262E+02 1.922E+02 NOT IDENT. IR-192 -1. 0?°8E-02 4.385E-01 8.034E-01 FAIL ABUN HG-203 -8.708E-01 2.268E+OO 4.059E+OO FAIL ABUN BI-207 3.316E-02 5.585E-02 1. OllE-01 FAIL ABUN PB-210 2. 724E+OO 5.364E+OO 1.063E+Ol NOT IDENT. BI-211 O.OOOE+OO 4.932E-01 7.483E-01 FAIL ABUN PB-211 3.927E-01. 8.775E-01 1.125E+OO FAIL ABUN RA-223 -5.476E-02 6.354E-01 1.098E+OO FAIL ABUN AC-227 1.169E-04 2.144E-01 4.012E-01 NOT IDENT. TH-227 l.169E-04 2.144E-01 4.012E-01 NOT IDENT. TH-229 -6.928E-02 4.499E-01 8.467E-01 FAIL ABUN PA-231 4.718E-01 4.815E-01 9.128E-01 NOT IDENT. TH-231 -5.476E-02 6.354E-01 l.098E+OO FAIL ABUN PA-233 -9.210E-03 5.821E-02 1.057E-01 NOT IDENT. PA-234 -5.350E-02 2.739E-01 5.133E-01 NOT IDENT. PA-234M 2.695E+OO 4.249E+OO '8. 528E+OO NOT IDENT. TH-234 1.332E-01 l.433E+OO 2.783E+OO FAIL ABUN U-235 2.973E-02 2.095E-01 3. 724E-01 FAIL ABUN NP-237 -9.210E-03 5.821E-02 1.057E-01 NOT IDENT. NP-238 O.OOOE+OO 4.546E+40 O.OOOE+OO SHORT HLIF U-238 1.332E-01 1.433E+OO -2.783E+OO FAIL ABUN NP-239 -1.035E-01 2. 480E-01. 4.323E-01 NOT IDENT. PU-239 4.394E+02 6.779E+02 6.716E+02 FAIL ABUN AM-241 7.547E-02 1.688E-01 3.304E-01 NOT IDENT. CM-243 -8.887E-02 l.004E-01 1. 701E-01 NOT IDENT: BK-247 -4. 871E-03 8.005E-02 1.328E-01 NOT IDENT. CF-249 2.464E-02 3.556E-02 6.923E-02 NOT IDENT. CF-251 4.699E-02 1.217E-01 2.176E-01 NOT IDENT. Page 150of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 11:26:27.97 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 581 10.66* 1. 911E+OO 1.818E+Ol 1.818E+Ol 8.34 CD-109 88.03 125 3.70* 6.049E+OO 3.547E+OO 5.506E+OO 56.49 SN-126 64.28 ------9.60 3.252E+OO ------Line Not Found ------86.94 125 8.90 6.049E+OO l.474E+OO 1.474E+OO 56.49 87.57 125 37.00* 6.049E+OO 3.547E-01 3.547E-01 56.49 CS-135 268.22 67 16.00* 6.231E+OO 4:296E-01 4. 296E-01 65.56 BA-137M 661. 66 47 89.90* 3.370E+OO 9.933E-02 l.012E-01 54.66 CS-137 661. 66 47 85.10* 3.370E+OO l.049E-01 1.069E-01 54.66 TL-208 277.37 ------6.60 6.127E+OO ------Line Not Found ------583.19 167 85.00* 3.675E+OO 3.408E-01 3.408E-01 27.70 860.56 39 12.50 2.812E+OO 7.060E-01 7.060E-01 68.39 BI-211 72.87 125 1. 23 4.750E+00 1.363E+Ol 1.363E+Ol 42.54 351.06 297 12.92* 5.217E+OO 2.813E+OO 2.813E+OO 17.89 BI-212 727.33 58 6.67* 3.159E+OO 1. 743E+OO 1. 743E+OO 56.60 785.37 ------1.10 2.998E+OO ------Line Not Found ------1620.50 14 1. 47 1. 756E+00 3.3'47E+OO 3.347E+OO 76.30 PB-212 74.82 125 10.28 4.750E+OO l.630E+OO l.630E+OO 42.54 77 .11 248 17 .10 5.043E+OO 1.836E+OO l.836E+00 21. 82 238.63 563 43.60* 6. 720E+OO l.224E+OO 1.224E+OO 10.55 300.09 ------3.30 5.819E+OO ------Line Not Found ------BI-214 609.32 252 45.49* 3.566E+OO 9.898E-01 9. 901E-01 18.56 1120.29 44 14.92 2.334E+OO 8. OllE-01 8.014E-01 110. 72 1764.49 37 15.30 l.632E+OO 9.475E-01 9.478E-01 51. 79 PB-214 74.82 125 5.80 4.750E+OO 2.890E+OO 2.891E+OO 42.54 77 .11 248 9.70 5.043E+00 3.237E+OO 3.238E+OO 21. 82 87.09 125 3.41 6.049E+OO 3.848E+OO 3.850E+OO 56.49 242.00 158 7.25 6.670E+OO 2.077E+OO 2.078E+00 36.97 295.22 219 18.42 5.879E+OO l.287E+OO 1.287E+00 25.22 351.93 297 35.60* 5.217E+00 l.021E+OO l.021E+00 17.89 RN-219 271. 23 67 10.80 6.231E+OO 6.365E-01 6.365E-01 65.56 401.81 11 6.60* 4.750E+OO 2.249E-01 2.249E-01 228.00 RN-222 609.32 252 45.49* 3.566E+OO 9.898E-01 9.901E-01 18.56 1120.29 44 14.92 2.334E+OO 8. OllE-01 8.014E-01 110. 72 1764.49 37 15.30 1.632E+OO 9.475E-01 9.478E-01 51.79 RA-224 240.99 158 4.10* 6.670E+OO 3.673E+OO 3.673E+OO 36.97 RA-226 609.32 252 45.49* 3.566E+OO 9.898E-01 9.901E-01 18.56 1120. 29 44 14.92 2.334E+OO 8 OllE-01 8.014E-01 110. 72 1764.49 37 15.30 l.632E+OO 9.475E-01 9.478E-01 51.79 AC-228 105.21 ------1.10 7.385E+00 ------Line Not Found ------338.32 112 11. 27 5.367E+OO l.177E+OO l.177E+OO 38.14 794.95 15 4.25 2. 968E+OO 7.373E-01 7.373E-01 154.20 835.71 ------1. 61 2.872E+00 ------Line Not Found ------911. 20 121 25.80* 2.703E+OO l.107E+00 1.107E+OO 31.37 968. 97 47 15.80 2.588E+OO 7.250E-01 7.250E-01 77. 72 RA-228 105.21 ------1.10 7.385E+OO ------Line Not Found ------338.32 112 11. 27 5.367E+OO l.177E+OO l.177E+00 38.14 794.95 15 4.25 2. 968E+OO 7.373E:-01 7.373E-01 154.20 Page, 151of614 Nuclide Line Activity Report (continued) Page : 2 Sample ID : R405245005 Acquisition date 3-0CT-2016 04:34:32 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 835.71 ------1. 61 2.872E+OO ------Line Not Found ------911.20 121 25.80* 2.703E+OO 1.107E+OO 1.107E+OO 31. 37 968.97 47 15.80 2.588E+OO 7.250E-01 7.250E-01 77. 72 TH-228 74.82 125 10.28 4.750E+OO l.630E+OO 1.630E+OO 42.54 77 .11 248 17.10 5.043E+OO 1.836E+OO 1.836E+OO 21. 82 238.63 563 43.60* 6. 720E+OO 1.224E+OO 1.224E+OO 10.55 300.09 ------3.30 5.819E+OO ------Line Not Found ------TH-230 609.32 252 45.49* 3.566E+OO 9.898E-01 9.898E-01 18.56 1120.29 44 14.92 2.334E+OO 8. OllE-01 8. OllE-01 110. 72 1764.49 37 15.30 1.632E+OO 9.475E-01 9.475E-01 51.79 TH-232 105.21 ------1.10 7.385E+OO ------Line Not Found ------338.32 112 11. 27 5.367E+OO l.177E+00 1. 177E+OO 38.14 835.71 ------1. 61 2.872E+OO ------Line Not Found ------911.20 121 25.80* 2.703E+00 1.107E+OO 1.107E+OO 31. 37 968. 97 47 15.80 2.588E+00 7.250E-01 7.250E-01 77.72 U-234 609.32 252 45.49* 3.566E+OO 9.898E-01 9.898E-01 18.56 1120.29 44 14.92 2.334E+OO 8. OllE-01 8. OllE-01 110. 72 1764.49 37 15.30 1.632E+OO 9.475E-01 9.475E-01 51. 79 AM-243 43.53 ------5.90 3.443E-01 ------Line Not Found ------74.66 125 67.20* 4.750E+OO 2.494E-01 2.494E-01 42.54 CM-247 278.00 ------3.40 6 .118E+OO ------Line Not Found ------287.50 ------2.00 5.986E+OO ------Line Not Found ------402.40 11 72.00* 4.750E+OO 2.062E-02 2.062E-02 228.00 ANH-511 511. 00 21 '100. 00* 4.026E+00 3.296E-02 3.296E-02 227.25 Flag: "*" Key line Page 152 of 614 Page : 3 Summary of Nuclide Activity Sample ID : R405245005 Acquisition date Total number of lines in spectrum 44 Number of unidentified lines 6 Number of lines tentatively identified by NID 38 Nuclide Type : Nuclide K-40 CD-109 CS-135 BA-137M CS-137 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 AM-243 CM-247 ANH-5.11 Hlife 1. 25E+09Y 461.40D 2.30E+05Y 2.30E+06Y 30.08Y 30.08Y l.41E+l0Y 7.04E+08Y 1.41E+l0Y 1.41E+10Y 1600.00Y 1600. OOY 7.04E+08Y 1600. OOY 1.41E+10Y 1600.00Y l.41E+l0Y 1. 41E+10Y l.41E+l0Y 7.54E+04Y 1. 41E+10Y 2.45E+05Y 7370.00Y 1.56E+07Y l.00E+09Y Decay 1. 00 1. 55 1. 00 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1..00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.818E+Ol 3.547E+00 3.547E-01 4.296E-01 9.933E-02 l.049E-01 3.408E-01 2.813E+OO 1. 743E+OO 1.224E+OO 9.898E-01 1. 021E+OO 2.249E-01 9.898E-01 3:673E+OO 9.898E-01 1.107E+OO 1.107E+OO 1.224E+00 9.898E-01 1.107E+OO 9.898E-01 2.494E-01 2.062E-02 3.296E-02 4.356E+Ol 4.356E+Ol Decay Corr pCi/GRAM l.818E+Ol 5.506E+OO 3.547E-01 4.296E-01 l.012E-01 l.069E-01 3.408E-01 2.813E+OO 1. 743E+OO 1.224E+OO 9. 901E-01 1. 021E+OO 2.249E-01 9. 901E-01 3.673E+OO 9. 901E-01 l.107E+OO 1.107E+OO 1.224E+OO 9.898E-01 1.107E+OO 9.898E-01 2.494E-01 2.062E-02 3.296E-02 4.552E+Ol 4.552E+Ol 86.36% Decay Corr 2-Sigma Error 0.152E+01 3. llOE+OO 2.003E-01 2.816E-01 0.553E-01 0.584E-01 0.944E-01 0.503E+OO 0.986E+OO 0.129E+OO l.838E-01 0.183E+OO 5.129E-01 l.838E-01 1.358E+00 l.838E-01 0.347E+OO 0.347E+OO 0.129E+OO 1.837E-01 0.347E+OO 1.837E-01 1.061E-01 4.701E-02 7.490E-02 "M" Manually accepted 2-Sigma %Error 8.34 56.49 56.49 65.56 54.66 54.66 27.70 17.89 56.60 10.55 18.56 17.89 228.00 18.56 36.97 18.56 31. 37 31. 37 10.55 18.56 31. 37 18.56 42.'54 228.00 227.25 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit. Page 153of614 Flags Unidentified Energy Lines Page : 4 Sample ID : R405245005 Acquisition date : 3-0CT-2016 04:34:32 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 92.50 153 320 1.19 185.77 179 14 3. 96E-02 55.9 6.59E+OO T 0 128.75 35 195 1. 56 258.19 254 10 9.16E-03 **** 8.03E+00 T 0 154.76 23 125 1. 39 310.19 306 8 6.lOE-03 **** 8.03E+OO T 0 186.35 139 174 1. 29 373.31 366 14 3. 71E-02 46.2 7.61E+OO T 0 209.31 48 130 1.19 419.19 415 11 l.29E-02 98.5 7.22E+OO T 0 328.61 15 69 0.69 657. 60 . 654 8 4. 21E-03 **** 5.47E+OO T 0 448.14 16 48 1. 00 896.50 887 12 4.44E-03 **** 4.41E+OO 2 463.21 51 20 2.09 92 6. 62 921 26 1.41E-02 49.2 4.31E+OO T 2 471. 91 26 23 1. 74 944.00 921 26 7.28E-03 60.4 4.26E+OO T 0 658.73 12 12 0.99 1317.42 1314 6 3.33E-03 **** 3.38E+OO T 0 666.37 26 16 1. 52 1332.68 1329 9 7.25E-03 69.6 3.36E+OO T 0 678.58 11 16 0.65 1357.09 1354 7 3.06E-03 **** 3.31E+OO T 0 703.87 34 47 7.76 1407.64 1396 18 9.62E-03 **** 3.23E+00 T 0 769.77 30 43 2.05 1539.35 1532 17 8.58E-03 **** 3.04E+OO 0 787.99 21 44 4.55 1575.79 1568 14 6.09E-03 **** 2.99E+OO 0 1070.11 12 17 4.74 2139.75 2134 14 3.57E-03 **** 2.41E+OO 0 1086.80 11 13 1. 84 2173.11 2163 12 3.06E-03 **** 2.39E+OO T 0 1095.35 18 35 4.46 2190.21 2181 18 5.08E-03 **** 2.37E+OO T 0 1190. 32 19 14 3.98 2380.06 2371 15 5.60E-03 94.8 2.24E+00 T 0 1379.12 15 6 0.95 2757.54 2752 12 4.27E-03 91. 0 2.00E+OO 0 1657.60 13 0 0.81 3314.36 3306 15 3.89E-03 53.5 1. 72E+OO Flags: "T" = Tentatively associated Page 154 of 614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 11:26:41.57 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245005.CNF;l *
  • Acquisition date 3-0CT-2016 04:34:32 Sensitivity : 3.000 *
  • Detector ID GAM18 Energy tolerance: 2.000 *
  • Elapsed live time: O 01:00:00.00 limit : 75.000 *
  • Elapsed real time: 0 01:00:00.96 Half life ratio : ***** *
  • Sample date 15-DEC-2015 11:42:00 Nuclide Library : SOLID *
  • Sample ID R405245005 Analyst initials: MXRl * **Batch Number 1596387 Sample Quantity : 1.1777E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 * * . Dry Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO * ******************************************************************************* Combined Critical Level Report NOTE: Not "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 CS-135 BA-137M CS-137 TL-208 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 AM-243 CM-247 ANH-511 Le (pCi/GRAM 2.630E-01 1.190E+OO 7. OOlE-02 1.129E-01 1.994E-02 2.106E-02 2.452E-02 3.722E-01 4.581E-02 5.475E-02 5.638E-02 2.815E-01 5.475E-02 4.908E-01 5.475E-02 8.143E-02 8.143E-02 4.581E-02 5.473E-:-02 8.143E-02 5.473E-02 4.671E-02 2.583E-02 2.432E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 155of614 Le (pCi/GRAM 8.936E+OO 3.928E-02 O.OOOE+OO 2.447E-02 3.lOOE-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 . SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 "GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 156 of 614 4.802E-02 3.672E-01 O.OOOE+OO 3,. 771E-02 4.528E-01 5.174E+OO 3.533E-02 1.554E-01 2.004E+OO 1.038E+Ol 0.000E+OO 1. 738E-01 O.OOOE+OO 0.000E+OO 5.508E-01 7.715E+OO 7.558E-01 0.000E+OO l.672E-01 4. 072E+02 2.819E-02 6.526E-01 1.912E+OO 1.243E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.745E-02 5.260E-02 4.339E+OO 4.477E-01 4.477E-01 2.578E-02 8.474E-02 1.789E-01 O.OOOE+OO O.OOOE+OO 1.lOOE-01 l.851E+00 9. 072E-02 2.229E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.479E-02 O.OOOE+OO 4.898E-02 O.OOOE+OO O.OOOE+OO 8.057E-02 O.OOOE+OO O.OOOE+OO 1. 968E+Ol O.OOOE+OO 3.090E-01 5.007E-02 4.346E+OO 4.448E-02 O.OOOE+OO 6.335E+02 O.OOOE+OO 2.341E-02 7.553E-02 1.603E-01 9.460E-02 9.808E-02 1.712E+OO 4.787E-02 2.698E+Ol l.902E-01 7.948E-02 l.951E-02 3.160E+OO 7.279E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN
  • FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CF-249 CF-251 Page 157of614 3.043E+OO 2.236E+Ol 8.943E+Ol 3.725E-01 1.894E+OO 4.570E-02 4.983E+OO 3.614E-01 5.140E-01 5.099E-01 1.864E-01 l.864E-01 3. 969E-01 4.284E-01 5.099E-01 4.888E-02 2.294E-01 3.860E+OO 1.315E+OO 1. 763E-01 4.888E-02 O.OOOE+OO 1.315E+OO 2.020E-01 3.185E+02 l.554E-01 7.916E-02 6.181E-02 3.192E-02 1.023E-01 NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 11:26:46.65 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040. Savage Road *
  • Charleston, SC 29407 * ***************************************************************t*************** *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245005.CNF;l *
  • Acquisition date 3-0CT-2016 04:34:32 Sensitivity : 3.000 *
  • Detector ID GAM18 Energy tolerance: 2.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.96 Half life ratio : ***** *
  • Sample date 15-DEC-2015 11:42:00 Nuclide Library : SOLID *
  • Sample ID R405245005 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity l.1777E+02 GRAM *
  • Quantity Err(%) l.6982E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • gff. Cal. date 25-JUN-2016 08:25:19 Eff: Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMlW CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.818E+Ol 1.764E+OO CD-109 3.665E+OO 3.105E+OO SN-126 2.361E-01 1. 996E-01 CS-135 4. 296E-01 2.775E-01 BA-137M 1.012E-01 5.437E-02 CS-137 1.069E-01 5.744E-02 TL-208 3.408E-01 9.365E.:..02 BI-212 1. 743E+OO 9.707E-Ql PB-212 1.224E+OO l.422E-01 BI-214 9.901E-01 1.850E-01 PB-214 1. 021E+OO 1. 840E-01 RN-219 2.249E-01 5.034E-01 RN-222 9.901E-01 1.850E-01 RA-224 1.398E+OO l.455E+OO RA-226 9.901E-01 1.850E-01 AC-228 1.107E+00 3.450E-01 RA-228 1.107E+OO 3.450E-01 TH-228 1.224E+00 1.422E-01 TH-230 9.898E-01 1.850E-01 TH-232 1.107E+OO 3.450E-01 U-234 9.898E-01 1.850E-01 AM-243 1.384E-01 1.0BBE-01 CM-247 2.062E-02 4.620E-02 ANH-511 3.296E-02 7.341E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 158 of 614 Key-Line Activity (pCi/GRAM -5.997E+OO 7'. 733E-03 1.000E+41 l.198E-02 -2.058E-02 1.146E+03 K.L Act error ( 1. 96-sigma) 1. l 74E+Ol 4.605E-02 3.280E+41 2. 600E"-02 3.819E-01 l.003E+04 TPU ( 1. 96-sigma) 1.764E+OO 3.105E+OO 1. 996E-01 2.775E-01 5.437E-02 5.744E-02 9.365E-02 9.707E-01 1.422E-01 l.850E-01 1. 840E-01 5.034E-01 l.850E-01 1.455E+OO 1.850E-01 3.450E-01 3.450E-01 1.422E-01 l.850E-01 3.450E-01 l.850E-01 1.0BBE-01 4.620E-02 7.341E-02 TPU ( 1. 96-sigma) 1. 205E+Ol 4.618E-02 O.OOOE+OO 2.655E-02 3.820E-01 l.004E+04 NOT IDENT.
  • NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 -5.564E+Ol 3.808E+02 3.816E+02 SHORT HI.IF MN-54 -2.032E-02 6.127E-02 6.195E-02 NOT IDENT. C0-56 2.021E-02 4.432E-01 4.433E-01 .NOT IDENT. MN-56 1.000E+41 2.498E+42 0.000E+OO SHORT HLIF C0-57 -2.383E-02 4. 696E-02 4.817E_:02 NOT IDENT. C0-58 -8.559E-02 5.596E-01 5.609E-01 NOT IDENT. FE-59 -1.668E+OO 7.386E+OO 7.424E+OO NOT IDENT. C0-60 1.261E-02 4.064E-02 4.103E-02 NOT IDENT. ZN-65 -5.153E-04 2.125E-01 2.125E-01 NOT IDENT. GE-68
  • 8.991E-01 2.875E+OO 2.904E+OO NOT IDENT. AS-73 6.839E+OO 1.114E+Ol l.156E+Ol NOT IDENT. AS-74 3.037E+03 4.525E+03 4. 728E+03 SHORT HLIF SE-75 8.365E-02 2.140E-01 2.173E-01 NOT IDENT. BR-77 2.756E+37 2.329E+38 0.000E+OO SHORT HLIF SR-82 8.600E+Ol 6.167E+02 6.179E+02 SHORT HLIF RB-83 5.939E-01 5.764E-01 6.356E-01 NOT IDENT. KR-85 1. 808"E+Ol 7.953E+OO l.139E+Ol NOT IDENT. SR-85 1. 769E+OO 7.794E-01 l.115E+OO NOT IDENT. RB-86 1. 023E+03 2.655E+04 2.656E+04 SHORT HLIF Y-88 -1.346E-03 2.0lOE-01 2.0lOE-01 NOT IDENT. Y-91 -3.102E+Ol 4.913E+02 4.915E+02 NOT IDENT. NB-94 6.700E-02 6.640E-02 7.295E-02 FAIL ABUN NB-95 3.984E-01 8.219E-01 8.413E-01 NOT IDENT. NB-95M -4.195E-01 2.467E+OO 2.474E+OO NOT IDENT. ZR-95 1.042E+OO *1.359E+OO 1.437E+OO NOT IDENT. NB-97 1. OOOE+41 1.059E+41 O.OOOE+OO SHORT HLIF ZR-97 1. OOOE+41 1.823E+41 0.000E+OO SHORT HLIF M0-99 8.127E+30 2.585E+31 O.OOOE+OO SHORT HLIF TC-99M l.000E+41 4.022E+41 O.OOOE+OO SHORT HLIF RH-101 4.825E-02 7.495E-02 7.804E-02 FAIL ABUN RH-102 4.322E-03 6 .135E-02 6.138E-02 NOT IDENT. RU-103 -2.988E+OO 5.330E+OO 5.497E+OO FAIL ABUN RH-106 l.282E-01 5. lllE-01 5.144E-01 NOT IDENT. RU-106 1. 282E-01 5 .lllE-01 5.144E-01 NOT IDENT. AG-108M 2.628E-02 2.837E-02 3.074E-02 NOT IDENT. AG-llOM 2. 548E-02 9. 968E-02 l.003E-01 FAIL ABUN SN-113 -6.546E-03 2.155E-01 2.156E-01 NOT IDENT. CD-115 2.290E+38 3.192E+38 O.OOOE+OO SHORT HLIF SN-117M 4.778E+03 7.633E+04 7.636E+04 SHORT HLIF TE-123M 6.066E-02 1.285E-01 l.314E-01 NOT IDENT. SB-124 3.184E-01 2 .137E+OO 2.142E+OO NOT IDENT. SB-125 4. 221E-02 1.052E-01 1.069E-01 FAIL ABUN TE-125M 9.814E+Ol 2.540E+02 2.579E+02 NOT IDENT. I-126 ' 9.666E+05 6.719E+05 8.008E+05 SHORT HLIF SB-126 -l.120E+05 9.605E+05 9.618E+05 SHORT HLIF SB-127 -4.906E+21 8. 966E+21 O.OOOE+OO SHORT HLIF I-131 l.750E+09 2.712E+09 2.825E+09 SHORT HLIF I-132 l.000E+41 1.806E+42 O.OOOE+OO SHORT HLIF TE-132 2.428E+25 7.900E+25 O.OOOE+OO SHORT HLIF BA-133 *1.302E-02 4.454E-02 4.492E-02 NOT IDENT. I-133 -1.000E+41 7.190E+41 O.OOOE+OO SHORT HLIF CS-134 4.795E-02 7.250E-02 7.565E-02 FAIL ABUN I-135 -l.000E+41 6.817E+41 O.OOOE+OO SHORT HLIF CS-136 5.177E+04 2.103E+05 2 .116E+05 SHORT HLIF CE-139 -1.645E-01 l.189E-01 1.401E-01 NOT IDENT. BA-140 5.939E+05 7.792E+05 8.239E+05 SHORT HLIF LA-140 -1. 965E+04 2.662E+05 2.664E+o5* SHORT HLIF CE-141 -6.220E+OO 2.412E+Ol 2.428E+Ol NOT IDENT. CE-143 1.000E+41 8.906E+40 O.OOOE+OO SHORT HLIF CE-144 -2.150E-01 3.879E-01 3.999E-01 NOT IDENT. PM-144 -2.227E-04 6. 791E-02 6.791E-02 NOT IDENT. PR-144 5.230E-02 5.884E+OO 5.884E+OO NOT IDENT. PM-146 2.906E-02 5.134E-02 5.298E-02 NOT IDENT. ND-147 6.406E+06 1. 789E+07 l.812E+07 SHORT HLIF PM-147 -2.415E+02 7.752E+02 7.828E+02 NOT IDENT. PM-149 -5. 952E+39 . 5.159E+39 O.OOOE+OO SHORT HLIF EU-150 2.422E-02 2.796E-02 3.002E-02 FAIL ABUN EU-152 -6.247E-02 9.582E-02 9.987E-02 FAIL ABUN GD-153 l.057E-01 1.916E-01 1. 975E-01 NOT IDENT. EU-154 -3.618E-02 1.195E-01 l.206E-01 NOT IDENT. EU-155 5.827E-02 1.103E-01 l.134E-01 FAIL ABUN TB-160 1.042E+OO l.952E+OO 2.008E+OO FAIL ABUN H0-166M 9.322E-03 5.584E-02 5.599E-02 FAIL ABUN TM-171 6.243E+00 2. 952E+Ol . 2. 965E+Ol NOT IDENT. HF-172 6. 244E-03. 2.448E-01 2.448E-01 FAIL ABUN LU-172 l.004E-01 1. 590E-01 1.653E-01 FAIL ABUN LU-176 1.384E-03 2.270E-02 2. 271E-02 NOT IDENT. HF-181 -1.493E+OO 4.074E+OO 4.129E+OO NOT IDENT. Page 159of614 TA-182 1.305E-01 8.530E-01 8.550E-01 FAIL ABUN RE-183 -5.188E-01 3.441E+OO 3.449E+OO NOT IDENT. RE-184 -1.lOlE+Ol 3.175E+Ol 3.214E+Ol NOT IDENT. W-188 -8. 881E+Ol 1. 2 66E+02 l.328E+02 NOT IDENT. IR-192 -1.078E-02 4.385E-01 4.386E-01 FAIL.ABUN HG-203 -8.708E-01 2.268E+OO 2.302E+OO FAIL ABUN BI-207 3.316E-02 5.587E-02 5.783E-02 FAIL ABUN PB-210 2. 724E+OO 5.370E+OO 5.509E+OO NOT IDENT. BI-211 2.813E+OO 5.089E-01 1.366E+OO FAIL ABUN PB-211 3.927E-01 8.778E-01 8.955E-Ol FAIL ABUN RA-223 -5.476E-02 6.354E-01 6.359E-01 FAIL ABUN AC-227 l.169E-04 2.144E-01 2.144E-01 NOT IDENT. TH-227 1.169E-04 2.144E-01 2.144E-01 NOT IDENT. TH-229 -6.928E-02 4.500E-01 4.510E-01 FAIL ABUN PA-231 4.718E-01 4.919E-01 5.359E-01 NOT IDENT. TH-231 -5.476E-02 6.354E-01 6.359E-01 FAIL ABUN PA-233 -9.210E-03 5.821E-02 5.836E-02 NOT IDENT. PA-234 -5.350E-02 2.807E-01 2.817E-01 NOT IDENT. PA-234M 2.695E+00 4.251E+OO 4.421E+OO NOT IDENT. TH-234 l.332E-01 1.433E+OO l.434E+OO FAIL ABUN U-235 2.973E-02 2.095E-01 2.099E-01 FAIL ABUN NP-237 -9.210E-03 5.821E-02 5. 83.6E-02 NOT IDENT. NP-238 -l.449E+40 4.546E+40 O.OOOE+OO SHORT HLIF U-238 l.332E-01 1.433E+OO 1.434E+OO FAIL ABUN NP-239 -l.035E-01 2.482E-01 2.525E-01 NOT IDENT. PU-239 4.394E+02 6.782E+02 7.065E+02 FAIL ABUN AM-241 7.547E-02 1. 689E-01 1. 723E-01 NOT IDENT. CM-243 -8.887E-02 ' 1. 008E-01 l.084E-01 NOT IDENT. BK-247 -4.871E-03 8.006E-02 8.009E-02 NOT IDENT. 2.464E-02 3.562E-02 3.731E-02 NOT IDENT. CF-251 4.699E-02 1.218E-01 l.237E-01 NOT IDENT. Page 160of614
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT
  • ENERGY MDA .COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 79.6968 87.09 112.3475 136.47 71. 8643 45.60 69.9273 87.57 109.9099 140.51 0.0000 46.54 56.2287 88.03 133.6644 143.76 92.4722 49.72 0.0000 88.34 133.8013 14.4. 24 79.9997 51. 35 68.6747. 88.47 133.8584 145.44 95.1088 51. 87 71.4034 89. 96 85.7185 152.43 69.7998 52.39 71. 5876 1093.63 85.9076 153.25 0.0000 52.97 64.-9547 91.11 0.0000 323.87 77.0688 53.44 62.5339 92.59 86.4452 156.02 0.0000 54.07 72.1766 93.35 86.6528 158.56 0.0000 57.36 0.0000 94.56 86.9827 159.00 67.2239 57.53 77.7290 94.65 87.0072 162.33 81.9291 57.98 76.1386 94.67 87.0125 162.66 0.0000 59.27 80.1058 94.87 70.9928 163.33 61. 8674 59.32 '80.1238 97.43 68.8545 165.86 96.8562 59.54 73.1522 98.43 81.2512 176.31 64.6649 60.96 94.0140 98.44 81.2537 176.60 0 .. 0000 61.17 94.1006 99.53 82.5400 177.52 72.1493 62.93 76.9310 100 .11 83.7035 181.07 0.0000 63.29 75.2577 102.03 65.7021 181.52 80.4873 63.58 77.1449 103.18 80.3435 184.41 65.6386 64.28 99.8665 103.37 81. 4187 143.76 65.7939 66.73 83.6207 105.21 67.3466 193.51 78.8736 67.24 87.4380 105.31 67.3660 197.03 79.3546 125.81 93.0694 106.12 62.3282 198.01 72.7226 67.75 93.0959 106.47 74.8680 201.83 68.0876 69.67 95.6560 109.28 67. 0767 203.43 66.5631 70.83 104.4090 111. 00 86.3511 205.31 55.2151 72. 81 111. 7310 111.76 0.0000 210.85 66.5157 72. 87 111. 7566 114. 06 70.0822 215.65 66 .15*91 74.66 94.7029 116. 30 0.0000 222 .11 62.4363 74.82 94.7599 116.74 78.0699 227.09 67.3458 74.97 94. 8131 119.76 65.7521 . 227 .38 60.2830 77 .11 95.5675 121.12 64.9008 228.16 0.0000 78.74 96 .1354 121. 22 64.9173 228.18 61.2440 79.69 82.7741 121. 78 76.9288 116.74 61.2440 80.12 86. 7272 122.06 75.8992 235.69 84.8235 80.19 0.0000 122.92 63.0251 235. 96 78.1225 80.57 91.9761 123.07 68.4842 238.63 79.3302 81. 00 99.7923 265.00 71.8557 238.98 0.0000 81. 07 99.8169 125.81 70.0498 240.99 79.6023 81. 75 61.5728 127.23 65.9017 242.00 79.7187 83.79 99.4740 127.91 81.4154 244.70 66.8419 84.00 111.1804 129.30 81.6906 252.40 0.0000 85.43 111. 7228 131. 20 84.2847 252.80 62.5485 86.55 112 .1445 133.02 80.1958 254.15 0.0000 86. 79 112. 2337 133.52 94.7884 256.23 57.3004 86.94 112.2906 136.00 85.2460 260.90 0.0000 Page 161of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 53.2844 355.39 0.0000 584.27 26.3696 264.80 53.2937 356,01 43.6953 595.83 0.0000 265.00 61. 7246 364.49 0.0000 427.87 51. 4078 268.22 56.3538 366.42 0.0000 .602.52 0.0000 269.46 52.6834 372. 51 32.7956 604. 72 51. 9264 270.03 52.7222 375.05 39.2417 607.14 53.5391 271.23 52.8053 377.52 41.4637 609.32 35.4237 273.65 0.0000 356.01 45.9998 610.33 35.4463 276.40 61. 7045 388,,16 34.3750 614.28 26.1242 277.37 62.7317 388.63 0.0000 618.01 35.6213 277.60 57.0459 391.69 42.0358 620.36 27. 9610 278.00 52.3189 264.66 47.2843 621. 93 32.8140 279.20 73.3577 401.81 34.8210 630.19 0.0000 279.54 80.0625 402.40 34.8398 631. 29 33.9789 279.70 67.6849 404.85 40.9210 633.25 34.0205 280.46 62.9801 410.95 50.4781 634.78 0.0000 283.69 57.4878 413.71 36.3039 635.95 32.1299 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 60.4929 423. 72 0.0000 645.85 36.2446 285.90 0.0000 427.09 42.3078 657.76 26.8381 287.50 59.6879 427.87 37.8806 657.90 0.0000 290.67 78.2867 433.94 32.4822 661.66 15.8242 293.27 0.0000 439.40 38.2625 664.57 0.0000 351. 93 '61.2299 453.88 43.2927 666.33 0.0000 295. 96 61. 2850 463.37 35. 5965 666.50 0.0000 879.38 83.4352 468.07 35.7334 667.71 0.0000 299.98 61.5824 473.00 0.0000 677.62 23. 9612 300.09 45.4594 475.06 24.3441 685.70 0.0000 300.13 45.4622 476.78 45. 2723 695.00 0.0000 301.36 55.2227 477.60 42.9792 696.49 38.7598 302.85 75.5259 482.18 41. 9700 696. 51 38.7598 256.23 .57.9845 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 30.6987 306.78 47.3008 497.08 41. 5775 697.49 35.5502 308.46 52.3304 505.52 48.4359 702.65 30.3873 311. 90 53.5320 507.63 0.0000 706. 68 17.8680 316.51 54.8143 511. 00 42.9155 711. 68 28.5059 319.41 0.0000 514.00 25.8073 720. 70 0.0000 320.08 0.0000 514.00 25.8073 721. 93 0.0000 321. 04 64 .1133 520.40 23.4102 722.78 27.8632 323.87 57.8859 520.69 0.0000 722.91 36.0605 325.23 45.2921 522.65 0.0000 723.31 36.0690 328.76 0.0000 527.90 0.0000 724 .19 34.4459 333.37 46.7178 528.26 22.6402 727. 33 .27. 7276 333.97 44.2080 529.59 29.9143 733.00 29.6684 334.37 47.2776 529.87 0.0000 735.93 28.8904 338.28 57.1781 531.02 0.0000 333.97 36.1429 338.32 57.1815 537.26 0.0000 739.50 0.0000 311. 90 39.9156 546.56 0.0000 747.24 30.1054 340.48 39.9156 552.55 38.7034 748.06 31.1572 340.55 0.0000 563.25 33.4226 752.31 34.3515 344.28 59.6025 569.33 48.4802 753.82 0.0000 345.93 48.3836 946.00 46.6202 756.73 22.9547 351.06 48.6457 569.70 45.6938 756.80 22.9554 351.93 48.6906 583.19 26.3508 884.68 31. 8398 Page 162of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 23.4842 1274.44 32.6724 1620.50 13.0887 766.'42 33. 5596 1001.03 18.7065 1621. 92 1.0. 5018 766.84 35.2458 1002.74 22.4637 1678.03 0.0000 772.60 0.0000 1004.73 28.1030 1690.97 10.6916 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 6.9294 778.90 19.0003 1028.54 0.0000 1063.66 6.7974 783.70 0.0000 1037.84 27.5316 1771.35 8.4992 785.37 15.2508 1038.76 0.0000 1791.20 0.0000 792.07 34.0068 631.29 22.8645 1808.65 4.0020 794.95 23.4139 1048.07 0.0000 1810.72 0.0000 795.86 19.1662 1049.04 27.6548 1836.06 7.0493 810. 06 31.1001 1050.41 25.7607 810.29 32.1762 1063.66 20.7801 344.28 32.1780 1077.00 . 0.0000 810.76 27.8924 1077.34 19.2832 815.77 0.0000 1085.87 19.3467 1048.07 0.0000 1093.63 21. 344 7 832.01 30.3541 1099.45 27.5489 834.85 28.2249 1112. 07 27.1376 835.71 31. 4948 1112. 84 28.0958 836.80 0.0000 1115. 54 29.3467 846.75 0.0000 1120.29 23.5184 846.77 25 .1120 1120.55 23.5207 856.80 0.0000 1221.41 23.5277 860.56 21. 9800 1129. 67 22.9448 871.09 32.0294 1131. 51 0.0000 873.19 18.7943 1147.95 0.0000 875.33 0.0000 1173.23 19.9800 879.38 25.5009 1177.95 23.0157 880.51 19. 9677 1189.05 17.0780 883.24 34.4323 1204.77 25.2539 884.68 22.2290 1221. 41 22. 3513 889.28 26.7312 1231.02 37. 7136 894.76 29.0310 1235.36 0.0000 898.04 23.4834 1238.28 34.7421 900. 72 23.5122 1260.41 0.0000 903 .. 28 31.3855 1271.87 22.7337 911.20 14.6238 1274.44 23.7873 18.0059 1274.54 18.6170 923.98 0.0000 1291.59 16.6414 926.50 19.0277 1298.22 0.0000 929 .11 21. 7711 1312 .11 0.0000 937.49 27.3142 1332.49 15.8071 944.13 0.0000 1362.66 0.0000 946.00 26.5014 1365.19 13.8411 949.00 22.8760 1368.63 0.0000 667.71 0.0000 1384.29 8.9246 962.31 39.8792 1408.01 15.1013 '964.08 36.8389 1457.56 0.0000 966 .17 33.7994 1460.82 13.1479 911. 20 56.9122 1489.16 16.5696 968. 97 56.9122 1505.03 19.4192 983.53 0.0000 1584.12 14.1772 984.45 0.0000 1596. 21 0.0000 Page 163of614
  • VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:37:47.25 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245006.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM24.CNF;330 Background date : Z-OCT-2016 11:01:18. Sample date 15-DEC-2015 11:46:00 Acquisition date : 3-0CT-2016 04:34:54. Sample ID R405245006 Sample quantity 1.16680E+02 GRAM Detector name : GAM24 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:02.16 0.1% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 *Batch ID 1596387 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 0 0 0 0 0 0 0 0 4 4 4 4 0 0 0 0 0 0 0 0 0 4 4 0 0 0 4 4 0 0 Page 164of614 Energy 47.10* 63.30* 74.91* 77.18* 82.94* 87.27 93.61* 122.95 129.60 143.71* 186.05* 202.36 207.68 209.44 238.76* 241.92 270.53 277.39 295.51 308.36 338.70 351. 95* 410.00 420.95 463.68 510.80* 514.57 583.20* 609.53* 646.74 661.89 666.53 675.49 727.41* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 36 18 206 310 26 100 74 9 37 19 126 18 17 57 418 129 25 44. 153 29 87 308 26 18 33 0 15 170 190 12 74 23 6 33 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 140 164 183 149 234 175 278 168 170 72 120 61 26 61 67 99 68 69 61 44 84 70 48 28 55 61 22 45 54 8 14 11 17 27 1.10 0.76 1. 26 1.12 3.89 1.12 1. 46 1. 43 1. 45 1. 31 1. 47 0.68 0.83 1. 23 1. 06 1. 82 0.73 2.32 1. 32 0.67 1. 20 1.12 1. 55 1. 09 2.32 2.18 1. 65 1. 44 1. 64 1. 41 1. 75 2.33 1. 22 1.13 94.24 126.65 149.89 154.43 165.95 174.61 187.29 245.98 259.28 287.51 372. 21 404.83 415. 48. 419.00 477.65 483.98 541.22 554.95 591.20 616.90 677.60 704.10 820.25 842.14 927.63 1021.91 1029.45 1166.76 1219.44 1293.88 1324 .19 1333.48 1351.40 1455.28 90 124 145 145 161 172 181 241 254 285 367 401 414 414 471 471 538 551 585 611 673 697 815 837 920 1015 1015 1158 1213 1291 1315 1315 1346 1449 9 1.0lE-02 62.4 6 5.04E-03117.9 16 5.72E-02 13.8 16 8.60E-02 9.1 10 7.16E-03112.9 7 2.78E-02 24.1 11 2.04E-02 47.4 11 2.50E-03280.3 11 1. 02E-02 71. 0 6 5.19E-03 77.7 12 3.49E-02 20.2 6 5.04E-03 72.2 9 4.68E-03 45.5 9 1. 60E-0-2 26. 4 19 l.16E-01 5.8 19 3.59E-02 19.1 8 6.85E-03 61.9 10 1.21E-02 38.5 10 4.25E-02 12.5 11 8.02E-03 50.1 12 2.43E-02 23.8 14 8.55E-02 8.2 10 7.18E-03 54.5 8 4.99E-03 57.3 14 9.26E-03 52.7 18 1.99E-05***** lR 4.03E-03 59.5 15 4.73E-02 11.7 16 5. 27E-02 11. 3 6 3.43E-03 45.3 27 2.07E-02 15.1 27 6.44E-03 48.5 7 1. 54E-03135. 8 12 9.18E-03 36.8 Fit 1.32E+OO 5.12E+OO 8.56E-01 1. 13E+00 1. 7 4E+OO Peak Search Report (continued) Page : 2 Sample ID : R405245006 Acquisition date 3-0CT-2016 04:34:54 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Flt 35 0 769.41* 9 20 0.84 1539.32 1533 8 2.51E-03 94.4 36 0 795.22* 34 15 2.36 1590.97 1584 12 9.55E-03 29.0 37 0 870.33 10 23 3.41 1741.26 1732 13 2.81E-03102.3 38 0 911.40* 84 34 1. 77 1823.43 1817 14 2.33E-02 18.8 39 0 951. 00 6 15 1. 07 1902.66 1898 6 1. 53E-03119. 4 40 0 969.40* 52 28 1.11 1939.49 1934 12 1. 45E-02 25.7 41 0 1009.31 11 10 i 0. 78 2019.35 2013 10 3. llE-03 60.6 42 0 1113 .14 25 3 0.87 2227.11 2222 11 6. 96E-03 23.8 43 0 1120.52* 47 20 1. 89 2241.89 2236 13 1.29E-02 24.9 44 0 1160. 45 11 6 0.78 2321. 80 2316 9 2.98E-03 52.8 45 0 1282.67 12 3 1. 53 2566.37 2564 6 3. 31E-03 39.2 46 0 1298.87 10 5 1. 51 2598.79 2595 8 2.64E-03 53.7 47 0 1378.62 7 5 1.18 2758.39 2754 7 1. 91E-03 67.0 48 0 1399.55 9 6 3.94 2800.28 2792 12 2.50E-03 63.8 49 0 1460.79* 470 3 2.06 2922.83 2916 15 1.30E-01 4.7 50 0 1588.22 12 3 2.48 3177.87 3172 10 3.44E-03 37.2 51 0 1764.87* 32 9 0.76 3531.43 3524 12 8.95E-03 26.7 Flag: "*" = Peak area was modified by background subtraction Page 165 of 614 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 05:37:49 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245006.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID *15-DEC-2015 11:46:00 R405245006 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 04:34:54 116. 68 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA24 0 01:00:00.00 1. 50 keV No
  • Linear 75.00 Interference Report Interfering Page 166of614 Nuclide PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74'. 82 74.82 74.82 351. 93 geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 . SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:02.16 10.00 0.00 % Peak Energy 0.1%

Nuclide Line Activity Report Page : 2 Sample ID : R405245006 Acquisition date 3-0CT-2016 04:34:54 *Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM . pCi/GRAM %Error Status K-40 1460.82 10.66* 1.354E+OO l.978E+Ol 1.978E+Ol 9.47 OK C0-57 122.06 85.60* 7.935E+OO 9.019E-03 l.903E-02 560.56 OK 136.47 10.68 7.753E+OO Line Not Found Absent KR-85 514.00 0.43* 3.075E+OO 6.937E+OO 7.312E+OO 118. 95 OK SR-85 514.00 96. 00* 3.075E+OO 3.136E-02 7.168E-01 118. 95 OK CD-109 88.03 3.70* 7.497E+OO l.438E+OO 2.232E+OO 85.32 OK SN-126 64.28 9.60 5.531E+OO 2.387E-Ol 2.387E-01 235.82 OK 86.94 8.90 7.497E+OO 5.978E-01 5.978E-01 85.32 OK 87.57 37.00* 7.497E+OO 1.438E-01 1.438E-01 85.32 OK BA-137M 661. 66 89.90* 2.533E+OO 2.060E-01 2. 098E-Q1l 30.21 OK CS-137 661. 66 85.10* 2.533E+OO 2.176E-01 2.216E-01 30.21 OK TL-208 277.37 6.60 5.023E+OO 8.633E-01 8.633E-01 76. 95 OK 583.19 85.00* 2.791E+OO 4.SSOE-01 4.SSOE-01 23.40 OK 860.56 12. so* 2.074E+OO Line Not Found Absent PB-210 46.54 4.25* 2.569E+OO 2.354E+OO . 2.413E+OO 124.76 OK BI-211 72.87 1. 23 6.565E+OO Line Not Found Absent 351.06 12.92* 4.155E+OO 5.897E-01 5.897E-01 168.07 OK PB-212 74.82 10.28 6.738E+OO 1.423E+OO 1.423E+OO 41. 7"1 OK 77 .11 17.10 6.913E+OO 1.815E+OO 1.815E+OO 18.27 OK 238.63 43.60* 5'.636E+OO 1.123E+OO 1.123E+OO 11. 67 OK 300.09 3.30 4.720E+OO Line Not Found Absent BI-214 609.32 45.49* 2.698E+OO 9.790E-01 9.793E-01 22.66 OK 1120.29 14.92 1. 689E+OO 1.136E+OO 1.137E+OO 49.78 OK 1764.49 15.30 l.138E+OO 1.114E+00 1.115E+OO 53.30 OK PB-214 74.82 5.80 6.730E+OO Line Not Found <<INT Reject 77.11 9.70 6.913E+OO 3.200E+OO 3.202E+OO 18.27 OK 87.09 3.41 7.489E+OO Line Not Found <<INT Reject 242.00 7.25 5.579E+OO Line Not Found <<INT Reject 295. 22* 18.42 4.778E+OO 1.137E+OO 1.137E+OO 24.94 OK 351. 93 35.60* 4.155E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.698E+OO 9.790E-01 9.793E-01 22.66 OK 1120.29 14.92 1.689E+OO 1.136E+OO l .137E+OO 49.78 OK 1764.49 15.30 1.138E+OO 1.114E+OO 1.115E+OO 53.30 OK RA-224 240.99 4.10* 5.581E+OO 1.717E+OO 1.717E+OO 88.00 OK RA-226 609.32 45.49* 2.698E+OO 9.790E-01 9.793E-01 22.66 OK 1120.29 14.92 1.689E+OO 1.136E+OO 1.137E+OO 49.78 OK 1764.49 15.30 1.138E+OO 1.114E+OO 1. llSE+OO 53.30 OK AC-228 105.21 1.10 7.950E+OO Line Not Found Absent 338.32 11. 27 4.285E+OO 1.177E+OO l.177E+OO 47.56 OK 794.95 4.25 2.203E+OO 2.297E+OO 2.297E+OO 57.96 OK 835. 71 1. 61 2 .121E+OO Line Not Found Absent 911. 20 25.80* 1.985E+OO 1.016E+OO 1.016E+OO 37.62 OK 968. 97 15.80 1.892E+OO 1.085E+OO 1.085E+OO 51. 41 OK RA-228 105.21 1.10 7.950E+OO Line Not Found Absent 338.32 11. 27 4. 285E+OO, 1.177E+OO 1.177E+OO 47.56 OK 794.95 4.25 2. 203E+O.O 2.297E+OO 2.297E+OO 57.96 OK 835.71 1. 61 2 .121E+OO Line Not Found Absent 911. 20 25.80* 1.985E+OO 1.016E+OO 1.016E+OO 37.62 OK 968. 97 15.80 1.892E+OO 1.085E+OO 1.085E+OO 51. 41 OK Page 167of614 Nuclide Line Activity Report (continued) Page : 3 Sample ID : R405245006 Acquisition date 3-0CT-2016 04:34:54 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-228 74.82 10.28 6.738E+OO 1. 423E+OO l.423E+OO 41.71 OK 77 .11 17.10 6.913E+OO 1.815E+OO l.815E+00 18.27 OK 238.63 43.60* 5.636E+OO 1.123E+OO 1.123E+OO 11. 67 OK 300.09 3.30 4. 720E+OO Line Not Found Absent TH-230 609.32 45.49* 2.698E+OO 9.790E-01 9.790E-01 22.66 OK 1120.29 14.92 1.689E+OO 1.136E+OO 1.136E+OO 49.78 OK 1764.49 15.30 1.138E+OO 1.114E+OO 53.30 OK TH-232 105.21 1.10 7.950E+OO Line Not Found Absent 338.32 11. 27 4.285E+OO 1. l 77E+OO l.177E+OO 47.56 OK 835.71 1. 61 2.121E+OO Line Not Found Absent 911.20 25.80* l.985E+OO l.016E+OO l.016E+OO 37.62 OK 968. 97 15.80 1.892E+OO l.085E+OO l.085E+OO 51. 41 OK TH-234 63.29 3.70* 5. 531E+OO 6.194E-01 6.194E-01 235.82 OK 92.59 4.23 7.730E+OO l.546E+OO l.546E+OO 94. 71 OK U-234 609.32 45.49* 2.698E+OO 9.790E-01 9.790E-01 22.66 OK 1120. 29 14.92 1.689E+OO l.136E+OO l.136E+00 49.78 OK 1764.49 15.30 1.138E+OO l .114E+OO l .114E+OO 53.30 OK U-235 89. 96 3.47 7.607E+OO Line Not Found Absent 93.35 5.60 7.730E+OO 1.168E+OO 1.168E+OO 94. 71 OK 143.76 *10. 96* 7.621E+OO l.509E-01 l.509E-01 155.48 OK 163.33 5.08 7.206E+OO Line Not Found Absent 185. 72 57.20 6.695E+OO 2.192E-01 2.192E-01 40.31 OK 205.31 5.01 6.280E+OO Line Not Found Absent U-238 63.29 3.70* 5. 531E+OO 6.194E-01 6.194E-01 235.82 OK 92.59 4.23 7.730E+OO l.546E+00 1.546E+OO 94.71 OK AM-243 43.53 5.90 1.694E+OO Line Not Found Absent 74:66 67.20* 6.738E+OO 2.177E-01 2.177E-01 41.71 OK ANH-511 511. 00 100.00* 3.093E+OO 1.475E-04 1.475E-04******* OK Flag: "*" = Keyline Page 168 of 614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:37:50.20 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245006.CNF;l * *Acquisition date 3-0CT-2016 04:34:54 Sensitivity. : 3.000 *
  • Detector ID GAM24 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:02.16 Half life ratio : ***** *
  • Sample date 15-DEC-2015 11:46:00 Analyst initials: MXRl *
  • Sample ID R405245006 Sample Quantity 1.1668E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0:00000 *
  • Nuclide Library : SOLID.NLB;6 . * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 17-JUN-2016 07:45:20 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;? .
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1. 96-sigma) K-40 1.978E+Ol 1.835E+OO C0-57 1.903E-02 1.045E-01 KR-85 7.312E+OO 8.523E+OO SR-85 7.168E-01 8.356E-01 CD-109 2.232E+OO 1.866E+OO SN-126 1.438E-01 1.202E-01 BA-137M 2.098E-01 6.212E-02 CS-137 2.216E-01 6.56-2E-02 TL-208 4.550E-01 1.043E-01 PB-210 2.413E+OO 2. 951E+OO BI-211 5.897E-01 9.713E-01 PB-212 1.123E+OO l.285E-01 BI-214 9.793E-01 2.175E-01 PB-214 1.352E+OO 2.169E-01 RN-222 9.793E-01 2.175E-01 RA-224 1.717E+OO 1. 481E+OO RA-226 9.793E-01 2.175E-01 AC-228 1.016E+OO 3.746E-01 RA-228 1.016E+OO 3.746E-01. TH-228 1.123E+OO 1.285E-01 TH-230 9.790E-01 2 .. 174E-01 TH-232 1.016E+OO 3.746E-01 TH-234 6.194E-01 1.432E+OO U-234 9.790E-01 2.174E-01 U-235 l.509E-01 2.300E-01 U-238 6.194E-01 1. 432E+OO AM-243 2.177E-01 8.898E-02 ANH-511 1. 475E-04 7. 713E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 Page 169 of 614 Key-Line Activity (pCi/GRAM 8.377E+OO 2.076E-02 -K.L. Cnt Uncert (1.96-sigma) l.166E+Ol 4.237E-02 MDA (pCi/GRAM 6. 251E-01 8.760E-02 1.479E+Ol l.450E+00 2:165E+OO 1.398E-01 6. 651E-02 7.026E-02 5.545E-02 2.730E+OO 3.545E-01 9. 911E-02 l.340E-01 3.809E-01 l.340E-01 1.063E+OO l.340E-01 2.692E-01 2.692E-01 9. 911E-02 1.339E-01 2.692E-01 1. 756E+OO 1.339E-01 3.270E-01 1.756E+OO 7.563E-02 6.060E-02 MDA (pCi/GRAM 2.405E+Ol 9.351E-02 NOT IDENT. NOT IDENT.

NA-24 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF AL-26 -1. 271E-02 2.384E-02 4.247E-02 NOT IDENT. SC-46 -8.079E-03 3*. 899E-01 7.408E-01 FAIL ABUN V-48 O.OOOE+OO 1.306E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3. 801E+02 O.OOOE+OO SHORT HLIF MN-54 -4.346E-02 7.237E-02 l.208E-01 NOT IDENT, C0-56 -3.249E-02 4.410E-01 8.225E-01 NOT IDENT. MN-56 0.000E+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-58 4.157E-02 5.748E-01 1.095E+OO NOT IDENT. FE-59 -9.791E+OO 7.740E+OO l.230E+Ol NOT IDENT. C0-60 -l.823E-02 4.942E-02 9.075E-02 NOT IDENT. ZN-65 5.287E-02 2.492E-01 3.470E-01 NOT IDENT. GE-68 1. 716E+OO 2.660E+OO 5. 672E+OO NOT IDENT. AS-73 -1.585E+OO 5.279E+OO 9.372E+OO . NOT IDENT. AS-74 O.OOOE+OO 5.185E+03 O.OOOE+OO SHORT HLIF SE-75 -1. 620E-01 2.032E-01 3.629E-01 NOT IDENT. BR-77 O.OOOE+OO 2.891E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7. 531E+02 O.OOOE+OO SHORT HLIF RB-83 2.444E-01 6.175E-01 1.241E+OO NOT IDENT. RB-86 O.OOOE+OO 2.602E+04 O.OOOE+OO SHORT HLIF Y-88 1.300E-01 3.165E-01 6.783E-01 NOT IDENT. Y-91 9.783E+Ol 5.441E+02 1.088E+03 NOT IDENT. NB-94 -1. 2 65E-02 3.475E-02 6.132E-02 FAIL ABUN NB-95 -7. 441E-01 1.055E+OO 1. 486E+OO NOT IDENT. NB-95M 9.138E-01 2.449E+OO 4.381E+OO NOT IDENT. ZR-95 4.605E-01 1.349E+OO 2.694E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 3.012E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 5.084E-03 4.348E-02 6.338E-02 NOT IDENT. RH-102 3.200E-02 6.658E-02 l.327E-01 FAIL ABUN RU-103 8.407E+OO 5.378E+OO 1. 200E+Ol FAIL ABUN RH-106 3.012E-01 5.429E-01. 1. 096E+00 NOT IDENT. RU-106 3.012E-01 5.429E-01 1. 096E+OO NOT IDENT. AG-108M -4.400E-03 3.287E-02 6.099E-02 NOT IDENT. AG-110M 8.467E-02 1.188E-01 2.430E-01 NOT IDENT. SN-113 -6.167E-02 2.509E-01 4.625E-01 NOT IDENT. CD-115 O.OOOE+OO 3.213E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 7.282E+04 O.OOOE+OO SHORT HLIF TE-123M 6.423E-02 l.405E-01 2.563E-01 NOT IDENT. SB-124 3.634E-01 1.504E+OO 3.632E+OO FAIL ABUN. SB-125 2.281E-02 9.007E-02 1.805E-01 FAIL ABUN TE-125M -l.043E+02 2.748E+02 4.746E+02 NOT IDENT. I-126 O.OOOE+OO 1.094E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 8.706E+05 0.000E+OO SHORT HLIF SB-127 O.OOOE+OO 7.065E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.789E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO *9.501E+40 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 9.289E+25 O.OOOE+OO SHORT HLIF BA-133 l.240E-02 4.128E-02 7.483E-02 FAIL ABUN I-133 O.OOOE+OO 8.163E+40 0.000E+OO SHORT HLIF CS-134 O.OOOE+OO 8.484E-02 1. 426E-01 FAIL ABUN CS-135 l.313E-01 1.545E-01 2. 921E-01 NOT IDENT. I-135 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.087E+05 O.OOOE+OO SHORT HLIF CE-139 l.570E-02 1.17 5E-01 2.086E-01 NOT IDENT. BA-140 O.OOOE+OO 9.213E+05 O.OOOE+OO SHORT HLIF LA-140 *o. OOOE+OO 3.024E+05 O.OOOE+OO SHORT HLIF CE-141 -l.345E+Ol 2.607E+Ol 4.002E+Ol NOT IDENT. CE-143 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CE-144 6.808E-02 3.711E-01 6.218E-01 NOT IDENT. PM-144 2.687E-02 6.863E-02 1.323E-01 NOT IDENT. PR-144 2.293E+00 5.935E+OO l.143E+Ol NOT IDENT. PM-146 -l.302E-02 4. 337E-02. 7.975E-02 NOT IDENT. ND-147 O.OOOE+OO 1. 8 64E+07 O.OOOE+OO SHORT HLIF PM-147 3.476E+Ol* 8.390E+02 l.394E+03 NOT IDENT. PM-149 O.OOOE+OO 5.288E+39 O.OOOE+OO SHORT HLIF EU-150 2.370E-02 2.936E-02 5.519E-02 FAIL ABUN EU-152 -6.812E-02 l .114E-01 1. 749E-01 FAIL ABUN GD-153 -9.474E-02 l.856E-01 2.924E-01 NOT IDENT. EU-154 5.883E-02 l.061E-01 2.355E-01 FAIL ABUN EU-155 -6.420E-03 l.158E-01 2.056E-01 FAIL ABUN TB_.:160* -3.894E-01 l.923E+OO 3.466E+OO FAIL ABUN H0-166M -l.446E-02 6.050E-02 l.095E-01 FAIL ABUN TM-171 9.517E+00 l.196E+Ol 2.332E+Ol NOT IDENT. HF-172 -l.215E-01 3.086E-01 4 .196E-01 FAIL ABUN LU-172 5. 472E-02 9.675E-02 2.006E-01 FAIL ABUN Page 170 of614 LU-176 4.886E-03 2.367E-02 4.643E-02 FAIL ABUN HF-181 l.335E+OO 3.898E+OO 7.756E+OO NOT IDENT. TA-182 6.620E-01 1. 031E+OO 2.162E+OO FAIL ABUN. RE-183 7.508E-02 1. 926E+00 3*. 531E+OO NOT IDENT. RE-184 2.128E+Ol 2. 931E+Ol 6.092E+Ol NOT IDENT. W-188 -1. 753E+Ol 1.204E+02 2.035E+02 FAIL ABUN IR-192 1.009E-01 4.482E-01 8.749E-01 FAIL ABUN HG-203 1.120E+OO 2.498E+OO 4.514E+OO NOT IDENT. BI-207 1.782E-02 5.140E-02 1.069E-01 FAIL ABUN PB-211 -3.460E-01 9.169E-01 1.467E+OO NOT IDENT. BI-212 1.319E+OO 9.515E-01 l.464E+OO FAIL ABUN RN-219. 2.150E-02 4.642E-01 8.744E-01 FAIL ABUN RA-223 1. 462E-01 5.805E-01 1.140E+OO FAIL ABUN AC-227 l.049E-01 2.419E-01 4.786E-01 NOT IDENT. TH-227 1.049E-01 2.419E-01 4.786E-01 NOT IDENT. TH-229 2.137E-01 5.566E-01 9.976E-01 FAIL ABUN PA-231 1.270E-01 4.947E-01 9.567E-01 NOT IDENT. TH-231 1.462E-01 5.805E-01 1.140E+OO FAIL ABUN PA-233 2.060E-02 6.012E-02 1. 096E-01 NOT IDENT. PA-234 -5.351E-02 3.945E-01 6.393E-01 FAIL ABUN PA-234M 1.471E+OO 4.979E+00 1. OllE+Ol NOT IDENT. NP-237 2.060E-02 6.012E-02 1. 096E-01 FAIL ABUN NP-238 O.OOOE+OO 5.423E+40 O.OOOE+OO SHORT HLIF NP-239 -5.837E-02 2.387E-01 4.182E-01 FAIL ABUN PU-239 5.036E+02 7.007E+02 6. 781E+02 FAIL ABUN AM-241 -2.704E-02 9.973E-02 l.786E-01 NOT IDENT. CM-243 -8.335E-02 l.017E-01 1. 701E-01 FAIL ABUN BK-247 -4.380E-02 7.150E-02 1. 301E-01 FAIL ABUN CM-247 -2.627E-02 4.190E-02 7.388E-02 FAIL ABUN CF-249 1.815E-02 4.056E-02 8.038E-02 NOT IDENT. CF-251 -2.968E-02 l.219E-01 2.090E-01 NOT IDENT. Page 171 of 614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:37:47.96 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 444 10.66* 1.354E+OO 1.978E+Ol 1. 978E+Ol 9.47 C0-57 122.06 10 85.60* 7.935E+OO 9.019E-03 l.903E-02 560.56 136.47 ------10.68 7.753E+OO ------Line Not Found ------KR-85 514.00 14 0.43* 3.075E+OO 6.937E+OO 7.312E+OO 118. 95 SR-85 514.00 14 96.00* 3.075E+OO 3 .136E-02 7.168E-01 118. 95 CD-109 88.03 107 3.70* 7.497E+OO 2.486E+OO 3.859E+OO 48.22 SN-126 64.28 20 9.60 5.531E+OO 2.387E-01 2.387E-01 235.82 86.94 107 8.90 7.497E+OO 1.033E+OO l.033E+00 48.22 87.57 107 37. 00'* 7.497E+OO 2.486E-01 2.486E-01 48.22 BA-137M 661.66 73 89.90* 2.533E+OO 2.060E-01 2.098E-01 30. 2*1 CS-137 661.66 73 85.10* 2.533E+OO 2.176E-01 2.216E-01 30.21 TL-208 277.37 44 6.60 5.023E+00 8.633E-01 8.633E-01 76.95 583.19 168 85.00* 2.791E+OO 4.550E-01 4.550E-01 23.40 860.56 ------12.50 2.074E+OO ------Line Not Found ------PB-210 46.54 40 4.25* 2.569E+OO 2.354E+OO 2.413E+OO 124.76" BI-211 72. 87 ------1. 23 6.565E+OO ------Line 'Not Found ------351.06 311 12.92* 4.155E+00 3. 723E+OO 3. 723E+OO 16.38 PB-212 74.82 222 10.28 6.738E+OO 2.064E+OO 2.064E+OO 27.68 77 .11 334 17.10 6.913E+OO 1.815E+OO 1.815E+OO 18.27 238.63 ' 429 43.60* 5.636E+OO l.123E+OO 1.123E+OO 11. 67 300.09 ------3.30 4.720E+OO ------Line Not Found ------BI-214 609.32 187 45.49* 2.698E+00 9.790E-01 9.793E-01 22.66 1120.29 44 14.92 1. 689E+OO l.136E+OO 1.137E+OO 49.78 1764.49 30 15.30 l .138E+OO 1.114E+OO l .115E+OO 53.30 PB-214 74.82 222 5.80 6.738E+OO 3.659E+OO 3.660E+OO 27.68 77 .11 334 9.70 6.913E+OO 3.200E+OO 3.202E+OO 18.27 87.09 107 3.41 7.497E+OO 2.697E+OO 2.698E+OO 48.22 242.00 133 7.25 5.581E+OO 2.108E+OO 2.109E+OO 38.24 295.22 156 18.42 4.778E+OO 1.137E+OO l.137E+00 24.94 351.93 311 35.60* 4.155E+OO 1.351E+OO 1.352E+OO 16.38 RN-222 609.32 187 45.49* 2.698E+OO 9.790E-01 9.793E-01 22.66 1120.29 44 14.92 1. 689E+OO 1.136E+OO 1.137E+OO 49.78 1764.49 30 15.30 l.138E+OO 1.114E+OO 1.115E+o*o 53.30 RA-224 240.99 133 4.10* 5.581E+OO 3.728E+OO 3.728E+OO 38.24 RA-226 609.32 187 45.49* 2.698E+00 9.790E-01 9.793E-01 22.66 1120.29 44 14.92 1.689E+OO 1.136E+OO 1.137E+OO 49.78 1764.49 30 15.30 1.138E+OO l .114E+OO 1.115E+00 53.30 AC-228 105.21 ------1.10 7.950E+OO ------Line Not Found ------338.32 88 11. 27 4.285E+OO l.177E+OO 1.177E+OO 47.56 794.95 33 4.25 2.203E+OO 2.297E+OO 2.297E+OO 57. 96 835.71 ------1. 61 2.121E+OO ------Line Not Found ------911.20 81 25.80* 1.985E+OO 1.016E+OO 1.016E+OO 37.62 968. 97 50 15.80 1. 892E+OO 1.085E+OO 1.085E+OO 51. 41 RA-228 105.21 ------1.10 7.950E+OO ------Line Not Found ------338.32 88 11. 27 4.285E+OO l.177E+OO 1.177E+OO 47.56 794.95 33 4.25 2.203E+OO 2.297E+OO 2.297E+OO 57. 96 835.71 ------1. 61 2.121E+00 ------Line Not Found ------Page 172 of 614 Nuclide Line Activity Report (continued) Page : 2 Sample ID : R405245006 Acquisition date 3-0CT-2016 04:34:54 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 911.20 81 25.80* 1.985E+OO 1.016E+OO 1.016E+OO 37 .. 62 968. 97 50 15.80 1.892E+OO 1.085E+OO 1.085E+OO 51. 41 TH-228 74.82 222 10.28 6.738E+OO 2.064E+OO 2.064E+OO 27.68 77 .11 334 17.10 6.913E+OO 1.815E+OO 1.815E+OO 18.27 238.63 429 43.60* 5.636E+OO 1.123E+OO 1.123E+OO 11. 67 300.09 ------3.30 4.720E+OO ------Line Not Found ------TH-230 609.32 18'7 45.49* 2.698E+OO 9.790E-01 9.790E-01 22.66 1120.29 44 14.92 1.689E+OO 1.136E+OO 1.136E+OO 49.78 1764.49 30 15.30 1.138E+OO 1.114E+OO 1.114E+OO 53.30 TH-232 105.21 ------1.10 7.950E+OO ------Line Not Found ------338.32 88 11. 27 4.285E+OO 1.177E+OO 1.177E+00 47.56 835.71 ------1. 61 2.121E+OO ------Line Not Found ------911.20 81 25.80* 1.985E+00 1.016E+OO l.016E+00 37.62 968. 97 50 15. 80 1. 892E+OO 1.085E+OO 1.085E+OO 51. 41 TH-234 63.29 20 3.70* 5.531E+OO 6.194E-01 6.194E-01 . 235. 82 92.59 79 4.23 7.730E+OO 1.546E+OO 1.546E+OO 94. 71 U-234 609.32 187 45.49* 2.698E+OO 9 .*7 90E-01 9.790E-01 22.66 1120.29 44 14.92 1.689E+OO 1.136E+OO l.136E+OO 49.78 1764.49 30 15.30 1.138E+OO 1.114E+OO 1.114E+OO 53.30 U-235 89.96 ------3.47 7.607E+OO ------Line Not Found ------93.35 79 5.60 7.730E+OO 1.168E+OO 1.168E+OO 94.71 143.76 20 10.96* 7. 621E+OO l.509E-01 1.509E-01 155.48 163.33 ------5.08 7.206E+00 ------Line Not Found ------185.72 130 57.20 6.695E+OO 2.192E-01 2.192E-01 40.31 205.31 ------5.01 6.280E+00 ------Line Not Found ------U-238 63.29 20 3.70* 5.531E+OO 6.194E-01 6.194E-01 235.82 92.59 79 4.23 7.730E+OO l.546E+00 1.546E+OO 94.71 AM-243 43.53 ------5.90 1.694E+OO ------Line Not Found ------74.66 222 67.20* 6.738E+OO 3.158E-01 3.158E-01 27.68 ANH-511 511. 00 0 100.00* 3.093E+OO 1.475E-04 l.475E-04 53366.13 Flag: "*" Key line Page 173 of614 Summary of Nuclide Activity Sample ID : R405245006 Acquisition date Page : 3 3-0CT-2016 04:34:54 Total number of lines in spectrum 51 Number of unidentified lines 11 Number of lines tentatively identified by NID 40 Nuclide Type : Nuclide K-40 C0-57 KR-85 SR-85 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlif e 1.25E+09Y 271. 74D 10.56Y 64.84D 461. 40D 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 22.20Y 7.04E+08Y l.41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1.41E+10Y 1600. OOY 1. 41E+10Y. l.41E+l0Y l.41E+10Y 7.54E+04Y 1.41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 2.11 1. 05 22.9 1. 55 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 . 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.978E+Ol 9.019E-03. 6.937E+OO 3.136E-02 2.486E+OO 2.486E-01 2.060E-01 2.176E-01 4.550E-01 2.354E+OO 3.723E+OO l.123E+OO 9.790E-01 1.351E+OO 9.790E-01 3.728E+OO 9.790E-01 1.016E+OO 1.016E+OO 1.123E+OO 9.790E-01 1.016E+OO 6.194E-01 9.790E-01 l.509E-01 6.194E-01 3.158E-01 1.475E-04 5.342E+Ol 5.342E+Ol Decay Corr pCi/GRAM 1.978E+Ol 1. 903E-02 7.312E+OO 7.168E-01 3.859E+OO 2.486E-01 2.098E-01 2.216E-01 4.550E-01 2.413E+OO 3. 723E+OO 1.123E+OO 9.793E-01 1.352E+OO 9.793E-01 3.728E+OO* 9.793E-01 l.016E+00 1.016E+OO 1.123E+OO 9.790E-01 1.016E+OO 6.194E-01 9.790E-01 1.509E-01 6.194E-01 3.158E-01 1.475E-04 5.593E+Ol 5.593E+Ol 78.43% Decay Corr 2-Sigma Error 0.187E+Ol 10.67E-02 8.697E+OO 8.526E-01 1. 8 61E+O'O 1.199E-01 0.634E-01 0.670E-01 1. 065E-01 3. OllE+OO 0.610E+OO 2-Sigma %Error 9.47 560.56 118. 95 118. 95 48.22 48.22 30.21 30.21 23.40 124.76 16.38 11. 67 22.66 16.38 22.66 38.24 22.66 37.62 37.62 11. 67 22.66 37.62 0 .131E+OO 2.219E-01 0.221E+OO 2.219E-01 1.425E+OO 2.219E-01 0.382E+OO 0.382E+OO 0.131E+OO 2.219E-01 0.382E+OO 14.61E-01 2.219E-01 2.347E-01 14.61E-01 0.874E-01 787.0E-04 235.82 22.66 155.48 235.82 27.68 53366.13 "K" Keyline not found "E" = Manually edited "M" -Manually accepted "A" = Nuclide specific abn. limit Page 174 of614 Flags Unidentified Energy Lines Page : 4 Sample ID : R405245006 AC".quisition date : 3-0CT-2016 04:34:54 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 82.94 28 251 3.89 165.95 161 10 7.16E-03 **** 7.28E+OO T 0 129.60 39 179 1. 45 259.28 254 11 1.02E-02 **** 7.86E+OO T 0 202.36 19 63 0.68 404.83 401 6 5.04E-03 **** 6.34E+OO T 4 207.68 17 27 0.83 415.48 414 9 4.68E-03 91. 0 6.23E+PO 4 209.44 59 63 1.23 419.00 414 9 1. 60E.:...02 52.8 6.19E+OO T 0 270.53 25 70 0.73 541.22 538 8 6.85E-03 **** 5.12E+OO T 0 308.36 Z9 45 0.67 616.90 611 11 8.02E-03 **** 4.62E+OO T 0 410.00 26 48 1. 55 820.25 815 10 7.18E-03 **** 3.68E+OO T 0 420.95 18 28 1. 09 842.14 837 8 4.99E-03 **** 3.60E+OO 0 463.68 33 54 2.32 927.63 920 14 9.26E-03 **** 3.34E+OO T 0 646.74 *12 8 1. 41 1293.88 1291 6 3.43E-03 90.5 2.58E+OO T 4 666.53 23 11 2.33 1333.48 1315 27 6.44E-03 97.0 2.52E+OO T 0 675.49 5 17 1. 22 1351.40 1346 7 1.54E-03 **** 2.49E+00 0 727.41 32 26 1.13 1455.28 1449* 1-2 9.18E-03 73.6* 2.36E+OO T 0 769.41 9 20 0.84 1539.32 1533 8 2.51E-03 **** 2.26E+OO 0 870.33 10 22 3.41 1741.26 1732 13 2.81E-03 **** 2.06E+OO T 0 951.00 5 15 1. 07 1902.66 1898 6 1. 53E-03 **** 1. 92E+OO 0 1009.31 11 9 0.78 2019.35 2013 10 3 **** 1. 83E+OO 0 1113 .14 24 3 0.87 2227 .11 2222 11 6.96E-03 47.6 1.70E+OO T 0 1160. 45 10 6 0.78 2321. 80 2316 9 2.98E-03 **** 1.64E+OO 0 1282.67 11 3. 1. 53 2566.37 2564 6 3.31E-03 78.4 1.51E+OO 0 1298.87 9 *4 1. 51 2598.79 2595 8 2.64E-03 **** 1. 50E+OO T 0 1378.62 7 5 1.18 2758.39 2754 7 l.91E-03 **** 1.42E+OO 0 1399.55 9 6 3.94 2800.28 2792 12 2.50E-03 *"*** 1. 40E+OO 0 1588.22 12 2 2.48 3177.87 3172 10 3.44E-03 74.4 1.26E+OO Flags: "T" = Tentatively associated Page 175 of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:38:02.55 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245006.CNF;l *
  • Acquisition date 3-0CT-2016 04:34:54 Sensitivity 3.000 *
  • Detector ID GAM24 Energy tolerance: 1.500. *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *
  • Elapsed real time: 0 01:00:02.16 Half life ratio : ***** *
  • Sample date 15-DEC-2015 11:46:00 Nuclide Library : SOLID *
  • Sample ID R405245006 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.1668E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 07:45:20 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;7
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 C0-57 KR-85 SR-85 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.525E-01 4.106E-02 6.707E+OO 6.575E-01 . 1.033E+OO 6.671E-02 2.935E-02 3.lOlE-02 2.404E-02 1.277E+OO l.609E-01 4.598E-02 5.988E-02 1.846E-01 5*. 988E-02 4.930E-01 5.988E-02 1.176E-01 1.176E-01 4.598E-02 5.986E-02 1.176E-01 8.348E-01 5.986E-02 1. 529E-Oi 8.348E-01 3.585E-02 2.747E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 176 of 614 Le (pCi/GRAM 1.086E+Ol 3.969E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 . SR-82 RB-83 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 cs...:134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page177of614 1.342E-02 3.220E-01 O.OOOE+OO O.OOOE+OO 5.253E-02 3.538E-01 O.OOOE+OO 4.768E-01 5.296E+OO 3.880E-02 1.503E-01 2.509E+OO 4.413E+OO O.OOOE+OO l.659E-01 O.OOOE+OO O.OOOE+OO 5.534E-01 O.OOOE+OO 2.858E-01 4.768E+02 2.705E-02 6.516E-01 2.043E+OO l.180E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.974E-02 5.949E-02 5.465E+00 4.909E-01 4.909E-01 2.774E-02 1.082E-01 2.107E-01 O.OOOE+OO O.OOOE+OO 1.202E-01 1.369E+OO 8.016E-02 2.232E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.380E-02 O.OOOE+OO 6.526E-02 1.354E-01 O.OOOE+OO O.OOOE+OO 9.756E-02 O.OOOE+OO O.OOOE+OO 1.877E+Ol O.OOOE+OO 2.901E-01 5.985E-02 5. l 72E+OO 3.549E-02 O.OOOE+OO 6.489E+02 O.OOOE+OO 2.546E-02 7.931E-02 1. 371E-01 l.004E-01 9.687E-02 1.499E+OO 4.801E-'02 1.099E+Ol 1. 965E-01 8.955E-02 2 .119E-02 NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. .SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. S.HORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 178 of 614 3.475E+OO . 9.610E-01 1.667E+OO 2.694E+Ol 9.350E+Ol 4.009E-01 2.089E+OO 4. 671E-02 6.713E-01 6.769E-Ol 4.018E-01 5.204E-01 2.220E-01 2.220E-Ol 4.683E-01 4.435E-01 5.204E-01 4.981E-02 2.821E-01 4 .. 497E+OO 4.981E-02 O.OOOE+OO 1. 951E-01 3.213E+02 8.434E-02 7.963E-02 5. 941E-02. 3.369E-02 3.673E-02 9.710E-02 NOT IDENT . FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN .NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:38:08.21 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245006.CNF;l * *Acquisition date 3-0CT-2016 04:34:54 Sensitivity : 3.000 *
  • Detector ID GAM2.4 Energy tolerance: 1. 500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:02.16 Half life ratio : ***** *
  • Sample date 15-DEC-2015 11:46:00 Nuclide Library : SOLID *
  • Sample ID R405245006 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity 1.1668E+02 GRAM *
  • Quantity Err ( % ) 1. 714 lE-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 07':45:20 Eff. Geometry : CAN *
  • Eff, File : DKAlOO: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1 . 96-sigma ) K-40 1.978E+Ol 2.104E+OO C0-57 l.903E-02 l.045E-01 KR-85 7.312E+OO 8.529E+OO SR-85 7.168E-01 8.361E-01 CD-109 2.232E+OO 1. 886E+OO SN-126 1.438E-01 1.213E-Ol BA-1'37M 2.098E-01 6.277E-02 CS--:137 2.216E-01 6.631E-02 TL-208 4.550E-01 1.061E-01 PB-210 2. 413E+OO 2.957E+OO BI-211 5.897E-01 9. 901E-01 PB-212 1.123E+OO l.415E-01 BI-214 9.793E-01 2.2l5E-01 PB-214 1. 352E+OO 2.240E-01 RN-222 9.793E-01 2.215E-01 RA-224 1.717E+OO 1.489E+OO RA-226 9.793E-01 2.215E-01 AC-228 1.016E+OO 3.782E-01 RA-228 1.016E+OO 3.782E-01 TH-228 1.123E+OO l.415E-01 TH-230 9.790E-01 2.214E-01 TH-232 1.016E+OO 3.782E-01 TH-234 6.194E-01 l.438E+OO U-234* 9.790E-01 2.214E-01 U-235 l.509E-01 2*. 301E-01 U-238 6.194E-01 1.438E+OO AM-243 2.177E-01 9.083E-02 ANH-511 l.475E-04 7.713E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 Page 179 of614 Key-Line Activity (pCi/GRAM 8.377E+OO 2.076E-02 K.L Act error (1. 96-sigma) l.166E+Ol 4.238E-02 TPU ( 1. 96-sigma) 2.104E+OO l.045E-01 8.529E+OO 8. 361E-01 l.886E+OO 1.213E-01 6.277E-02 6. 631E-02 . 1.061E-01 2.957E+OO 9. 901E-01 1.415E-01 2.215E-01 2.240E-01 2.215E-01 1.489E+OO 2.215E-01 3.782E-01 3.782E-01 l.415E-01 2.214E-01 3.782E-01 1.438E+00 2.214E-01 2.301E-01 l.438E+OO 9.083E-02 7.713E-02 TPU ( 1. 96-sigma) 1.226E+Ol NOT IDENT. 4.340E-02 NOT IDENT.

NA-24 -1.000E+41 1.284E+43 O.OOOE+OO SHORT HLIF AL-26 -1.271E-02 2.385E-02 2.453E-02 NOT IDENT. SC-46 -8.079E-03 3.899E-01 3.899E-01 FAIL ABUN V-48 -4.229E+03 1.306E+04 1.320E+04 SHORT HLIF CR-51 9.950E+OO 3.801E+02 3.802E+02 SHORT HLIF MN-54 -4.346E-02 7.239E-02 7.499E-02 NOT IDENT. C0-56 -3.249E-02 4.410E-01 4.412E-01 NOT IDENT. MN-56 -1.000E+41 3.525E+41 O.OOOE+OO SHORT HLIF C0-58 4.157E-02 5.748E-01 5.752E-01 NOT IDENT. FE-59 -9.791E+OO 7.773E+OO 8.939E+OO NOT IDENT. C0-60 -l.823E-02 4.943E-02 5. OllE-02 NOT IDENT. ZN-65 5.287E-02 2.492E-01 2.503E-01 NOT IDENT. GE-68 1.716E+OO 2.661E+OO 2.771E+OO NOT IDENT. AS-73 -l.585E+OO 5.289E+OO 5.338E+OO NOT IDENT. AS-74 l.241E+03 5.186E+03 5.216E+03 SHORT HLIF SE-75 -1. 62 OE-01 2.034E-01 2.161E-:Ol NOT IDENT. BR-77 2.528E+37 2.136E+38 O.OOOE+OO SHORT HLIF SR-82 -4.481E+02 7.533E+02 7.800E+02 SHORT HLIF RB-83 2.444E-01 6.185E-01 6.282E-01 NOT IDENT. RB-86 6.200E+03 2.603E+04 2:618E+04 SHORT HLIF Y-88 l.300E-01 3.166E-01 3.220E-01 NOT IDENT. Y-91 9.783E+Ol 5.442E+02 5.459E+02 NOT IDENT. NB-94 -l.265E-02 3.476E-02 3.522E-02 FAIL ABUN NB-95 -7.441E-Ol 1.055E+OO l.107E+OO NOT IDENT. NB-95M 9 .138E-01 2.450E+OO 2.484E+OO NOT IDENT. ZR-95 4.605E-01 1.349E+OO '1.365E+OO NOT IDENT. NB-97 -1.000E+41 5.339E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.OOOE+41 4. 343E+41 O.OOOE+OO SHORT HLIF M0-99 -1.017E+31 3.013E+31 O.OOOE+OO SHORT HLIF TC-99M l.000E+41 2.855E+41 O.OOOE+OO SHORT HLIF RH-101 5.084E-03 4.349E-02 4.355E-02 NOT IDENT. RH-102 3.200E-'02 6.663E-02 6.817E-02 FAIL ABUN RU-103 8.407E+OO 5.393E+OO 6.592E+OO FAIL ABUN RH-106 3.012E-01 5.432E-01 5.599E-01 NOT IDENT. RU-106 3.012E-01 5.432E-01 5.599E-01 NOT IDENT. AG-108M -4.400E-03 3.287E-02 3.293E-02 NOT IDENT. AG-llOM 8.467E-02 1.188E-01 l.248E-01 NOT IDENT. SN-113 -6.167E-02 2.509E-01 2.524E-01 NOT IDENT. CD-115 l.124E+38 3.219E+38 O.OOOE+OO SHORT HLIF SN-ll 7M 4.657E+04 7.302E+04 7.597E+04 SHORT HLIF TE-123M 6.423E-02 l.405E-01 l.435E-01 NOT IDENT. SB-124 3.634E-01 1.504E+OO 1.513E+OO FAIL ABUN SB-125 2.281E-02 9.008E-02 9.066E-02 FAIL ABUN TE-125M -1.043E+02 2.749E+02 2.789E+02 NOT IDENT. I-126 l .151E+o6 l.105E+06 l.220E+06 SHORT HLIF SB-126 7.010E+05 8.802E+05 9.352E+05 SHORT HLIF SB-127 6.793E+21 1.153E+22 O.OOOE+OO SHORT HLIF I-131 6.858E+08 2.789E+09 2.807E+09 SHORT HLIF I-132 l.000E+41 1.807E+42 O.OOOE+OO SHORT HLIF TE-132 4.876E+25 9.489E+25 O.OOOE+OO SHORT HLIF BA-133 1.240E-02 4.128E-02 4.166E-02 FA'IL ABUN I-133 -1. OOOE+41 l.946E+41 O.OOOE+OO SHORT HLIF CS-134 l.494E-01 8.508E-02 l.085E-01 FAIL ABUN CS-.135 1.313E-01 1.548E-01 l.657E-01 NOT IDENT. I-135 -1.000E+41 7.754E+41 O.OOOE+OO SHORT HLIF CS-136 6.614E+03 2.087E+05 2.087E+05 SHORT HLIF CE-139 1.570E-02 1.17 5E-01 l.177E-01 NOT IDENT. BA-140 l.470E+05 9.213E+05 9.237E+05 SHORT HLIF LA-140 -9.474E+04 3.024E+05 3.054E+05 SHORT HLIF CE-141 -l.345E+Ol 2.607E+Ol 2.677E+Ol NOT IDENT. CE-143 -1.000E+41 5. 967E+42 0.000E+OO SHORT HLIF CE-144 6.808E-02 3. 711E-01 3. 724E-01 NOT IDENT. PM-144 2.687E-02 6.865E-02 6.971E-02 NOT IDENT. PR-144 2.293E+OO 5.936E+OO 6.025E+OO NOT IDENT. PM-146 -1.302E-02 4. 3.38E-02 4.377E-02 NOT IDENT. ND-147 -3.468E+06 1. 8'64E+07 l.870E+07 SHORT HLIF PM-147 3.476E+Ol 8.390E+02 8.392E+02 NOT IDENT. PM-149 -3.972E+39 5.357E+39 O.OOOE+OO SHORT HLIF EU-150 2.370E-02 2.938E-02 3.126E-02 FAIL ABUN EU-152 -6.812E-02 l .114E-01 1.156E-01 FAIL ABUN GD-153 -9.474E-02 1.856E-01 l.905E-01 NOT IDENT. EU-154 5.883E-02 l.061E-01 1.094E-01 FAIL ABUN EU-155 -6.420E-03 1.158E-01 l.158E-01 FAIL ABUN TB-160' -3.894E-01 1.923E+OO l.9j1E+OO FAIL ABUN H0-166M -l.446E-02 6.050E-02 6.085E-02 FAIL ABUN TM-171 9.517E+00 1.198E+Ol l.273E+Ol NOT IDENT. HF-172 -l.215E-01 3.092E-01 3.140E-01 FAIL ABUN LU-172 5.472E-02 9.691E-02 l.OOOE-01 FAIL ABUN Page 180 of 614 LU-176 4.886E-03 2.367E-02 2.378E-02 FAIL ABUN HF-181 i.335E+OO 3.899E+OO 3.945E+OO NOT IDENT. TA-182 6.620E-Ol 1.032E+OO 1.074E+OO FAIL ABUN RE-183 7.508E-02 1.926E+OO 1.926E+OO NOT IDENT. RE-184 2.128E+Ol 2.973E+Ol 3.124E+Ol NOT IDENT. W-188 -1. 7 53E+Ol l.204E+02 l.206E+02 FAIL ABUN IR-192 1. 009E-Ol ' 4.482E-01 4.505E-01 FAIL ABUN HG-203. 1.120E+OO 2.499E+OO 2.549E+OO NOT IDENT. BI-207 1. 782E-02 5 .141E-02 5.203E-02 FAIL ABUN PB-211 -3.460E-01 9 .171E-01 9.302E-01 NOT IDENT. l.319E+OO 9.538E-01 l.124E+OO FAIL ABUN RN-219 2.150E-02 4.642E-01 4.643E-01 FAIL ABUN RA-223 l.462E-01 5.806E-01 5.843E-01 FAIL ABUN AC-227 l.049E-01 2.423E-01 2.469E-01. NOT IDENT. TH-227 l.049E-01 2.423E-01 2.469E-01 NOT IDENT. TH-229 2.137E-01 5.567E-01 5.649E-01 FAIL ABUN PA-231 1.270E-01 4.954E-01 4.987E-01 NOT IDENT. TH-231 1. 462E-01 5.806E-01 5.843E-01 FAIL ABUN PA-233 2.060E-02 6.013E-02 6.084E-02 NOT IDENT. PA-234 -5.351E-02 3.992E-01 4.000E-01 FAIL ABUN PA-234M 1.471E+OO 4.979E+OO 5.023E+OO NOT IDENT. NP-237 2.060E-02 6. 013E-02 6.084E-02 FAIL ABUN NP-238 4.382E+40 5.426E+40 O.OOOE+OO SHORT HLIF NP-239 -5.837E-02 2.388E-01 2.402E-01 FAIL ABUN PU-239 5. o*36E+02 7. 011E+02 7.369E+02 FAIL ABUN AM-241 -2.704E-02 9.975E-02 l.005E-01 NOT IDENT. CM-243 -8.335E-02 l.020E-01 1.087E-01 FAIL ABUN BK-247 -4.380E-02 7.205E-02 7.470E-02 FAIL ABUN CM-247 -2.627E-02 4.213E-02 4.377E-02 FAIL ABUN

  • CF-249 1. 815E-02 4.059E-02 . 4.140E-02 NOT IDENT. CF-251 -2.968E-02 1.219E-01 l.227E-01 NOT IDENT. Page 181 of 614
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 46.6934 87.09 145.6589 136.47 61. 3499 45.60 66.4874 8'7.57 145. 7721 140.51 0.0000 46.54 69.5789 88.03 145.8800 143.76 69.9058 49. 72 0.0000 88.34 148.7874 144.24 81.0290 51. 35 83.2463 88.47 148.8184 145.44 91. 8591 51. 87 83.3441 89. 96 149.1730 152.43 83.3357 52.39 68.5410 1093.63 119.4674 153.25 0.0000 52.97 76.5867 91.11 0.0000 323.87 75.3844 53.44 92.5970 92.59 110.2045 156.02 0.0000 54.07 97. 7106 93.35 110. 3341 158.56 0.0000 57.36 0.0000 94.56 110.5408 159.00 66.4568 57.53 102.4584 94.65 67.2642 162.33 77.2279 57.98 93.5059 94.67 67.2661 162.66 0.0000 59.27 103.8389 94.87 67.2866 163.33 58.5693 59.32 103.8499 97.43 90.5452 165.86 66.9491 59.54 103.8970 98.43 75.5681 176.31 59.3689 60. 96 106.5601' 98.44 75.5692 176.60 0.0000 61.17 106.6055 99.53 91.9123 177. 52 63.0087 62.93 122.8957 100 .11 85.4979 181.07 0.0000 63. 29 122.9836 102.03 86.8256 181.52 58.8859 63.58 123.0547 *103.18 97.8429 184.41 57.4592 64.28 137 .14.2 8 103.37 92.4324 143.76 57.5339 66.73 124.1539 105.21 83.9562 193.51 68.8391 67.24 110.6186 105.31 90.5109 197.03 55.7403 125.81 106. 6113 106.12 198.01 67.9210 67.75 104.5751 106.47 79.7379 201.83 57.2088 69.67 113.1866 109.28 88.8286 203.43 71. 5161 70.83 96.2443 111. 00 75.8504 205.31 43. 9607 72.81 120.0533 111.76 0.0000 210.85 52.3646 72.87 120.0666 114. 06 86.1052 215.65 64.0939 74.66 110.7633 116. 30 0.0000 222 .11 55.7817 74.82 llO. 7951 ll6.74 70.9072 227.09 57.2670 74.97 llO. 8244 ll9.76 68.2260 227.38 57.2810 77. ll lll.2451 121.12 59.4332 228.16 0.0000 78.74 lll.5617 121.22 59.4409 228.18 48.5977 79.69 83.8080 121.78 74.7273 116.74 48.5977 80.12 83.8702 122.06 74.7550 235.69 55.1766 80.19 0.0000 122.92 74.8383 235. 96 61.4601 80.57 83.9343 123.07 74.8531 238.63 55.3ll5 81. 00 83. 9960 265.00 74.9ll9 238.98 0.0000 81. 0*7 84.0057 125.81 85.2078 240.99 55.4189 81. 75 103.0259 127.23 74.1297 242.00 55.4653 83.79 103.3788 127.91 70.8214 244.70 50.5341 84.00 103.4147 129.30 70.9452 252.40 0.0000 85.43 139.6226 131.20 61. 7069 252.80 50.8636 86.55 ll2.3274 133. 02 57 .. 3208 254.15 0.0000 86.79 145.5877 133. 52 60.3752 256.23 46.7520 86.94 145.6233 136.00 63.5862 260.90 0.0000 Page 182of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 52.1935 355.39 0.0000 584.27 14.3486 264.80 52.1985 356.01 24.6055 595.83 0.0000 265.00 47.9279 364.49 0.0000 427.87 27.8657 268.22 37.3217 366.42 0.0000 602.52 ' 0.0000 269.46 55.3903 372.51 30.3789 604. 72 17.0586 270.03 52.4082 375.05 26.7373 607.14 18. 6284. 271.23 52.4554 377.52 31.3936 609.32 23.8254 273.65 0.0000 356.01 25.9509 610.33 23.8348 276.40 49.2070 388.16 30.6622 614.28 32. 6971 277.37 44.9224 388.63 0.0000 618.01 30.1493 277.60 44.9308 391.69 39.1050 620.36 24.9756 278.00 44.9435 264.66 29.9486 621.93 17.7021 279.20 42.8210 401.81 42.1436 630.19 0.0000 279.54 44.1301 402.40 46.8414 631.29 18.8159 279.70 44 .1353 404.85 46.4375 633.25 20.9229 280.46 41. 5625 410.95 31. 0651 634.78 0.0000 283.69 45.1329 413.71 29.6992 635.95 23.0402 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 53.8804 423. 72 0.0000 645.85 12.6177 285.90 0.0000 427.09 16.1467 657.76 22.1860 287.50 35.6844 427.87 18.0541 657.90 0.0000 290.67 45.7986 433.94 36.2273 661.66 19.0459 293.27 0.0000 439.40 34.4209 664.57 0.0000 351. 93 45.5106 453.88 26.0140 666.33 0.0000 295.96 42.0313 463.37 31. 9513 666.50 0.0000 879.38 47.3730 468.07 23.2935 667.71 0.0000 299.98 43.2052 473.00 0.0000 677. 62 14.3734 300.09 45. 6672 475.06 31.1680 685.70 0.0000 300.13 45.6682 476.78 25.3462 695.00 0.0000 301.36 49.2244 477.60 19.5052 696.49 24.6659 302.85 52.7954 482.18 20.5275 696. 51 24.6659 256.23 44.9280 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 25.7461 306.78 33.5283 497.08 13.7858 697.49 26.8209 308.46 33.5677 505.52 25. 2131 702.65 23.6480 311. 90 27.8913 507.63 0.0000 706.68 17.2246 316.51 36.4172 511. 00 31. 7227 711.68 17.2565 319.41 0.0000 514.00 31.7682 720.70 0.0000 320.08 0.0000 514.00 31. 7 682 721. 93 0.0000 321.04 37.4199 520.40 17.9238 722.78 12.9961 323.87 33.0276 520.69 0.0000 722.91 12. 9966 325.23 34.8447 522.65 0.0000 723.31 17.8730 328.76 0.0000 527.90 0.0000 724.19 26.0049 333.37 37.7267 528.26 12.9931 727.33 18.4416 333.97 32. 3496 529.59 24.0020 733.00 18.2622 334.37 32.3577 529.87 0.0000 735.93 14.1468 338.28 43.2539 531.02 0.0000 333.97 16.3324 338.32 43.2549 537.26 0.0000 739.50 0.0000 311. 90 43.3154 546.56 0.0000 747.24 16.3898 340.48 43.3154 552.55 18.1912 748.06 13 .1157 340.55 0.0000 563.25 24.3721 752.31 17.5143 344.28 43.4209 569.33 27.4922 753.82 0.0000 345.93 42 .*1075 . 946.00 27.4944 756.73 13 .1563 351.06 32.7056 569.70 23.4230 756.80 13.1567 351.93 32. 7231 583.19 14.3418 884.68 18.1362 Page 183of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 28.0473 1274.44 15.9730 1620.50 4.1082 766.42 24,7522 1001.03 15.1064 1621.92 3.0818 766.84 21. 4551 1002.74 13.0392 1678.03 0.0000 772.60 0.0000 1004.73 22. 7727 1690.97 2.0818 776.52 0.0000 507.63 0.0000 1750.46* 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 6.3307 778.90 24.3087 1028.54 0.0000 1063.66 9.5059 783.70 0.0000 1037.84 13.4683 1771.35 5.2823 785.37 23.2550 1038.76 0.0000 1791.20 0.0000 792.07 9.9895 631. 29 8.1002 1808.65 3.1906 794.95 19.9988 1048 .. 07 0.0000 1810.72 0.0000 795.86 21. 6725 1049.04 11.7083 1836.06 6.4120 810.06 17.8685 1050.41 14.4160 810.29 15.6361 1063.66 12.6593 344.28 13.4028 1077.00 0.0000 810.76 14.5213 1077. 34 12.7072 815.77 0.0000 1085.87 11.8265 1048.07 0.0000 1093.63 16.4092 832.01 12.3746 1099.45 28.3038 834.85 22.5203 1112. 07 16.1229 835. 71 15.7688 1112.84 13. 6130 836.80 0.0000 1115.54 11. 0024 846.75 0.0000 1120. 29 13.6393 846'. 77 13.5649 1120.55 13.6402 856.80 0.0000 1221.41 13.6429 860.$6 20.4382 1129. 67 9.2029 871.09 20.5078 1131.51 0.0000 873.19 13.6807 1147.95 0.0000 875.33 0.0000 1173.23 13.9590 879.38 15.9921 1177.95 13.0438 880.51 18.2832 1189.05 14.0140 883.24 19. 4432' 1204.77 15.0068 884.68 13.7305 1221. 41 14.1266 889.28 11. 4587 1231. 02 16.0475 894.76 13.7739 1235.36 0.0000 898.04 10.3411 1238.28 18.9124 900.72 '21. 84 97 1260.41 0.0000 903.28 11. 508 8 1271.87 14.2987 911.20 16.1516 1274.44 6.6766 912.08 16.1562 1274.54 6.6770 923.98 0.0000 1291.59 4.7882 926.50 11. 5910 1298.22 0.0000 929 .11 11. 6003 1312 .11 0.0000 937.49 26.7482 1332.49 15.4678 944.13 0.0000 1362.66 0.0000 946.00 17.4890* 1365.19 5.8433 949.00 15.4038 1368.63 0.0000 667.71 0.0000 1384.29 7.8242 962. 31 28.1182 1408.01 4.9158 964. 08 12.6598 1457.56 0.0000 966 .17 21.1121 1460.82 5. 9659 911.20 26.4120 1489.16 5.0012 968. 97 26. 4120 1505.03 3.0106 983.53 0.0000 1584.12 4.8946 984.45 0.0000 1596.21 0.0000 Page 184of614 VAX/VMS Nuclide Identif.ication Report Generated 3-0CT-2016 05: 38: 49. 60 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245007.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM29.CNF;354 Background date : Z-OCT-2016 11:01:41. Sample date 15-DEC-2015 12:17:00 Acquisition date : 3-0CT-2016 04:35:17. Sample ID R405245007 Sample quantity : 1.26520E+02 GRAM Detector name : GAM29 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.44 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596387 Detector SN# Matrix Spike ID : . LCS ID . 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 .12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 1 1 3 3 0 3 3 0 0 0 0 0 0 0. 0 0 0 0 0 0 0 0 5 5 0 0 0 0 0 0 0 0 0 Page 185of614 Energy 46.47* 63.61* 67.42 74.85* 77.18* 87.38 90.01 92.83* 99.13 129.34* 153.20 186.27* 209.50 238.56* 241.86 258.67 270.26 295.05* 300.33 330.08 338.27* 351.99* 464.01 511.10* 516.93 540.89 583.12* 609.57* 638.53* 661.67 668.71 677.84 680.98 727. 93 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 57 7 39 138 205 75 47 82 21 12 10 73 45 274 59
  • 19 40 117 26 94 67 207 19 0 14 28 128 149 17 62 20 12 9 49 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 128 150 88 150 118 101 55 136 137 122 84 151 97 .139 85 51 76 103 79 94 59 78 48 30 22 37 27 51 18 41 7 5 5 22 1. 47 1. 06 1. 09 1.10 1. 02 0.95 0.93 1. 37 1. 35 l. 59 1. 33 1. 07 1.12 1. 04 1. 54 1. 67 1. 20 1.10 0.89 7.04 1. 05 1. 24 0.65 2.22 1. 84 6.78 1.11 1.26 3.10 1.18 1. 70 1.16 0.76 3.41 92. 96 127.20 134.80 149.64 154.29 174.65 179.90 185.54 198.12 258.47 306.12 372 .18 418.56 476.62 483.22 516.78 539.94 589.46 600.03 659.46 675.83 703.24 927.07 1021.17 1032.83 1080.72 1165 .11 1275.88 1322 .12 1336.20 1354.46 1360.73 1454.59 89 124 124 145 145 172 178 178 193 253 305 367 415 473 . 481 513 535 585 595 649 672 698 920 1013 1013 1072 1159 1211 1271 1316 1333 1351 1358 1448 9 1. 59E-02 39. 5 14 1.99E-03273.6 1.0lE+OO 14 1. 08E-02 41. 4 14 3.84E-02 17.0 4.56E-01 14 5.70E-02 11.4 6 2.09E-02 24.5 13 1.31E-02 28.0 1.27E+OO 13 2.29E-02 28.3 9 5.73E-03105.3 8 3.23E-03169.9 6 2.80E-03146.2 11 2.04E-02 36.2 9 1. 25E-02 42. 2 8 7.61E-02 9.7 7 1. 63E-02 30. 7 7 5.41E-03 64.6 10 1.llE-02 43.4 11 3.24E-02 19.3 9 7.15E-03 65.8 20 2.60E-02 28.0 9 1.86E-02 24.4 11 5.76E-02 11.0 10 5. 3'4E-03 71. 0 25 1.13E-04***** 1.39E+OO 25 3.93E-03 73.8 17 7.84E-03 53.5 12 3.55E-02 12.3 13 4 .13E-02 13 .1 10 4.61E-03 55.1 11 1.72E-02 23.8 7 5.56E-03 31.3 7 3.33E-03 42.6 6 2.56E-03 49.-4 15 1.36E-02 26.7 Peak Search Report (continued) Page : 2 Sample ID : R405245007 Acquisition date 3-0CT-2016 04:35:17 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 844.31 19 4 1. 07 1687.29 1683 9 5.31E-03 30.1 36 0 861.44 22 20 0.92 1721.56 1714 12 6. llE-03 46.6 37 0 883.46 14 15 0.63 1765.58 1761 9 3.75E-03 59.4 38 0 911.32* 100 22 1. 55 1821.30 1812 18 2.79E-02 15.2 39 0 969.29* 36 21 0.95 1937.23 1932 12 9.91E-03 31. 6 40 0 1001.44* 21 3 1. 42 2001. 54 1996 11 5.92E-03 28.8 41 0 1011.73 9 9 1. 03 2022.12 2018 7 2.48E-03 67.4 42 0 1107. 69 14 5 3.23 2214.07 2209 10 3.89E-03 40.1 43 0 1121.76* 42 47 1. 94 2242.22 2233 20 1.16E-02 42.8 44 0 1175.01 12 14 2.51 2348.76 2341 12 3.33E-03 70.3 45 0 1181. 49 6 12 0.86 2361. 72 2356 8 l.77E-03101.4 46 0 1201.49 8 9 1. 52 2401. 75 2397 9 2.22E-03 76.3 47 0 1239.76 15 30 2.65 2478.33 2471 11 4.16E-03 75.6 48 0 1280.36 12 10 0.52 2559.56 2553 13 3.42E-03 59.5 49 0 1378.36* 8 8 2.84 2755.69 2749 11 2.18E-03 82.9 50 0 1460.95* 335 12 1. 95 2921.01 2913 13 9.30E-02 5.9 51 0 1508.40 12 0 0. 96 3016.00 3012 9 3.33E-03 28.9 52 0 1629.16 13 0 0.98 3257.77 3251 12 3.61E-03 27.7 53 0 1729.76 9 0 1. 42 3459.22 3453 10 2.50E-03 33.3 54 0 1764.66* 35 0 2.37 3529.12 3524 11 9. 72E-03 18.7 Flag: "*" = Peak area was modified by background subtraction Page 186of614 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 05:38:51 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245007.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 15-DEC-2015 12:17:00 R405245007 Acq0isition date : Sample quantity Sample geometry : 3-0CT-2016 04:35:17 126.52 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA29 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Page 187of614 Nuclide PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:01.44 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : R405245007 Acquisition date 3-0CT-2016 04:35:17 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1. 34 7E+OO l.315E+Ol 1.315E+Ol 11. 90 OK CD-109 88.03 3.70* 6.278E+OO 1.385E+OO 2.149E+00 79.49 OK SN-126. 64.28 9.60 3.641E+OO 1.398E-01 l.398E-01 547.22 OK 86.94 8.90 6.278E+OO 5.757E-01 5.757E-01 79.49 OK 87.57 37.00* 6.278E+OO 1.385E-01 l.385E-01 79.49 OK BA-137M 661. 66 89.90* 2.522E+OO l.617E-01 1. 647E-01 47.63 OK CS-137 661. 66 85.10* 2.522E+OO 1. 708E-01 1.740E-01 47.63 OK TL-208 277.37 6.60 4.914E+OO Line Not Found Absent 583.19 85.00* 2.773E+OO 3.242E-01 3.242E-01 24.66 OK 860.56 12.50 2.068E+OO 4.970E-01 4.970E-01 93.10 OK PB-210 46.54 4.25* l.128E+OO 8.245E+OO 8.454E+OO 79.01 OK BI-211 72.87 1. 23 4.875E+OO Line Not Found Absent 351. 06 12.92* 4.087E+OO 1.012E-01 1.012E-011033.04 OK PB-212 74.82 10.28 5.107E+OO 1.302E+OO 1.302E+OO 48.63 OK 77 .11 17.10 5.363E+OO l.506E+OO 1.506E+OO 22.83 OK 238.63 43.60* 5.497E+OO 7.221E-01 7 .221E-01 19.36 OK 300.09 3.30 4.623E+OO 1. 051E+OO 1.051E+OO 131. 60 OK BI-214 609.32 45.49* 2.682E+OO 7.268E-01 7. 271E-01 26.22 OK 1120.29 14.92 1.684E+OO 9.567E-01 9.570E-01 85.59 OK 1764.49 15.30 l.129E+OO l.129E+00 l.129E+OO 37.30 OK PB-214 74.82 5.80 5.103E+OO Line Not Found <<INT Reject 77 .11 9.70 5.363E+OO 2.655E+OO 2.656E+OO 22.83 OK 87.09 3.41 6.257E+OO Line Not Found <<INT Reject 242.00 7.25 5.441E+OO Line Not Found <<INT Reject 295.22 18.42 4.687E+OO 8.430E-01 8.433E-01 38.68 OK 351.93 35.60* 4.087E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.682E+OO .7.268E-01 7. 271E-01 26.22 OK 1120.29 14.92 1. 684E+00 9.567E-01 9.570E-01 85.59 OK 1764.49 15.30 l.129E+OO 1.129E+oo* 1.129E+OO 37.30 OK RA--:-224 240.99 4.10* 5.443E+OO 1.682E-01 l.682E-01 695.88 OK RA-226 609.32 45.49* 2.682E+00 7.268E-01 7. 271E-01 26. 22 OK 1120. 29 14.92 l.684E+00 9.567E-01 9.570E-01 85.59 OK 1764.49 15.30 1.129E+OO l.129E+00 1.129E+OO 37.30 OK AC-228 105.21 1.10 7.155E+OO Line Not Found Absent 338.32 11. 27 4.215E+OO 8.694E-01 8.694E-01 48.80 OK 794.95 4.25 2.197E+00 Line Not Found Absent 835. 71 1. 61 2 .116E+00 Line Not Found Absent 911. 20 25.80* l.981E+OO 1.142E+OO 1.142E+OO 30.33 OK 968.97 15.80 1.889E+OO 6.924E-01 6.924E-01 63.27 OK RA-228 105.21 1.10 7.155E+OO Line Not Found Absent 338.32 11.27 4.215E+OO 8.694E-01 8.694E-01 48.80 OK 794.95 4.25 2.197E+OO Line Not Found Absent 835.71. 1. 61 2 .116E+OO Lipe Not Found Absent 911.20 25.80* 1. 981E+OO 1.142E+OO 1.142E+OO 30.33 OK 968. 97 15.80 l.889E+00 6.924E-01 6.924E-01 63.27 OK TH-228 74.82 10.28 5.107E+OO 1.302E+OO l.302E+00 48.63 OK 77 .11 17.10 5.363E+OO 1.506E+OO 1.506E+OO 22.83 OK 238.63 43.60* 5.497E+OO 7.221E-01 7. 221E-01 19.36 OK 300.09 3.30 4.623E+OO 1.051E+OO 1. 051E+OO 131. 60 OK Page 188of614 Nuclide Line Activity Report (continued) Page : 3 Sample ID : R405245007 Acquisition date*: 3-0CT-2016 04:35:17 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error .Status TH-230 609.32 45.49* 2.682E+OO 7.268E-01 7.268E-01 26. 22 OK 1120.29 14.92 1.684E+OO 9.567E-01 9.567E-01 85.59 OK 1764.49 15.30 1.129E+OO l.129E+OO l.129E+OO 37.30 OK PA-231 . 283.69 1. 70 4.831E+OO Line Not Found Absent 301.36 5.35* 4.623E+00 6.486E-01 6.486E-01 131. 60 OK TH-232 105.21 1.10 7.155E+00 Line Not Found Absent 338.32 11.27 4.215E+OO 8.694E-01 8.694E-01 48.80 OK 835. 71 1. 61 2 .116E+00 Line Not Found Absent 911. 20 25.80* l.981E+OO 1.142E+OO l.142E+OO 30.33 OK 968. 97 15.80 l.889E+OO 6.924E-01 6.924E-01 63.27 OK TH-234 63.29 3.70* 3.641E+OO 3.627E-01 3.627E-01 547.22 OK 92.59 4.23 6.635E+OO 1.959E+OO 1.959E+00 56.66 OK U-234 609.32 45.49* 2.682E+OO 7.268E-01 7.268E-01 26.22 OK 1120.29 14.92 1.684E+OO 9.567E-01 9.567E-01 85.59 OK 1764.49 15.30 1.129E+OO l.129E+OO 1.129E+OO 37.30 OK U-235 89.96 3.47 6.461E+OO 1.402E+OO 1.402E+OO 56. 04 OK 93.35 5.60 6.635E+OO 1.480E+OO 1.480E+OO 56.66 OK 143.76 10. 96* 7.247E+OO Line Not Found Absent 163.33 5.08 6.922E+OO -----Line Not Found Absent 185.72 57.20 6.470E+OO 1. 271E-01 1. 271E-01 72. 41 OK 205.31 5.01 6.095E+OO .Line Not Found Absent U-238 63.29 3.70* 3. 641E+OO 3.627E-01 3.627E-01 547.22 OK 92.59 4.23 6.635E+OO l.959E+OO 1.959E+OO 56.66 OK AM-243 43.53 5.90 7.707E-01 Line Not Found Absent 74.66 67.20* 5.107E+OO 1.992E-01 1.992E-01 48.63 OK ANH-511 511. 00 100.00* 3.064E+OO 7.983E-04 7.983E-048182.15 OK Flag: "*" = Keyline Page 189of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:38:52.71 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245007.CNF;l *
  • Acquisition date 3-0CT-2016 04:35:17 Sensitivity : 3.000 *
  • Detector ID GAM29 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.44 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:17:00 Analyst initials: MXRl *
  • Sample ID R405245007 Sample Quantity 1.2652E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25-JUN-2016 09:55:57 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM29 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.315E+Ol 1.533E+OO CD-109 2.149E+OO 1.674E+OO SN-126 1.385E-01 1. 07 9E-01 BA-137M 1.647E-01 7.688E-02 CS-137 1. 740E-01 8.122E-02 TL-208 3.242E-01 7.835E-02 PB-210 8.454E+OO 6.546E+OO BI-211 1.012E-01 1.024E+OO PB-212 7.221E-01 1.370E-01 BI-214 7.271E-01 1.868E-01 PB-214 8.800E-01 1.898E-01 RN-222 7. 271E-01 1. 868E-01 RA-224 l.682E-01 1.147E+OO RA-226 7. 271E-01 1. 868E-01 AC-228 1.142E+OO 3. 396E-01 RA-228 1.142E+OO 3. 396E-01 TH-228 7. 221E-01 1.370E-01 TH-230 7.268E-01 1.867E-01 PA-231 6.486E-01 8.365E-01 TH-232 1.142E+OO 3. 396E-01 TH-234 3.627E-01 1.945E+OO U-234 7.268E-01 1. 867E-01 U-235 9.382E-04 1.875E-01 U-238 3.627E-01 1.945E+OO AM-243 1.992E-01 9. 493E...:02 ANH-511 7.983E-04 6.401E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 190of614 Key-Line Activity (pCi/GRAM 2.844E+00 1. 911E-02 O.OOOE+OO 1.419E-02 K.L. Cnt Uncert ( 1. 96-sigma) 1.027E+Ol 4.536E-02 1. 96.0E+41 2.670E-02 MDA (pCi/GRAM 6.263E-01 1. 475E+OO 1.243E-01 7.161E-02 7.565E-02 6.103E-02 5.389E+OO 3.674E-01 1.131E-01 1.207E-01 3.130E-01 1.207E-01 1.368E+OO 1.207E-01 1.990E-01 1.990E-01 1.131E-01 1.207E-01 7.562E-01 l.990E-01 2.137E+OO 1.207E-01 3.345E-01 2.137E+OO 8.325E-02 4.250E-02 . MDA (pCi/GRAM 2.080E+Ol 8.754E-02 O.OOOE+OO 6.789E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 1. 539E-02 3.942E-01 7.530E-01 FAIL ABUN 'v-48 O.OOOE+OO 1.066E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.357E+02 O.OOOE+OO SHORT HLIF MN-54 2.750E-02 6.173E-02 l.259E-01 NOT IDENT. C0-56 1. 496E-01 3.405E-01 6.886E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO *sHORT HLIF C0-57 -1.336E-02 4.823E-02 8.606E-02 NOT IDENT. C0-58 5.866E-02 4.429E-01 8.978E-01 NOT IDENT. FE-59 1.494E+OO 4.330E+OO 9.374E+OO NOT IDENT. C0-60 -1.082E-02 3.991E-02 7.207E-02 NOT IDENT. ZN-65 7.578E-03 1. 753E-01 3.022E-01 NOT IDENT. GE-68 1.038E+OO l.636E+OO 3.755E+OO NOT IDENT. AS-73 2.238E+OO 7.462E+OO l.453E+Ol NOT IDENT. AS-74 O.OOOE+OO 4.379E+03 O.OOOE+OO SHORT HLIF SE-75 -2.532E-02 l.922E-01 3.390E-01 NOT IDENT. BR-77 O.OOOE+OO 3.064E+36 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 5.642E+02 0.000E+OO SHORT HLIF RB-83 -9.645E-02 6.192E-01 1.062E+OO NOT IDENT. KR-85 8.031E+OO 6.466E+OO l.422E+Ol NOT IDENT. SR-85 7.838E-01 6.333E-01 1.392E+OO NOT IDENT. RB-86 O.OOOE+OO l.633E+04 O.OOOE+OO SHORT HLIF Y-88 -5.384E-02 2.669E-01 5.267E-01 NOT IDENT. Y-91 2.864E+02 5.246E+02 9. 951E+02 NOT IDENT. NB-94 -9.021E-03 2.547E-02 4.715E-02 NOT IDENT. NB-95 -:-2 .114E-01 8.058E-01 1. 478E+OO NOT IDENT. NB-95M 7.705E-01 2.395E+OO 4.067E+OO NOT IDENT. ZR-95 -4.164E-01 l.274E+OO 2.341E+OO NOT IDENT. NB-97 O.OOOE+OO 1.058E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.517E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -3.203E-03 3.519E-02 5.880E-02 NOT IDENT. RH-102 -2.377E-02 4.801E-02 8.744E-02 NOT IDENT. RU-103 2.039E+OO 4.658E+OO 9.598E+OO FAIL ABUN RH-106 1. 499E-01 4 :927E-01 9.892E-01 NOT IDENT. RU-106 1. 499E-01 4.927E-01 9.892E-01 NOT IDENT. AG-108M 3.944E-03 2.763E-02 5.458E-02 NOT IDENT. AG-llOM 1.203E-01 l.400E-01 2.095E-01 FAIL ABUN SN-113 -l.558E-01 2.038E-01 3. 661E-01 NOT IDENT. CD-115 O.OOOE+OO 3.316E+38 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 6.815E+04 O.OOOE+OO SHORT HLIF TE-123M -3.122E-02 l.335E-01 2.358E-01 NOT IDENT. SB-124 -4.386E-01 1.858E+OO 3.761E+OO NOT IDENT. SB-125 -8.428E-02 l.003E-01 l.773E-01 FAIL ABUN TE-125M 2.564E+02 2.582E+02 5.075E+02 NOT IDENT. I-126 O.OOOE+OO 6.290E+05 0.000E+OO SHORT HLIF SB-126 O.OOOE+OO 7.296E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 5.054E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.474E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 6.140E+40 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 9.306E+25 O.OOOE+OO SHORT HLIF BA-133 . 7.536E-03 4.327E-02 7.800E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-134 2.247E-02 5.406E-02 1.079E-01 NOT IDENT. CS-135 6.219E-03 l.458E-01 2. 411E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO l.524E+05 O.OOOE+OO SHORT HLIF CE-139 3. 591E-02 1.037E-01 l.934E-01 NOT IDENT. BA-140 O.OOOE+OO 9.682E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2. 964E+05 O.OOOE+OO SHORT HLIF CE-141 -9.569E+OO 1.945E+Ol 3.382E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -1.167E-01 3.449E-01 6.104E-01 NOT IDENT. PM-144 l.222E-02 5.330E-02 1.056E-01 NOT IDENT. PR-144 l.058E+OO 4.613E+OO 9.138E+00 NOT IDENT. PM-146 4.367E-02 8.728E-02 NOT IDENT. ND-147 0. OOOE+.00 l.957E+07 O.OOOE+OO SHORT HLIF PM-147 2.843E+02 8.157E+02 l.535E+03 NOT IDENT. PM-149 O.OOOE+OO 4.687E+39 O.OOOE+OO SHORT HLIF EU-150 2.654E-02 2.728E-02 4.735E-02 FAIL ABUN EU-152 -5.804E-02 8.370E-02 1.530E-01 NOT IDENT. GD-153 l.235E-02 l.577E-01 2.939E-01 NOT IDENT. EU-154 4. 941E-02 l.121E-01 2.171E-01 NOT IDENT. EU-155 7.790E-02 l.129E-01 2.170E-01 FAIL ABUN TB-160 -9.389E-02 1. 764E+OO 3.031E+00 FAIL ABUN H0-166M 2.543E-03 5.259E-02 1. 026E-01 NOT IDENT. TM-171 -5.438E+OO 1. 886E+Ol 3.507E+Ol FAIL ABUN HF-172 -2 .132E-02 2.480E-01 4.142E-01 FAIL ABUN Page 191of614 LU-172 -3.585E-02 6.940E-02 l.199E-01 FAIL ABUN LU-176 9.202E-03 2.512E-02 4. 651E-02 FAIL ABUN HF-181 5.144E-01 3.488E+OO 6. 971E+OO NOT IDENT. TA-182 8.766E-02 8.137E-01 1.578E+OO FAIL ABUN RE-183 2.304E-01 2.747E+OO 5.202E+OO FAIL ABUN RE-184 -l.563E+Ol 2.594E+Ol 4.456E+Ol NOT IDENT. W-188 7.409E+Ol 1.185E+o2 2.090E+02 FAIL ABUN IR-192 -6.484E-02 4.067E-01 7.120E-01 FAIL ABUN HG-203 -7.166E-01 2.233E+OO 3.818E+OO NOT IDENT. BI-207 -3.030E-02 4.137E-02 6.770E-02 FAIL ABUN PB-211 -3.806E-01 7.174E-01 l.316E+OO NOT IDENT. BI-212 O.OOOE+OO 9.610E-01 1.272E+OO FAIL ABUN RN-219 3.989E-02 4.234E-01 8.220E-01 FAIL ABUN RA-223 -2.549E-03 6.051E-01 1.071E+OO FAIL ABUN AC-227 -7.370E-02 2.373E-01 3.735E-01 FAIL ABUN TH-227 -7.370E-02 2.373E-01 3.735E-01 FAIL ABUN TH-229 2.674E-01 4. 719E-01 8.894E-01 FAIL ABUN TH-231 -2.549E-03 6. 051E-01 1. 071E+OO FAIL ABUN PA-233 -5.143E-02 6.763E-02 l.077E-01 FAIL ABUN PA-234 -l.517E-01 2.721E-01 4.706E-01 FAIL ABUN PA-234M 7.961E+00 4.489E+OO 9.439E+OO FAIL ABUN NP-237 -5.143E-02 6.763E-02 1.077E-01 FAIL ABUN NP-238 0.000E+OO 3.992E+40 O.OOOE+OO SHORT HLIF NP-239 -1.200E-02 2.290E-01 4.190E-01 FAIL ABUN PU-239 1. 634E+02 5.439E+02 5.986E+02 FAIL ABUN AM-241 -9.037E-02 1.391E-01 2.488E-01 NOT IDENT. CM-243 -3.328E-02 9.787E-02 1. 7 53E-01 FAIL ABUN BK-247 4.563E-03 6.873E-02 1.242E-01 NOT IDENT. CM-247 1.239E-02 3.695E-02 7.362E-02 NOT IDENT. CF-249 4.764E-03 3.469E-02 6.893E-02 NOT IDENT. CF-251 -3.102E-02 1.201E,-01 2.108E-01 NOT IDENT. Page i92of614 Nuclide Identification Report Generated 3-0CT-2016 05:38:50.35 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 318 10.66* 1.347E+OO 1.315E+Ol 1.315E+Ol 11. 90 *CD-109 88.03 85 3.70* 6.278E+OO 2.162E+OO 3.355E+OO 48.99 SN-126 64.28 8 9.60 3.641E+OO l.398E-01 1.398E-01 547.22 *8 6. 94 85 8.90 6.278E+OO 8.987E-01 8.987E-01 48.99 87.57 85 37.00* 6.278E+OO 2.162E-01 2.162E-01 48.99 BA-137M 661.66 62 89.90* 2.522E+OO *1.617E-01 l.647E-01 47.63 CS-137 661. 66 62 85.10* 2.522E+OO l.708E-01 l.740E-01 47.63 TL-208 277.37 ------6.60 4.914E+OO ------Line Not Found ------583.19 129 85.00* 2.773E+OO 3.242E-01 3.242E-01 24.66 860.56 22 12.50 2.068E+OO 4.970E-01 4.970E-01 93.10 PB-210 46.54 67 4.25* 1.128E+OO 8.245E+OO 8.454E+OO 79.01 BI-211 72.87 ------1.23 4.875E+OO ------Line Not Found ------351.06 216 12.92* 4.087E+OO 2.424E+OO 2.424E+OO 22.01 PB-212 74.82 157 10.28 5.107E+OO 1.778E+OO 1.778E+OO 34.08 77 .11 *233 17.10 5.363E+OO 1.506E+OO 1.506E+OO 22.83 238.63 292 43.60* 5.497E+OO 7. 221E-01 7.221E-01 19.36 300.09 27 3.30 4.623E+OO 1. 051E+OO 1. 051E+OO 131. 60 BI-214 609.32 149 45.49* 2.682E+OO 7.268E-01 7. 271E-01 26. 22 1120.29 41 14.92 1.684E+OO 9.567E-01 9.570E-01 85.59 1764.49 33 15.30 1.129E+OO 1.129E+OO 1.129E+OO 37.30 PB...:214 74.82 157 5.80 5.107E+OO 3.151E+OO 3.152E+OO 34.08 77 .11 233 9.70 5.363E+OO 2.655E+OO 2.656E+OO 22.83 87.09 85 3.41 6.278E+OO 2.345E+OO 2.346E+OO 48.99 242.00 62 7.25 5.443E+OO 9.381E-01 9.385E-01 61. 42 295.22 123 18.42 4.687E+OO 8.430E-01 8.433E-01 38.68 351. 93 216 35.60* 4.087E+OO 8.797E-01 8.800E-01 22.01 RN-222 609.32 149 45.49* 2.682E+OO 7.268E-01 7. 271E-01 26.22 1120.29 41 14.92 1.684E+OO 9.567E-01 9.570E-Ol 85.59 1764.49 33 15.30 1.129E+OO 1.129E+OO 1.129E+OO 37.30 RA-224 240.99 62 4.10* 5.443E+OO 1.659E+OO 1. 659E+OO 61.42 RA-226 609.32 149 45.49* 2.682E+OO 7.268E-01 7. 271E-01 26.22 1120.29 41 14.92 1.684E+00 9.567E-01 9.570E-01 85.59 1764.49 33 15.30 1.129E+OO 1.129E+OO 1.129E+OO 37.30 AC-228 105.21 ------1.10 7.155E+OO ------Line Not Found ------338.32 70 11. 27 4.215E+OO 8.694E-01 8.694E-01 . 48. 80 794.95 ------4.25 ------Line Not Found ------835. 71 ------1.61 2 .116E+OO ------Line Not Found ------911. 20 98 25.80* 1. 981E+OO 1.142E+00 1.142E+OO 30. 33. 968.97 35 15.80 1.889E+OO 6.924E-01 6.924E-01 63.27 RA-228 105.21 ------1.10 7.l55E+OO ------Line Not Found ------338.32 70 11. 27 4.215E+OO 8.694E-01 8.694E-01 48.80 794.95 ------4.25 2.197E+OO ------Line Not Found ------835.71 ------1. 61 2 .116E+OO ------Line Not Found ------911. 20 98 25.80* 1. 981E+OO 1.142E+OO 1.142E+OO 30.33 968.97 35 15.80 1.889E+OO 6.924E-01 6.924E-01 63.27 TH-228 74.82 157 10.28 5.107E+OO 1.778E+OO 1.778E+OO 34.08 77.11 233 17.10 5.363E+OO 1.506E+OO 1.506E+OO 22.83 Page 193 of 614 Nuclide Line Activity Report (continued) Page : 2 Sample ID : R405245007 Acquisition date 3-0CT-2016 04:35:17 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area. %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 292 43.60* 5.497E+OO 7.221E-01 7. 221E-01 19.36 300.09 27 3.30 4.623E+OO 1.051E+OO 1.051E+OO 131.60 TH-230 609.32 149 45.49* 2.682E+OO 7.268E-01 7.268E-01 26.22 1120.29 41 14.92 1.684E+OO 9.567E-01 9.567E-01 85.59 1764.49 33 15.30 1.129E+OO 1.129E+OO 1.12 9E+OO 37.30 PA-231 .283. 69 ------1. 70 4.831E+OO ------Line Not Found ------301.36 27 5. 35_* 4.623E+OO 6.486E-01 6.486E-01 131. 60 TH-232 105.21 ------1.10 7.155E+OO ------Line Not Found ------338.32 70 11. 27 4.215E+OO 8.694E-01 8.694E-01 48.80 835. 71 ------1. 61 2 .116E+OO ------Line Not Found ------911.20 98 25.80* 1.981E+OO 1.142E+OO 1.142E+OO* 30.33 968. 97 35 15.80 1.889E+OO 6.924E-01 6.924E-01 63.27 TH-2.34 63. 29 8 3.70* 3.641E+OO 3.627E-01 3.627E-01 547.22 92.59 93 4.23 6.635E+OO 1.959E+OO 1.959E+OO 56.66 U-234 609.32 149 45.49* 2.682E+OO 7.268E-Ol* 7.268E-01 26.22 1120.29 41 14.92 1.684E+OO 9.567E-01 9.567E-01 85.59 1764.49 33 15.30 1.129E+OO 1.12 9E+OO 1.129E+OO 37.30 U-235 89. 96 53 3.47 6.461E+OO 1.402E+OO 1.402E+OO 56.04 93.35 93 5.60 6.635E+OO 1.480E+OO 1.480E+OO 56.66 143.76 ------10. 96* 7.247E+OO ------Line Not Found ------163.33 ------5.08 6.922E+OO ------Line Not Found ------185.72 79 57.20 6.470E+OO 1. 271E-01 1. 271E-01 72.41 205.31 ------5.01 6.095E+OO ------Line Not Found ------U-238 63.29 8 3.70* 3.641E+00 3.627E-01 547.22 92.59 93 4.23 6.635E+OO 1.959E+00 1.959E+OO 56.66 AM-243 43.53 ------5.90 7.707E-01 ------Line Not Found ------74.66 157 67.20* 5.107E+OO 2. 720E-01 2.720E-01 34.08 ANH-511. 511.00 0 100.00* 3.064E+OO 7.983E-04 7.983E-04 8182.15 Flag: "*" Key line Page 194of614 Page : 3 Summary of Nuclide Activity Sample ID : R405245007 Acquisition date 3-0CT-2016 04:35:17 Total number of lines in .spectrum 54 Number of unidentified lines 16 Number of lines tentatively identified by NID 38 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+lOY 22.20Y 7.04E+08Y 1. 41E+l0Y 1600. OOY 1600. OOY 1600. OOY l.41E+l0Y 1600. OOY 1. 41E+10Y 1.41E+10Y l.41E+l0Y 7.54E+04Y 7.04E+08Y 1.41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 1. 55 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.315E+01 2.162E+OO 2.162E-01 l.617E-01 1.708E-01 3.242E-01 8.245E+OO 2.424E+OO 7.221E-01 7 :268E-01 8.797E-01 7.268E-01 1.659E+OO 7.268E-01 1.142E+OO 1.142E+'OO 7.221E-01 7.268E-01 6.486E-01 1.142E+OO 3.627E-01 7.268E-01 1. 271E-01 3.627E-01 2.720E-01 7.983E-04 3.967E+Ol 3.967E+Ol Decay Corr pCi/GRAM l.315E+Ol 3.355E+OO 2.162E-01 l.647E-01 1.740E-01 3.242E-01 8.454E+.00 2.424E+OO 7.221E-01 7. 271E-01 8.800E-01 7. 271E-01 1.659E+OO 7. 271E-01 1.142E+OO 1.142E+OO 7. 221E-01 7.268E-01 6.486E-01 1.142E+OO 3.627E-01 7.268E-01 1. 271E-01 3.627E-01 2.720E-01 7. 983E.:._04 4.108E+Ol 4.108E+Ol 70.37% Decay Corr 2-Sigma Error 0.156E+Ol 1.644E+OO 1.059E-01 0.784E-Ol 0.829E-01 0.800E-01 6.679E+OO 0.534E+OO l.398E-01 l.906E-01 l.937E-01 1.906E-01 1.019E+OO l.906E-01 0.347E+OO 0.347E+OO 1. 398E-01 l.906E-01 8.535E-01 0.347E+OO 19.85E-01 1.906E-01 0.920E-01 19.85E-01 0.927E-01 653.2E-04 "M" Manually accepted 2-Sigma %Error 11. 90 48.99 48.99 47.63 47.63 24.66 79.01 22.01 19.36 26.22 22.01 26.22 61.42 26 .22 30.33 30.33 19.36 26 .22 131.60 30.33 547.22 26.22 72. 41 547.22 34.08 8182.15 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 195of614 Flags K Unidentified Energy Lines Page : 4 Sample ID : R405245007 Acquisition date : 3-0CT-2016 04:35:17 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 1 67.42 44 100 1. 09 134.80 124 14 1. 08E-02 82.7 4.18E+OO T 0 99.13 23 154 1. 35 198.12 193 9 5.73E-03 **** 6.94E+OO T 0 129.34 13 134 1. 59 258.47 253 8 3.23E-03 **** 7.38E+OO T 0 153.20 11 92 1. 33 306.12 305 6 2.80E-03 **** 7.lOE+OO T 0 209.50 48 104 1.12 418.56 415 9 1. 25E-02 84.4 6.0lE+OO T 0 258.67 21 53 1. 67 516.78 513 7 5.41E-03 **** 5.18E+OO 0 270.26 42 80 1. 20 539.94 535 10 1. llE-02 86.8 5.0lE+OO T 0 330.08 98 98 7.04 659.46 649 20 2.60E-02 56.0 4.30E+OO T 0 464.01 20 49 0.65 927.07 920 10 5.34E-03 **** 3.30E+OO T 5 516.93 14 23 1. 84 1032.83 1013 25 3.93E-03 **** 3.04E+OO 0 540.89 29 37 6.78 1080.72 1072 17 7.84E-03 **** 2.94E+OO 0 638.53 17 18 3.10 1275.88 1271 10 4.61E-03 **** 2.59E+OO 0 668. 71 20 7 1. 70 1336.20 1333 7 5.56E-03 62.6 2.50E+00 T 0 677.84 12 5 1.16 1354.46 1351 7 3.33E-03 85.3 2.48E+OO T 0 680.98 9 5 0.76 1360.73 1358 6 2.56E-03 98.9 2.47E+OO 0 727.93 48 22 3.41 1454.59 1448 15 l.36E-02 53.4 2.35E+OO T 0 844.31 19 4 1. 07 1687.29 1683 9 5.31E-03 60.2 2.lOE+OO 0 883.46 13 15 0.63 1765.58 1761 9 3.75E-03 **** 2.03E+00 T 0 1001.44 21 3 1. 42 2001.54 1996 11 5.92E-03 57.5 1.84E+OO T 0 1011.73 9 9 1. 03 2022.12 2018 7 2.48E-03 **** 1. 83E+OO 0 1107. 69 14 5 3.23 2214.07 2209 10 3.89E-03 80.2 1.*70E+OO 0 1175.01 12 14 2.51 2348.76 2341 12 3.33E-03 **** 1. 62E+OO 0 1181. 49 6 11 0.86 2361. 72 2356 8 l.77E-03 **** 1. 61E+OO 0 1201. 49 8 9 1. 52 2401.75 2397 9 2.22E-03 **** 1. 59E+O.O 0 1239.76 14 29 2.65 2478.33 2471 11 4.16E-03 **** 1.55E+OO T 0 1280.36 12 9 0.52 2559.56 2553 13 3.42E-03 **** 1. 51E+OO 0 1378. 36 7 8 2.84 2755.69 2749 11 2.18E-03 **** l.42E+00 0 1508.40 11 0 0. 96 3016.00 3012 9 3.33E-03 57.7 l.31E+00 0 1629.16 12 0 0.98 3257.77 3251 12 3. 61E-03 55.5 1.22E+OO 0 1729.76 8 0 1. 42 3459.22 3453 10 2.50E-03 66.7 l.15E+OO Flags: "T" = Tentatively associated Page 196of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:39:06.42 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245007.CNF;l *
  • Acquisition date 3-0CT-2016 04:35:17 Sensitivity : 3.000 *
  • Detector ID GAM29 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.44 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:17:00 Nuclide Library : SOLID *
  • Sample ID R405245007 Analyst initials: MXRi' *
  • Batch Number 1596387 Sample Quantity : 1.2652E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 25-JUN-2016 09:55:57 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM29 CAN.CNF;lO
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 *RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.574E-01 6.823E-01 5. 8 61E-02 3.217E-02 3.398E-02 2.708E-02 2.517E+OO 1.683E-01 5.312E-:02 5. 372E-02 1.509E-01 5.372E-02 6.477E-01 5.372E-02 8.371E-02 8. 5.312E-02 5.370E-02 3.449E-01 8. 371E-02 1.006E+OO 5.370E-02 l.569E-01 1.006E+OO 3.919E-02 l.860E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 197of614 Le (pCi/GRAM 9.306E+OO 3.721E-02 O.OOOE+OO 2.667E-02 3.315E-01 NOT IDENT: NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 .C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM:-171 HF-172 LU-172 Page 198of614 O.OOOE+OO O.OOOE+OO 5.567E-02 2.909E-01 O.OOOE+OO 4.027E-02 3.831E-Ol 3.892E+OO 2.992E-02 1.295E-01 1.573E+OO 6.783E+OO O.OOOE+OO 1. 547E-01 O.OOOE+OO 0.000E+OO 4.682E-01 6.462E+OO 6.327E-01 O.OOOE+OO 2.136E-01 4.352E+02 2.021E-02 6.537E-01 1. 892E+00 1.015E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.746E-02 3.729E-02 4.298E+OO 4.413E-01 4.413E-01 2.470E-02 9.240E-02 1. 636E-01 O:OOOE+OO O.OOOE+OO l.102E-01 1.465E+OO 7.913E-02 2.393E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.558E-02 O.OOOE+OO 4.831E-02* 1.104E-01 O.OOOE+OO O.OOOE+OO 9.015E-02 O.OOOE+OO O.OOOE+OO 1.570E+Ol O.OOOE+OO 2.846E-01 4.694E-02 4.062E+00 3.952E-02 O.OOOE+OO 7.189E+02 O.OOOE+OO 2.1658-02 6.881E-02 1. 373E-01 . 9.240E-02 l.024E-01 1. 297E+OO 4.506E-02 1. 632E+Ol l.938E-01 4.993E-02 SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT *IDENT. SHORT HLIF ' SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HiiIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234* PA_.:.234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 199of614 2.133E-02 3.108E+OO 6.776E-01 2.444E+OO 1. 901E+Ol 9.666E+Ol 3.212E-01 1. 749E+OO 2.760E-02 5.990E-01 5.844E-01 3.775E-01 4.886E-01 1. 702E-01 1. 702E-01 4.153E-01 4.886E-01 4.913E-02 2.004E-Ol 4.200E+OO 4. 913E-02 O.OOOE+OO l.954E-01 2.816E+o2 l.168E-01 8.194E-02 5.675E-02 3.374E-02 3.120E-02 9.825E-02 FAIL ABUN NO'r IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:39:13.25 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245007.CNF;l *
  • Acquisition date 3-0CT-2016 04:35:17 Sensitivity : 3.000 *
  • Detector ID GAM29 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.44 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:17:00 Nuclide Library : SOLID *
  • Sample ID R405245007 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.2652E+02 GRAM *
  • Quantity Err(%) : 1.5808E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25-JUN-2016 09:55:57 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM29 CAN.CNF;lO * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ) ( 1. 96-sigma) ( 1. 96-sigma) K-40 l.315E+Ol 1.680E+OO 1. 680E+OO CD-109 2.149E+OO 1.690E+OO 1.690E+OO SN-126 1.385E-01 1. 086E-01 1. 086E-01 BA-137M l.647E-01 7.721E-02 7. 721E-02 CS-137 1.740E-01 8.156E-02 8.156E-02 TL-208 3.242E-01 7.956E-02 7.956E-02 PB-210 8.454E+OO 6.590E+OO 6.590E+OO BI-211 1.012E-01 1.034E+OO 1.034E+OO PB-212 7 .221E-01 1.423E-01 1.423E-01 BI-214 7. 271E-01 1.894E-01 l.894E-01 PB-214 8.800E-01 l.933E-01 1.933E-01 RN-222 7.271E-01 1. 8 94E-01 l.894E-01 RA-224 1.682E-01 1.152E+OO l.152E+OO RA-226 7.271E-01 1. 894E-01 1.894E-01 AC-228 1.142E+OO 3.446E-01 3.446E-01 RA-228 1.142E+OO 3.446E-01 3.446E-01 TH-228 7. 221E-01 1.423E-01 1. 423E-01 TH-230 7.268E-01 1.893E-01 1.893E-01 PA-231 6.486E-01 8.478E-01 8.478E-01 TH-232 l.142E+00 3.446E-01 3.446E-01 TH-234 3.627E-01 1.947E+OO 1. 947E+OO U-234 7.268E-01 l.893E-01 1.893E-01 U-235 9.382E-04 l.875E-01 l.875E-01 U-238 3.627E-01 1.947E+OO 1. 947E+OO AM-243 1.992E-01 9.617E-02 9.617E-02 ANH-511 7.983E-04 6.401E-02 6.401E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide ( 1. 96-sigma) ( 1. 96-sigma) BE-7 2.844E+OO 1.027E+Ol l.035E+Ol NOT IDENT. 'NA-22 1. 911E-02 4.536E-02 4.617E-02 NOT IDENT. NA-24 1. OOOE+41 1.300E+42 0.000E+OO SHORT HLIF AL-26 l.419E-02 2. 671E-02 2.747E-02 NOT IDENT. Page 200of614 SC-46 1.539E-02 3.942E-01 3.942E-01 FAIL ABUN V-48 -4.341E+03 1.066E+04 l.084E+04 SHORT HLIF CR-51 3.162E+02 3.360E+02 3.650E+02 SHORT HLIF MN-54 2.750E-02 6.174E-02 6.298E-02 NOT IDENT. C0-56 1. 496E-01 3.406E-01 3.472E-01 FAIL ABUN MN-56 l.000E+41 2.299E+41 O.OOOE+OO SHORT HLIF C0-57 -l.336E-02 4.823E-02 4.861E-02 NOT IDENT. C0-58 5.866E-02 4.429E-01 4.437E-01 NOT IDENT. FE-59 1. 494E+OO 4.331E+OO 4.383E+OO NOT IDENT. C0-60 ...,.1. 082E-02 3. 991E-02 4. 021E-02 . NOT IDENT. ZN-65 7.578E-03 1.753E-01 1. 7 53E-01 NOT IDENT. GE-68 1.038E+OO 1.637E+OO 1. 702E+OO NOT IDENT. AS-73 2.238E+OO 7.476E+OO 7.544E+OO NOT IDENT. AS-74 -2.488E+03 4.384E+03 4.525E+03 SHORT HLIF SE-75 -2.532E-02 1.922E-01 1.926E-01 NOT IDENT. BR-7.7 l.614E+37 1.364E+38 O.OOOE+OO SHORT HLIF . SR-82 -3.250E+Ol 5.642E+02 5.644E+02 SHORT HLIF RB-83 -9.645E-02 6.194E-01 6.209E-01 NOT IDENT. KR-85 8.031E+OO 6.474E+OO 7.417E+OO NOT IDENT. SR-85 7.838E-01 6.341E-01 7.259E-01 NOT IDENT. RB-86 8.635E+03 1. 633E+04 l.679E+04 SHORT HLIF Y-88 -5.384E-02 2.670E-01 2.681E-01 NOT IDENT. Y-91 2.864E+02 5.247E+02 5.403E+02 NOT IDENT. NB-94 -9.021E-03 2.547E-02 2.579E-02 NOT IDENT. NB-95 -2 .114E-01 8.059E-01 8 .115E-01 NOT IDENT. NB-95M 7.705E-01 2.395E+OO 2.420E+OO NOT IDENT. ZR-95 -4.164E-01 1.274E+OO l.288E+OO NOT IDENT. NB-97 1.000E+41 1.059E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 2.439E+41 O.OOOE+OO SHORT HLIF M0-99 -1.259E+31 2.519E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 2.350E+41 O.OOOE+OO SHORT HLIF RH-101 -3.203E-03 3.519E-02 3.522E-02 NOT IDENT. RH-102 -2.377E-02 4.805E-02 4.923E-02 NOT IDENT. RU-103 2.039E+OO 4.660E+OO 4.749E+OO FAIL ABUN RH-106 1.499E-01 4.928E-01 4.974E-01 NOT IDENT. RU-106 l.499E-01 4.928E-01 4.974E-01 NOT IDENT. AG-108M 3.944E-03 2.763E-02 2.769E-02 NOT IDENT. AG-llOM l.203E-01 1. 402E-01 1.503E-01 FAIL ABUN SN-113 -1.558E-01 2.039E-01 2.156E-01 NOT IDENT. CD-115 3.763E+37 3.316E+38 0.000E+OO SHORT HLIF SN-ll 7M 8.756E+03 6.816E+04 6.827E+04 SHORT HLIF TE-123M -3.122E-02 1.335E-01 l.342E-01 NOT IDENT. SB-124 -4.386E-01 1.858E+OO l.868E+OO NOT IDENT. SB-125 -8.428E-02 1.004E-01 l.073E-01 FAIL ABUN TE-125M 2.564E+02 2.587E+02 2.833E+02 NOT IDENT. I-126 3.543E+04 6.290E+05 6.292E+05 SHORT HLIF SB-126 -4.653E+05 7.346E+05 7.639E+05 SHORT HLIF SB-127 3.325E+21 6.742E+21 O.OOOE+OO SHORT HLIF I-131 -2.205E+09 2.476E+09 2.668E+09 SHORT HLIF I-132 1.000E+41 1.805E+42 O.OOOE+OO SHORT HLIF TE-132 8.062E+24 9.312E+25 O.OOOE+OO SHORT HLIF BA-133 7.536E-03 4.328E-02 4. 341E-02 NOT IDENT. I-133 -l.OOOE+41 l.150E+42 O.OOOE+OO SHORT HLIF CS-134 2.247E-02 5.407E-02 5.501E-02 NOT IDENT. CS-135 6.219E-03 1.458E-01 1.458E-01 NOT IDENT. I-135 -1.000E+41 2.864E+43 O.OOOE+OO SHORT HLIF CS-136 8.459E+03 1.524E+05 1.525E+05 SHORT HLIF CE-139 3. 591E-02 1.039E-01 l.052E-01 NOT IDENT. BA-140 -3.940E+05
  • 9. 683E+05 9.845E+05 SHORT HLIF LA-140 -8.729E+04 2.964E+05 2.990E+05 SHORT HLIF CE-141 -9.569E+OO 1.945E+Ol 1. 9.92E+Ol NOT IDENT. CE-143 l.000E+41 3.707E+41 O.OOOE+OO SHORT HLIF CE-144 -l.167E-01 3.449E-01 3.489E-01 NOT IDENT. PM-144 1.222E-02 5. 331E-02 5.359E-02 NOT IDENT. PR-144 1.058E+OO 4. 613E+OO 4.638E+OO NOT IDENT. PM-146 1.193E-02 4.368E-02 4.401E-02 NOT IDENT. ND-147 1. 014E+07 l.958E+07 2.010E+07 SHORT HLIF PM-147 2.843E+02 8.159E+02 8.259E+02 NOT IDENT. PM-149 4.823E+38 4.688E+39 O.OOOE+OO SHORT HLIF EU-150 2.654E-02 2.730E-02 2.981E-02 FAIL ABUN EU-152 -5.804E-02 8.376E-02 8.775E-02 NOT IDENT. GD-153 1.235E-02 1.577E-01 l.578E-01 NOT IDENT. EU-154 4.941E-02 l.121E-01 l.143E-01 NOT IDENT. EU-155 7.790E-02 l.130E-01 l.183E-01 FAIL ABUN TB-160 -9.389E-02 1. 764E+OO 1. 765E+OO FAIL ABUN H0-166M 2.543E-03 5.259E-02 5.260E-02 NOT IDENT. TM-171 -5.438E+OO 1.886E+Ol l.902E+Ol FAIL ABUN HF-172 -2.132E-02 2.480E-01 2.482E-01 FAIL ABUN Page 201of614 LU-172 -3.585E-02 6.950E-02 7.135E-02 FAIL ABUN LU-176 9.202E-03 2.512E-02 2.546E-02 FAIL ABUN HF-181 5.144E-01 3.488E+OO 3.496E+OO NOT IDENT. TA-182 8.766E-02 8.137E-01 8.146E-01 FAIL ABUN RE-183 2.304E-01 2.747E+OO 2.749E+OO FAIL ABUN
  • RE-184 -1.563E+Ol 2.619E+Ol 2.712E+Ol NOT IDENT. W-188 7.409E+Ol l.188E+o2 l.234E+02 FAIL ABUN IR-192 -6.484E-02 4.067E-01 4.078E-01 FAIL ABUN HG-203 -7.166E-01 2.233E+OO 2.256E+OO NOT IDENT. BI-207 -3.030E-02 4.139E-02 4.358E-02 FAIL ABUN PB-211 -3.806E-01 7.177E-01 7.379E-01 NOT IDENT. BI-212 1.837E+OO 9.655E-01 1.272E+OO FAIL ABUN RN-219 3.989E-02 4.234E-01 FAIL ABUN RA-223 -2.549E-03 6.051E-01 6.051E-01 FAIL ABUN AC-227 -7.370E-02 2.375E-01 2.398E-01 FAIL ABUN TH-227 -7.370E-02 2.375E-01 2.398E-01 FAIL ABUN TH-229 2.674E-01 4.720E-01 4. 872E-01 FAIL ABUN TH-231 -2.549E-03 6.051E-01 6. 051E-01 FAIL ABUN PA-233 -5.143E-02 6.768E-02 7.154E-02 FAIL ABUN PA-234 -1.517E-01 3.227E-01 3.299E-01 FAIL ABUN PA-234M 7. 961E+OO 4.502E+OO 5.758E+OO FAIL ABUN NP-237 -5.143E-02 6.768E-02 7.154E-02 FAIL ABUN NP-238 -2.273E+39 3.992E+40 O.OOOE+OO SHORT HLIF NP-239 -l.200E-02 2.290E-01 2.291E-01 FAIL ABUN PU-239 1.634E+02 5.440E+02 5.490E+02 FAIL ABUN AM-241 -9.037E-02 1.392E-01 l.451E-01 NOT IDENT. CM-243 -3.328E-02 9.792E-02 9.906E-02 FAIL ABUN BK-247 4.563E-03 6.873E-02 6.876E-02 NOT IDENT .. CM-247 1.239E-02 3.701E-02 3.743E-02 NOT IDENT. CF-249 4.764E-03 3.469E-02 3.476E-02 NOT IDENT. CF-251 -3.102E-02 l.202E-01 1.210E-01 NOT IDENT. Page 202 of 614
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 76.0217 87.09 90.0471 136.47 69.5029 45.60 66.8087 87.57 90.1075 140.51 0.0000 46.54 66.9380 88.03 51. 2302 143.76 67.8409 49. 72 0.0000 88.34 51.2524 144.24 64.5898 51. 35 59.8572 88.47 51.2615 145.44 66.8602 51. 87 60.8834 89. 96 69.8589 152.43 73.5809 52.39 66.7482 1093.63 69.9237 153.25 0.0000 52.97 66.8219 91.11 0.0000 323.87 64.1269 53.44 60.0961 92.59 70.1087 156.02 0.0000 54.07 66. 9604 93.35 70.1800 158.56 0.0000 57.36 0.0000 94.56 80.6309 159.00 74.4201 57.53 77.1533 94.65 80.6404 162.33 62.3984 57.98 78.1931 94.67 80.6428 162.66 0.0000 59.27 90.1287 94.87 91.0051 163.33 71.3789 59.32 94.0558 97.43 65.3711 165.86 55.8968 59;54 94.0924 98.43 65.4561 176.31 60.9445 60. 96 86.'4662 98.44 65. 4571 17'6. 60 0.0000 61.17 86.4978 99.53 65.5489 177.52 68.9182 62.93 85.7740 100 .11 58.3093 181.07 0.0000 63.29 85.8270 102.03 57.0603 181. 52 80.1211 63.58 85.8691 103.18 77.3524 184.41 62.1365 64.28 85.9707 103.37 77.3705 143.76 62.5858 66.73 86.3223 105.21 70.2132 193.51 53.8374 67.24 86.3947 105.31 74.4143 197.03 68.9310 125.81 86.4570 -106.12 72.3902 198.01 41.3921 67.75 86.4663 106.47 .94.4632 201.83 56.5157 69.67 85.0742 109.28 66.3516 203.43 63.5182 70.83 77.2413 111. 00 93.9297 205.31 66.3135 72.81 93.5135 111.76 0.0000 210.85 51.1.174 72. 87 93.5220 114.06 75.2059 215.65 48.9784 74.66 86.4134 116. 30 0.0000 222 .11 53. 9112 74.82 86.4344 116.74 64.8167 227.09 70.5844 74.97 86.4540 119.76 72.5068 227.38 68.2466 77 .11 86. 7362 121.12 65.1439 228.16 0.0000 78.74 72.7938 121.22 65.1508 228.18 55.3370 79.69 82.3454 121. 78 74.8108 116.74 55.3370 80.12 79.6960 122.06 78.0420 235.69 52.0942 80.19 0.0000 122.92 78.1178 235. 96 52.1043 80.57 66.2320 123.07 77.0603 238.63 80.6826 81. 00 73.0366 265.00 68.5449 238.98 0.0000 Bl. 07 73.0443 125.81 73.0023 240.99 104.5913 81. 75 79.2092 127.23 68.8154 242.00 65.0209 83.79 84 .1961 127.91 68. 8672 244.70 46.0795 84.00 74.7125 129.30. 68.9717 252.40 0.0000 85.43 87 .1152 131.20 70.5541 252.80 40.7516 86.55 115.8824 133.02 70.3310 254.15 0.0000 86.79 115.9213 133.52 71. 4513 256.23 41.6501 86.94 90.0283 136. 00 62.9561 2 60. 90 0.0000 Page 203 of 614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 38.6689 355.39 0.0000 584.27 20.8175 264.80 38.6729 356.01 33.2228 595.83 0.0000 265.00 36.2604 364.49 0.0000 427.87 24.7580 268.22 38.7627 366.42 0.0000 602.52 0.0000 269.46 40.0073 372.51 30.9448 604.72 21. 4590 270.03 40.0224 375.05 26.6829 607.14 27.2058 271. 23 40.0546 377.52 31. 027 6 609.32 21. 9733 273.65 0.0000 356.01 31.1316 610.33 21. 9818 276.40 46.2823 388.16 28.6011 614.28 18.6645 277.37 43.8739 388.63 0.0000 618.01 19.1699 277.60 43.8805 391.69 34.7323 620.36 16.3090 278.00 46.3311 264.66 34.0203 621. 93 19.1984 279.20 46.3670 401.81 41.0227 630.19 0.0000 279.54 53.7002 402.40 34.9235 631.29 16.3747 279.70 53.7056 404.85 43.7083 633.25 12.7236 280.46 32. 9722 410.95 22.7981 634.78 0.0000 283.69 41.6077 413. 71 37. 7571 635.95 13.0259 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 41.6544 423.72 0.0000 645.85 30.9870 285.90 0.0000 427.09 33. 5871* 657.76 14.5874 287.50 38.0301 427.87 35.3687 657.90 0.0000 290.67 37. 6969 433.94 28.3776 661.66 26.2936 293.27 0.0000 439.40 28.4525 664.57 0.0000 351. 93 49.3115 453.88 26.8567 666 .'33 0.0000 295. 96 49.3347 463.37 26.9751 666.50 0.0000 87.9.38 44.4749, 468.07 22.7078 667.71 0.0000 299.98 51.1079 473.00 0.0000 677.62 7.3450 300.09 51.1117 475.06 20.7913 685.70 0.0000 300.13 51.1129 476.78 20.8077 695.00 0.0000 301.36 36.3014 477.60 20.8152 696.49 18.7294 302.85 39.6377 482.18 20.8583 696. 51 18.7294 256.23 44.6385 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.7069 306.78 34.7676 497.08 19.1701 697.49 16.7634 308.46 41. 0184, 505.52 20.6149 702.65 15.8053 311. 90 48.5774 507.63 0.0000 706.68 9.8918 316.51 31.2263 511. 00 16.5308 711. 68 16.8444 319.41 0.0000 514.00 16.5520 720.70 0.0000 320.08 0.0000 514.00 16.5520 721. 93 0.0000 321.04 34.2334' 520.40 20.7468 722.78 11.9346 323.87 36.3819 520.69 0.0000 722-. 91 16.4107 325.23 31.3889 522.65 0.0000 723.31 16.4127 328.76 0.0000 527.90 0.0000 724.19 17.9099 333.37 28.5948 528.26 24.0534 727. 33 19.9211 333.97 20.1914 529.59 23.1405 733.00 20.9556 334.37 25.2454 529.87 0.0000 735.93 12.9852 338.28 38.7966 531.02 0.0000 333.97 13.9909 338.32 38.7975 537.26 0.0000 739.50 0.0000 311. 90 25.3339 546.56 0.0000 747.24 14.0359 340.48 25.3339 552.55 15.8849 748.06 13.0365 340.55 0.0000 563.25 18.7687 752.31 16. 0671 344.28 37.2369 569.33 16.9329 753.82 0.0000 345.93 33.0364 946.00 17.8751 756.73 18.1018 351.06 39.9278 569.70 17.8759 756.80 18.1018 351. 93 39.9479 583.19 20 .. 8085 884.68 20.1595 Page 204 of 614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 23.1975 1274.44 12.9336 1620.50 3.6975 766.42 21.1837 1001.03 7.5540 1621. 92 1. 0567 766.84 21.1871 1002.74 8. 0972 1678.03 0. 0000. 772.60 0.0000 1004.73 6.4812 1690.97 5.6155 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 1.8954 778.90 19.2428 1028.54 0.0000 1063.66 3.7944 783.70 0.0000 1037.84 10.8944 1771.35 1. 8976 785.37 15.2222 1038.76 0.0000 1791.20 0.0000 792.07 21.3555 631.29 8.7344 1808.65 1.9094 794.95 17.3037 1048.07 0.0000 1810.72 0.0000 795.86 19.3448 1049.04 13.1094 1836.06 7. 6719 810.06 9.2032 1050.41 9.8357 810.29 9.2040 1063.66 13 .1582 344.28 10. 2271 1077.00 0.0000 810.76 10.2283 1077.34 4.4007 815.77 0.0000 1085.87 16.5381 1048.07 0.0000 1093.63 13.2549 832.01 21. 6178 1099.45 5.5310 834.85 14.4238 1112. 07 11. 6501 835.71 11. 3361 1112. 84 15.9809 836.80 0.0000 1115. 54 H. 6595 846.75 0.0000 1120. 29 12.2291 846.77 6.2036 1120. 55 12.2300 856.80 0.0000 1221.41 12.2318 860.56 10.3813 1129.67 9.3598 871.09 13.5374 1131. 51 0.0000 873.19 8.3356 1147.95 0.0000 875.33 0.0000 1173.23 9.0052 ' 879.38 12.5259 1177.95 10.1418 880.51 14.0960 1189.05 13.5566 883.24 14.6295 1204.77 10.2041 884.68 18.8174 1221. 41 11.3802 889.28 17.7955 1231.02 12.5451 894.76 12.5811 1235.36 0.0000 898.04 16.7904 1238.28 18.2773 900.72 10.5017 1260.41 0.0000 903.28 16.8151 1271. 87 10. 3564* 911. 20 9.4797 1274.44 6.9082 912.08 9.4819 1274.54 6.9087 923.98 0.0000 1291.59 5.7784 926.50 9.5200 1298.22 0.0000 929 .11 9.5270 1312 .11 0.0000 937.49 11.6709 1332. 49 10.4912 944.13 0.0000 1362. 66 0.0000 946.00 17.0150 1365.19 3.5210 949.00 13.8363 1368. 63 0.0000 667.71 0.0000 1384.29 5.3020 962. 31 25.6357 1408.01 2.6636 964. 08 16.0297 1457.56 0.0000 966.17 24.0582 1460.82 7.1777 911.20 16.0510 1489.16 2.7063 968. 97 16.0510 1505.03 1. 4478 983.53 0.0000 1584.12 10.1010 984.45 0.0000 1596.21 0.0000 Page 205 of 614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:39:*44.31 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245008.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM30.CNF;300 Background date : Z-OCT-2016 11:01:47. Sample date 15-DEC-2015 12:20:00 Acquisition date : 3-0CT-2016 04:35:39. Sample ID R405245008 Sample quantity 1.53247E+02 GRAM Detector name : GAM30 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.40 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596387 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 0 2 4 3 4 4 5 5 5 6 5 7 0 8 0 9 0 10 0 11 0 12 0 13 3 14 3 15 3 16 . 0 17 0 18 0 19 3 20 3 21 0 22 0 23 0 24 0 25 0 26 5 27 5 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Page 206 of 614 Energy 63.49* 74. 71 77.16* 87.38 89.93 92.88* 128.40 153.68 186.'17* 198.23* 205.49 209.30 238.65* 240.95 242.24 266.29 269.81 295.39* 328.04 333.13* 338.35* 352.07* 446.57 450.03 466.47 492.17 495.38 499.55 511. 44* 567.32* 583.43* 609.37* 614.86 641.50 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 26 142 190 122 68 96 40 28 111 27 15 51 318 46 85 18 34 136 24 14 92 250 16 14 53 36 22 18 45 13 113 152 7 27 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 110 121 136 109 133 128 105 91 101 88 68 64 48 38 56 38 46 37 37 38 47 46 17 33 87 4 5 18 51 11 30 32 20 11 1. 57 1. 30 1.10 1. 62 1. 63 1. 64 2.19 0.70 1.13 1. 09 0.44 0.97 1.17 0.93 1. 45 1. 20 2.05 1. 05 1. 68 1. 69 1. 00 1. 25 0.97 1. 61 9.54 1. 81 2.23 1.18 1. 88 1. 56 1. 25 1. 25 1. 41 2.29 126.70 149.15 154.05 174.49 179.58 185.49 256.53 307.10 372.08 396.19 410.71 418.34 477.05 481. 64 484.21 532.33 539.36 590.52 655.84 666.03 676.46 7 0'3. 91 892.93 899.85 932.73 984.16 990.58 998.91 1022. 71 1134. 48 1166.70 1218.59 1229.57 1282.88 124 146 146 171 171 171 253 303 367 392 407 415 470 470 470 530 536 587 652 652 671 697 888 896 921 981 981 995 1016 1131 11*62 1212 1225 1277 7 7.25E-03 71.8 14 3.96E-02 14.5 3.25E+OO 14 5.29E-02 12.6 20 3.38E-02 17.5 1.35E+OO. 20 1.89E-02 36.7 20 2.67E-02 26.7 9 1.12E-02 48.1 7 7.79E-03 59.8 11 3.07E-02 20.6 10 7.46E-03 70.5 7 4.19E-03 95.1 7 1.42E-02 29.3 22 8.85E-02 6.8 1.07E+OO 22 1. 28E-02 31. 5 22 2.37E-02 20.9 6 5.06E-03 58.2 7 9.31E-03 37.6 9 3.79E-02 12.0 19 6.79E-03 48.3 1.26E+OO 19 3.78E-03 94.7 11 2.54E-02 18.2 13 6.95E-02 8.5 8 4.36E-03 53.0 10 3.84E-03 80.0 26 1.48E-02 50.9 14 1.0lE-02 18.6 1.99E-01 14 6.14E-03 30.1 11 5.llE-03 49.1 16 1.26E-02 44.3 7 3.49E-03 57.7 10 3.14E-02 13.4 14 4.22E-02 11.5 8 1: 94E-03116. 9 14 7.50E-03 32.0 Peak Search Report (continued) Page : 2 Sample ID : R405245008 Acquisition date : 3-0CT-2016 04:35:39 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 662 ."03 83 30 1. 66 1323. 94 1318 12 2.32E-02 17.1 36 0 701.54 20 19 4.72 1402.97 1395 13 5.52E-03 50.9 37 0 728. 46 35 28 1. 67 1456.83 1449 14 9.84E-03 35.8 38 0 768.73 25 38 2.82 1537.40 1529 19 6.94E-03 62.4 39 0 821.13 15 4 *0.67 1642.22 1638 8 4.24E-03 34.0 40 0 835.83 7 10 0.92 1671. 65 1666 8 1.99E-03 85.1 41 0 855.60 17 10 0.89 1711.20 1704 13 4.84E-03 44.0 42 0 860.70 36 9 1. 61 1721. 40 1717 9 9.93E-03 43 0 870.81 12 9 0.55 1741.63 1734 10 3.33E-03 56.5 44 0 911. 52 100 15 1. 93 1823.06 1817 12 2.78E-02 12. 6 45 0 922.00* 15 3 3.15 1844.03 1838 12 4.13E-03 36.3 46 0 935.22 8 18 1.18 1870.48 1863 11 2.22E-03111.1 47 0 965.17* 19 7 1. 23 1930.40 1924 10 5.23E-03 37.0 48 0 969.22* 57 17 1. 46 1938.50 1934 13 1. 58E-02 20 .1 49 0 1082.13 11 15 3.92 2164.42 2156 13 3. 03E-03 81. 4 50 0 1085.82 10 1 1. 32 2171.79 2169 6 2.70E-03 37.4 51 0 1120.85* 38 14 1. 00 2241. 88 2235 15 1.04E-02 28.2 52 0 1222.18 8 19 2.48 2444.63 2438 12 2 .15E-03116. 3 53 0 1272.81 15 5 4.23 2545.95 2540 11 4:14E-03 39.8 54 0 1289.24 5 14 0.64 2578.83 2571 13 1.25E-03172.5 55 0 1299.15 9 5 0.76 2598.65 2592 9 2. 36E-03 56. 6' 56 0 1461.17* 358 0 1. 69 2922.86 2915 14 9.93E-02 5.3 57 0 1730.00 11 2 1. 46 3460.84 3456 8 3.0lE-03 38.0 58 0 1764.69* 31 0 2.15 3530.26 3524 12 8.60E-03 *19.5 Flag: "*" = Peak area was modified by background subtraction Page 20Tof 614 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 05:39:46 . DKAl 0 0: [CANBERRA .-GAMMA. ARCHIVE. GAMMA] R4 0 5 2 4 5 0 0 8 . CNF; 1 PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 15-DEC-2015 12:20:00 R405245008 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 04:35:39 153.25 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA30 0 01:00:00.00 1. 50 keV No Empirical 75.00 Interference Report Interfering Page 208 of 614 Nuclide PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:01.40 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : R405245008 Acquisition date 3-0CT-2016 04:35:39 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Ef f pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.307E+OO 1.215E+Ol l.215E+Ol 10.67 OK MN-54 834.85 99.98* 2.109E+OO 1.708E-02 3.272E-02 170.22 OK NB-94 702.65 99.81* 2.428E+OO 4.209E-02 4.209E-02 101.83 OK 871. 09 99.89 2.038E+OO 2. 956E-0.2 2.956E-02 113. 04 OK RH-101 127.23 68.00* 7.332E+OO 4.911E-02 5.811E-02 96.13 OK 198.01 73.00 6.055E+OO 3.534E-02 4.182E-02 141.07 OK 325.23 11. 80 4.299E+OO Line Not Found Absent CD-109 88.03 3.70* 6.561E+OO 2.265E+OO 3.516E+OO 49 .11 OK SN-126 64.28 9.60 3. 911E+OO 4.476E-01 4.476E-01 143.59 OK 86.94 8.90 6.561E+OO 9.416E-01 9.416E-01 49 .11 OK 87.57 37.00* 6.561E+OO 2.265E-01 2.265E-01 49 .11 OK BA-137M 661.66 89.90* 2.540E+OO l.886E-01 1. 922E-01 34.16 OK CS-137 661.66 85.10* 2.540E+OO l.993E-01 2.030E-01 34.16 OK TL-208 277.37 6.60 4.820E+OO Line Not Found Absent 583.19 85.00* 2.799E+OO 2. 485E-:01* 2.485E-01 26.79 OK 860. 56 12.50 2.058E+OO 6.977E-01 6.977E-01 45.20 OK BI-211 72.87 1. 23 5.213E+OO Line Not Found Absent 351.06 12.92* 4.059E+OO 2.077E-03 2.077E-03******* OK PB-212 '74. 82 10.28 5.429E+00 1.083E+OO 1.083E+OO 44.47 OK 77*.11 17.10 5.697E+OO L 238E+00 1.238E+OO 25.15 OK 238.63 43.60* 5.357E+OO 7.797E-01 7.797E-01 13.69 OK 300.09 3.30 4.556E+OO Line Not Found Absent BI-214 609.32 45.49* 2.708E+OO

  • 6. 430E-01 6.432E-01 23.00 OK 1120.29 14.92 l.645E+00 7.457E-01 7.460E-01 56.45 OK 1764.49 15.30 1.122E+OO 8.354E-01 8.357E-01 38.95 OK PB-214 74.82 5.80 5.442E+OO Line Not Found <<INT Reject 77 .11 9.70 5.697E+OO 2.182E+OO 2.182E+OO 25.15 OK 87.09 3.41 6.542E+OO Line Not Found <<INT Reject 242.00 7.25 5.302E+OO 1.266E+OO l.266E+OO 41. 89 .OK 295.22 18.42 4.608E+OO 8.999E-01 9.002E-01 24.01 OK 351. 93 35.60* 4.060E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.708E+OO 6.430E-01 6.432E-01 23.00 OK 1120.29 14.92 1.645E+OO 7.457E-01 7.460E-01 56. 45 OK 1764.49 15.30 1.122E+OO 8.354E-01 8.357E-01 38.95 OK RA-224 240.99 4.10* 5. 321E+OO L 205E+OO 1. 205E+OO 62.94 OK RA-226 609.32 45.49* 2.708E+OO 6.430E-01 6.432E-01 23.00 OK 1120.29 14.92 1.645E+OO 7.457E-01 7.460E-01 56.45 OK 1764.49 15.30 l.122E+OO 8.354E-01 8.357E-01 38.95 OK AC-228 105.21 1.10 7.278E+OO Line Not Found Absent 338.32 11. 27 4.178E+OO 1.075E+OO 1.075E+OO 36.31 OK 794.95 4.25 2.197E+OO Lin.e Not Found Absent 835. 71 1. 61 2.109E+OO 1.061E+OO 1.061E+OO 170.22 OK 911.20 25.80*' 1. 962E+OO 9.867E-01 9.867E-01 25.27 OK 968. 97 15.80 1.863E+oo. 9.599E-01 9.599E-01 40.12 OK RA-228 105.21 1.10 7.278E+OO Line Not Found Absent 338.32 11.27 4.178E+OO 1.075E+OO 1. 07 5E+OO* 36.31 OK 794.95 4.25 2.197E+OO Line Not Found Absent 835. 71 1. 61 2.109E+OO 1.061E+OO 1. 061E+OO 170.22 OK 911.20 25.80* 1. 962E+OO 9.867E-01 9.867E-01 25.27 OK Page 209of614 Nuclide Line Activity Report (continued) Page : 3 Sample ID : R405245008 Acquisition date 3-0CT-2016 04:35:39 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status 968. 97 15.80 l.863E+OO 9.599E-01 9.599E-01 40.12 OK TH-228 74.82 10.28 5 .. 429E+OO l.083E+OO l.083E+OO 44.47 OK 77 .11 17.10 5.697E+OO 1.238E+OO 1.238E+OO 25.15 OK 238.63 43.60* 5.357E+OO 7.797E-01 7.797E-01 13.69 OK 300.09 3.30 4.556E+OO Line Not Found Absent TH-230 609.32 45.49* 2.708E+OO 6.430E-01 6.430E-01 23.00 OK 1120.29 14.92 1.645E+OO 7.457E-01 7.457E-01 56.45 OK 1764.49 15.30 l.122E+OO 8.354E-01 8.354E-01 38 .*95 OK TH-232 105.21 1.10 7.278E+OO Line Not Found Absent 338.32 11. 27 4.178E+OO 1.075E+OO 1. 075E+00 36.31 OK 835.71 1. 61 2.109E+OO 1.061E+OO 1.061E+00 170.22 OK 911.20 25.80* l.962E+OO 9.867E-01 9.867E-01 25.27 OK 968. 97 15.80 1.863E+OO 9.599E-01 9.599E-01 40.12 OK TH-234 63.29 3.70* 3. 911E+OO l.161E+OO l .161E+OO 143.59 OK 92.59 4.23 6.875E+OO 2.063E+OO 2.063E+00 53.47 OK U-234 609.32 45.49* 2.708E+OO 6.430E-01 6.430E-01 23.00 OK 1120.29 14.92 1.645E+OO 7.457E-01 7.457E-01 56.45 OK 1764.49 15.30 1.122E+OO 8.354E-01 8.354E-01 38.95 OK U-235 89. 96 3.47 6.718E+OO 1.826E+OO 1.826E+OO 73.46 OK 93.35 5.60 6.875E+OO 1.558E+OO 1.558E+OO 53.47 OK 143.76 10.96* 7 .121E+OO Line Not Found Absent 163.33 5.08 6.750E+OO Line Not Found Absent 185. 72 57.20 6.289E+00 1.798E-01 1. 798E-01 41. 28 OK 205.31 5.01 5.919E+OO 2.949E-01 2.949E-01 190.14 OK U-238 63.29 3.70* 3. 911E+OO 1.161E+OO 1.161E+OO 143.59 OK 92.59 4.23 6.875E+OO 2.063E+OO 2.063E+OO 53.47 OK AM-243 43.53 5.90 8.765E-01 Line Not Found Absent 74.66 67.20* 5.429E+OO l.657E-01 1.657E-01 44.47 OK ANH-511 511. 00 100.00* 3.089E+OO 7.775E-02 7.775E-02 88.62 OK Flag: "*" = Keyline Page 210of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:39:47.91 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245008.CNF;l *
  • Acquisition date 3-0CT-2016 04:35:39 Sensitivity : 3.000 *
  • Detector ID , GAM30 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.40 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:20:00 Analyst initials: MXRl *
  • Sample ID R405245008 Sample Quantity 1.5325E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date ll-MAR-2016 05:58:49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM30 CAN.CNF;7 . *. Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 MN-54 NB-94 RH-101 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Activity (pCi/GRAM 1.215E+Ol 3. 272E-02 4.209E-02 5. 811E-02 *3. 516E+OO 2.265E-01 1.922E-01 2.030E-01 2.485E-01 2.077E-03 7.797E-01 6.432E-01 9. 531E-01 6.432E-01 l.205E+OO 6 .-432E-01 9.867E-01 9.867E-01 7.797E-01 6.430E-01 9.867E-01 1.161E+OO 6.430E-01 3.623E-02 l.161E+OO l.657E-01 7.775E-02 Cnt uncert ( 1. 96-sigma) 1.270E+OO 5.458E-02 4.201E-02 5.474E-02 1.692E+OO l.090E-01 6.432E-02 6.795E-02 6.525E-02 6.950E-01 1.046E-01 1.450E-01 l.587E-01 1.450E-01 7.432E-01 1.450E-01 2.444E-01 2.444E-01 1.046E-01 l.449E-01 2.444E-01 1.634E+OO 1.449E-01 1. 490E-01 1 .. 634E+OO 7.221E-02 6.753E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 211 of 614 Key-Line Activity (pCi/GRAM -3.910E+00 2.047E-02 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 8.235E+OO 3.501E-02 1. 960E+41 MDA (pCi/GRAM 3.705E-01 7.373E-02 3.708E-02 4.419E-02 1. 42 6E+OO 9.227E-02 4.640E-02 4.901E-02 5.420E-02 2.561E-01 *7.143E-02 9.089E-02 2.729E-01 9.089E-02 7.652E-01 9.089E-02 1.616E-01 1.616E-01 7.143E-02 9.086E-02 l.616E-01 1.594E+OO 9.085E-02 2.855E-01 1.594E+OO 6.542E-02 4.201E-02 MDA (pCi/GRAM l.549E+Ol 7.466E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -8.719E-03 2.125E-02 4.149E-02 NOT IDENT. SC-46 4. 351E-02 2. 631E-01 5.348E-01 FAIL ABUN V-48 O.OOOE+OO 8.330E+03 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 2.635E+02 O.OOOE+OO SHORT HLIF C0-56 9.365E-02 3.160E-01 6.569E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -1.007E-02 3.789E-02 7.049E-02 NOT IDENT. C0-58 -4.636E-02 4.034E-01 7.803E-01 NOT IDENT. FE-59 -1.699E+OO 5.572E+OO 9.989E+OO NOT IDENT. C0-60 -2.156E-02 2.915E-02 5.178E-02 NOT IDENT. ZN-65 3. 968E-02 l.349E-01 2.526E-01 NOT IDENT. GE-68 1.282E-01 1.908E+OO 3.483E+OO NOT IDENT. AS-73 3.426E+OO 5.666E+OO 1.184E+Ol NOT IDENT. AS-74 O.OOOE+OO 3.627E+03 O.OOOE+OO SHORT HLIF SE-75 l.405E-01 1.446E-01 2.885E-01 NOT IDENT. BR-77 O.OOOE+OO 2.337E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 4.454E+02 O.OOOE+OO SHORT HLIF RB-83 2.836E-01 4.446E-01 9.637E-01 NOT IDENT. KR-85 5.739E+OO 5.947E+OO 1.273E+Ol NOT IDENT. SR-85 5.600E-01 5.825E-01 1.246E+OO NOT IDENT. RB-86 O.OOOE+OO 1. 793E+04 O.OOOE+OO SHORT HLIF Y-88 -2.717E-02 1.228E-01 2.827E-01 NOT IDENT. Y-91 8.980E+Ol 3.834E+02 7.663E+02 NOT IDENT. NB-95 1.502E-01 6.558E-01 l.196E+00 NOT IDENT. NB-95M -5.338E-01 1. 988E+OO 3.286E+OO NOT IDENT. ZR-95 4. 441E-02 1.099E+OO 2.152E+OO NOT IDENT. NB-97 O.OOOE+OO l.835E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.014E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.688E+41 O.OOOE+OO SHORT HLIF RH-102 -3.449E-02 4.743E-02 8.346E-02 NOT IDENT. RU-103 2.905E+OO 2.635E+OO 5.942E+OO FAIL ABUN RH-106 -1.830E-01 3.254E-01 5.937E-01 NOT IDENT. RU-106 -1.830E-01 3.254E-01 5.937E-01 NOT IDENT. AG-108M 1.677E-03 1.889E-02 3.868E-02 FAIL ABUN AG-110M 3.085E-02 6.544E-02 1. 428E-01 NOT IDENT. SN-113 1.159E-01 l.663E-01 3.576E-01 NOT IDENT. CD-115 O.OOOE+OO 2.668E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 5.498E+04 O.OOOE+OO SHORT HLIF TE-123M 4.559E-02 1.018E-01
  • 1. 989E-01 NOT IDENT. SB-124 1. 834E-01 . 1.077E+OO 2.664E+00 NOT IDENT. SB-125 -4.942E-02 8.336E-02 l.550E-01 NOT IDENT. TE-125M -7.246E+Ol l.849E+02 3.369E+02 NOT IDENT. I-126 O.OOOE+OO 4.635E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 5.674E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 4.648E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 1.850E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.473E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 7.413E+25 O.OOOE+OO SHORT HLIF BA-133 l.862E-02 3.032E-02 6.054E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-134 4.428E-02 4.583E-02 9.800E-02 NOT IDENT. CS-135 9.437E-02 l.350E-01 2.255E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF .CS-136 O.OOOE+OO 1. 893E+05 O.OOOE+OO SHORT HLIF CE-139 -8.007E-02 8.755E-02 l.497E-01 NOT IDENT. BA-140 O.OOOE+OO 6.285E+05 O.OOOE+OO SHORT*HLIF LA-140 O.OOOE+OO 1.924E+05 O.OOOE+OO SHORT HLIF CE-141 -5.936E+OO 1. 7 52E+Ol 3.198E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 7.252E-02 2.833E-01 5.492E-01 *NOT IDENT. PM-144 -3.216E-02 4.882E-02 7.745E-02 NOT IDENT. PR-144 -2.783E+OO 4.225E+OO 6.703E+OO NOT IDENT. PM-146 l.021E-03 3.583E-02 6.482E-02 NOT IDENT. ND-147 O.OOOE+OO 1.653E+07 O.OOOE+OO SHORT HLIF PM-147 4.447E+02 6. 28'1E+02 l.271E+03 NOT IDENT. PM-149 O.OOOE+OO 3.970E+39 O.OOOE+OO SHORT HLIF EU-150 1. 887E-02 3.503E-02 3.598E-02 FAIL ABUN EU-152 2.827E-02 7.040E-02 l.472E-01 FAIL ABUN GD-153 -4.664E-02 1.289E-01 2.388E-01 NOT IDENT. EU-154 5.241E-02 8.661E-02 1.852E-01 NOT IDENT. EU-155 6.361E-02 8.243E-02 1. 678E-01 FAIL ABUN TB-160 -3.478E-02 1. 089E+OO 2.189E+OO FAIL ABUN H0-166M 1.352E-02 8.421E-02 NOT IDENT. TM-171 -6.732E+00 1.388E+Ol 2.671E+Ol NOT IDENT. HF-172 -7.864E-02 1.798E-01 3.0lBE-01 FAIL ABUN LU-172 -2.036E-02 6.756E-02 l.216E-01 FAIL ABUN LU-176 -l.822E-02 1. 967E-02 3.139E-02 FAIL ABUN Page 212 of 614 HF-181 -6.783E-01 2.835E+OO 5.505E+OO NOT IDENT. TA-182 5.347E-01 1.219E+OO 1.556E+OO FAIL ABUN RE-183 5.669E-01 1.723E+00 3.542E+OO NOT IDENT. RE-184 l.103E+Ol 2.154E+01 4.517E+Ol NOT IDENT. W-188 5.016E+Ol 7.594E+01 1.523E+02 FAIL ABUN IR-192 -2. 441E-01 3.176E-01. 5.934E-Ol FAIL ABUN HG-203 -3.068E-02 1.886E+OO 3.430E+OO NOT IDENT. BI-207 l.634E-02 3.859E-02 8.016E-02 FAIL ABUN PB-210 6.192E-01 2.030E+OO 4.191E+OO NOT IDENT. PB-211 -6.223E-01 5.380E-01 9.360E-01 NOT IDENT. BI-212 0.000E+OO 8.089E-01 l.076E+OO FAIL ABUN RN-219 l.924E-01 2.769E-01 5.975E-01 FAIL ABUN. RA-223 2.142E-01
  • 4.675E-01 9.051E-01 FAIL ABUN AC-227 -2.918E-02 l.850E-01 3.346E-01 FAIL ABUN TH-227 -2.918E-02 1.850E-01 3.346E-Ol FAIL ABUN TH-229 4.778E-01 4.062E-01 8.276E-Ol FAIL ABUN PA-231 2.423E-01 3.508E-01 6. 941E-01 NOT IDENT. TH-231 2.142E-01 4.675E-01 9. 051E-01 FAIL ABUN PA-233 9.276E-03 4.407E-02 9. 096E-02 NOT IDENT. PA-234 -1.176E-01 2.065E-01 3.591E-01 NOT IDENT. PA-234M -2.237E+OO 3.336E+OO 5.617E+OO NOT IDENT. NP-237 9.276E-03 4.407E-02 9. 096E-02 NOT IDENT. NP-238 O.OOOE+OO 3.502E+40 O.OOOE+OO SHORT HLIF NP-239 -6.840E-02 1.685E-01 3.121E-01 NOT IDENT. PU-239 O.OOOE+OO 4.986E+02 5.107E+02 FAIL ABUN AM-241 -4.540E-02 9.022E-02 1. 720E-01 NOT IDENT. CM-243 -4.864E-02 7.603E-02 l.384E-01 NOT IDENT, BK-247 6.926E-02 7. 897E-02 . l.096E-01 FAIL ABUN CM-247 l.714E-02 2.577E-02 5.532E-02 NOT IDENT. CF-249 -1.530E-02 2.665E-02 5.022E-02 FAIL ABUN CF-251 -1.160E-01 9.376E-02 1.534E-01 NOT IDENT. Page 213of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:39:45.30 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 346 10.66* 1.307E+OO 1.215E+Ol 1.215E+Ol 10.67 MN-54 834.85 7 99.98* 2.109E+OO 1.708E-02 3.272E-02 170.22 NB-94 702.65 21 99.81* 2.428E+OO 4.209E-02 4.209E-02 101.83 871.09 12 99.89 2.038E+OO 2.956E-02 2.956E-02 113. 04 RH-101 127.23 50 68.00* 7.332E+OO 4. 911E-02 5. 811E-02 96.13 198.01 32 73.00 6.055E+OO 3.534E-02 4.182E-02 141.07 325.23 ------11. 80 4.299E+OO ------Line Not Found ------CD-109 88.03 156 3.70* 6.561E+OO 3.142E+OO 4.878E+00 34.91 SN-126 64.28 34 9.60 3. 911E+OO 4.476E-01 4.476E-01 143.59 86.94 156 8.90 6.561E+OO 1.306E+OO 1.306E+OO 34.91 87.57 156 37.00* 6.561E+OO 3.142E-01 3.142E-01 34.91 BA-137M 661.66 88 89.90* 2.540E+OO 1.886E-01 1.922E-01 34.16 CS-137 661.66 88 85.10* 2.540E+OO 1.993E-01 2.030E-01 34.16 TL-208 277.37 ------6.60 4.820E+OO ------Line Not Found ------583.19 121 85.00* 2.799E+OO 2.485E-01 2.485E-01 26.79 860.56 37 12.50 2.058E+OO 6.977E-01 6. 977E'-01 45.20 BI-211 72. 87 ------1. 23 5.213E+OO ------Line Not Found ------351. 06 281 12.92* 4.059E+00 2.625E+OO 2.625E+OO 16.99 PB-212 74.82 185 10.28 5.429E+OO 1.620E+OO 1.620E+OO 28.90 77 .11 246 17.10 5.697E+OO 1.238E+OO 1.238E+OO 25.15 238.63 372 43.60* 5.357E+OO 7.797E-01 7.797E-01 13.69 300.09 ------3.30 4.556E+OO ------Line Not Found ------BI-214 609.32 162 45.49* 2. 708E+OO . 6.430E-01 6.432E-01 23.00 1120. 29 37 14.92 1.645E+00 7.457E-01 7.460E-01 56.45 1764.49 29 15.30 1.122E+OO 8.354E-01 8.357E-01 38.95 PB-214 74.82 185 5.80 5.429E+OO 2. 871E+OO 2. 872E+00 28.90 77 .11 .246 9.70 5.697E+OO 2.182E+OO 2.182E+OO 25.15 87.09 156 3.41 6.561E+OO 3.409E+OO 3. 411E+00 34.91 242.00 99 7.25 5.302E+OO l.266E+OO 1.266E+00 41. 89 295.22 156 18.42 4.608E+OO 8.999E-01 9.002E-01 24.01 351.93 281 35.60* 4.059E+OO 9.528E-01 9. 531E-01 16.99 RN-222 609.32 162 45.49* 2.708E+OO 6.430E-01 23.00 1120. 29 37 14.92 1.645E+OO 7.457E-01 7.460E-01 56.45 1764.49 29 15.30 1.122E+OO 8.354E-01 8.357E-01 38.95 RA-224 240.99 54 4.10* 5.321E+OO 1.205E+OO 1.205E+OO 62.94 RA-226 609.32 162 45.49* 2.708E+OO 6.430E-01 6.432E-01 23.00 1120.29 37 14.92 1.645E+OO 7.457E-01 7.460E-01 56.45 1764.49 29 15.30 l.122E+00 8.354E-01 8.357E-01 38.95 AC-228 105.21 ------1.10 7.278E+OO ------Line Not Found ------338.32 103 11. 27 4.178E+OO 1. 075E+OO 1. 075E+OO 36.31 794.95 ------4.25 2.197E+OO ------Line Not Found ------835.71 7 1. 61 2.109E+OO 1. 061E+OO 1. 061E+OO 170.22 911.20 102 25.80* 1. 962E+OO 9.867E-01 9.867E-01 25.27 968. 97 58 15.80 1.863E+OO 9.599E-01 9.599E-01 40.12 RA-228 105.21 ------1.10 7.278E+OO ------Line Not Found ------338.32 103 11. 27 4.178E+OO 1.075E+OO 1.075E+OO 36.31 794.95 ------4.25 2.197E+OO ------Line Not Found ------Page 214of614 Nuclide Line Activity Report (continued) Page : 2 Sample ID : R405245008 Acquisition date 3-0CT-2016 04:35:39 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Eff pCi/GRAM pCi7GRAM %Error 835. 71 7 1. 61 2.109E+OO l.061E+OO 1.061E+OO 170.22 911.20 102 25'. 80* 1.962E+OO 9.867E-01 9.867E-01 25.27 968. 97 58 15.80 1.863E+OO 9.599E-01 9.599E-01 40.12 TH-228 74.82 185 10.28 5.429E+OO l.620E+00 1.620E+OO 28.90 77 .11 246 17.10 5.697E+OO l.238E+00 1.238E+OO 25.15 238.63 372 43.60* 5.357E+OO 7.797E-01 7.797E-Ol 13.69 300.09. ------3.30 4.556E+OO ------Line Not Found ------TH-230 609.32 162 45.49* 2.708E+OO 6.430E-01 6.430E-01 23.00 1120.29 37 14.92 1.645E+OO 7.457E-01 7.457E-01 56. 45. 1764.49 29 15.30 1.122E+OO 8.354E-01 8.354E-01 38.95 TH-232 105.21 ------1.10 7.278E+OO ------Line Not Found ------338.32 103 .11.27 4.178E+OO 1.075E+OO 1.075E+OO 36.31 835.71 7 1. 61 2.109E+OO 1.061E+OO 1.061E+OO 170.22 911. 20 102 25.80* 1. 962E+OO 9.867E-01 9.867E-01 25.27 968. 97 58 15.80 1.863E+OO 9.599E-01 9.599E-01 40.12 TH-234 63.29 34 3.70* . 3. 911E+OO 1.161E+OO 1.161E+OO 143.59 92.59 122 4.23 6.875E+OO 2.063E+OO 2.063E+OO 53.47 U-234 609.32 162 45.49* 2.708E+OO 6.430E-01 6.430E-01 23.00 1120.29 37 14.92 1.645E+OO '7.457E-01 7.457E-01 56.45 1764.49 29 15.30 1.122E+OO 8.354E-01 .8.354E-01 38.95 U-235 89.96 87 3.47 6.718E+OO 1. 826E+OO 1.826E+OO 73.46 93.35 122 5.60 6.875E+OO 1.558E+OO 1.558E+OO 53.47 143.76 ------10.96* 7.121E+OO ------Line Not Found ------1.63.33 ------5.08 6.750E+OO ------Line Not Found ------185 .. 72 132 57.20 6.289E+OO 1. 798E-01 1. 798E-01 41. 28 205.31 18 5.01 5.919E+OO 2.949E-01 2.949E-01 190.14 U-238. 63.29 34 3.70* 3. 911E+OO 1.161E+OO 1 .. 161E+OO 143.59 92.59 122 4.23 6.875E+OO 2.063E+OO 2.063E+OO 53.47 AM-243 43.53 ------5.90 8.765E-01 ------Line Not Found ------74.66 185 67.20* 5.429E+OO 2.478E-01 2.479E-01 28.90 ANH-511 511. 00 49 100.00* 3.089E+OO 7.775E-02 7.775E-02 88.62 Flag: "*" Key line Page 215of614 Page : 3 Summary of Nuclide Activity Sample ID : R405245008 Acquisition date 3-0CT-2016 04:35:39 Total number of lines in spectrum 58 Number of unidentified lines 15 Number of lines tentatively identified by NID 43 Nuclide Type : Nuclide K-40 MN-54 NB-94 RH-101 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-2'14 RN-222 RA-224 RA-226' AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 312.05D 20300.00Y 3.30Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y 7.04E+08Y 1. 41E+.10Y 1600. OOY 1600. O*OY 1600.00Y 1. 41E+10Y 1600. OOY 1.41E+10Y 1. 41E+10Y 1. 41E+10Y 7.54E+04Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 92 1. 00 1.18 1. 55 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.215E+Ol 1. 708E-02 4.209E-02 4. 911E-02 3.142E+OO 3.142E-01 1.886E-01 1.993E-01 2.485E-01 2.625E+00 7.797E-01 6.430E-01 9.528E-01 6.430E-01 1.205E+OO 6.430E-01 9.867E-01 9 .*8 67E-01 7.797E-01 6.430E-01 9.867E-01 1.161E+OO 6.430E-01 1. 798E-01 1.161E+OO 2.478E-01 7.775E-02 3.170E+Ol 3.170E+Ol Decay Corr pCi/GRAM 1. 215E+Ol 3.272E-02 4.209E-02 5. 811E-02 4.878E+00 3.142E-01 1.922E-01 2.030E-01 2.485E-01 2.625E+OO 7.797E-01 6.432E-01 9.531E-01 6.432E-01 1.205E+OO 6.432E-01' 9.867E-01 9.867E-01 6.430E-01 9.867E-01 1.161E+OO 6.430E-01 1.798E-01 1.161E+OO 2.479E-01 7.775E-02 3.346E+Ol 3.346E+Ol 74.14% Decay Corr 2-Sigma Error 0.130E+Ol 5.569E-02 4.287E-02 5.586E-02 1. 703E+OO 1.097E-01 0.656E-01 0.693E-01 0.666E-01 0.446E+OO 1. 067E-01 1.479E-01 1. 620E-01 1.479E-01 0.758E+OO 1.479E-01 2.494E-01 2.494E-01 1.067E-01 1. 479E-01 2.494E-01 1.668E+OO 1.479E-01 0.742E-01 1.668E+OO 0.716E-01 6. 890E-0.2 "M" Manually accepted 2-Sigma %Error 10.67 170.22 101.83 96.13 34.91 34.91 34.16 34.16 26. 79 16.99 13,69 23.00 16.99 23.00 62.94 23.00 25.27 25.27 13.69 23.00 25. 2-7 143.59 23.00 41. 28 143.59 28.90 88.62 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 216 of 614 Flags K Unidentified Energy Lines Page : 4 Sample ID : R405245008 Acquisition date : 3-0CT-2016 04:35:39 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 153.68 34 111 0.70 307.10 303 7 7.79E-03 **** 6.94E+OO T 0 209.30 60 75 0.97 418.34 415 7 1. 42E-02 58.7 5.85E+00 0 266.29 21 44 1. 20 532.33 530 6 **** 4.96E+OO T 0 *269.81 39 52 2.05 539.36 536 7 9.31E-03 75.2 4.92E+OO T 3 328.04 28 42 1. 68 655.84 652 19 6.79E-03 96. 5 4.27E+OO T 3 333 .13 15 43 1. 69 666.03 652 19 3.78E-03 **** 4.23E+OO T 0 446.57 17 19 0.97 892.93 888 8 4.36E-03 **** 3.41E+OO 0 450.03 15 36 1. 61 899.85 896 10 3.84E-03 **** 3.39E+OO 0 466.47 58 95 9.54 932.73 921 26 1.48E-02 **** 3.31E+OO 5 492.17 40 . 4 1. 81 984.16 981 14 1. OlE-02 37.3 3.18E+OO T 5 495.38 24 5 2.23 990.58 981 14 6.14E-03 60.2 3.16E+OO 0 499.55 20 19 1.18 998.91 995 11 5. llE-03 98.1 3.14E+OO 0 567.32 13 11 1. 56 1134. 48 1131 7 3.49E-03 **** 2.86E+OO 0 614.86 7* 21 1. 41 1229.57 1225 8 1.94E-03 **** 2.69E+OO T 0 641.50 29 12 2.29 1282.88 1277 14 7.50E-03 64.1 2.60E+OO 0 728.46 37 29 1. 67 1456.83 1449 14 9.84E-03 71. 6 2.36E+OO T 0 768.73 26 39 2.82 1537.40 1529 19 6.94E-03 **** 2.26E+OO 0 821.13 16 4 0.67 1642.22 1638 8 4.24E-03 68.1 2.14E+00 0 855.60 18 10 0.89 1711.20 1704 13 4.84E-03 87.9 2.07E+OO T 0 922.00 15 3 3.15 1844.03 1838 12 4.13E-03 72.6 1. 94E+OO 0 935.22 8 18 1.18 1870.48 1863 11 2.22E-03 **** 1.92E+OO 0 19 7 1.*23 1930.40 1924 10 5.23E-03 74.1 1. 87E+OO' T 0 1082 .13 11 15 3.92 2164.42 2156 13 3.03E-03 **** 1.70E+OO 0 1085.82 10 1 1. 32 2171.79 2169 6 2.70E-03 74.8 1.69E+OO T 0 1222.18 8 19 2.48 2444.63 2438 12 2.15E-03 **** 1.53E+OO T 0 1272.81 15 5 4. 23. 2545.95 2540 11 4.14E-03 79.6 1.47E+OO T 0 1289.24 4 13 0.64 2578.83 2571 13 1.25E-03 **** 1.46E+00 0 1299.15 8 4 I 0.76 2598.65 2592 9 2.36E-03 **** 1.45E+OO T 0 1730.00 10 2 1. 46 3460.84 3456 8 3. OlE-03 76.0 1. 14E+OO Flags: ,;T" = Tentatively associated Page 217 of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:40:04.33 *******************************************************************************
  • G.EL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245008.CNF;l *
  • Acquisition date 3-0CT-2016 04:35:39 Sensitivity 3.000 *
  • Detector ID GAM30 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.40 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:20:00 Nuclide Library : SOLID *
  • Sample ID R405245008 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.5325E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : O.OOOOD * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 11-MAR-2016 05:58:49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM30 CAN.CNF;7 * ******************************************************************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 MN-54 NB-94 RH-101 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1. 373E-01 3.072E-02 1. 573E-02 2.042E-02 6.678E-01 4.320E-02 2.016E-02 2.130E-02 2.423E-02 1.149E-01 3.273E-02 3.991E-02 1.317E-01 3.991E-02 3.507E-01 3.991E-02 6.745E-02 6.745E-02 3.273E-02 3.989E-02 6.745E-02 7.469E-01 3.989E-02 l.338E-01 7.469E-01 3.075E-02 1.879E-02 ----Non-Identified Nuclides Nl,lclide BE-7 NA-22 NA-24 AL-26 Page 218of614 Le (pCi/GRAM 6.829E+OO 3.169E-02 O.OOOE+OO 1. 470E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 219of614 2.294E-01 O.OOOE+OO O.OOOE+OO 2.836E-01 O.OOOE+OO 3.288E-02 3.350E-01 4.316E+OO 2.063E-02 1.078E-01 1.482E+OO 5.537E+OO O.OOOE+OO 1.313E-01 O.OOOE+OO O.OOOE+OO 4.294E-01 5.824E+OO 5.703E-01 O.OOOE+OO 1. 002E-01 3. 296E+02 5.266E-01 l.519E+00 9.461E-01 O.OOOE+OO O.OOOE+OO 'O.OOOE+OO O.OOOE+OO 3.638E-02 2.552E+OO 2.524E-01 2.524E-01 1. 716E-02 6.lOlE-02 O.OOOE+OO O.OOOE+OO 9.276E-02 9. 813E-01 6.947E-02 l.562E+02 O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.736E-02 O.OOOE+OO 4.428E-02 1. 039E-01 O.OOOE+OO O.OOOE+OO 6.914E-02 O.OOOE+OO O.OOOE+OO 1.494E+Ol O.OOOE+OO 2.568E-01 3.383E-02 2.928E+OO 2.895E-02 O.OOOE+OO 5.942E+02 0.000E+OO 1. 626E-02 6.702E-02 l.113E-01 7. 871E-02 7.872E-02 9.108E-01 3.687E-02 1.239E+Ol 1.394E-01 5.227E-02 l.404E-02 2.436E+OO FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF . NOT I DENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 220 of 614 6.822E-01 1.645E+OO 1.982E+Ol 6.939E+Ol 2.669E-01 1.577E+OO 3.476E-02 1.956E+OO 4.183E-01 4. 950E.:..01 2.705E-01 4.123E-01 1. 529E-01 1.529E-01 3.880E-01 3.186E-01 4.123E-01 4.142E-02 l.500E-01 2.366E+OO 4.142E-02 O.OOOE+OO l.439E-01 2.401E+02 7.992E-02 6.441E-02 5.015E-02 2'.506E-02 2.234E-02 7.040E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:40:10.05 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245008.CNF;l *
  • Acquisition date 3-0CT-2016 04:35:39 Sensitivity : 3.000 *
  • Detector ID' GAM30 Energy tolerance: 1. 500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.40 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:20:00 Nuclide Library : SOLID *
  • Sample ID R405245008 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.5325E+02 GRAM *
  • Quantity Err ( % ) : 1. 3051E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 11-MAR-2016 05:58:49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM30 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1. 96-sigma) K-40 1.215E+Ol 1.669E+OO 1.669E+OO MN-54 3. 272E-02 5.471E-02 5.471E-02 NB-94 4.209E-02 4.217E-02 4.217E-02 RH-101 5. 811E-02 5.583E-02 5.583E-02 CD-109 3.510E+OO 1.737E+OO l.737E+00 SN-126 2.261E-01 l .112E-01 l .112E-01 BA-137M 1.922E-01 6.607E-02 6.607E-02 CS-137 2.030E-01 6.979E-02 6.979E-02 TL-208 2.485E-01 6.835E-02 6.835E-02 PB-212 7.797E-01 1.225E-01 l.225E-01 BI-214 6.432E-01 1. 541E-01 1. 541E-01 PB-214 9.531E-01 1. 771E-01 1. 771E-01 RN-222 6.432E-01 1. 541E-01 1. 541K-01 RA-224 1.205E+OO 7.498E-01 7.498E-01 RA-226 6.432E-01 1.541E-01 1. 541E-01' AC-228 9.867E-01 2.805E-01 2.805E-01 RA-228 9.867E-01 2.805E-01 2.805E-01 TH-228
  • 7.797E-01 1.225E-01 1.225E-01 TH-230 6.430E-01 1.540E-01 l.540E-01 TH-232 9.867E-01 2.805E-01 2.805E-01 TH-234 1.161E+OO 1.655E+OO 1.655E+OO U-234 6.430E-01 l.540E-01 1.540E-01 U-235 3.623E-02 1.490E-01 1. 49.0E-01 U-238 l.161E+OO 1.655E+OO l.655E+OO AM-243 l.654E-Ol 7.418E-02 7.418E-02 ANH-511 7.775E-02 6.783E-02 6.783E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1 . 96-s gma ) BE-7 -3.910E+OO 8.241E+OO 8.428E+OO NOT IDENT. NA-22 2.047E-02 3.506E-02 3.626E-02 NOT IDENT. NA-24 1. OOOE+41 8.310E+41 O.OOOE+OO .SHORT HLIF AL-26 -8.719E-03 2.126E-02 2.162E-02 NOT IDENT. Page 221 of 614 SC-46 4.35iE-02 2.631E-01 2.639E-01 FAIL ABUN V-48 -3.699E+03 8.350E+03 8.515E+03 SHORT HLIF CR-51 -1.356E+Ol 2.635E+02 2.636E+02 SHORT HLIF C0-56 9.365E-02 3.162E-01 3.190E-01 NOT IDENT. MN-56 1.000E+41 3.250E+41 O.OOOE+OO SHORT HLIF C0-57 -1.007E-02 3.790E-02 3.817E-02 NOT IDENT. C0-58 -4.636E-02 4.034E-01 4.040E-01 NOT IDENT. FE-59 -1.699E+OO 5.582E+OO 5.635E+OO NOT IDENT. C0-60 -2.156E-02 2.920E-02 3.078E-02 NOT IDENT. ZN-65 3. 968E-02 1.351E-01 1.363E-01 NOT IDENT. GE-68 1.282E-01 1.908E+OO 1.909E+OO NOT IDENT. AS-73 3.426E+OO 5.710E+OO 5.915E+OO NOT IDENT. AS-74 1.077E+03 3.629E+03 3.662E+03 SHORT HLIF SE-75 1.405E-01 l.451E-01 1.583E-01 NOT IDENT. BR-77 1. 742E+37 1.472E+38 O.OOOE+OO SHORT HLIF SR-82 l.069E+02 4.456E+02 4.482E+02 SHORT HLIF RB-83 2.836E-01 4.467E-01 4.646E-01 NOT IDENT. KR-85 5.739E+OO 5. 966E+OO 6.502E+OO NOT IDENT. SR-85 5.600E-01 5.844E-01 6.366E-01 NOT IDENT. RB-86 1.207E+03 l.793E+04 1. 7 93E+04 SHORT HLIF Y-88 -2.717E-02 1.228E-01 l.234E-01 NOT IDENT. Y-91 8.980E+Ol 3.835E+02 3.857E+02 NOT IDENT. NB-95 1.502E-01 6.560E-01 6.595E-01 NOT IDENT. NB-95M -5.338E-01 1. 989E+OO 2.003E+OO NOT IDENT. ZR-95 4.441E-02 1.099E+OO 1.099E+OO NOT IDENT. NB-97 -1. 000E+41 1.837E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 7.018E+41 O.OOOE+OO SHORT HLIF . M0-99 -2.581E+30 2.015E+31 O.OOOE+OO SHORT HLIF TC-99M 1. 000E+41 l.692E+41 O.OOOE+OO SHORT HLIF RH-102 -3.449E-02 4.757E-02 5.005E-02 NOT IDENT. RU-103 2.905E+OO 2.647E+OO 2.953E+OO FAIL ABUN RH-106 -l.830E-01 3.259E-01 3.362E-01 NOT IDENT. RU-106 -1.830E-01 3.259E-01 3.362E-01* NOT IDENT. AG-108M l.677E-03 1.889E-02 1. 8 90E-02 FAIL ABUN AG-110M. 3.085E-02 6.556E-02 6.702E-02 NOT IDENT. SN-113 l.159E-01 1. 666E-'01 1. 746E-01 NOT IDENT. CD-115 1.009E+38 2.674E+38 O.OOOE+OO SHORT HLIF SN-117M 1.497E+04 5.501E+04 5.542E+04 SHORT HLIF TE-123M 4.559E-02 1.019E-01 1.039E-01 NOT IDENT. SB-124 1.834E-01 1.077E+OO 1.080E+OO NOT IDENT. SB-125 -4.942E-02 8.345E-02 8.638E-02 NOT IDENT. TE-125M -7.246E+Ol l.850E+02 1. 878E+02 NOT IDENT. I-126 1.735E+05 4.642E+05 4.707E+05 SHORT HLIF SB-126 l.149E+05 5.679E+05 5.702E+05 SHORT HLIF SB-127 -4.990E+20 4.697E+21 O.OOOE+OO SHORT HLIF I-131 3.013E+08 l.850E+09 1.855E+09 SHORT HLIF I-132 1.000E+41 l.810E+42 O.OOOE+OO SHORT HLIF TE-132 -6.238E+25 7.824E+25 O.OOOE+OO SHORT HLIF BA-133 1. 862E-02 3.036E-02 3.150E-02 NOT IDENT. I-133 1.000E+41 3.955E+42 0.000E+OO SHORT HLIF CS-134 4.428E-02 4.608E-02 5.022E-02 NOT IDENT. CS-135 9.437E-02 l.353E-01 l.418E-01 NOT IDENT. I-135 -1.000E+41 2.020E+42 O.OOOE+OO SHORT HLIF CS-136 -2.097E+05 1.940E+05 2.159E+05 SHORT HLIF CE-139 -8.007E-02 8. 911E-02 9.615E-02 NOT IDENT. BA-140 -3.339E+05 6.291E+05 6.469E+05 SHORT HLIF LA-140 -3.947E+04 l.924E+05 1. 932E+05 SHORT HLIF CE-141 -5.936E+OO 1.753E+Ol 1.773E+Ol NOT IDENT. CE-143 1.000E+41 1.142E+42 O.OOOE+OO SHORT HLIF CE-144 7.252E-02 2.833E-01 2.852E-01 NOT IDENT. PM-144 -3.216E-02 4.892E-02 5.102E-02 NOT IDENT. PR-144 -2.783E+OO 4.232E+OO 4.414E+OO NOT IDENT. PM-146 1. 021E-03 3.583E-02 3.584E-02 NOT IDENT. ND-147 -1.077E+07 l.655E+07 1. 725E+07 SHORT HLIF PM-147 4.447E+02 6.289E+02 6. 601E+02 NOT IDENT. PM-149 -2.528E+39 4. 011E+39 O.OOOE+OO SHORT HLIF EU-150 1.887E-02 3.507E-02 3.608E-02 FAIL ABUN EU-152 2.827E-02 7.044E-02 7.159E-02 FAIL ABUN GD-153 -4.664E-02 1.289E-01 l.306E-01 NOT IDENT. EU-154 5.241E-02 8.674E-02 8.990E-02 NOT IDENT. EU-155 6.361E-02 8.261E-02 8.744E-02 FAIL ABUN TB-160 -3.478E-02 1. 089E+OO 1. 089E+OO FAIL ABUN H0-166M 1.352E-02 4.050E-02 4. 096E-02 NOT IDENT. TM-171 -6.732E+OO 1.389E+Ol l.422E+O:L NOT IDENT. HF-172 -7.864E-02 1.803E-01 1.838E-01 FAIL ABUN LU-172 -2.036E-02 6.770E-02 6.832E-02 FAIL ABUN LU-176 -l.822E-02 1.973E-02 2.137E-02 FAIL ABUN HF-181 -6.783E-01 2.836E+OO 2.852E+OO NOT IDENT. Page 222 of 614 TA-182 5.347E-01 1.220E+OO 1.243E+OO FAIL ABUN RE-183 5.669E-01 1. 725E+OO 1.744E+OO NOT IDENT. RE-184 1.103E+Ol 2.174E+Ol 2.230E+Ol NOT IDENT. W-188 5.016E+Ol* 7.622E+Ol 7.951E+Ol FAIL ABUN IR-192 -2. 441E-01 3.183E-01 3.367E-01 FAIL ABUN HG-203 -3.068E-02 1.886E+OO 1. 886E+OO NOT IDENT. BI-207 l.634E-02 3.870E-02 3.940E-02 FAIL ABUN PB-210 6.192E-01 2.031E+OO 2.0SOE+OO NOT IDENT. BI-211 2.625E+OO 4.898E-01 1. 281E+OO FAIL ABUN PB-211 -6.223E-01 5.407E-01 *6.091E-01 NOT IDENT. BI-212 1.152E+OO .8.164E-01 9.677E-01 FAIL ABUN RN-219 l.924E-01 2.783E-01 2.915E-01 FAIL ABUN RA-223 2.142E-01 4.679E-01 4.778E-01 E:'AIL ABUN AC-227 -2.918E-02 1. 851E-01 l.855E-01 FAIL ABUN TH-227 -2.918E-02 l.851E-01 1.855E-01 FAIL ABUN TH-229 4.778E-01 4.077E-01 4. 611E-01 FAIL ABUN PA-231 2.423E-01 3.SSOE-01 3.714E-01 NOT IDENT. TH-231 2.142E-01 4.679E-01 4.778E-01 FAIL ABUN PA-233 9.276E-03 4.408E-02 4.428E-02 NOT IDENT. PA-234 -1. l 76E-01 2.470E-01 2.527E-01 NOT IDENT. PA-234M -2.237E+OO 3.356E+OO 3.504E+OO NOT IDENT. NP-237 9.276E-03 4.408E-02 4.428E-02 NOT IDENT. NP-238 2.516E+39 3.502E+40 O.OOOE+OO SHORT HLIF NP-239 -6.840E-02 l.686E-01 1.714E-01 NOT IDENT. PU-239 5.293E+02 4.999E+02 5.539E+02 FAIL ABUN AM-241 -4.540E-02 9.029E-02 9.258E-02 NOT IDENT. CM-243 -4.864E-02 7.620E-02 7.929E-02 NOT IDENT. BK-247 6.926E-02, 8.033E-02 8.618E-02 FAIL ABUN ' CM-247 1. 714E-02 2.596E-02 2.708E-02 NOT IDENT. CF-249 -l.530E-02 2.670E-02 2.758E-02 FAIL ABUN CF-251 -1.160E-01 9.486E-02 1.083E-01 NOT IDENT. Page 223 of 614
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 48.1902 87.09 72.4828 136.47 58.0729 45.60 53.0822 87.57 72.5367 140.51 0.0000 46.54 53.1977 88.03 72.5883 143.76 61. 8123 49. 72 0.0000 88.34 72.6229 144.24 59.6762 51. 35 58.4877 88.47 72.6378 145.44 74.9665 51. 87 63.2754 89. 96 72.8036 152.43 68.6105 52.39 65.2368 1093.63 72.8789 153.25 0.0000 52.97 54.9045 91.11 0.0000 323.87 54 .1164 53.44 56.8542 92.59 73.0937 156.02 0.0000 54.07 52.1856 93.35 73.1766 158.56 0.0000 57.36 0.0000 94.56 63.8050 159.00 54.0252 57.53 56.3807 94.65 63.8137 162.33 65.2767 57.98 50.6927 94.67 63.8156 162.66 0.0000 59.27 80.5502 94.87 69.2669 163.33 50.9463 59.32 80.5582 97.43 67.4819 165.86 68.8456 59.54 68.1204 98.43 71.6748 176.31 52.7387 60.96 65.4242 98.44 71. 6759 176.60 '0.0000 61.17 65.4509 99.53 56.4049 177.52 68.5291 62.93 74.3649 100 .11 56.4515 181.07 0.0000 63. 29 74.4160 102.03 71. 0136 181.52 48 .1191 63.58 74.4569 103.18 70.0975 184.41 52.7763 64.28 74.5556 103.37 75.2718 143.76 55.4839 66.73 62.2515 105.21 58.9239 193.51 49.0462 67.24 76.5894 105.31 58.9322 197.03 49.2043 125.81 82.8217 106.12 72.4535 198.01 49.2483 67.75 82.8321 106.47 78.7014 201.83 50.5675 69.67 86.0543 109.28 60.2911 203.43 55.2429 70.83 91.1318 111. 00 70.8492 205.31 49.-1869 . 72. 81 93.0885 111.76 0.0000 210.85 50.9710 72.87 93.0979 114.06 57.5362 215.65 44.2031 74.66 81.8779 116. 30 0.0000 222 .11 61.9905 74.82 81. 9001 116.74 55.6376 227.09 50.5028 74.97 81. 9210 119.76 61.1219 227.38 48.1657 77 .11 82.2192 121.12 52.7817 228.16 0.0000 78.74 82.4434 121.22 52.7885 228.18 63.4798 79.69 82.2409 121. 78 65.5037 116.74 63.4798 80.12 78.3168 122.06 70.8113 235.69 52.0412 80-.19 0.0000 122.92 55.0171 235. 96 52.0526 80.57 82.3601 123.07 58.2021 238.63 40.3086 81. 00 83.7469 265.00 65.6593 238.98 0.0000 81. 07 83.7565 125.81 59.4611 240.99 40.3843 81. 75 85.1803 127.23 49.6371 242.00 40.4165 83.79 74.7772 127.91 55.3559 244.70 38.1201 84.00 73.4665 129.30 55.4492 252.40 0.0000 85.43 96.3926 131.20 64.1254 252.80 39.5591 86.55 72.4219 133. 02 61. 0513 254.15 0.0000 86.79 72.4488 133.52 60.0161 256.23 40.8647 86.94 72.4658 136. 00 56. 9659 260.90 0.0000 Page 224 of 614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 19.3530 355.39 0.0000 584.27 24.0112 264.80 19.3550 356.01 20.5693 595.83 0.0000 265.00 19.3579 364.49 0.0000 427.87 19.3400 268.22 31.5312 366.42 0.0000 602.52 0.0000 269.46 42.0797 372. 51 32.0227 604.72 14.5294 270.03 42.0977 375.05 26.8696 607.14 20.3617 271.23 32. 4113 377.52 29.5120 609.32 17.4683 273.65 0.0000 356.01 22.6506 610.33 17.4756 276.40 42.7000 388.16 *29.6926 614.28 18. 9620 277.37 37.8456 388.63 0.0000 618.01 8.7649 277.60 35.4101 391. 69 22.7511 620. 36 13.6468 278.00 37.8636 264.66 28.1419 621.93 16.5822 279.20 44.0079 401.81 21.1201 0.0000 279.54 44.0189 402.40 22.0072 631.29 24.4761 279.70 35.4632 404.85 41.4291 633.25 10.7780 280.46 36.7062 410.95 25.6482 634.78 0.0000 283.69 28.2060 413.71 21. 2578 635.95 14.7125 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 41. 7467 423.72 0.0000 645.85 16.2469 285.90 0.0000 427.09 28.5475 657.76 19.2897 287.50 33.2004 427.87 33.9141 657.90 0.0000 290.67 24.6478 433.94 19.6971 661. 66 14.8602 293.27 0.0000 439.40 21. 5488 664.57 0.0000 351.93' 27.1979 453.88 23.0663 666.33 0.0000 295.96 27.2120 19.9952 666.50 0.0000 879.38 31.3907 468.07 20.0418 667.71 0.0000 299.98 36.3820 473.00 0.0000 677.62 14.9506 300.09 36.3847 475.06 15.0830 685.70 0.0000 300.13 35.9721 476.78 25.6171 695.00 0.0000 301.36 29.7949 477.60 24.7121 696.49 21.0786 302.85 42.2520 482.18 22.9324 696.51 21.0786 256.23 34.8351 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 22.5906 306.78 39. 8721 497.08 2.7716 697.49 19.5801 308.46 28.6903 505.52 14.8408 702.65 10.5628 311. 90 31.6736 507.63 0.0000 706.68 10.8809 316.51 38.4578 511. 00 24.1780 711. 68 13 .1211 319.41 0.0000 514.00 24.2110 720.70 0.0000 320.08 0.0000 514.00 24.2110 721. 93 0.0000 321.04 43.6031 520.40 14.9434 722.78 15.2002 323.87 27. 7216 520.69 0.0000 722.91 18.2410 325.23 35.3136 522.65 0.0000 723.31 18.2439 328.76 0.0000 527.90 0.0000 724.19 18.2498 333.37 26.6230 528.26 17.8086 727. 33 14. 2096 333.97 26.6326 529.59 16.8816 733.00 3. 0511 334.37 17.7598 529.87 0.0000 735.93 17.3078 338.28 19.0750 531.02 0.0000 333.97 8.1491 338.32 19.0755 537.26 0.0000 739.50 0.0000 311. 90 24.1947 546.56 0.0000 747.24 10.2214 . 340.48 24.1947 552.55 18.9494 748.06 9.2018 340.55 0.0000 563. 2.5 14.2786 752.31 14.33-SO 344.28 28.9324 569.33 15.7474 753.82 0.0000 345.93 31.6872 946.00 14.3170 756.73 17.4337 351.06 25.6348 569.70 14.3182 756.80 19.4855 351.93 25.6482 583.19 24.0000 884.68 10.7948 Page 225of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 15.4309 1274.44 14.3595 1620.50 0.9555 766.42 14.4050 1001.03 16.5906 1621.92 2.8674 766.84 14.4073 1002.74 8.8525 1678.03 0.0000 772.60 0.0000 1004.73 13.2861 1690.97 1.9364 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 0.9811 778.90 7.2333 1028.54 0.0000 1063.66 4.9106 783.70 0.0000 1037.84 8.9382 1771.35 0.9823 785.37 12.4268 1038.76 0.0000 1791.20 0.0000 792.07 21.7955 631. 29 6.7197 1808.65 3.9551 794.95 13.5057 1048.07 0.0000 1810.72 0.0000 *795.86 16.6276 1049.04 13. 4482 1836.06 1.9869 810.06 10.4411 1050.41 12.3320 810.29 9.3977 1063.66 10.1257 344.28 8.3538 1077.00 0.0000 810.76 13.5761 1077.34 8.4686 815.77 0.0000 1085.87 10.1851 1048.07 0.0000 1093.63 15.8753 832.01 12 .. 6187 1099.45 17.0349 834.85 8.4202 1112. 07 14. 8112 835.71 11. 0546 1112.84 9. 1165 836.80 0.0000 1115.54 8.5529 846.75 0.0000 1120.29 7.9924 846.77 10.5652 1120.55 7.9929 856.80 0.0000 1221.41 7.9941 860.56 12.7334 1129. 67 11. 4445 871.09 12.7754 1131.51 0.0000 873.19 15.9796 1147.95 0.0000 875.33 0.0000 1173.23 10.4128 879.38 8.5387 1177.95 12.7420 880.51 9.6094 1189.05 11. 6146 883.24 12.8232 1204.77 10.4934 884.68 7.4836 1221.41 14.9248 889.28 10.7060 1231. 02 14.0791 894.76 10.7239 1235.36 0.0000 898.04 13.9548 1238.28 12.3406 900.72 16.1145 1260*. 41 0.0000 903.28\ 11.8267 1271. 87 7.1069 911.20 8.6217 1274.44 5.6891 912.08 8.6240 1274.54 5.6891 923.98 0.0000 1291.59 8.5670 926.50 6.4958 1298.22 0.0000 92 9 .11 6.5007 1312 .11 0.0000 937.49 17.9213 1332.49 10.8076 944.13 0.0000 1362.66 0.0000 946.00 14.1547 1365.19 6.3502 949.00 3.2694 1368.63 0.0000 667. 71 0.0000 1384.29 1.8219 962.31 9.8459 1408.01 2.7468 964.08 11. 4929 1457.56 0.0000 966 .17 6. 5713 1460.82 2.7773 911.20 4.9323 1489.16 4.6558 968.97 4.9323 1505.03 8. 40*73 983.53 0.0000 1584.12 5.6931 984.45 0.0000 1596.21 0.0000 Page 226of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:40:41.02 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245009.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM32.CNF;277 Background date : Z-OCT-2016 11:01:57. Sample date 15-DEC-2015 12:31:00 Acquisition date : 3-0CT-2016 04:36:09. Sample *ID R405245009 Sample quantity 1. 39119E+02 GRAM Detector name : GAM32 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.52 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596387 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 1 1 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 227of614 Energy 62.96* 75.35 77.51 87.47 90.31 93 .13* 130.17 186.20* 238.91* 242.26 248.18 270.49 295.42* 300.57 338.80 352.25* 464.93 476.46 583.51* 590.97 609.73* 647..93 661. 84 680.85* 728. 93* 769.32 837.69 861.25* 893.50 912.02* 935.85 989.09 1120.99* 1461.21* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 41 91 102 31 27 48 21. 82 270 73 12 42 100 36 80 201 20 18 110 12 120 17 91 14 32 16 15 12 9 58 21 20 23 280 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 100 147 118 143 61 119 91 104 171 65 69 64 58 37 39 45 38 33 32 11 28 7 26 14 19 1 14 8 10 37 19 0 11 7 2.53 1. 29 1.17 1. 03 1.18 1.15 1. 62 1. 39 1.11 1. 59 0.45 0. 72 1. 09 1. 98 1. 52 i.75 2 .11 3.32 1. 38 1. 27 1. 32 1. 29 1. 23 1. 44 1. 34 1. 03 1. 41 0.75 0.52 1. 68 5.09 4.16 0.74 2.00 127.13 151.91 156.23 176.14 181. 84 187.47 2 61. 5 6 373.61 479.04 485.74 497.59 542.21 592.06 602.36 678.82 705.73 931.08 954.16 1168. 25 1183 .19 1220.70 1297.11 1324. 92 1362.94 1459 .11 1539.90 1676.64 1723.75 1788.25 1825.30 1872. 95 1979.45 2243.26 2923.71 124 146 146 174 180 180 256 368 473 483 492 536 586 598 674 698 923 945 1160 1177 1213 1293 1319 1357 1451 1538 1669 1720 1781 1819 1861 1974 2238 2918 9 1.13E-02 48. 2 14 2.51E-02 25.8 8.19E-01 14 2.83E-02 21.0 7 8.61E-03 66.0 17 7.45E-03 40.5 1.02E+OO 17 1. 32E-02 42. 9 8 5.73E-03 85.1 11 2.29E-02 27.4 11 7:49E-02 11.3 7 2.02E-02 22.1 9 3.42E-03125.4 12 1.17E-02 41.4 10 2.78E-02 17.8 9 1. OlE-02 34. 6 11 2.21E-02 18.8 14 5.59E-02 10.1 10 5.67E-03 60.3 14 4.92E-03 74.3 16 3.06E-02 15.1 9 3.27E-03 59.0 16 3.34E-02 13.7 8 4.75E-03 37.0 13 2.53E-02 15.6 11 3.89E-03 59.6 16 8.86E-03 36.6 5 4.47E-03 26.8 15 4.24E-03 60.5 8 3.29E-03 52.7 11 2.56E-03 76.2 12 1. 62E-02 25. 3 19 5.83E-03 54.3 12 5.56E-03 22.4 11 6.31E-03 36.l 13 7.78E-02 6.3 Peak Search Report (continued) Sample ID : R405245009 Pk It Energy Area Bkgnd 35 0 1539.57 7 0 36 0 1621.95 10 0 37 0 1764.67* 31 0 FWHM 0.73 0.98 2.12 Acquisition date Channel Left Pw 3080.43 3077 6 3245.20 3240 9 3530.65 3525 11 Page : 2 3-0CT-2016 04:36:09 Cts/Sec %Err Fit l.94E-03 37. 8. 2.78E-03 31. 6 8.62E-03 18.9 Flag: "*" = Peak area was modified by background subtraction Page 228of614 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 05:40:43 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245009.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID.V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 15-DEC-2015 12:31:00 R405245009 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 04:36:09 139.12 GRAM *sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA32 0 01:00:00.00 1.50 keV No Linear 75.00 erence Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93* Page 229 of 614 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.52 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : R405245009 Acquisition date 3-0CT-2016 04:36:09 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status BE-7 477.60 10.4'4* 2.742E+OO 3.520E-01 1.593E+Ol 148.62 OK K-40 1460.82 10.66* 1.119E+OO l.214E+Ol 1.214E+Ol 12.66 OK CD-109 88.03 3.70* 4.574E+OO 4.569E-01 7.091E-01 347.08 OK SN-126 64.28 9.60 2.071E+OO 1.352E+OO 1.352E+OO 96. 47 OK 86.94 8.90 4.574E+OO l.899E-01 l.899E-01 347.08 OK 87.57 37.00* 4.574E+OO 4.569E-02 4.569E-02 347.08 OK BA-137M 661.66 89.90* 2.105E+OO 2.661E-01 2. 711E-01 31. 20 OK CS-137 661. 66 85.10* 2.105E+OO 2.812E-01 2.864E-01 31. 20 OK TL-208 277.37 6.60 4.277E+OO Line Not Found Absent 583.19 85.00* 2.327E+OO 3.120E-01 3.120E-01 30.16 OK 860.56 12.50 1. 713E+OO 2.998E-01 2.998E-01 105.30 OK BI-211 72.87 1.23 3.214E+OO Line Not Found Absent 351.06 12.92* 3.521E+OO 4.026E-01 4.026E-01 232.30 OK PB-212 74.82 10.28 3.478E+OO 1.210E+OO 1.210E+OO 71.77 OK 77*_ 11 17.10 3.697E+OO 1.052E+OO 1.052E+00 41. 92 OK 238.63 43.60* 4.789E+OO 7.757E-01 7.757E-01 22. 67 OK 300.09 3.30 4. OllE+OO l.626E+00 1.626E+OO 69.15 OK BI-214 609.32 45.49* 2.246E+OO 6.550E-01 6.552E-01 27.44 OK 1120. 29 14.92 1.392E+OO 5.783E-01 5.785E-01 72 :11 OK 1764.49 15.30 9.462E-01 1.089E+OO 1.090E+OO 37.89 OK PB-214 74.82 5.80 3.423E+OO Line Not Found <<INT Reject 77 .11 9.70 3.697E+00 1.854E+OO 1.855E+00 41. 92 OK 87.09 3.41 4.545E+00 Line Not Found <<INT Reject 242.00 7.25 4.745E+OO Line Not Found <<INT Reject 295.22 4.067E+OO 7.895E-01 7.898E-01 35.68 OK 351.93 35.60* 3.524E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.246E+OO 6.550E-01 6.552E-01 27.44 OK 1120.29 14.92 1.392E+OO 5.783E-01 5.785E-01 72.11 OK 1764.49 15.30 9.462E-01 1.089E+OO 1.090E+OO 37.89 OK RA-224 240.99 4.10* 4.741E+OO 8.469E-01 8.469E-01 130.88 OK RA-226 609.32 45.49* 2.246E+OO 6.550E-01 6.552E-01 27.44 OK 1120.29 14.92 1. 392E+OO 5. 783E-Cll 5.785E-01 72 .11 OK 1764.49 15.30 9.462E-01 1.089E+OO 1.090E+OO 37.89 OK TH-228 74.82 10.28 3.478E+OO 1.210E+OO 1.210E+OO 71.77 OK 77 .11 17.10 3.697E+OO 1.052E+OO 1.052E+OO 41. 92 OK 238.63 43.60* 4.789E+OO 7.757E-01 7.757E-01 22.67 OK 300.09 3.30 4. OllE+OO 1.626E+OO 1. 626E+OO 69.15 OK TH-230 609.32 45.49* 2.246E+OO 6.550E-01 6.550E-01 27.44 OK 1120.29 14.92 l.392E+OO 5*. 7 83E-01 5.783E-01 72.11 OK 1764.49 15.30 9.462E-01 l.089E+OO 1.089E+OO 37.89 OK PA-231 283.69 1. 70 4.201E+OO Line Not Found Absent 301.36 5.35* 4.0llE+OO l.003E+00 l.003E+00 69.15 OK TH-234 63.29 3.70* 2. 071E+OO .3.508E+OO 3.508E+OO 96.47 OK ' 92. 59 4.23 . 4. 971E+OO 1.459E+OO 1.459E+OO 85.87 OK U-234 609.32 45.49* 2.246E+OO 6.550E-01 6.550E-01 27.44 OK 1120.29 14.92 1.392E+OO 5.783E-01 5.783E-01 72 .11 OK 1764.49 15.30 9.462E-01 1.089E+OO 1.089E+OO 37.89 OK U-235 89. 96 3.47 4.783E+OO 1.042E+OO l.042E+00 80.99 OK 93.35 5.60 4.971E+OO 1.102E+OO 1.102E+OO 85.87 OK Page 230of614 Nuclide Line Activity Report (continued) Sample ID : R405245009

  • Acquisition date Nuclide Type: Nuclide U-238 AM-243 Energy 143.76 163.33 185. 72 205.31 63. 29 92.59 43.53 74.66 Flag: "*" = Keyline Page 231of614 %Abn 10. 96* 5.08 57.20 5.01 3.70* 4.23 5.90 67.20* Uncorrected Decay Corr %Ef;f pCi/GRAM pCi/GRAM 6.095E+OO Line Not Found 5.924E+OO -----Line Not Found 5.602E+OO 1.574E-01 1.574E-01 5.302E+OO -----. Line Not Found 2.071E+OO 3.508E+OO 3.508E+OO 4.971E+OO 1.459E+OO 1.459E+OO l.701E-01 Line Not Found 3.478E+OO l.851E-01 1. 851E-Ol Page : 3 3-0CT-2016 04:36:09 2-Sigma %Error Status Absent Absent 54.78 OK Absent 96. 47 OK 85.87 OK Absent 71.77 OK VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:40:44.73 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 . * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245009.CNF;l *
  • Acquisition date 3-0CT-2016 04:36:09 Sensitivity : 3.000 *
  • Detector ID GAM32 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.52 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:31:00 Analyst initials: MXRl *
  • Sample ID R405245009 Sample Quantity 1.3912E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
  • E'ff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
  • Combined Activity-MDA Report NOTE: Not all Identified Nuclides" are valid. Please refer to of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide* (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 1.593E+Ol 2.320E+Ol 2.254E+Ol K-40 1.214E+Ol 1.506E+OO 6.359E-01 CD-109 7.091E-01 2.412E+OO 2.671E+00 SN-126 4.569E-02 1.554E-01 1.734E-01 BA-137M 2.711E-01 8.289E-02 5.983E-02 CS-137 2.864E-01 8.756E-02 6.320E-02 TL-208 3.120E-01 9.221E-02 5.926E-02 BI-211 4.026E-01 9.166E-01 3.383E-01 PB-212 7.757E-01 1.723E-01 l.245E-01 BI-214 6.552E-01 1.762E-01 l .151E-Ol PB-214 9.360E-01 1.856E-01 3.073E-01 RN-222 6.552E-01 1. 762E-01 1.151E-01 RA-224 8.469E-01 1.086E+OO 1.112E+OO RA-226 6.552E-01 1. 762E-01 l .151E-01 TH-228 7.757E-01 1.723E-01 1.245E-01 TH-230 6.550E-01 1. 761E-01 l.150E-01 PA-231 l.003E+OO 6.794E-01 8.047E-01 TH-234 3.508E+OO 3.317E+OO 3.189E+OO U-234 6.550E-01 1. 7 61E-01 l.150E-01 U-235 l.278E-01 1. 752E-Ol 3.622E-01 U-238 3.508E+OO 3.317E+OO 3.189E+OO AM-243 l.851E-01 l.302E-01 l.139E-01 Non-Identified Nuclides Nuclide NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 232 of 614 Key-Line Activity (pCi/GRAM 2. 726E-02 O.OOOE+OO -7.971E-03 3:357E-01 O.OOOE+OO O.OOOE+OO 2.388E-03 -2.663E-01 K.L. Cnt Uncert MDA (1. 96-sigma). (pCi/GRAM 4.208E-02 l.960E+41 3.494E-02 4.104E-01 8.869E+03 3.203E+02 6.494E-02 4.683E-01 9.653E-02 O.OOOE+OO 6.916E-02 8.265E-01 O.OOOE+OO O.OOOE+OO 1.117E-01 7.932E-01 NOT IDENT. SHORT HLIF NOT 'IDENT. FAIL ABUN SHORT' HLIF SHORT HLIF NOT IDENT. NOT IDENT.

MN-56 O.OOOE+OO 1. 771E+41 O.OOOE+OO SHORT HLIF C0-57 -2. 271E-03 5.369E-02 9.577E-02 NOT IDENT. C0-58 3.072E-03 5.371E-01 1.032E+OO NOT IDENT. FE-59 -2.852E+OO 5.919E+OO l.101E+Ol NOT IDENT. C0-60 1.087E-02 3. 313E-02 7.484E-02 NOT IDENT. ZN-65 5.159E-02 l.098E-01 2.474E-01 NOT IDENT. GE-68 8.988E-Ol 2. 396E+OO 5.098E+OO NOT IDENT. AS-73 -3.439E+OO 1.441E+Ol 2.639E+Ol NOT IDENT. AS-74 O.OOOE+OO 4.428E+03 O.OOOE+OO SHORT HLIF SE-75 -2.089E-02 1.929E-01 3.552E-01 NOT IDENT. BR-77 0.000E+OO 3.842E+36 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 5.537E+02 0.000E+OO SHORT HLIF RB-83 1.804E-02 5.658E-01 l.107E+OO NOT IDENT. KR-85 -2.830E+Ol 1.095E+Ol 1.493E+Ol NOT IDENT. SR-85 -2.776E+OO l.073E+OO 1.462E+OO NOT IDENT. RB-86 O.OOOE+OO 2.375E+04 0.000E+OO SHORT HLIF Y-88 -2.870E-02 1. 481E-01 3.262E-01 NOT IDENT. Y-91 1.081E+02 5.702E+02 1.14 7E+03 NOT IDENT. NB-94 -3.lOOE-02 3.104E-02 4.743E-02 NOT IDENT. NB-95 5.086E-01 8.389E-01 1.608E+00 NOT IDENT. NB-95M 2.394E+OO 2.423E+OO 4.624E+OO NOT IDENT. ZR-95 l.230E+OO 1.256E+OO 2.822E+OO NOT IDENT. NB-97 O.OOOE+OO 9.780E+40 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 6.087E+40 O.OOOE+OO SHORT HLIF M0-99 0.000E+OO 3.267E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF RH-101 l.074E-02 3.946E-02 6.696E-02 NOT IDENT. RH-102 -4.306E-02 6.404E-02 1.091E-01 FAIL ABUN RU-103 -l .116E+OO 4.919E+OO 9.197E+OO FAIL ABUN RH-106 -8.046E-02 4.323E-01 8.168E-01 NOT IDENT. RU-106 -8.046E-02 4.323E-01 8.168E-01 NOT IDENT. AG-108M -2.460E-03 2.976E-02 5.643E-02 NOT IDENT. AG-llOM 3.590E-03 9.854E-02 1.900E-01 NOT IDENT. SN-113 1. 917E-02 2.158E-01 4.213E-01 NOT IDENT. CD-115 O.OOOE+OO 2.916E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 6.746E+04 O.OOOE+OO SHORT HLIF TE-123M l.029E-01 1. 2 66E-01 2.622E-01 NOT IDENT. SB-124 -1. 464E-01 2.070E+OO 4.284E+OO NOT IDENT. SB-125 7.467E-02 l.023E-01 2.144E-01 NOT IDENT. TE-125M .9.634E+Ol 2.909E+02 5.390E+02 NOT IDENT. I-126 O.OOOE+OO 6.584E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 7.638E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.515E+21 O.OOOE+OO SHORT HLIF* I-131 O.OOOE+OO 2.692E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 8.294E+25 O.OOOE+OO SHORT HLIF BA-133 -3.108E-03 4.507E-02 7. 716E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 2. 8 65E-03 5.395E-02 l.024E-Ol NOT IDENT. CS-135 -1. 598E-02 1.575E-01 2.699E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.402E+05 O.OOOE+OO SHORT HLIF CE-139 -2.330E-02 l .119E-01 2.153E-01 NOT IDENT. BA-140 O.OOOE+OO 9.048E+05 O.OOOE+OO SHORT HLIF LA-:-140 O.OOOE+OO 2.098E+05 O.OOOE+OO SHORT HLIF CE-141 1.068E+OO 2. 013E+Ol 3.982E+Ol NOT IDENT. CE-143 O.OOOE+OO l.522E+41 O.OOOE+OO SHORT HLIF CE-144 1.lOOE-01 3.555E-01 6.580E-01 NOT IDENT . PM-144 . -1.103E-02 6.246E-02 1.142E-01 FAIL ABUN PR-144 -9.873E-01 5.400E+OO 9.865E+OO NOT IDENT. PM-146 4.710E-03 4.180E-02 8.209E-02 NOT IDENT. ND-147 O.OOOE+OO 1.988E+07 O.OOOE+OO SHORT HLIF PM-147 2.399E+02 9.339E+02 l.714E+03 NOT IDENT. PM-149 O.OOOE+OO 4.536E+39 0.000E+OO SHORT HLIF EU-150 -6.151E-03 2.936E-02 4.913E-02 FAIL ABUN EU-152 l.512E-02' 8.901E-02 1.690E-01 NOT IDENT. GD-153 7.509E-02 2.154E-01 3.727E-01 NOT IDENT. EU-154 8.372E-02 1.017E-01 2.405E-01 NOT IDENT. EU-155 l.717E-OI 1.336E-01 2.646E-01 FAIL ABUN TB-160 5.577E-02 1. 736E+OO 3.348E+OO FAIL ABUN HQ-166M -1.553E-02 5.126E-02 9.367E-02 NOT IDENT. TM-171 -3.239E+Ol 3.893E+Ol 6.707E+Ol NOT IDENT. HF-172 -2.922E-02 2. 696E-01 4.384E-01 FAIL ABUN LU-172 1.815E-03 5.625E-02 1.204E-01 FAIL ABUN LU-176 1.709E-02 2.428E-02 5.0lOE-02 FAIL ABUN HF-181 -2.315E+OO 3.646E+OO 6.404E:+oo NOT IDENT. TA-182 6.416E-01 8.935E-01 1.970E+OO FAIL ABUN RE-183 5.889E-01 4.234E+OO 7.997E+OO NOT IDENT. Page 233of614 RE-184 -6.637E+OO 2.181E+Ol 3.983E+Ol FAIL ABUN W-188 3.910E+Ol 1.002E+02 1.857E+02 FAIL ABUN IR-192 -4.607E-02 4.508E-01 8.594E-01 FAIL ABUN HG-203 8.268E-01 2.023E+OO 4.083E+OO NOT IDENT. BI-207 -l.226E-02 4.759E-02 9.283E-02 FAIL ABUN PB-210 -1.255E+OO 8.573E+OO l.590E+Ol NOT IDENT. PB-211 -4.274E-03 7.059E-01 1.350E+OO NOT IDENT. BI-212 8.229E-01 5.425E-01 1.225E+OO FAIL ABUN RN-219 6.176E-02 3. 967E-01 7.736E-01 FAIL ABUN RA-223 3.619E-01 5.686E-01 1.171E+OO FAIL ABUN AC-227 -1. 77 4E-02 2.245E-01 4.325E-01 FAIL ABUN TH-227 -1. 77 4E-02 2.245E-01 4.325E-01 FAIL ABUN AC-228 O.OOOE+OO 3.703E-01 5.950E-01 FAIL ABUN RA-228 O.OOOE+OO 3.703E-01 5.950E-01 FAIL ABUN TH-229 l.lOlE-01. 4.582E-01 9.090E-01 FAIL ABUN TH-231 3.619E-01 5.686E-01 l. l 71E+OO FAIL ABUN TH-232 O.OOOE+OO 3.703E-01 5.950E-01 FAIL ABUN PA-233 3.504E-02 5.833E-02 1. 196E-01 FAIL ABUN PA-234 -l.849E-01 2.482E-01 4.442E-01 FAIL ABUN PA-234M -1.640E+OO 3.307E+OO 6.338E+OO NOT IDENT. NP-237 3.504E-02 5.833E-02 1.196E-01 FAIL ABUN NP-238 O.OOOE+OO 4.437E+40 0.000E+OO SHORT. HLIF NP-239 l.512E-01 2. 572E-01 4.901E-01 NOT IDENT. PU-239 3.370E+02 5.622E+02 6.677E+02 FAIL ABUN AM-241 1. 97 5E-02 2.272E-01 3.923E-01 NOT IDENT. CM-243 -l.577E-01 1.269E-01 2.031E-01 NOT IDENT. BK-247 5.209E-03 7.533E-02 1.330E-01 NOT *I DENT. CM-247 -l.545E-02 , 3. 669E-02 6.689E-02 NOT IDENT. CF-249 2.531E-02 3.452E-02 7. 28*2E-02 NOT IDENT. CF-251 -9.790E-02 1.164E-01 2.129E-01 NOT IDENT. ANH-511 -7.453E-03 5.072E-02 1.061E-01 NOT IDENT. Page 234 of 614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:40:41.92 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area. %Abn %Eff pCi/GRAM pCi7GRAM %Error BE-7 477.60 19 10.44* 2.742E+OO 3.520E-01 1.593E+Ol 148.62 K-40 1460.82 268 10.66* 1.119E+OO 1.214E+Ol 1.214E+Ol 12.66 CD-109 88.03 37 3.70* 4.574E+OO l.184E+OO 1.839E+OO 132.06 SN-126 64.28 50 9 .'60 2. 071E+OO l.352E+OO 1.352E+OO 96. 47 86.94 37 8.90 4.574E+OO 4.924E-01 4.924E-01 132.06 87.57 37 37.00* 4.574E+OO 1.184E-01 1.184E-01 132. 0.6 BA-137M 661. 66 93 89.90* 2.105E+OO 2.661E-01 2. 711E-01 31. 20 CS-137 661. 66 93 85.10* 2.105E+OO 2.812E-01 2.864E-01 31. 20 TL-208 277.37 ------6.60 4.277E+OO ------Line Not Found ------583.19 114 85.00* 2.327E+OO 3 .'120E-01 3.120E-01 30.16 860.56 12 12.50 1.713E+OO 2.998E-01 2.998E-01 105.30 BI-211 72.87 ------1. 23 3.214E+OO ------Line Not Found ------351.06 217 12.92* 3. 521E+OO 2.578E+OO 2.578E+OO 20.24 PB-212 '74.82 110 10.28 3.478E+00 1.655E+OO 1. 655E+OO 51. 57 77 .11 123 17.10 3.697E+OO 1.052E+OO 1.052E+OO 41. 92 238.63 300 43.60* 4.789E+OO 7.757E-01 7.757E-01 22.67 300.09 40 3.30 4.0llE+OO 1.626E+OO 1. 626E+00 69.15 BI-214 609.32 124 45.49* 2.246E+OO 6.550E-01 6.552E-01 27.44 1120.29 22 14.92 1.392E+OO 5.783E-01 5.785E-01 72.11 1764.49 29 15.30 9.462E-01 1.089E+OO 1.090E+00 37.89 PB-214 74.82 110 5.80 3.478E+OO 2.934E+OO 2.935E+OO 51. 57 77 .11 123 9.70 3.697E+OO 1.854E+OO 1.855E+OO 41. 92 87.09 37 3.41 4.574E+OO 1.285E+OO 1. 286E+OO 132.06 242.00 81 7.25 4. 741E+OO 1. 268E+OO 1. 2 69E+OO 44.14 295.22 110 18.42 4.067E+OO 7.895E-01 7.898E-01 35.68 351. 93 217 35.60* 3. 521E+OO 9.356E-01 9.360E-01 20.24 RN-222 609.32 124 45.49* 2.246E+OO 6.550E-01 6.552E-Ol. 27.44 1120.29 22 14.92 1.392E+OO 5.783E-01 5.785E-01 72 .11 1764.49 29 15.30 9.462E-01 l.089E+OO 1.090E+OO 37.89 RA-224 240.99 81 4.10* 4.741E+OO 2.243E+OO 2.243E+OO 44.14 RA-226 609.32 124 45.49* 2.246E+OO 6.550E-01 6.552E-01 27.44 1120.29 22 14.92 1.392E+OO 5.783E-01 5.785E-01 72 .11 1764.49 29 15.30 9.462E-01 1. 089E+OO 1.090E+OO 37.89 TH-228 74.82 110 10.28 3.478E+OO 1.655E+OO 1.655E+OO 51. 57 77 .11 123 17.10 3.697E+OO 1.052E+OO 1.052E+OO 41. 92 238.63 300 43.60* 4.789E+OO 7.757E-01 7.757E-01 22.67 300.09 40 3.30 4. OllE+OO 1. 626E+OO 1.626E+OO 69.15 TH-230 609.32 124 45.49* 2.246E+OO 6.550E-01 6.550E-01 27.44 1120.29 22 14.92 1.392E+OO 5.783E-01 5.783E-01 72.11 1764.49 29 15.30 9.462E-01 1.089E+OO 1.089E+OO .37. 89 PA-231 283.69 ------1.70 4.201E+OO ------Line Not Found ------301.36 40 5.35* 4. OllE+OO 1.003E+OO 1.003E+OO 69.15 TH-234 63.29 50 3.70* 2.071E+OO 3.508E+OO 3.508E+OO 96. 47 92.59 57 4.23 4. 971E+OO 1.459E+OO 1.459E+OO 85.87 U-234 609.32 124 45.49* 2.246E+OO 6.550E-01 6.550E-01 27. 44 1120.29 22 14.92 1.392E+OO 5.783E-01 5.783E-01 72 .11 1764.49 29 15.30 9.462E-01 1.089E+OO 1.089E+OO 37.89 Page 235of614 Nuclide Line Activity Report (continued) Page. : 2 Sample ID : R405245009 Acquisition date 3-0CT-2016 04:36:09 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error U-235 89.96 32 3.47 4.783E+OO 1.042E+OO l.042E+OO 80.99 93.35 57 5.60 4.971E+OO l.102E+OO 1.102E+OO 85.87 143.76 ------10.96* 6.095E+OO ------Line Not Found ------163.33 ------5.08 5.924E+OO ------Line Not Found ------185. 72 93 57.20 5.602E+OO l.574E-01 l.574E-01 54.78 205.31 ------5.01 5.302E+OO ------Line Not Found ------U-238 63.29 50 3.70* 2.071E+OO 3.508E+OO 3.508E+OO 96. 47 92.59 57 4.23 4.971E+OO l.459E+OO 1.459E+OO 85.87 AM-243 43.53 ------5.90 1.701E-01 ------Line Not Found ------74.66 110 67.20* 3.478E+OO 2.532E-01 2.532E-01 51. 57 Flag: "*" Key line Page 236of614 Summary of Nuclide Activity Sample ID : R405245009 Acquisition date Page : 3 3-0CT-2016 04:36:09 Total number of lines in spectrum 37 Number of unidentified lines 10 Number of lines tentatively identified by NID 27 Nuclide Type : Nuclide BE-7 K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-230 PA-231 TH-234 U-234 U-235 U-238 AM-243

  • Hlife 53.22D 1. 25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 7.04E+08Y l.41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1.41E+10Y 1600. OOY l.41E+l0Y 7.54E+04Y 7.04E+08Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y Decay 45.2 1. 00 1. 55 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Tota.l Activity Grand Total Activity Uncorrected pCi/GRAM 3.520E-01 l.214E+Ol 1.184E+OO 1.184E-01 2.661E-01 2.812E-01 3.120E-01 2.578E+OO 7.757E-01 6. 550E-O.l 9.356E-01 6.550E-01 2.243E+OO 6.550E-01 7.757E-01 6.550E-01 1.003E+OO 3.508E+OO 6.550E-01 l.574E-01 3.508E+00 2.532E-01 3.367E+Ol 3.367E+Ol Decay Corr pCi/GRAM 1.593E+Ol 1.214E+Ol l.839E+OO 1.184E-01 2.711E-01 2.864E-01 3.120E-01 2.578E+OO 7.757E-01 6.552E-01 9.360E-01 6.552E-01 2.243E+OO 6.552E-01 7.757E-01 6.550E-01 1.003E+OO 3.508E+OO 6.550E-01 l.574E-01 3.508E+OO 2.532E-01 4.991E+Ol 4. 991E+Ol 72.97% Decay Corr 2-Sigma Error 2.367E+Ol 0.154E+Ol 2.428E+OO l.564E-01 0.846E-01 0.894E-01 0. 941E-01 0.522E+OO 1. 758E-01 1.798E-01 1.894E-01 1.798E-01 0.990E+OO 1.798E-01 1. 758E-01 . 1. 7 97E-01 0.693E+00 3.385E+OO 1. 797E-01 0.862E-01 3.385E+OO 1.306E-01 "M" Manually accepted 2-Sigma %Error 148.62 12.66 132.06 132.06 31.20 31.20 30.16 20.24 22.67 27.44 20.24 . 27.44 44.14 27.44 22.67 27.44 69.15 96. 47 27 .. 44 54.78 96. 47 51. 57 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 237 of 614 Flags K Unidentified Energy Lines Page : 4 Sample ID : R405245009 Acquisition date : 3-0CT-2016 04:36:09 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 130.17 24 106 1. 62 261.56 256 8 5.73E-03 **** 6.09E+OO T 0 248.18 14 76 0.45 497.59 492 9 3.42E-03 **** 4.66E+OO 0 270.49 46 70 0. 72 542.21 536 12 l.17E-02 82.8 4.36E+OO T 0 338.80 86 42 1. 52 678.82 674 11 2.21E-02 37.6 3.64E+OO T 0 464.93 22 40 2 .11 931. 08 923 10 5.67E-03 **** 2.80E+OO 0 590.97 12 12 1. 27 1183 .19 1177 9 3.27E-03 **** 2.30E+OO 0 647.93 18 7 1. 29 1297 .11 1293 8 4.75E-03 74.0 2.14E+OO 0 680.85 14 14 1. 44 1362.94 1357 11 3.89E-03 **** 2.06E+OO 0 728.93 32 19 1. 34 1459.11 1451 16 8.86E-03 73.3 1. 95E+OO 0 769.32 16 1 .1. 03 1539.90 1538 5 4.47E-03 53.6 1.87E+OO 0 837.69 15 14 1. 41 1676.64 1669 15 4.24E-03 **** 1. 7 5E+OO T 0 893.50 9 10 0.52 1788.25 1781 11 2.56E-03 **** 1.66E+OO T 0 912.02 58 37 1. 68 1825.30 1819 12 1. 62E-02 50.7 1. 64E+OO T 0 935.85 21 19 5.09 1872.95 1861 19 5.83E-03 **** 1.60E+OO 0 989.09 20 0 4.16 1979.45 1974 12 5.56E-03 44.7 1.54E+OO 0 1539.57 7 0 0.73 3080.43 3077 6 1. 94E-03 75.6 1.07E+OO 0 1621.95 9 0 0.98 3245.20 3240 9 2.78E-03 63.2 1. 02E+OO T Flags: "T" = Tentatively associated Page 238 of 614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:40:59.41 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245009.CNF;l *
  • Acquisition date 3-0CT-2016 04:36:09 Sensitivity : 3.000 *
  • Detector ID GAM32 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.52 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:31:00 Nuclide Library : SOLID *
  • Sample ID R405245009 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.3912E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll'
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide BE-7 K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-230 PA-231 TH-234 U-234 U-235 U-238. AM-243 Le (pCi/GRAM 1.009E+Ol 2.566E-01 1.266E+OO 8.217E-02 2.591E-02 2.738E-02 2.586E-02 1.527E-01 5.865E-02 5.025E-02 l.477E-01 5.025E-02 5 .171E-01 5.025E-02 5.865E-02 5.023E-02 3.672E-01 l.496E+OO 5.023E-02 1.697E-01 1.496E+OO 5.357E-02 ----Non-Identified Nuclides Nuclide NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 Page 239of614 Le *(pCi/GRAM 4.102E-02 O.OOOE+OO 2.668E-02 3.635E-01 O.OOOE+OO O.OOOE+OO 4.777E-02 3.376E-01 O.OOOE+OO NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLI'F SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115
  • SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 cs-Us I-135 CS-136
  • CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 Page 240 of 614 4.476E-02 4.435E-01 4.626E+OO 3.068E-02 9.981E-02 2.213E+OO 1.222E+Ol 0.000E+OO l.619E-01 O.OOOE+OO O.OOOE+OO 4.852E-01 6.761E+OO 6.621E-01 O.OOOE+OO 1.090E-01 5.045E+02 2. OOlE-02 7.102E-01 2.162E+00 1.240E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.129E-02 4.749E-02 4.055E+OO' 3.499E-01 3.499E-01 2.542E-02 8.135E-02 1.898E-01 O.OOOE+OO O.OOOE+OO 1.228E-01 l.688E+OO 9. 696E-02 2.526E+02 O.OOOE+OO O.OOOE+OO *o.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.493E-02 O.OOOE+OO 4.499E-02 1.242E-01 O.OOOE+OO O.OOOE+OO l.006E-01 O.OOOE+OO O.OOOE+OO 1.858E+Ol O.OOOE+OO 3.060E-01 5.065E-02 4.374E+OO 3.659E-02 O.OOOE+OO 8.017E+02 O.OOOE+OO 2.240E-02 7.628E-02 1. 746'E-01 l.024E-01 1.250E-01 1.433E+OO 3.993E-02 3.097E+Ol 2.042E-01 4.910E-02 2.301E-02 2.792E+OO 8.618E-01 3. 721E+OO 1.629E+Ol NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. .NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT* IDENT. FAIL ABUN NOT IDENT. FAIL ABUN W-188 IR-192 HG-203 BI-207 PB-210 PB_:..211 BI-212 RN-219 RA-223 AC-227 TH-227 AC-228 RA-228 TH-229 TH-231 TH-232 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-24'9 CF-251 ANH-511 Page 241of614 8.450E+Ol 3.928E-01 1. 872E+OO 3.950E-02 7.410E+OO 6 .119E-01 5.555E-01 3.509E-01 5.355E-01 1.988E-01 1.988E-01 2.802E-01 2.802E-01 4.232E-Ol 5.355E-01 2.802E-01 5.478E-02 l.834E-01 2.592E+OO 5.478E-02 O.OOOE+OO 2.288E-Ol 3.140E+02 9.478E-02 6.084E-02 3.014E-02 3.291E-02 9.876E-02 5.017E-02 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.* NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. .NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Ge.nerated 03-0CT-2016 05: 41: 05. 78 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245009.CNF;l *
  • Acquisition date 3-0CT-2016 04:36:09 Sensitivity : 3.000 *
  • Detector ID GAM32 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.52 Half life ratio : ***** * *. Sample date 15-DEC-2015 12: 31: 00 Nuclide Library : SOLID *
  • Sample ID R405245009 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : l.3912E+02 GRAM *
  • Quantity Err(%) : l.4376E-03 % * *Wet wt*corr 1.00000 Wet Weight 0.00000
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. 'Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to .Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) BE-7 l.593E+Ol 2.32J:E+Ol K-40 l.214E+Ol l.634E+OO CD-109 7.091E-01 2.417E+OO SN-126 4.569E-02 l.557E-01 BA-137M 2.711E-01 8. 371E-02 CS-137 2.864E-01 8.842E-02 TL-208 3.120E-01 9.316E-02 BI-211 4.026E-01 9. 2 65E-01 PB-212 7.757E-01 1. 772E-01 BI-214 6.552E-01 1. 784E-01 PB-214 9.360E-01 1. 897E-01 RN-.222 6.552E-01 l.784E-01 RA-224 8.469E--01 l.091E+OO RA-226 6.552E-01 l.784E-01 TH-228 7.757E-01 l.772E-01 TH-230 6. 550-E-01 1. 784E-01 PA-231 l.003E+OO 7.124E-01 TH-234 3.508E+OO 3.407E+OO U-234 6.550E-01 l.784E-01 U-235 1. 278E-01 l.754E-01 .U-238 3.508E+OO 3.407E+OO AM-243 l.851E-01 l.310E-01 Non-Identified Nuclides Nuclide NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 242of614 Key-Line Activity (pCi/GRAM 2. 726E-02 l.OOOE+41 -7. 971E-03 3.357E-01 9.835E+03 l.544E+02 2.388E-03 -2.663E-01 K.L Act error ( 1. 96-sigma) 4.209E-02 7.998E+41 3.495E-02 4.106E-01 8.878E+03 3.203E+02 6.494E-02 4.685E-01 TPU ( 1. 96-sigma) 2. 321E+Ol l.634E+OO 2.417E+OO l.557E-01 8. 371E-02 8.842E-02 9.316E-02 9.265E-01 1. 772E-01 l.784E-01 l.897E-01 1. 784E-01 l.091E+00 l.784E-01 l.772E-01 l.784E-01 7.124E-01 3.407E+OO 1. 784E-01 1. 754E-01 3.407E+OO l.310E-01 TPU '(l. 96-sigma) 4.385E-02 O.OOOE+OO 3.513E-02 4.376E-01 9.923E+03 3.278E+02 6.495E-02 4.836E-01 NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT.

MN-56 -l.000E+41 1. 772E+41 O.OOOE+OO SHORT HLIF C0-57 -2.271E-03 5.369E-02 5.370E-02 NOT IDENT .. C0-58 3.072E-03 5.371E-01 5. 371E-01 NOT IDENT. FE-59 -2.852E+OO 5.923E+OO 6.061E+00 NOT IDENT. C0-60 l.087E-02 3.313E-02 3.349E-02 NOT IDENT. ZN-65 5.159E-02 1.098E-01 1.122E-01 NOT IDENT. GE-68 8.988E-01 2. 396E+OO 2.430E+OO NOT IDENT. AS-73 -3.439E+OO 1.442E+Ol 1. 451E+Ol NOT IDENT. AS-74 -2.688E+03 4.434E+03 4.597E+03 SHORT HLIF SE-75 -2.089E-02 1.929E-01 1. 93.lE-01 NOT IDENT. BR-77 1. 730E+37 l.462E+38 O.OOOE+OO SHORT HLIF SR-82 4.688E+OO 5.537E+02 5.537E+02 SHORT HLIF RB-83 1. 804E-02 5.658E-01 5.659E-01 NOT IDENT. KR-85 -2.830E+Ol 1.101E+Ol l.685E+Ol NOT IDENT. SR-85 -2.776E+OO 1.079E+OO 1.652E+OO NOT IDENT. RB-86 2.786E+03 2.375E+04 2.378E+04 SHORT HLIF Y-'-88 -2.870E-02 l.481E-01 1. 487E-01 NOT IDENT. Y-91 1. 081E+02 5.702E+02 5. 723E+02 NOT IDENT. NB-94 -3.lOOE-02 3.107E-02 3.407E-02 NOT IDENT. NB-95 5.086E-01 8.392E-01 8.700E-01 NOT IDENT. NB-95M 2.394E+OO 2.430E+OO 2.659E+OO NOT IDENT. ZR-95 1. 230E+OO l.257E+OO 1.374E+OO NOT IDENT. NB-97 1. OOOE+41 9.789E+40 O.OOOE+OO SHORT HLIF ZR-97 -l.OOOE+41 6.100E+40 O.OOOE+OO SHORT HLIF M0-99 -2.443E+31 3.272E+31 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 8.175E+41 O.OOOE+OO SHORT HLIF RH-101 1. 074E-02 3.950E-02 3.980E-02 NOT IDENT. RH-102 -4.306E-02 6.'414E-02 6.701E-02 FAIL ABUN RU-103 -l.116E+OO 4.919E+OO 4.945E+OO FAIL ABUN RH-106 -8.046E-02 4.323E-01 4.338E-01 NOT IDENT. RU-106 -8.046E-02 4.323E-01 4.338E-01 NOT IDENT. AG-108M -2.460E-03 2.976E-02 2.978E-02 NOT IDENT. AG-llOM 3.590E-03 9.854E-02 9.856E-02 NOT IDENT. SN-113 l.917E-02 2.158E-01 2.160E-01 NOT IDENT. CD-115 2.609E+38 2.953E+38 O.OOOE+OO SHORT HLIF SN-ll 7M 4.473E+04 6. 7 66E+04 7.060E+04 SHORT HLIF TE-123M l.029E-01 1. 267E-01 1.349E-01 NOT IDENT. SB-124 -l.464E-01 2.070E+OO 2. 071E+OO NOT IDENT. SB-125 7.467E-02 1.024E-01 1.078E-01 NOT IDENT. TE-125M 9.634E+Ol 2.909E+02 2.941E+02 NOT IDENT. I-126 2.302E+05 6.591E+05 6. 672E+05 SHORT HLIF SB-126 4.040E+05 7.675E+05 7.888E+05 SHORT HLIF SB-127 9.444E+20 6.637E+21 O.OOOE+OO SHORT HLIF I-131 -6. 7 62E+08 2.693E+09 2. 710E+09 SHORT HLIF I-132 1.000E+41 1.904E+42 O.OOOE+OO SHORT HLIF TE-132 4.067E+25 8.450E+25 O.OOOE+OO SHORT HLIF BA-133 -3.108E-03 4.507E-02 4.509E-02 NOT IDENT. I-133 -1. OOOE+41 7.605E+41 O.OOOE+OO SHORT HLIF CS-134 2.865E-03 5.395E-02 5.397E-02 NOT IDENT. CS-135 -1.598E-02 l.575E-01 l.577E-01 NOT IDENT. I-135 -l.OOOE+41 7. 211E+41 O.OOOE+OO SHORT HLIF CS-136 1. 096E+05 2.405E+05 2.455E+05 SHORT HLIF . CE-139 -2.330E-02 1.120E-01 1.125E-01 NOT IDENT. BA-140 -4.455E+05 9.049E+05 9.270E+05 SHORT HLIF LA-140 -1.184E+04 2.098E+05 2.098E+05 SHORT HLIF CE-141 1.068E+OO 2.013E+Ol 2.014E+Ol NOT IDENT. CE-143 1.000E+41 1.525E+41 O.OOOE+OO SHORT HLIF CE-144 1.lOOE-01 3.555E-01 3.589E-01 NOT IDENT. PM-144 -l.103E-02 6.246E-02 6.266E-02 FAIL ABUN PR-144 -9.873E-01 5.400E+OO 5.419E+OO NOT IDENT. PM-146 4.710E-03 4.181E-02 4.186E-02 NOT IDENT. ND-147 -1.067E+07 1.989E+07 2.046E+07 SHORT HLIF PM-147 2.399E+02 9.340E+02 9.402E+02 NOT IDENT. PM-149 2.694E+39 4.573E+39 0.000E+OO SHORT HLIF EU....:150 -6.151E-03 2.937E-02 2.950E-02 FAIL ABUN EU-152 1.512E-02 8. 901E-02 8.927E-02 NOT IDENT. GD-153 7.509E-02 2.155E-01 2.181E-01 NOT IDENT. EU-154 8.372E-02 1. 017E-01 l.085E-01 NOT IDENT. EU-155 1.717E-01 l.342E-01 1. 549E-01 FAIL ABUN TB-160 5.577E-02 l.736E+00 l .. 736E+OO FAIL ABUN H0-166M -l.553E-02 5.126E-02 5.174E-02 NOT IDENT. TM-171 -3.239E+Ol 3.904E+01 4.168E+Ol NOT IDENT. HF-172 -2.922E-02 2. 696E-01 2.699E-01 FAIL ABUN LU-172 1. 815E-03 5.625E-02 5.625E-02 FAIL ABUN LU-176 1. 709E-02 2.429E-02 2.548E-02 FAIL ABUN HF-181 -2.315E+OO 3.647E+OO 3.794E+OO NOT IDENT. TA-182 6.416E-01 8.938E-01 9.395E-01 FAIL ABUN RE-183 5.889E-01 4.235E+OO 4.243E+OO NOT IDENT. Page 243of614 RE-184 -6.637E+OO 2.187E+Ol 2.207E+Ol FAIL ABUN W-188 3.910E+Ol l.003E+02 1.019E+02 FAIL ABUN IR-192 -4.607E-02 4.508E-01 4.512E-01 FAIL ABUN HG-203 8.268E-01 2.024E+OO 2.058E+OO NOT IDENT. BI-207 -1.226E-02 4.759E-02 4.791E-02 FAIL ABUN PB-210 -1.255E+OO 8.574E+OO 8.593E+OO NOT IDENT. PB-211 -4.274E-03 7.059E-01 7.059E-01 NOT IDENT. BI-212 8.229E-01 5.441E-01 6.585E-01 FAIL ABUN RN-219 6.176E-02 3. 968E-01 3.978E-01 FAIL ABUN RA-223 3.619E-01 5.690E-01 5.920E-01 FAIL ABUN AC-227 -l.774E-02 2.246E-01 2.247E-01 FAIL ABUN TH-227 -1.774E-02 2.246E-01 2.247E-01 FAIL ABUN AC-228 7.458E-01 3. 723E-01 5.016E-01 FAIL ABUN RA-228 7.458E-01 3. 723E-01 5.016E-01 FAIL ABUN TH-229

  • 1.lOlE-01 4.582E-01 4.609E-01 FAIL ABUN TH-231 3.619E-01 5.690E-01 5.920E-01 FAIL ABUN TH-232 7.458E-01 3. 723E-01 5.016E-01 FAIL ABUN PA-233 3.504E-02 5.836E-02 6.046E-02 FAIL ABUN PA-234 -1,. 849E-01 3.262E-01 3.366E-01 FAIL ABUN PA-234M -1.640E+OO 3.307E+00 3.389E+OO NOT IDENT. NP-237 3.504E-02 5.836E-02 6.046E-02 FAIL ABUN NP-238 1.398E+40 4.438E+40 O.OOOE+OO SHORT HLIF NP-239 1.512E-01 2.575E-01 2.664E-01 NOT IDENT. PU-239 3.370E+02 5.624E+02 5.826E+02 FAIL ABUN AM-241 1. 975E-02 2. 272E-01 2.274E-01 NOT IDENT. CM-243 -1.577E-01 1.278E-01 1.462E-01 NOT IDENT. BK-247 5.209E-03 7.533E-02 7.537E-02 NOT IDENT. CM-247 -l.545E-02 3.678E-02 3.743E-02 NOT IDENT. CF-249 2. 531E-02 3.458E-02 3. 641E-02 NOT IDENT. CF-251 -9.790E-02 1.169E-01 l.250E-01 NOT IDENT. ANH-511 -7.453E-03 5.072E-02 5.083E-02 NOT IDENT. -Page 244of614
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 74.66 61.2999 105.31 95.0122 131.20 63.1200 879.38 50.3431 86.79 95.0403 133.02 64.8921 46.54 59.3921 86.94 99.8109 133.52 52. 4372 228.16 0.0000 87.09 99.8288 136. 00 61.7352 52.39 57.6248 87.57 109.4002 136.47 61. 7 623 1093.63 71. 2453 88.03 109.4613 739.50 0.0000 52.39 66.7792 306.78 109.5020 140.51 0.0000 125.81 55.5136 88.47 99. 9961 143.76 57.9717 53.44 57.8238 143.76 100.1749 144.24 68.9239 54.07 40.8586 90.64 92.2994 145.44 63.9487 293.27 0.0000 531.02 0.0000 152. '43 78.7327 482.18 67.3322 92.59 92.5124 1048.07 0.0000 57.98 57 .1011 93.35 92.5944 154.21 66.9833 59.27 56.4521 94.56 92.7254 158.56 0.0000 59.32 64.0855 311. 90 92.7349 159.00 55.3370 59.54 64.1072 946.00 92.7372 162.33 68.2959 60.96 58'.1270 94.87 92.7585 537.26 0.0000 61.17 58.1454 97.43 64.1593 163.33 69.2073 62.93 7 5. 9*413 98.43 75.4728 165.86 72.7754 63.29 75.9816 98.44 75.4738 427.87 71.6608 290.67 76.0140 103.37 85.2133 176.60 0.0000 87.57 76.0921 116.74 85.2133 177.52 73.4567 66.73 84.8465 100 .11 74.8113 181.07 0.0000 67.24 49.4014 102.03 82.2265 181.52 76.7200 67.68 67. 9694 103.18 88.3845 184.41 63.8579 1221. 41 67.9761 103.37 98.0909 185.72 70.4441 97.43 84.8125 911. 20 64. 3119 193.51 55.9857 279.20 66.7177 105.31 64.3192 197.03 56.1309 1063.66 96. 4587 106.12 75.3071 198.01 56.1712 72.87 90.2427 106.47 85.0562 201.83 58. 9671 351.06 90.2427 109.28 65.8121 203.43 67.8465 74.66 84.2217 111. 00 85.4674 205.31 54.7028 238.63 84.2399 111.76 0.0000 210.85 57.5746 351. 93 84.2399 114. 06 61.2431 215.65 51.5459 238.63 84.2399 116. 30 0.0000 222 .11 49.0963 74.97 84.2569. 116.74 52. 8137 227.09 55.5303 77 .11 84.4958 119.76 67.7589 227.38 48.3745 78.74 87.8116 2 64. 66 64.1502 228.16 0.0000 256.23 81. 6393 121.22 64.1566 228.18 47.5040 133.52 91.1094 344.28 71. 5991 235.69 47.2892 364.49 0.0000 122.06 69.1494 235. 96 47.2972 711. 68 84.8749 122.92 54.3776 238.63 87.9904 356.01 86.4936 1274.44 54.3857 238.98 0.0000 323.87 86.5015 123.68 44.5240 240.99 59.6534 81. 75 87.3635 125.81 64.4466 242.00 85.0154 83.79 91.1385 127.23 61.2255 244.70 54.3591 265.00 96.2923 127.91 71. 2010 685.70 0.0000 193.51 101.2077 129.30 62.1765 388.16 38.2454 Page 245of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 507.63 0.0000 345.93 33.0941 569.50 25.2979 256.23 44.7145 351.06 28.8513 569.70 22.1373 527.90 0.0000 351. 93 28.8641 583.19 15.8887 264.66 37.4241 355.39 0.0000 584.27 15.8948 264.80 37.1522 356.01 31.8150 595.83 0.0000 265.00 37.1563 364.49 0.0000 600.6.0 28.7732 268 .22 46.8797 366.42 0.0000 602.52 0.0000 269.46 41.3956 372. 51 18.4658 604. 72 16.0077 270.03 41.4093 375.05 16.5421 607.14 12.8169 401.81 41.4386 377.52 24.3551 609.32 16.0333 273.65 0.0000 383.85 22.4740 610.33 16.0388 276.40 34.1764 388.16 19.5821 614.28 20.8782 583.19 32.3475 666.33 0.0000 618.01 22.5125 277.60 35.1248 391.69 26.4792 884.68 10.7288 402.40 31.4344 400.66 21.6652 621. 93 13. 9548 279.20 34.2321 401.81 29.5587 630.19 0.0000 279.54 44.4180 402.40 34.4944 631.29 23.6901 279.70 44.4219 404.85 31. 5729 633.25 18.3177 280.46 39.8121 410.95 30.6708 634.78 0.0000 301.36 29.6836 413.71 22.7838 635.95 19.4128 284.31 0.0000 720.70 0.0000 636.99 0.0000 285.41 31. 5699 423. 72 0.0000 1690.97 17.8528 285.90 0.0000 427.09 21. 9226 657.76 4.8880 287.50 39.0443 427.87 19.9365 657'.90 0.0000 290.67 27.9395 433.94 28.9841 661. 66 14.1383 293.27 0.0000 439.40 30.0543 664.57 0.0000 295.22 34.7342 453.88 21.1675 666.33 0.0000 316.51 44.8369 463.37 20.2393 666.50 0.0000 298.58 30.8704 468.07 18.2509 667. 71 0.0000 299.98 40. 443'7 473.00 0.0000 677.62 19.6765 '300.09 40.4464 631. 2 9 21.3533 685.70 0.0000 300 .13 40.4473 696.49 21. 3683 695.00 0.0000 311. 90 40.4473 477.60 24.4292 696.49 23.0918 301.36 36.5395 482.18 23.4544 696.51 23.0918 302.85 -36.5696 '487.02 0.0000 697.00 0.0000 304.50 32.3795 492.35 0.0000 697.30 25.2976 304.85 0.0000 497.08* 21.5422 697.49 26.3994 306.78 31.0107 505.52 29. 8472 702.65 19. 8311 308.46 40.4446 507.63 0.0000 706.68 13.2368 311. 90 30.1549 511. 00 36.0994 711. 68 14.3621 316.51 39 .. 6766 514.00 86.7378 .720.70 0.0000 319.41 0.0000 514.00 86.7378 721.93 0.0000 320.08 0.0000 520.40 16.5625 722.78 13.3022 321.04 30.3027 520.69 0.0000 722.91 14. 9656 323.87 28.4515 667.71 0.0000 723.31 19.9563 325.23 37.9622 527.90 0.0000 756.73 16.6345 1596.21 0.0000 528.26 12.4590 727.33 8.8802 333.37 34.3118 529.59 18.6973 733.00 11. 6749 333.97 40.0424 529.87 0.0000 735.93 6. 6772 334.37 35.7597 531.02 0.0000 737.46 17.8145 338.28 32. 4872 537.26 0.0000 739.50 0.0000 338.32 32.4879 1260.41 0.0000 747.24 18.9825 340.48 31.5673 552.55 22.0006 748.06 15.6366 340.55 0.0000 795.86 19.9826 752.31 14.5377 344.28 26.4528 569.33 25.2969 753.82 0.0000 Page 246 of 614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:41:37.60 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245010.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM39.CNF;l34 *Background date : Z-OCT-2016 11:02:13. Sample date 15-DEC-2015 12:35:00 Acquisition date : 3-0CT-2016 04:36:41. Sample ID R405245010 Sample quantity l.42421E+02 GRAM Detector name GAM39 Detector geometry: CAN Elapsed live 0 01:00:00.00 Elapsed real time: 0 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596387 Detector SN# Matrix Spike ID LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 2 2 2 0 4 4 0 0 5 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 4 4 0 0 0 0 0 Page 248of614 Energy 46.78* 49.54 63.16* 72.80 74.73* 77.04* 83.93* 87.39 92. 62* 135. 32 186.50* 238.71* 242.10 245.01 269.78 295.48* 339.17* 345.83 352.01* 373.54 464.09 511. 65* 569.43* 583.22* 609.30* 656.55 661.54 709.52 712.69 728.90 786.54 860.21 911. 7 5* 917.45 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 56 29 32 31 167 280 29 81 93 19 61 301 83 21 46 92 55 9 190 23 21 21 6 63 124 10 89 10 14 53 25 22 59 10 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 76 88 216 93 123 128 88 156 176 73 114 45 55 18 44 99 93 38 39 . 24 25 43 23 36 25 20 14 7 11 16 18 9 22 1 1. 54 0.91 1. 06 1.24 1. 20 1. 28 1. 08 1. 70 1. 54 0.53 1. 21 1. 29 2.21 1.11 1. 47 1. 65 1. 32 0.82 1. 61 3.31 1. 50 2.50 0.80 1. 72 1. 64 0.64 1. 99* 1. 66 2.51 5.34 1. 63 0.91 1. 52 1. 69 93.40 98.92 126.17 145.44 149.30 153.92 167.71 174.63 185.08 270.48 372. 85 477.27 484.04 489.86 539.41 590.82 678.19 691.51 703.88 746.93 928.04 1023.18 1138. 73 1166.32 1218.49 1312.99 1322.98 1418.95 1425.28 1457.71 1572.99 1720.35 1823.44 1834.85 91 97 121 143 143 143 166 171 171 267 367 469 469 4 69 535 585 671 687 699 741 922 1016 1133 1160 1213 1307 1316 1417 1417 1446 1565 1715 1818 1832 6 6 10 18 18 18 5 20 20 6 12 24 24 24 9 14 15 8 13 10 10 *21 9 12 13 9 14 14 14 23 16 12 14 6 1.57E-02 29.8 8.lOE-03 53.7 8.77E-03 93.1 8.53E-03 48.8 4.65E-02 13.9 7.78E-02 9.9 7.97E-03 55.0 2.24E-02 28.9 2.57E-02 29.9 5.28E-03 74.8 1.71E-02 38.6 8.35E-02 7.2 2.31E-02 30.5 5.76E-03 40.0 1.28E-02 30.1 2.55E-02 25.5 1. 53E-02 41. 7 2.42E-03127.3 5.27E-02 9.8 6.45E-03 45.0 5.93E-03 48.8 5 .. 77E-03 97. 4 l.69E-03149.7 1.75E-02 23.8 3.45E-02 12.6 2.81E-03 82.9 2.47E-02 13.8 2.86E-03 40.1 3.97E"'-03 55.0 l.48E-02 24.3 6.91E-03 44.6 5.98E-03 35.4 1. 65E-02 23. 4 2.69E-03 37.6 Fit 2.32E+00 2.40E+OO l.80E+OO 1.34E+OO Peak Search Report (continued) Page : 2 Sample ID : R405245010 Acquisition date .. 3-0CT-2016 04:36:41 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 948. 96 5 16 0.89 1897.88 1890 10 1.51E-03155.2 36 3 969. 63* 30 27 2.46 1939.22 1933 17 8.47E-03 39.5 1. 85E+OO 37 3 972. 92 16 4 2.13 1945.80 1933 17 4.40E-03 51.1 38 0 998.39 4 7 0.81 1996.75 1991 . 7 1.17E-03114.1 39 0 1009.76 20 0 0.54 2019.50 . 2014 12 5.56E-03 22.4 40 0 1025.22* 8 14 0.79 2050.42 2040 14 2.24E-03106.0 41 0 1028.62 10 4 0.54 2057.21 2054 7 2.64E-03 46.0 42 0 1069.85 17 3 4.39 2139.70 2134 11 4.80E-03 30.4 43 0 1121.09 33 24 1. 87 2242.20 2234 19 9.05E-03 40.0 44 0 1239.08 14 22 1. 54 2478.21 2470 14 3.97E-03 73.1 45 0 1283.25 7 3 1. 06 2566.57 2563 6 2.00E-03 52.9 46 0 1311.41 4 7 *i. 32 2622.89 2617 8 l.llE-03129.9 47 0 1460.96* 234 0 1. 87 2922.06 2915 15 6.50E-02 6.7 48 0 1764.78* 29 4 1. 42 3529.83 3523 15 8.07E-03 24.2 Flag:."*" = Peak area was modified by background subtraction Page 249of614 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 05:41:40 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245010.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 15-DEC-2015 12:35:00 R405245010 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 04:36:41 142.42 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA39 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfer1ng ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 250of614 Detector geometry: Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 TH-229 88.47 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:06.98 10.00 o. oo* % Peak Energy 0.2%

Nuclide Line Activity Report Page : 2 Sample ID : R405245010 Acquisition date 3-0CT-2016 04:36:41 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error. Status K-40 1460.82 10.66* 8.983E-01 1.236E+Ol 1.236E+Ol 13.38 OK CD-109 88.03 3.70* 6.753E+OO L 310E+OO 2.033E+00 96.33 OK SN-126 64.28 9.60 6.932E+OO 3 .118E-01 3 .118E-01 186.15 OK 86.94 8.90 6.753E+00 5.444E-01 5.444E-01 96.33 OK 87.57 37.00* 6.753E+OO l.310E-01 l.310E-01 96. 33 OK BA-137M 661. 66 89.90* 1.758E+OO 3.066E-01 3.123E-01 27.69 OK CS-137 661.66 85.10* l.758E+OO 3.238E-01 3.299E-01 27.69 OK TL-208 277.37 6.60 3.709E+OO Line Not Found Absent 583.19 85.00* 1.953E+OO 2.085E-01 2.085E-01 47.55 OK 860.56 12.50 1.417E+00 6.458E-01 6.458E-01 70.79 OK PB-210 46.54 4.25* 6.846E+00 1.304E+OO l.337E+OO OK BI-211 72. 87 1. 23 6.824E+OO 2.380E+OO 2.380E+OO 97.58 OK 351.06 12.92* 3.013E+OO 5.164E-01 5.164E-01 249.10 OK PB-212 74.82 10.28 6.812E+OO 1.085E+OO 1.085E+OO 45.42 OK 77 .11 17.10 6.800E+OO 1.560E+OO l.560E+00 19.83 OK 238.63 43.60* 4.210E+OO 9.716E-01 9.716E-01 14.44 OK 300.09 3.30 3.465E+OO Line Not Found Absent BI-214 609.32 45.49* 1. 883E+OO 7.959E-01 7. 962E-01 25.23 OK 1120. 29 14. 92 . l.136E+00 9.977E-01 9.981E-01 79.98 OK 1764.49 15.30 7.484E-01 1.261E+OO 1.261E+OO 48.47 OK PB-214 74.82 5.80 6.812E+OO Line Not Found <<INT Reject 77 .11 9.70 6.800E+OO 2.750E+OO 2. 7 51E+OO 19.83 OK 87.09 3.41 6.755E+OO -----Line Not Found <<INT Reject 242.00 7.25 4.163E+OO Line Not Found <<INT Reject 295.22 18.42 3.512E+OO 8.285E-01 8.288E-01 50.97 OK 351.93 35.60* 3.014E+OO Line Not Found <<INT Reject RN-222 60.9. 32 45.49* 1.883E+OO 7.959E-01 7.962E-01 25:23 OK 1120.29 14.92 1.136E+OO 9.977E-01 9. 981E-01 79.98 OK 1764.49 15.30 7.484E-01 1.261E+OO 1.261E+OO 48.47 OK RA-224 240.99 4.10* 4.161E+OO 1.424E+oo* 1.424E+OO 134.26 OK RA-226 609.32 45.49* l.883E+OO 7.959E-01 7. 962E-01 25.23 OK 1120.29. 14.92 1.136E+OO 9.977E-01 9.981E-01 79.98 OK 1764.49 15.30 7.484E-01 1.261E+OO

  • 1.261E+OO 48.47 OK AC-228 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11.27 3 .113E+OO 9.020E-01 9.020E-01 83.48 OK 794.95 4.25 l.512E+OO Line Not Found Absent 835.71 1. 61 1.451E+OO Line Not Found Absent 911.20 25.80* 1.350E+OO 8.992E-01 8.992E-01 46.87 OK 968. 97 15.80 1.283E+OO 7.905E-01 7.905E-01 78.97 OK RA-228 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11. 27 3 .113E+00 9.020E-01 9.020E-01 83.48 OK 794.95 4.25 1.512E+OO Line Not Found Absent 835.71 1. 61 1.451E+OO Line Not Found Absent 911. 20 25.80* 1.350E+OO 8.992E-01 8.992E-01 .46. 87 OK 968.97 15.80 1.283E+OO 7.905E-01 7.905E-01 78.97 OK TH-228 74.82 10.28 6.812E+OO 1.085E+OO 1.085E+00 45.42 OK 77 .11 17.10 6.800E+OO 1. 560E+OO 1.560E+OO 19.83 OK 238.63 43.60* 4.210E+OO 9. 716E-01 9.716E-01 14.44 OK 300.09 3.30 3.465E+OO Line Not Found Absent Page 251.of 614 Nuclide Line Activity Report (continued) Page : 3 Sample ID : R405245010 Acquisition date 3-0CT-2016 04:36:41 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status TH-229 85.43 14.70 6.769E+OO 1.855E-01 1.855E-01 109.93 OK 88.47 24.00 6.753E+OO 2.019E-01 2.019E-01 96. 33 OK 193.51 4.41* 4. 960E+OO Line Not Found Absent 210.85 2.80 4.650E+OO Line Not Found Absent TH-230 609.32 45.49* 1.883E+OO 7.959E-01 7.959E-01 25.23 OK 1120.29 14.92 1.136E+OO 9.977E-01 9.977E-01 79.98 OK 1764.49 15.30 7.484E-01 1.261E+OO 1.261E+OO 48.47 OK TH-232 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11. 27 3 .113E+OO
  • 9. 020E-01 9.020E-01 83.48 OK 835.71 1. 61 1. 451E+OO Line Not Found Absent 911.20 25.80* 1.350E+OO 8.992E-01 8.992E-01 46.87 OK 968. 97 15.80 1.283E+OO 7.905E-01 7.905E-01 78.97 OK TH-234 63.29 3.70* 6.932E+00 8.089E-01 8.089E-01 186.15 OK 92.59 4.23 6. 724E+OO 2.079E+OO 2.079E+OO 59.80 OK U-234 609.32 45.49* 1.883E+OO 7.959E-01 7.959E-01 25.23 OK 1120.29 14.92 1.136E+OO 9.977E-01 9.977E-01 79.98 OK 1764.49 15.30 7.484E-01 1.261E+OO 1.261E+OO 48.47 OK U-238 63.29 3.70* 6.932E+00 8.089E-01 8.089E-01 186.15 OK 92.59 4.23 6.724E+OO 2.079E+OO 2.079"E+OO 59.80 OK AM-243 43.53 5.90 6.236E+OO Line Not Found Absent 74.66 67.20* 6.812E+OO 1.660E-01 1.660E-01 45.42 OK ANH-511 511. 00 100.00* 2.180E+OO 5.304E-02 5.304E-02 194.87 OK Flag: "*" = Keyline Page 252 of 614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016.05:41:41.78 *******************************t***********************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245010.CNF;l *
  • Acquisition date 3-0CT-2016 04:36:41 Sensitivity : 3.000 *
  • Detector ID GAM39 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:35:00 Analyst initials: MXRl *
  • Sample ID R405245010 Sample Quantity 1.4242E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 27-JUL-2016 13:04:01 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide *K-40 CD-109 SN-126 BA-137M CS-137 . TL-208 PB-210 BI-211 PB-212 BI-214 Pff-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Activity (pCi/GRAM l.236E+Ol 2*. 033E+OO 1.310E-01 3. 123E-01 3.299E-01 2.085E-01 l.337E+OO 5.164E-01 9.716E-01 7. 962E-01 1.016E+OO 7.962E-01 1.424E+OO 7. 962E-01 8.992E-01 8.992E-01 9.716E-01 -3.357E-01 7.959E-01 8.992E-01 8.089E-01 7.959E-01 8.089E-01 1.660E-01 5.304E-02 Cnt.uncert (1. 96-sigma) 1.622E+OO 1 .. 919E+OO l.236E-01 8.473E-02 8.951E-02 9.713E-02 7.804E-01 l.261E+'OO 1. 37 5E-01 l.969E-01 l.952E-01 1. 969E-01 1.873E+OO 1. 969E-01 4.130E-01 4.130E-01 1.375E-01 4.928E-01 1. 968E-01 4.130E-01 1. 476E+OO 1. 968E-01 l.476E+OO 7.388E-02 L 013E-01 Non-Identified Nuclides Nucl*ide BE-7 *. NA-22 NA-24 AL-26 SC-46 Page 253 of 614. Key-Line Activity (pCi/GRAM -2.659E-01 2.376E-02 O.OOOE+OO 1. 726E-02 -3.753E-01 K.L. Cnt Uncert ( 1. 96-sigma) l.444E+Ol 6.601E-02 l.960E+41 3.072E-02 3.491E-01 MDA (pCi/GRAM 6. 722E-01 1.635E+OO l.053E-01 7.225E-02 7.633E-02 7.203E-02 8.744E-01 4.023E-01 9.343E-02 l.362E-01 3.554E-01 1. 362E-01 1.002E+OO 1. 362E-01 3.521E-01 3.521E-01 9.343E-02 9.107E-01 l.362E-01 3.521E-01 1.133E+00 1. 362E-01 1.133E+OO 6.221E-02 6. 491E-02 MDA (pCi/GRAM 2.721E+Ol 1. 365E-01 O.OOOE+OO 8.241E-02 5.662E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 O.OOOE+OO 1.187E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3. 772E+02 O.OOOE+OO SHORT HLIF MN-54 5.205E-03 6.949E-02 l.427E-01 NOT IDENT. C0-56 8.486E-02 5.644E-01 1.152E+OO FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 1.664E-02 4.453E-02 8.366E-02 FAIL ABUN C0-58 -6.510E-02 6.t88E-01 l.241E+OO NOT IDENT. FE-59 2.245E+OO 8.150E+OO 1. 675E+Ol NOT IDENT. C0-60 1. 896E-02 5.428E-02 l.145E-01 NOT IDENT. ZN-65 7.579E-04 2.433E-01 4.241E-01 NOT IDENT. GE-68 4.505E-01 2.922E+OO 5.970E+OO NOT IDENT. AS-73 -l.928E+OO 2.855E+OO 4.613E+OO NOT IDENT. AS-74 O.OOOE+OO 5.752E+03 O.OOOE+OO SHORT HLIF SE-75 1.959E-01 2.232E-01 4.535E-01 FAIL ABUN BR-77 0.000E+OO 3.065E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.145E+02 O.OOOE+OO SHORT HLIF RB-83 2.993E-01 8.004E-01 l.467E+00 NOT IDENT. KR-85 2.655E-01 8.398E+OO 1.597E+Ol NOT IDENT. SR-85 2.671E-02 8.231E-01 1.566E+OO NOT IDENT. RB-86 O.OOOE+OO 2.758E+04 O.OOOE+OO SHORT HLIF Y-88 -1.399E-01 1.976E-01 2.949E-01 NOT IDENT. Y-91 -5.847E+02 6.436E+02 1.062E+03 NOT IDENT. NB-94 2.375E-02 3.749E-02 7.769E-02 NOT IDENT. NB-95 6.289E-01 1.004E+OO 2.049E+OO NOT IDENT. NB-95M -5.176E-02 2.399E+OO 4.192E+OO NOT IDENT. ZR-95 7.320E-01 1.697E+OO '3.420E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 625E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.960E+41 0.000E+OO SHORT HLIF M0-99 O.OOOE+OO 3.569E+31 O,OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 840E+41 O.OOOE+OO SHORT HLIF
  • RH-101 -l.655E-02 3.729E-02 6.406E-02 NOT IDENT. RH-102 9.056E-02 7. 272E-02 l.622E-01 NOT IDENT. RU-103 7.915E-01 6.392E+OO 1.235E+Ol FAIL ABUN RH-106 -2.803E-01 5. 651E-01 9.913E-01 NOT IDENT. RU-106 -2.803E-01 5. 651E-01 9.913E-01 NOT IDENT. AG-108M 2.456E-02 3.280E-02 6.854E-02 NOT IDENT. AG-llOM l.353E-01 1.161E-01 2.734E-01 FAIL ABUN SN-113 -l.597E-01 2.636E-01 4.690E-01 NOT IDENT. CD-115 O.OOOE+OO 3.874E+38 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 6. 964E+04 O.OOOE+OO SHORT HLIF TE-123M 9.339E-02 1. 24 7E-01 2. 596E-01 NOT IDENT. SB-124 l.578E+00 2.329E+OO 5.815E+OO NOT IDENT. SB-125 9.192E-02 9.939E-02 2.198E-01 FAIL ABUN TE-125M 2.568E+02 2.486E+02 4.894E+02 NOT IDENT. I-126 O.OOOE+OO 6.809E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1. 013E+06 0.000E+OO SHORT HLIF SB-127 O.OOOE+OO 6.875E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.346E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 8.056E+25 O.OOOE+OO SHORT HLIF BA-133 6.415E-03 5.219E-02 9.158E-02 NOT IDENT. I-133 O.OOOE+OO 1. 788E+41 O.OOOE+OO SHORT HLIF CS-134 -4.108E-04 6.857E-02 l.355E-01 FAIL ABUN CS-135 6. 722E-02 l.648E-01 3.021E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.438E+05 O.OOOE+OO SHORT HLIF CE-139 4. 640.E-02 1.104E-01 2.236E-01 NOT IDENT. BA-140 O.OOOE+OO 1.086E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO l.959E+05 O.OOOE+OO SHORT HLIF CE-141 -7.910E+00 2.234E+Ol 4.302E+Ol NOT IDENT. CE-143 O.OOOE+OO 8.752E+40 0. oo*OE+OO SHORT HLIF CE-144 -l.524E-01 3.712E-01 6.390E-01 NOT IDENT. PM-144 -l.919E-02 7.792E-02 l.394E-01 NOT IDENT. PR-144 1.581E+OO 6.224E+OO 1.206E+Ol NOT IDENT. PM-146 -2.063E-02 4.868E-02 8.833E-02 NOT IDENT. ND-147 O.OOOE+OO 2.9S4E+07 O.OOOE+OO SHORT HLIF PM-147 4. 996E+Ol 7.505E+02 l.374E+03 NOT IDENT. PM-149 O.OOOE+OO 5.053E+39 O.OOOE+OO SHORT HLIF EU-150 l.169E-02 3.197E-02 5.793E-02 FAIL ABUN EU-152 8.427E-02 1. 34 7E-01 2 .131E-01 EAIL ABUN GD-153 -l.630E-01 l.919E-01 2.917E-01 NOT IDENT. EU-154 6.480E-02 1. 636E-01 3.397E-01 NOT IDENT. EU-155 2.543E-02 l.040E-01 l.924E-01 FAIL ABUN TB-160 4.781E-01 1.877E+OO 4. 011'E+oo FAIL ABUN H0-166M 8.648E-02 9.315E-02 1.338E-01 FAIL ABUN TM-171 2.135E+OO 5.933E+OO *1.063E+Ol NOT IDENT. HF-172 l.431E-01 2. 372E-01 4.498E-01 FAIL ABUN LU-172 3.190E-02 9.279E-02 1. 960E-01 FAIL ABUN Page 254 of 614 LU-176 1. 896E-02 2.814E-02 5.625E-02 FAIL ABUN HF-181 2.934E-01 4. 941E+OO 9.460E+OO FAIL ABUN TA-182 4.146E-01 1.153E+OO 2.379E+OO FAIL ABUN RE-183 8.348E-01 1.000E+OO l.984E+00 NOT IDENT. RE-184 -5.391E-01 3.014E+Ol 6.101E+Ol NOT IDENT. W-188 -1. 740E+Ol l.253E+02 2.138E+02 FAIL ABUN IR-192 -5.687E-01 4.783E-01 8.008E-01 FAIL ABUN HG-203 -2.884E-01 2.545E+OO 4.851E+OO FAIL ABUN BI-207 3.734E-02 5. 726E-02 1.221E-01 FAIL ABUN PB-211 1.592E-01 7.647E-01 1. 505E+OO NOT IDENT. BI-212 1. 017E+OO 6.763E-01 1.503E+OO FAIL ABUN RN-219 -5.459E-02 4.470E-01 8.445E-01 FAIL ABUN RA-223 -2.404E-02 7.lOlE-01 1.358E+OO FAIL ABUN AC-227 -5.393E-02 2.419E-01 4. 611E-01 NOT IDENT. TH-227 -5.393E-02 2.419E-01 4. 611E-01 NOT IDENT. PA-231 4.035E-01 5.419E-01 1.026E+OO NOT IDENT. TH-231 -2.404E-02 7.lOlE-01 1.358E+OO FAIL ABUN PA-233 -1. 411E-02 7.038E-02 l.328E-01 FAIL ABUN PA-234 2. 013E-01 4.275E-01 8 .118E-01 FAIL ABUN PA-234M -3.466E+OO 5.030E+OO 7.949E+OO NOT IDENT. U-235 -3.661E-02 l.930E-01 3.758E-01 FAIL ABUN NP-237 -1. 411E-02 7.038E-02 l.328E-01 FAIL ABUN NP-238 O.OOOE+oo 4.939E+40 O.OOOE+OO SHORT HLIF NP-239 2.433E-01 2.721E-01 5.232E-01 NOT IDENT. PU-239 1. 7 55E+02 3.388E+02 6.329E+02 NOT IDENT. AM-241 -2.320E-02 6.113E-02 1.006E-01 NOT IDENT. CM-243 2.088E-02 9.693E-02 1. 7-88E-01 NOT IDENT. BK_..:247 4.546E-02 8.789E-02 1. 631E-01 FAIL ABUN CM-247 -2.342E-02 4.219E-02 7.538E-02 NOT IDENT. CF-249 3.872E-02 4.366E-02 9.195E-02 NOT IDENT. CF-:-251 -4.147E-02 1.153E-01 2.204E-01 NOT IDENT. Page 255 of 614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:41:38.49 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460. 82 225 10.66* 8.983E-01 1.236E+Ol 1.236E+Ol 13.38 CD-109 88.03 98 3.70* 6.753E+OO 2.073E+OO 3.218E+OO 57.88 SN-126 64.28 39 9.60 6.932E+OO 3 .118E-01 3 .118E-01 186.15 86.94 98 8.90 6.753E+OO 8.618E-01 8.618E-01 57.88 87.57 98 37.00* 6.753E+00 2.073E-01 2.073E-01 57.88 BA-137M 661.66 92 89.90* 1. 758E+OO 3.066E-01 3.123E-01 27.69 CS-137 661.66 92 85.10* 1.758E+OO 3.238E-01 3.299E-01 27.69 TL-208 277.37 ------6.60 3.709E+OO ------Line Not Found ------583.19 66 85.00* 1.953E+OO 2.085E-01 2.085E-01 47.55 860.56 22 12.50 1.417E+OO 6.458E-01 6.458E-01 70.79 PB-210 46.54 72 4.25* 6.846E+OO 1.304E+OO 1.337E+OO 59.54 BI-211 72. 87 38 1. 23 6.824E+OO 2.380E+OO 2.380E+OO 97.58 351.06 207 12.92* 3. 013E+OO 2.799E+OO 2.799E+OO 19.60 PB-212 74.82 206 10.28 6.812E+OO 1.552E+OO 1.552E+OO 27.79 77 .11 344 17.10 6.800E+OO 1.560E+00 1. 560E+00 19.83 238.63 ' 338 43.60* 4.210E+OO 9.716E-01 9.716E-01 14.44 300.09 ------3.30 3.465E+OO ------Line* Not Found ------BI-214 609.32 129 45.49* 1.883E+OO 7.959E-01 7. 962E-01 25.23 1120.29 32 14.92 1.136E+OO 9.977E-01 9.981E-01 79.98 1764.49 27 15.30 7.484E-01 1. 261E+OO 1.261E+OO 48.47 PB-214 74.82 206 5.80 6.812E+OO 2.752E+OO 2.753E+OO 27.79 77 .11 344 9.70 6.800E+OO 2.750E+OO 2.751E+00 19.83 87.09 98 3.41 6.753E+OO 2.249E+OO 2.250E+OO 57.88 242.00 94 7.25 4 .161E+OO 1.634E+OO 1.634E+OO 60.91 295.22 102 18.42 3.512E+OO 8.285E-01 8.288E-01 50.97 351.93 207 35.60* 3.013E+OO 1.016E+OO 1.016E+OO 19.60 RN-222 609.32 129 45.49* 1.883E+OO 7.959E-01 7. 962E-01 25.23 1120.29 32 14.92 1.136E+OO 9.977E-01 9.981E-01 79.98 1764.49 27 15.30 7.484E-01 1.261E+OO 1.261E+OO 48.47 RA-224 240.99 94 4.10* 4.161E+OO 2.889E+00 2.889E+00 60.91 RA-226 609.32 129 45.49* 1.883E+OO 7.959E-01 7. 962E-01 25.23 1120.29 32 14.92 1.136E+OO 9.977E-01 9. 981E-01 79.98 1764.49 27 15.30 7.484E-01 1. 261E+OO 1.261E+00 48.47 AC-228 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 60 11. 27 3 .113E+OO 9.020E-01 9.020E-01 83.48 794.95 ------4.25 1. 512E+OO ------Line Not Found ------835.71 ------1. 61 1. 451E+OO ------Line Not Found ------911.20 59 25.80* 1. 350E+OO 8.992E-01 8.992E-01 46.87 968' 97 30 15.80 1. 283E+OO 7.905E-01 7.905E-01 78.97 RA-228 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 60 11. 27 3 .113E+OO 9.020E-01 9.020E-01 83.48 794.95 ------4.25 1.512E+OO ------Line Not Found ------835. 71 ------1. 61 1.451E+OO ------Line Not Found ------911.20 59 25.80* 1.350E+OO 8.992E-01 8.992E-01 46.87 968. 97 30 15.80 1.283E+OO 7.905E-01 7.905E-01 78.97 TH-228 74.82 206 10.28 6.812E+OO 1.552E+OO 1.552E+OO 27.79 77 .11 344 17.10 6.800E+OO 1. 560E+OO 1.560E+OO 19.83 Page 256of614 Nuclide Line Activity Report (c.ontinued) Page : 2 Sample ID : R405245010 Acquisition date 3-0CT-2016 04:36:41 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 338 43.60* 4.210E+OO 9.716E-01 9.716E-01 14.44 300.09 ------3.30 3.465E+OO ------Line Not Found ------TH-229 . 85.43 35 14.70 6.769E+OO 1.855E-01 1.855E-01 109.93 88.47 98 24.00 6.753E+OO 3.196E-Ol 3.196E-01 57.88 193.51 ------4.41* 4. 960E+OO ------Line Not Found ------210.85 ------2.80 4.650E+OO ------Line Not Found ------TH-230 609.32 129 45.49* 1.883E+OO 7.959E-01 7.959E-01 25.23 1120.29 32 14.92 1.136E+OO 9.977E-01 9.977E-01 79.98 1764.49 27 15.30 7.484E-01 1. 261E+OO 1.261E+OO 48.47 TH-232 105.21 ------1.10 6.612E+OO ------Line Not Found ------. 338.32 60 11. 27 3 .113E+OO 9.020E-01 9.020E-01 83.48 835.71 ------1. 61 1. 451E+OO ------Line Not Found. ------911.20 59 25.80* l.350E+OO 8.992E-01 8.992E-01 46.87 968.97 30 15.80 1. 283E+OO 7.905E-01 7.905E-01 78.97 TH-234 63.29 39 3.70* 6.932E+OO 8.089E-01 8.089E-01 186.15 92.59 112 4.23 6. 724E+OO 2.079E+OO 2.079E+OO 59.80 U-234 609.32 129 45.49* 1.883E+OO 7.959E-01 7.959E-01 25.23 1120.29 32 14.92 l.136E+OO 9.977E-01 9.977E-01 79.98 1764.49 27 15.30 7. 484E-01 . 1.261E+OO 1. 2 61E+OO 48.47 U-238 63.29 39 3.70* 6.932E+OO 8.089E-01 8.089E-01 186.15 92.59 112 4.23 6. 724E+OO 2.079E+OO 2.079E+00 59.80 AM-243 43.53 ------5.90 6.236E+OO ------Line Not Found ------74.66 206 67.20* 6.812E+OO 2.375E-01 2.375E-01 27.79 ANH-511 511. 00 22 100.00* 2.180E+OO 5.304E-02 5.304E-02 194.87 Flag: "*" Key line Page 257of614 Summary of Nuclide Activity Sample ID : R405245010 Acquisition date Page : 3 3-0CT-2016 04:36:41 Total number of lines in spectrum 48 Number of unidentified lines 8 Number of lines tentatively identified by NID 40 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife l.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+1CiY 22.20Y 7.04E+08Y 1.41E+10Y 1600.00Y 1600. OOY 1600.00Y l.41E+l0Y 1600. OOY 1. 41E+10Y l.41E+l0Y l.41E+l0Y 7340.00Y 7.54E+04Y l.41E+l0Y *4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 55 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 *Total Activity Grand Total Activity Uncorrected pCi/GRAM l.236E+Ol 2.073E+OO 2.073E-01 3.066E-01 3.238E-01 2.085E-01 l.304E+00 2.799E+OO 9.716E-01 7.959E-01 l.016E+OO 7.959E-01 2.889E+OO 7.959E-01 8.992E-01 8.992E-01 9.716E-01 3 .196E-01 7.959E-01 8.992E-01 8.089E-01 7.959E-01 8.089E-01 2.375E-01 5.304E-02 3.434E+Ol 3.434E+Ol Decay Corr pCi7GRAM 1. 236E+Ol 3.218E+OO 2.073E-01 3.123E-01 3.299E-01 2.085E-01 1.337E+OO 2.799E+OO 9. 716E-01 7.962E-01 l.016E+OO 7.962E-01 2.889E+OO 7. 962E-01 8.992E-01 8.992E-0! 9 .. 716E-01 3 .196E-01 7.959E-01 8.992E-01 8.089E-01 7.959E-01 8.089E-01 2.375E-01 5.304E-02 3.553E+Ol 3.553E+Ol 83.33% Decay Corr 2-Sigma 2-Sigma Error* %Error 0.165E+Ol 13.38 l.863E+OO 57.88 l.200E-01 57.88 0.865E-01 27.69 0.913E-01 27.69 0.991E-01 47.55 0.796E+OO 59.54 0.549E+OO 19.60 l.403E-01 14.44 2.009E-01 25.23 0.199E+OO 19.60 2.009E-01 25.23 l.760E+00 60.91 2.009E-01 25.23 4.214E-01 46.87 4.214E-01 46.87 l.403E-01 14.44 l.850E-01 57.88 2.008E-01 25.23 4.214E-01 46.87 15.06E-01 186.15 2.008E-01 25.23 15.06E-01 186.15 0.660E-01 27.79 10.34E-02 194.87 Flags: "K" Keyline not found "E" = Manually edited "M" Manually aqcepted "A" = Nuclide specific abn. limit Page 258 of 614 Flags K Unidentified Energy Lines Page : 4 Sample ID : R405245010 Acquisition date : 3-0CT-2016 04:36:41 It Energy Area Bkgnd FWHM Channel Lef.t Pw Cts/Sec %Err %Eff Flags 0 49.54 37 111 0.91 98.92 97 6 8.lOE-03 **** 7.05E+OO T 0 135.32 22 86 0.53 270.48 267 6 5.28E-03 **** 6.13E+OO T 0 186.50 71 130 1. 21 372. 85 367 12 1. 71E-02 77.2 5.09E+OO T 5 245.01 23 20 1.11 489.86 469 24 5.76E-03 80.0 4.12E+OO T 0 269.78 51 49 1. 47 539.41 535 9 l.28E-02 60.2 3.80E+OO T 0 345.83 10 42 0.82 691.51 687 8 2.42E-03 **** 3.06E+OO T 0 373.54 25 26 3.31 746.93 741 10 6.45E-03 90.1 2.86E+OO T 0 464.09 23 26 1. 50 928.04 922 10 5.93E-03 97.6 2.37E+oo* T 0 569.43 6 24 0.80 1138 .. 73 1133 9 1. 69E-03 **** 1.99E+OO T 0 656.55 10 21 0.64 1312. 99 1307 9 2.81E-03 **** 1.77E+OO T 4 709.52 11 7 1. 66 1418.95 1417 14 2.86E-03 80.2 *1.66E+OO 4 712. 69 15 11 2.51 1425.28 1417 14 3.97E-03 **** 1.65E+OO T 0 728. 90 55 16 5.34 1457.71 1446 23 1.48E-02 48.5 1 .. 62E+OO 0 786.54 -2 5 18 1. 63 1572.99 1565 16 6.91E-03 89.1 1.52E+OO T 0 917.45 10 1 1. 69 1834.85 1832 6 2.69E-03 75.2 1.34E+OO 0 948. 96 5 16 0.89 1897.88 1890 10 1. 51E-03 **** 1.31E+OO T* 3 972. 92 16 4 2.13 1945.80 1933 17 4.40E-03 **** 1.28E+OO 0 998.39 4 7 0.81 1996.75 1991 7 1. 17E-03 **** l.25E+00 0 1009.76 20 0 *o. 54 2019.50 2014 12 5.56E-03 44.7 l.24E+OO 0 1025.22 8 13 0.79 2050.42 2040 14 2.24E-03 **** 1. 22E+OO
  • T 0 1028.62 9 3 0.54 2057.21 2054 7 2.64E-03 92.1 1.22E+OO T 0 1069.85 17 3 2139.70 2134 11 4.80E-03 60.8 1.18E+OO 0 1239.08 14 21 1. 54 2478.21 2470 14 3.97E-03 **** l.04E+OO T 0 1283.25 7 3 1. 06 2566.57 2563 6 2.00E-03 **** 1. OlE+OO 0 1311.41 4 7 1. 32 2622.89 2617 8 1. llE-03 **** 9.91E-01 T Flags: "T" = Tentatively associated Page 259 of 614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:41:55.33 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245010.CNF;l *
  • Acquisition date 3-0CT-2016 04:36:41 Sensitivity 3.000 *
  • Detector ID
  • GAM39 Energy tolerance: 1. 500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.98 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:35:00 Nuclide Library : SOLID *
  • Sample ID R405245010 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.4242E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* *
  • CALIBRATION INFORMATION * * * *
  • Eff. Cal. date 27-JUL-2016 13:04:01 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
  • Combined Critical Level Report NOTE: Not all "Identified Nuc1ides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40
  • CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.614E-01 7.707E-01 4. 962E-02 3.144E-02 3.321E-02 3.162E-02 4.102E-01 1.823E-01 4.268E-02 5. 961E-02 l.709E-01 5. 961E-02 4.578E-01 5. 961E-02 1.553E-01 1.553E-01 4.268E-02 4.213E-01 5.958E-02 l.553E-01 5.369E-01 5.958E-02 5.369E-01 2.945E-02 2. 911E-02 ----Non-Identified Nuclides Nuclide . BE-7 NA-22 NA-24 AL-26 SC-46 V-48 . Page 260of614 Le (pCi/GRAM 1.223E+Ol 5:953E-02 O.OOOE+OO 3.142E-02 2.240E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 . SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 261 of 614 O.OOOE+OO 6.180E-02 5.065E-Ol O.OOOE+OO 3.893E-02 5.347E-01 7.321E+OO 4.908E-02 1.835E-01 2.583E+OO 2.176E+OO O.OOOE+OO 2. 091E-01 O.OOOE+OO O.OOOE+OO 6.539E-01 7.170E+OO 7.029E-01 O.OOOE+OO 8.040E-02 4.479E+02 3.450E-02 9.138E-01 1.929E+OO 1.509E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.995E-02 7.287E-02 5.543E+OO 4.272E-01 4. 272E-01 3.104E-02 1. 205E-01 2.105E-01 O.OOOE+OO O.OOOE+OO .1.212E-01 2.349E+OO 9.804E-02 2.302E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.160E-02 O.OOOE+OO 6.039E-02 l.390E-01 O.OOOE+OO O.OOOE+OO l.044E-01 0.000E+OO O.OOOE+OO 2.017E+Ol O.OOOE+OO 2.972E-01 6.212E-02 5.376E+OO 3.900E-02 O.OOOE+OO 6.360E+02 O.OOOE+OO 2.650E-02 9.718E-02 1.368E-01 1.483E-01 9.016E-02 1. 720E+OO 5.881E-02 5.008E+OO 2.107E-01 8.476E-02 2.581E-02 SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDE.NT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT .* SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 PA-231 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 262 of 614 4.255E+OO 1.041E+OO 9.350E-01 2.621E+Ol 9.746E+Ol 3.583E-01 2.234E+OO 5.280E-02 6.797E-01 6.848E-01 3.808E-01 6.218E-01 2.109E-01 2.109E-01. 4.730E-01 6.218E-01 6.067E-02 3.600E-01 3.287E+OO 1.764E-01 6.067E-02 0.000E+OO 2.470E-01 2.975E+02 4.729E-02 8.389E-02 7.514E-02 3'.389E-02 4.195E-02 1.020E-01 FAIL ABUN FAIL ABUN NOT IDENT. N.OT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT: FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:42:01.34 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************t************************************ * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245010.CNF;l *
  • Acquisition date 3-0CT-2016 04:36:41 Sensitivity : 3.000 *
  • Detector ID GAM39 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.98 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:35:00 Nuclide Library : SOLID *
  • Sample ID R4052.45010 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity l.4242E+02 GRAM *
  • Quantity Err(%) 1.4043E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 27-JUL-2016 13:04:01 Eff. Geometry :*CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (1.96-sigma) K-40 1.236E+Ol 1.746E+OO CD-109 2.033E+OO 1.932E+OO SN-126 1.310E-01 l.243E-01 BA-137M 3.123E-01 8.579E-02 CS-137 3.299E-01 9.062E-02 TL-208 2.085E-01 9.754E-02 PB-210 1.337E+OO 7.879E-01 BI-211 5.164E-01 1.269E+OO PB-212 9.716E-01 l.469E-01 BI-214 7. 962E-01 l.998E-01 PB-214 l.016E+00 1.998E-01 RN-222 7.962E-01 l.998E:-01 RA-224 1.424E+OO 1.877E+OO RA-226 7.962E-01 AC-228 8.992E-01 4.155E-01 RA-228 8.992E-01 4.155E-01 TH-228 9.716E-01 l.469E-01 TH-229 -3.357E-01 4.930E-01 TH-230 7.959E-01 l.998E-01 TH-232 *8. 992E-01 4.155E-01 TH-234 8.089E-01 1.487E+OO U-234 7.959E-01 l.997E-01 U-238 8.089E-01 1.487E+OO AM-243 l.660E-01 7. 513E-02 ANH-511 5.304E-02 1. 013E-01 Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 263 of 614 Key-Line Activity (pCi/GRAM -2.659E-01 2.376E-02 -1.000E+41 1. 726E-02 -3.753E-01 K.L Act error ( 1. 96-sigma) 1.444E+Ol 6.602E-02 3.291E+41 3.074E-02 3.494E-01 TPU ( 1. 96-sigma) 1. 746E+OO 1.932E+OO 1.243E-01 8.579E-02 9.062E-02 9.754E-02 7.879E-01 1.269E+OO 1.469E-01 l.998E-01 1.998E-01 l.998E-01 1.877E+OO 1.998E-01 4.l55E-01 4.155E-01 l.469E-01 4.930E-01 1.998E-01 4.155E-01 1.487E+OO 1.997E-01 l.487E+00 7.513E-02 l.013E-01 TPU ( 1. 96-sigma) 1.444E+Ol 6.688E-02 0.000E+OO 3 .171E-02 3.883E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 2.359E+03 l.187E+04 1.192E+04 SHORT HLIF CR-51 1.085E+02 3.773E+02 3.804E+02 SHORT HLIF MN-54 5.205E-03 6.949E-02 6.953E-02 NOT IDENT. C0-56 8.486E-02 5.645E-01 5.658E-01 FAIL ABUN MN-56 1. OOOE+41 6.500E+41 O.OOOE+OO SHORT HLIF C0-57 l.664E-02 4.454E-02 4.516E-02 FAIL ABUN C0-58 -6.510E-02 6.188E-01 6.195E-01 NOT IDENT. FE-59 2.245E+OO 8.152E+OO 8.215E+OO NOT IDENT. C0-60 1. 896E-02 5.429E-02 5.495E-02 NOT IDENT. ZN-65 7.579E-04 2.433E-01 2.433E-01 NOT IDENT. GE-68 4.505E-01 2.922E+OO 2.929E+OO NOT IDENT. AS-73 -l.928E+OO 2.882E+OO 3.0lOE+OO NOT IDENT. AS-74 -1.007E+03 5.752E+03 5.770E+03 SHORT HLIF SE-75 1.959E-01 2.234E-01 2.402E-01 FAIL ABUN BR-77 2.165E+37 1.829E+38 O.OOOE+OO SHORT HLIF SR-82 2.512E+02 6.147E+02 6.250E+02 SHORT HLIF RB-83 2.993E-01 8.015E-01 8.128E-01 NOT IDENT. KR-85 2.655E-01 8.398E+OO 8.399E+OO NOT IDENT. SR-85 2.671E-02 8.231E-01 8.232E-01 NOT IDENT. RB-86 1.514E+04 2.759E+04 2.842E+04 SHORT HLIF Y-88 -l.399E-01 1.978E-01 2.076E-01 NOT IDENT. Y-91 -5.847E+02 6.440E+02 6.958E+02 NOT IDENT. NB-94 2.375E-02 3.750E-02 3.900E-02 NOT IDENT. NB-95 6.289E-01 1.004E+OO 1.044E+OO NOT IDENT. NB-95M -5.176E-02 2.399E+OO 2.399E+OO NOT IDENT. ZR-95 7.320E-01 1.698E+OO 1. 729E+OO NOT IDENT. NB-97 l.OOOE+41 1. 626E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 6.768E+41 O.OOOE+OO SHORT HLIF M0-99 -2.124E+31 3. 572E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 1.843E+41 0.000E+OO SHORT HLIF RH-101 -l.655E-02 3.741E-02 3.815E-02 NOT IDENT. RH-102 9.056E-02 7.310E-02 8.373E-02 NOT IDENT. RU-103 7.915E-01 6.392E+OO 6.402E+00 FAIL ABUN RH-106 .:...2.803E-01 5.654E-01 5.794E-01 NOT IDENT. RU-106 -2.803E-01 5.654E-01 5.794E-01 NOT IDENT. AG-108M 2.456E-02 3.282E-02 3.464E-02 NOT IDENT. . AG-llOM 1.353E-01 l.163E-01 l.313E-01 FAIL ABUN SN-113 -l.597E-01 2.637E-01 2.733E-01 NOT IDENT. CD-115 1. 331E+38 3. 881E+38 0.000E+OO SHORT HLIF SN-11 (M 3.866E+04 6.979E+04 7.193E+04 SHORT HLIF TE-123M 9.339E-02 1.248E-01 l.317E-01 NOT IDENT. SB-124 l.578E+OO 2.331E+OO 2.437E+OO NOT IDENT. SB-125 9.192E-02 9.946E-02 l.077E-01 FAIL ABUN TE-125M 2.568E+02 2.490E+02 2.746E+02 NOT IDENT. I-126 3. 962E+05 6.829E+05 7*. 059E+05 SHORT HLIF SB-126 -1.386E+05 1.0l4E+06 l.016E+06 SHORT HLIF SB-127 -1.909E+21 7. 337E+21* O.OOOE+OO SHORT HLIF I-131 -2.660E+09 3.348E+09 3.556E+09 SHORT HLIF I-132 -1. OOOE+41 1. 820E+42 O.OOOE+OO SHORT HLIF TE-132 5.302E+25 8.327E+25 O.OOOE+OO SHORT HLIF BA-133 6.415E-03 5.219E-02 5.227E-02 NOT IDENT. I-133 -1. OOOE+41 2. 513E+41 O.OOOE+OO SHORT HLIF CS-134 -4.108E-04 6.857E-02 6.857E-02 FAIL ABUN CS-135 6. 722E-02 l.649E-01 1. 676E-01 NOT IDENT. I-135 l.000E+41 7. 396E+41 O.OOOE+OO SHORT HLIF CS-136 -6. 396E+04 2.439E+05 2.456E+05 SHORT HLIF CE-139 4.640E-02 1.108E-01 l.128E-01 NOT IDENT. BA-140 -6.938E+04 1.086E+06 l.087E+06 SHORT HLIF LA-140 6.498E+04 1.959E+05 1.981E+05 SHORT HLIF CE-141 -7.910E+OO 2.234E+Ol 2.262E+Ol NOT IDENT. CE-143 l.OOOE+41 8. 809E+4*0 O.OOOE+OO SHORT HLIF CE-144 -1.524E-01 3.713E-01 3.776E-01 NOT IDENT. PM-144 -l.919E-02 7.793E-02 7.840E-02 NOT IDENT. PR-144 1. 581E+OO 6.224E+OO 6.265E+OO NOT IDENT. PM-146 -2.063E-02 4.870E-02 4.959E-02 NOT IDENT. ND-147 -2.062E+07 2. 956E+'07 3.099E+07 SHORT HLIF PM-147 4. 996E+Ol 7.505E+02 7.509E+02 NOT IDENT. PM-149 -2.614E+39 5.085E+39 O.OOOE+OO SHORT HLIF EU-150 l.169E-02 3 .197E...:02 3.240E-02 FAIL ABUN EU-152 8.427E-02 1.348E-01 1.400E-01 FAIL ABUN GD-153 -1.630E-01 1.922E-Ol 2.057E-01 NOT IDENT. EU-154 6.480E-02 1.636E-01 l.662E-01 NOT IDENT. EU-155 2.543E-02 1.040E-01 1.046E-01 FAIL ABUN TB-160 4. 781E-01 1.878E+OO 1. 8 90E+o*o FAIL ABUN H0-166M 8.648E-02 9.327E-02 1. OllE-01 FAIL ABUN TM-171 2 .135E+OO 5.936E+OO 6.014E+OO NOT IDENT. HF-172 l.431E-01 2.383E-01 2.469E-01 FAIL ABUN LU-172 3.190E-02 9.285E-02 9.396E-02 FAIL ABUN Page 264 of 614 LU-176 1. 896E-02 2.815E-02 2.942E-02 FAIL ABUN HF-181 2.934E-01 4.941E+OO 4.943E+OO FAIL ABUN TA-182 4.146E-01 1.153E+OO l.168E+OO FAIL ABUN RE-183 8.348E-01 1.009E+OO l.076E+OO NOT IDENT. RE-184 -5.391E-01 3.014E+Ol 3.014E+Ol NOT IDENT. W-188 -1. 740E+Ol 1.253E+02 l.256E+02 FAIL ABUN IR-192 -5.687E-01 4.790E-01 5.433E-01 FAIL ABUN HG-203 -2.884E-01 2.545E+OO 2.549E+OO FAIL ABUN BI-207 3.734E-02 5. 728E-02 5.970E-02 FAIL ABUN PB-211 l.592E-01 7.647E-01 7. 681E-01 NOT IDENT. BI-212 1. 017E+OO 6.783E-01 8.187E-01 FAIL ABUN RN-219 -5.459E-02 4.470E-01 4.477E-01 FAIL ABUN RA-223 -2.404E-02 7. lOlE-01 7.lOlE-01 FAIL ABUN AC-227 -5.393E-02 2.421E-01 2.433E-01 NOT IDENT. TH-227 -5.393E-02 2.421E-01 2.433E-01 NOT IDENT. PA-231 4.035E-01 5.487E-01 5.781E-01 NOT IDENT. TH-231 -2.404E-02 7.lOlE-01 7.lOlE-01 FAIL ABUN PA-233 -1. 411E-02 7.038E-02 7.067E-02 FAIL ABUN PA-234. 2.013E-01 4.855E-01 4.939E-01 FAIL ABUN PA-234M -3.466E+OO 5.032E+OO 5.269E+OO NOT IDENT. U-235 -3.661E-02 1.930E-01 l.937E-01 FAIL ABUN NP-237 -1. 411E-02 7.038E-02 7.067E-02 FAIL ABUN NP-238 -1.229E+40 4.939E+40 O.OOOE+OO SHORT HLIF NP-239 2.433E-01 2.728E-01 2.941E-01 NOT IDENT. PU-239 1. 755E+02 3.389E+02 3.480E+02 NOT IDENT. AM-241 -2.320E-02 6 .116E-02 6.205E-02 NOT IDENT. CM-243 2.088E-02 9.695E-02 9.740E-02 NOT IDENT. BK-247 4. 546E-02' 8.837E-02 9.071E-02 FAIL ABUN' CM-247 -2.342E-02 4.237E-02 4.367E-02 NOT IDENT. CF-249 3.872E-02 4.378E-02 4.713E-02 NOT IDENT. CF-251 -4.147E-02 l.154E-01 l.169E-01 NOT IDENT. Page 265of614
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA REPORT
  • SPECTROSCOPY BACKGROUND ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 80.5991 87.09 89.8737 136.47 76.5106 45.60 92.7203 87.57 89.9328 140.51 0.0000 46.54 76.6776 88.03 89.9902 143.76 71. 6081 49.72 0.0000 88.34 90.0285 144.24 71.6427 51. 35 92.2908 88.47 90.0442 145.44 71. 7291 51. 87 80.4619 89. 96 90.2274 152.43 68.8258 52.39 68.6090 1093.63 90.3103 153.25 0.0000 52.97 83.6152 91.11 0.0000 323.87 51.0693 53.44 103 .1164 92.59 90.5469 156.02 0.0000 54.07 94.2597 93.35 90.6379 158.56 0.0000 57.36 0.0000 94.56 84.4121 159.00 50.4480 57.53 85.8204 94.65 79.6432 162.33 54.0368 57.98 67.8069 94.67 79.6458' 162.66 0.0000 59.27 92.1252 94.87 79.6666 163.33 59.2379 59.32 92.1332 97.43 102.3132 165.86 57.6558 59.54 92.1686 98.43 75.6330 176.31 56.4631 60. 96 86.3370 98.44 75.6339 176.60 0.0000 61.17 77.2766 99.53 61. 3127 177.52 59.1320 62.93 109.4238 100 .11 73.3888 181.07 0.0000 63.29 109.4905 102.03 94.0687 181.52 54.9750 63.58 109.5438 103.18 71.2567 184.41 65.6097 64.28 120.3347 103.37 71. 2738 143.76 56.0495 66.73 85.6452 105.21 67.8035 193.51 65.2333 67.24 139.2891 105.31 67.8121 197.03. 60.1184 125.81 136.7076 106.12 76.3640 198.01 53.9732 67.75 140.1699 106.47 76.3967 201.83 57.6909 69.67 113.7107 109.28 58.4055 203.43 58.6544 70.83 95.4452 111. 00 92.6650 205.31 46.2818 72.81 105.3916 111.76 0.0000 210.85 59.8941 72.87 105.4013 114. 06 74.6446 215.65 49.3508 74.66 105.6909 116. 30 0.0000 222 .11 47.7919 74.82 105.7165 116.74 71.194 6 227.09 43.4453 74.97 105.7402 119.76 68.9767 227.38 38.9281 77 .11 106.0810 121.12 50.5784 228.16 0.0000 78.74 106.3379 121. 22 50.5840 228.18 34.4222 79.69 98.2946 121.78 51.8505 116.74 34.4222 80.12 98.3561 122.06 51. 8 668 235.69 45.0880 80.19 0.0000 122. 92' 61.8053 235. 96 37.3527 80.57 92.1719 123.07 53.1615 238.63 37.4253 81. 00 75.0342 265.00 58.1461 238.98 0.0000 81.'07 75.0415 125.81 59.5228 240.99 37.4887 81. 75 63.3785 127.23 80.7288 242.00 37.5158 83.79 105.1540 127.91 77.0601 244.70 37.5879 84.00 105.1850 129.30 68.4624 252.40 0.0000 85.43 92.0257 131.20 *69. 8496 252.80 40.5683 86.55 89.8064 133.02 69.9855 254.15 0.0000 86.79 89.8360 133.52 68.7718 256.23 42.5129 86.94 89.8551 136.00 66.4441 260.90 0.0000 Page 266 of 614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 31. 2313 355.39 0.0000 584.27 14. 7195 264.80 35. 6969 356.01 30.9463 595.83 0.0000 265.00 36.2594 364.49 0.0000 427.87 26.3320 268.22 36.3372 366.42 0.0000 602.52 0.0000 269.46 37.2998 372.51 23.7891 604. 72 21.4281 270.03 37.3136 375.05 29.7766 607.14 19.7974 271. 23 29.4082 377.52 23.8521 609.32 16.5112 273.65 0.0000 356.01 24.9288 610.33 16.5179 276.40 44.9648 388.16 22.9855 614.28 18 .1966 277.37 37.4943 388.63 0.0000 618.01 16.5649 277.60 36.5625 391.69 35.0420 620.36 15.4743 278.00 36.5720 264.66 30.1733 621. 93 18.8013 279.20 47.8623 401. 81 30.1910 630.19 0.0000 279.54 49.7500 402.40 35.2336 631. 29 11. 097 4 279.70 49.7554 404.85 26.2058 633.25 22.2111 280.46 49.7802 410*. 95 34.3735 634.78 0.0000 283.69 37.6481 413. 71 17.2103 635.95 18.8974 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 31.0939 423. 72 0. 0000. 645.85 21.1964 .285.90 0.0000 427.09 23.4371 657.76 3. 3611 287.50 31.1356 427.87 12.2327 657.90 0.0000 290.67 38.2885 433.94 20.4472 661. 66 15.1458 293.27 0.0000 439.40 22.5505 664.57 0.0000 351. 93 45.5088 453.88 24.7676 666.33 0.0000 295. 96 45.5303 463.37 17.6205 666.50 0.0000 879.38 48.4548 468.07 21.8130' 667. 71 0.0000 299.98 38.5117 473.00 0.0000 677. 62 21. 4353 300.09 38.5142 475.06 26.0498 685.70 0.0000 300.13 38.5150 476.78 25.0269 695.00 0.0000 301.36 32.8344 477.60 25.0361 696.49 26.1165 302.85 48.5824 482.18 26.1327 696. 51 19.3035 256.23 39.0956 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 14.7657 306.78 28.6462 497.08 24.1993 697.49 14.7662 308.46 42.0575 505.52 19.0078 702.65 13.6543 311. 90 41.1873 507.63 0.0000 706.68 22.2184 316.51 43.2220 511. 00 25.4028 711. 68 14.8371 319.41 0.0000 514.00 25.4355 720.70 0.0000 320.08 0.0000 514.00 25.4355 721. 93 0.0000 321. 04 40.4491. 520.40 17.5339 722.78 12.0283 323.87 40.5166 520.69 0.0000 722. 91 12.0287 325.23 42.4791 522.65 0.0000 723.31 13.7490 328.76 0.0000 527.90 0.0000 724.19 10.3147 333.37 29.1003 528.26 22.3894 727.33 9.1781 333.97 32. 0211 529.59 21. 3354 733.00 13.7925 334.37 45 .1311 529.87 0.0000 735.93 6.9031 338.28 33.5594 5-31. 02 0.0000 333.97 9.6691 338.32 33.5602 537.26 0.0000 739.50 0.0000 311. 90 33.6009 546.56 *o. 0000 747.24 10.3923 340.48 33.6009 552.55 25.8428 748.06 19.6355 340.55 0.0000 563.25 7.7862 752.31 8.0963 344.28 23.4248 569.33 19.5125 753.82 0.0000 345.93 24.9122 946.00 19.5132 756.73 13.8989 351.06 31.3516 569.70 26.0195 756.80 13.8994 351.93 31.3665 583.19 17 . .4382 884.68 22.0569 Page 267. of 614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 7 65. 81 15.1005 1274.44 13.4002 1620.50 1.0632 766.42 15.1037 1001.03 10.4351 1621. 92 4.2539 766.84 18.5918 1002.74 6.5249 1678.03 0.0000 772. 60 0.0000 1004.73 7.4609 1690.97 2.1528 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 1.0899 778.90 10.4974 1028.54 0.0000 1063.66 3.4912 783.70 0.0000 1037.84 5.6429 1771.35 5.4559 785.37 14.0249 1038.76 0.0000 1791.20 0.0000 792.07 22.4859 631.29 6.5980 1808.65 1.0979 794.95 17.5830 1048.07 0.0000 1810. 72 0.0000 795.86 22.8643 1049.04 10.3749 1836.06 3.3083 810.06 14.1313 1050.41 11. 3218 810.29 14.1323 1063.66 7.5728 344.28 14.1333 1077.00 0.0000 810.76 14.1348 1077.34 12.3470 815.77 0.0000 1085.87 18.0839 1048.07 0.0000 1093.63 10.4891 832.01 10.6688 1099.45 13.3685 834.85 13.3475 1112. 07 15.3242 835.71 15.1308 1112.84 9.8532 836.80 0.0000 1115.54 13.8032 846.75 0.0000 1120.29 12.4755 846.77 16.0730 1120.55 12.4763 856.80 0.0000 1221.41 12.4787 860.56 10.7585 1129. 67 10.9919 871.09 14.3887 1131. 51 0.0000 873.19 11. 697 9 1147.95 0.0000 875.33 0.0000 1173.23. 13. 6027 879.38 9.9157 1177.95 8.7539 880.51 18.0341 1189.05 9.7510 883.24 14.4385 1204.77 18.5930 884.68 7.2224 1221.41 12.7691 889.28 13.5594 1231.02 12.3742 894.76 10.8644 1235.36 0.0000 898.04 12.6866 1238.28 14.7885 900. 72 11. 7896 1260.41 0.0000 903.28 12.7054 1271.87 13.9043 911.20 18.9186 1274.44 11. 9246 912.08 18.9230 1274.54 11. 9246 923.98 0.0000 1291.59 8.9758 926.50 15.5276 1298.22 0.0000 929 .11 8. 22 63 1312 .11 0.0000 937.49 19.2389 1332.49 9.0538 944.13 0.0000 1362.66 0.0000 946.00 14;6919 1365.19 5.0638 949.00 5.8816 1368.63 0.0000 667. 71 0.0000 1384.29 3.0500 962. 31 15.6786 1408.01 3.0646 964.08 19.1928 1457.56 0.0000 966 .17 25.1124 1460.82 4.1287 911. 20 13.8588 1489.16 10.3778 968. 97 13.8588 1505.03 7.2867 983.53 0.0000 1584.12 6.3376 984.45 0.0000 1596. 21 0.0000 Page 268 of 614 VAX/VMS Nuclide Identification Report Gen.erated 3-0CT-2016 05: 46: 25. 24 ********************************************************************************
  • GEL.Laboratories LLC *
  • 2040 Savage Road. *
  • Charleston, SC 29407 * ********************************************************************************* Configuration : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245011.CNF;l Background file : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM08.CNF;320 Background date : 2-0CT-2016 11:00:23. Sample date :. 15-DEC-2015 12:53:00 Acquisition date : 3-0CT-2016 04:45:57. Sample ID : R405245011 Sample quantity : 1.34661E+02 GRAM Detector name : GAM08 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.63 0.0% Energy tolerance : 1.50000 keV Analyst Initials : MXRl Abundance limit : 75.00000 Sensitivity : 3.00000 Batch ID : 1596387 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 1 1 0 0 0 0 0 0 0 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 3 3 0 Page 269of614 Energy 30.20* 63.99* 74.77* 76.97* 86.96* 93.05* 105.94 117. 30 128.15 143.80* 185.68* 210.21 238.61* 241.91 295.42* 338.69*' 351. 84* 463.12 511. 20* 583.17* 609.24* 661. 99 681.17 727. 15* 734.16 911. 20* 969.48* 990.07 1120. 43* 1166. 61 1172.34 1235.58 1238.09 1288.00 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 13 28 76 115 24 30 24 30 14 34 78 10 313 84 92 86 163 43 47 99 126 91 8 30 19 75 56 6 19 14 6 11 23 7 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 138 180 158 149 180 182 130 64 89 115 76 108 49 63 50 45 68 33 32 30 38 39 15 18 9 4 14 15 16 3 2 5 9 8 1. 40 1. 68 1.18 1.17 0.98 1. 00 1. 40 0.80 1. 56 1. 52 1.13 0.73 1. 37 1. 79 1. 27 1. 45 1. 23 1. 92 1. 87 1. 42 1. 44 1. 69 1. 34 0.89 1. 34 1. 65 2.12 3.31 1. 66 2.84 0.48 1. 88 2.32 1. 00 60.62 128.22 149.80 154.20 174.19 186.38 212.17 234.91 256.61 287.92 371. 71 420.80 477.62 484.23 591.29 677.86 704.18 926.82 1023.02 1167. 02 1219.17 1324. 71 1363.10 1455.08 1469.11 1823.30 1939.91 1981.10 2241. 89 2334.28 2345.73 2472.24 2477.27 2577.13 58 122 145 145 170 181 207 232 255 282 368 414 470 470 587 671 699 921 1014 1160 1212 1318 1355 1448 1462 1818 1932 1973 2236 2327 2341 2470 '2470 2570 10 3.74E-03169.4 11 7. 7 8E-03 97. 0 13 2.12E-02 29.1 2.12E+OO' 13 3.19E-02 20.3 9 6.67E-03104.2 9 8.47E-03 86.7 10 6.78E-03 90.2 7 8.20E-03 48.8 8 3.81E-03121.8 11 9.42E-03 65.5 9 2.17E-02 24.8 8 2.78E-03182.8 28 8.68E-02 7.0 1.40E+OO 28 2.34E-02 24.2 8 2.54E-02 17.4 13 2.40E-02 19.7 12 4.53E-02 12.9 12 1. 20E-02 31. 4 19 1.31E-02 38.6 15 2.74E-02 15.9 15 3.49E-02 14.1 11 2.52E-02 16.9 11 2.28E-03100.9 14 8.21E-03 36.9 12 5.37E-03 38.4 13 2.09E-02 13.l 20 1.55E-02 21.9 14 1. 71E-03136. 2 13 5.29E-03 50.4 15 3.86E-03 40.1 8 1. 70E-03 56. 6 13 2.93E-03 36.4 3.05E-01 13 6.45E-03 35.0 11 1.96E-03 86.9 Peak Search Report (continued) Sample ID : R405245011 Acquisition date Page : 2 3-0CT-2016 04:45:57 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1460.93 36 0 1560.44 245 8 15 2.06 2923.05 2915 15 6.BOE-02 7.3 0 3.30 3122.13 3116 11 2.2iE-03 35.4 Flag: "*" = Peak area was modified by background subtraction Page 270 of 614 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 05:46:27 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245011.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 15-DEC-2015 12:53:00 R405245011 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 04:45:57 134.66 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMAS 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfe.ring Page 271of614 Nuclide PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 87.09 87.09 87.09 87.09 242.00 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide EU-155 SN-126 SN-126 CD-109 RA-224 AM-243 TH-228 PB-212' BI-211 Line 86.55 86.94 87.57 88.03 240.99 74.66 74.82 74.82 351.06 CAN 0 01:00:00.63 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID R405245011 Acquisition date 3-0CT-2016 04:45:57 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 9.670E-01 1.264E+Ol 1.264E+Ol 14.54 OK CD-109 88.03 3.70* 4.279E+OO 2.106E-01 3.268E-01 990.75 OK SN-126 64.28 9.60 2.216E+OO 8.784E-01 8.784E-01 194.00 OK 86.94 8.90 4. 279E+O.O 8.754E-02 8.754E-02 990.75 OK 87.57 37.00* 4.279E+OO 2.106E-02 2.106E-02 990.75 OK BA-137M 661.66 89.90* l.814E+OO 3.158E-01 3.217E-01 33.79 OK CS-137 661.66 85.10* 1 .. 814E+OO 3.336E-01 3.398E-01 33.79 OK EU-155 86.55 30.70 4.279E+OO 2.538E-02 2.852E-02 990.75 OK 105.31 21.10* 5.159E+OO 1.449E-01 l.629E-01 180.40 OK TL-208 277.37 6.60 3. 710E+OO Line Not Found Absent 583.19 85.00* 2.007E+OO 3.312E-01 3.312E-01 31. 90 OK 860.56 12.50 l.478E+OO Line Not Found Absent BI-211 72. 87 1. 23 3.135E+OO Line Not Found Absent 351. 06 12.92* 3.046E+00 l.246E-01 1.246E-01 829.07 OK PB-212 74.82 10.28 3.314E+OO 9.993E-01 9.993E-01 87". 79 OK 77 .11 17.10 3.512E+OO 1. 263E+OO 1. 263E+00 40.63 OK 238.63 43.60* 4.174E+OO l.049E+00 1.049E+OO 14.02 OK 300.09 3.30 3.479E+OO Line Not Found Absent BI-214 .609.32 45.49* 1.938E+OO 8.132E-01 8.134E-01 28". 23 OK 1120.29 14.92 l.202E+OO 5.780E-01 5.782E-01 100.70 OK 1764.49 15.30 8.180E-01 Line Not Found Absent PB-214 74.82 5.80 3.318E+OO Line Not Found <<INT Reject 77 .11 9.70 3.512E+OO 2.227E+OO 2.227E+OO 40.63 OK 87.09 3.41 4.288E+OO Line Not Found <<INT Reject 242.00 7.25 4.130E+OO Line Not Found <<INT Reject 295.22 18.42 3.524E+OO 8.489E-01 8.492E-01 34.78 OK 351.93 35.60* 3.046E+OO Line Not Found <<INT Reject RN-2?2 609.32 45.49* l.938E+00 8.132E-01 8.134E-01 28.23 OK 1120.29 14.92 t.202E+OO 5.780E-01 5.782E-01 100.70 OK 1764.49 15.30 8.180E-01 Line Not Found Absent RA-224 240.99 4.10* 4.131E+OO l.528E+00 1. 528E+OO 101.81 OK RA-226 609.32 45.49* 1.938E+00 8.132E-01 8.134E-01 28.23 OK 1120.29 14.92 1. 202E+OO 5. 780E-Ol* 5.782E-01 100.70 OK 1764.49 15.30 8.180E-01 Line Not Found Absent AC-228 105.21 1.10 5.159E+OO 2.779E+OO 2.779E+OO 180.40 OK 338.32 11. 27 3.145E+OO 1. 453E+OO 1.453E+OO 39.44 OK 794.95 4.25 l.572E+00 Line Not Found Absent 835. 71 1. 61 1.512E+OO Line Not Found Absent 911.20 25.80* 1.414E+OO l.140E+OO 1.140E+OO 26.14 OK 968.97 15.80 1. 347E+OO 1.445E+OO 1.445E+OO 43.78 OK RA-228 105.21 1.10 5.159E+OO 2.779E+OO 2.779E+OO 180.40 OK 338.32 11. 27 3.145E+OO 1.453E+OO 1.453E+OO 39.44 OK 794.95 4.25 1.572E+OO Line Not Found Absent 835. 71 1. 61 1.512E+OO Line Not Found Absent 911. 20 25.80* 1.414E+OO 1.140E+00 1.140E+OO 26.14 OK 968. 97 15.80 1. 347E+OO 1.445E+OO 1.445E+OO 43.78 OK TH-228 74.82 10.28 3.314E+OO 9.993E-01 9.993E-01 87.79 OK 77 .11 17.10 3.512E+OO l.263E+OO 1. 263E+OO 40.63 OK 238.63 43.60* 4.174E+OO 1.049E+OO l.049E+00 H.02 OK 272 of 614 Nuclide Line Activity Report (continued) Page : 3 Sample ID : R405245011 Acquisition date 3-0CT-2016 04:45:57 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 3.479E+OO Line Not Found Absent TH-230 609.32 45.49* 1.938E+OO 8 .132E-01 8.132E-01 28.23 OK 1120.29 14.92 1.202E+OO 5.780E-01 5.780E-01 100.70 OK 1764.49 15.30 8.180E-01 Line Not Found Absent TH-232 105.21 1.10 5.159E+OO 2.779E+OO 2.779E+OO 180.40 OK 338.32 11.27 3.145E+OO 1.453E+OO 1.453E+OO 39.44 OK 835. 71 1. 61 1.512E+OO -----Line Not Found Absent 911.20 25.80* l.414E+OO 1.140E+OO 1.140E+OO 26.14 OK 968.97 15.80 1.347E+OO 1.445E+OO 1.445E+OO 43.78 OK TH-234 63. 29 3.70* 2.216E+OO 2.279E+OO 2.279E+OO 194.00 OK 92. 59 4.23 4.640E+OO 1.012E+OO 1.012E+OO 173.37 OK U-234 609.32 45.49* 1.938E+OO 8.132E-01 8.132E-01 28.23 OK 1120.29 14.92 1.202E+OO 5.780E-01 5.780E-01 100.70 OK 1764.49 15.30 8.180E-01 Line Not Found Absent U-235 89. 96 3.47 4.467E+OO Line Not Found Absent 93.35 5.60 4.640E+OO 7.645E-01 7.645E-01 173.37 OK 143.76 10. 96* 5.443E+OO 3.595E-01 3.595E-01 130.91 OK 163.33 5.08 5.246E+OO Line Not Found Absent 185. 72 57.20 4.933E+OO 1. nrn.:..01 1. 721E-01 49.68 OK 205.31 5.01 4.641E+00 Line Not .Pound Absent U-238 63.29 3.70* 2.216E+OO 2.279E+OO 2.279E+OO 194.00 OK 92. 59 4.23 4.640E+OO 1.012E+OO 1. 012E+OO 173.37 OK AM-243 43.53 5.90 2.327E-01 Line Not Found* Absent 74.66 67.20* 3.314E+OO 1.529E-01 1.529E-01 87.79 OK ANH-511 511. 00 100.00* 2.232E+OO 1.225E-01 1.225E-01 77.20 OK Flag: "*" = Keyline Page 273 of 614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:46:28.29 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245011:CNF;l * *Acquisition 3-0CT-2016 04:45:57 Sensitivity : 3.000 *
  • Detector ID GAM08 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.63 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:53:00 Analyst initials: MXRl *
  • Sample ID R405245011 Sample Quantity 1.3466E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1 . 96-sigma) K-40 1.264E+Ol 1. 801E+OO CD-109 3.268E-01 3.173E+OO SN-126 2.106E-02 2.044E-01 BA-137M 3.217E-01 l.065E-01 CS-137 3.398E-01 l.125E-01 EU-155 l.629E-01 2.879E-01 TL-208 3.312E-01 1.035E-01 BI-211 1. 24 6E-01 1.012E+OO PB-212 1. 049E+OO l.442E-01 BI-214 8.134E-01 2.250E-01 PB-214 8.944E-01 2.264E-01 RN-222 8 .134E-01 2.250E-01 RA-224 l.528E+OO 1.524E+OO RA-226 8 .134E-01 2.250E-01 AC-228 l.140E+OO 2.920E-01 RA-228 l.140E+00 2.920E-01 TH-228 1.049E+OO l.442E-01 TH-230 8.132E-01 2.249E-01 TH-232 l.140E+OO 2.920E-01 TH-234 2.279E+OO 4.333E+OO U-234 8.132E-01 2.249E-01 U-235 3.595E-01 4.612E-01 U-238 2.279E+OO 4.333E+OO AM-243 1. 52 9E-01 1:315E-01 ANH-511 l.225E-01 9.268E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 274 of 614 Key-Line Activity (pCi/GRAM -1.330E+OO -4.432E-02 O.OOOE+OO 1. 886E-02 2.636E-01 K.L. Cnt Uncert ( 1. 96-sigma) 1.339E+Ol 6. 096E-02 l.336E+41 2.930E-02 4.071E-01 MDA (pCi/GRAM 8.505E-01 2.838E+OO 1. 831E-01 9.083E-02 9.595E-02 2.397E-01 7.035E-02 4.464E-01 l.092E-01 1.565E-01 3.620E-01 1.565E-01 1.170E+OO 1.565E-01 2.528E-01 2.528E-01 1.092E-01 l.565E-01 2.528E-01 3.044E+OO l.564E-01 3.495E-01 3.044E+OO l.345E-01 4. 960E-02 MDA (pCi/GRAM 2.512E+Ol l.013E-01 O.OOOE+OO 8.094E-02 9.025E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 O.OOOE+OO 1. 363E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.268E+02 O.OOOE+OO SHORT HLIF MN-54 8.086E-02 7.036E-02 1.639E-01 NOT IDENT. C0-56 3.830E-02 5.338E-01 1.074E+OO FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 8.816E-03 6 .114E-02 l .118E-01 NOT IDENT. C0-58 -8.355E-02 6.033E-01 l.192E+OO NOT IDENT. FE-59 -3.504E+OO 6.768E+OO 1.211E+Ol NOT IDENT. C0-60 1. 727E-02 4. 713E-02 1.018E-01 FAIL ABUN ZN-65 -3.176E-05 2.086E-01 3.646E-01 NOT IDENT. GE-68 -2.089E+OO 3.026E+OO 5.196E+OO NOT IDENT. AS-73 2.129E+OO l.479E+Ol 2.825E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.112E+03 O.OOOE+OO SHORT HLIF SE-75 -1.073E-01 2.257E-01 4.173E-01 NOT IDENT. BR-77 0.000E+OO 3.207E+36 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 6.100E+02 O.OOOE+OO SHORT HLIF RB-83 -1.315E-01 7.615E-01 1.406E+OO NOT IDENT. KR-85 1.102E+Ol 8.017E+OO l.782E+Ol NOT IDENT. SR-85 1.077E+OO 7.852E-01 .1. 7 45E+OO NOT IDENT. RB-86 O.OOOE+OO 2.735E+04 O.OOOE+OO SHORT HLIF Y-88 4.602E-02 2.413E-01 5.645E-01 NOT IDENT. Y-91 7.625E+00 5.774E+02 1.131E+03 NOT IDENT. NB-94 l.393E-02 3.426E-02 7.282E-02 NOT IDENT. NB-95 -1.565E-01 1.035E+OO 1.990E+00 NOT IDENT. NB-95M 3.007E-01 2. 872E+OO 5.029E+OO NOT IDENT. ZR-95 7.957E-01 1. 721E+OO 3. 613E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 24 7E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 3.184E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.835E+41 0.000E+OO SHORT HLIF RH-101 2.777E-02 6.627E-02 6.666E-02 FAIL ABUN RH-102 7.343E-02 7.262E-02 l.573E-01 NOT IDENT. RU-103 -3.574E-01 5.327E+OO 1.019E+Ol FAIL ABUN RH-106 -3.463E-01 6.066E-01 1.031E+OO NOT IDENT. RU-106 -3.463E-01 6.066E-01 1.031E+OO NOT IDENT. AG-108M 3.395E-02 3 .119E-02 6.814E-02 NOT IDENT. AG-llOM' 7.868E-02 l.082E-01 2. "442E-01 NOT IDENT. SN-113 -8.900E-02 2. 811E-01 5.141E-01 NOT IDENT. CD-115 O.OOOE+OO 3.562E+38 0.000E+OO SHORT HLIF SN..,.117M 0.000E+OO 8:922E+04 O.OOOE+OO SHORT HLIF TE-123M 1.445E-02 1.540E-01 2.773E-01 NOT IDENT. SB-124 1.202E+OO 1.360E+OO 4.310E+OO NOT IDENT. SB-125 9.768E-02 l.210E-01 2.539E-01 FAIL ABUN TE-125M -4.586E+Ol 3.318E+02 5.479E+02 NOT IDENT. I-126 O.OOOE+OO 9.824E+05 0.000E+OO SHORT HLIF SB-126 O.OOOE+OO 7.982E+05 0.000E+OO SHORT HLIF SB-127 O.OOOE+OO 6.321E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.350E+09 O.OOOE+OO SHORT HLIF I-132 0 .. OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 9. 724E+25 O.OOOE+OO SHORT HLIF BA-133 -3.252E-02 5.774E-02 9.021E-02 NOT IDENT. I-133 *o. OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-134 3.421E-02 5.578E-02 l.215E-01 NOT IDENT. CS-135 -6.406E-02 1.522E-01 2.828E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.924E+05 0.000E+OO SHORT HLIF CE-139 8.620E-03 1.300E-01 2.329E-01 NOT IDENT. BA-140 O.OOOE+OO l.070E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.502E+05 O.OOOE+OO SHORT HLIF CE-141 1.307E+Ol 2.434E+Ol 4. 311E+Ol NOT IDENT. CE-143 0.000E+OO l.095E+41 O.OOOE+OO SHORT HLIF CE-144 -7.755E-02 4.497E-01 7.864E-01 NOT IDENT. PM-144 4. 964E-03 5.599E-02 1.153E-01 NOT IDENT. PR-144 4.296E-01 4.846E+OO 9.979E+OO NOT IDENT. PM-146 4.815E-02 5.826E-02 1.200E-01 NOT IDENT. ND-147 O.OOOE+Od l.954E+07 0.000E+OO SHORT I-iLIF PM-147 4. 691E+02 l.107E+03 1.934E+03 NOT IDENT. PM-149 O.OOOE+OO 5.560E+39 O.OOOE+OO SHORT HLIF EU-150 1.063E-03 2.835E-02 4.971E-02 FAIL ABUN EU-152 l.170E-02 1.045E-01 1. 959E-01 NOT IDENT. GD-153 4.474E-02 2.049E-01 3.848E-01 NOT IDENT. EU-154 -1.122E-01 1.494E-01 2.466E-01 NOT IDENT. TB-160 -1.259E+00 l.840E+OO 3.255E+OO FAIL ABUN H0-166M -2.834E-03 6.056E-02. 1.219E-01 FAIL ABUN TM-171 -6.785E+OO 3.711E+Ol 6.920E+Ol NOT IDENT. HF-172 -2.480E-01 2.936E-01 4.393E-01 FAIL ABUN LU-172 1.984E-02 8.757E-02 l.850E-01 FAIL ABUN LU-176 7.158E-03 2.943E-02 5. 781E-02. FAIL ABUN Page 275 of 614 HF-181 -2.444E+OO 4.463E+OO 7. 821E+OO NOT IDENT. TA-182 6.995E-01 1.166E+OO 2.445E+OO FAIL ABUN RE-183 -9.270E-01 4.306E+OO 8.004E+OO NOT IDENT. RE-184 -2.450E+Ol 3.041E+Ol 5.210E+Ol NOT IDENT. W-188 -2.303E+Ol 1. 305E+02 2.207E+02 FAIL ABUN IR-192 3.943E-01 5.591E-01 1.135E+OO FAIL ABUN HG-203 -2.502E+OO 2.633E+OO 4.582E+OO NOT IDENT. BI-207 -1.114E-02 6.555E-02 1.239E-01 FAIL ABUN . PB-210 -l.649E+OO 6. 727E+OO 1.265E+Ol NOT IDENT. PB-211 3.165E-01 8.197E-01 l.626E+OO NOT IDENT. BI-212 l.480E+OO 1. 070E+OO l.568E+OO FAIL ABUN RN-219 -2. 221E-01 4.547E-01 8.143E-01 NOT IDENT. RA-223 -9.873E-03 6.912E-01 l.290E+OO FAIL ABUN AC-227 2.809E-01 2.651E-01 5.592E-01 NOT IDENT. TH-227 2.809E-01 2.651E-01 5.592E-01 NOT IDENT. TH-229 -5.536E-02 5.361E-01 l.037E+OO FAIL ABUN PA-231 9.694E-03 5.179E-01 9.950E-01 NOT IDENT. TH-231 -9.873E-03 6.912E-01 1.290E+OO FAIL ABUN PA-233 2.849E-02 7.125E-02 1. 421E-01 NOT IDENT. PA-234 -8.599E-02 3.127E-01 5. 964E-01 FAIL ABUN PA-234M -1. 644E+OO 5.129E+OO 1.003E+Ol NOT IDENT. NP-237 2.849E-02 7.125E-02 1.421E-01 NOT IDENT. NP-238 O.OOOE+OO 4.612E+40 O.OOOE+OO SHORT HLIF NP-239 4.421E-01 4.225E-01 5.632E-01 FAIL ABUN PU-239 2.529E+02 6.035E+02 7.063E+02 FAIL ABUN AM-241 1.417E-0.1 2.217E-01 4 .115E:_Ol NOT IDENT. CM-243 1. 966E-02 1.340E-01 2.297E-01 NOTc IDENT. BK-247 -6.146E-02 8.287E-02 1.488E-01 FAIL ABUN CM-247 -3.382E-02 4.227E-02 7.239E-02 NOT IDENT. CF-249 5.843E-03 4. 813E-02 9.244E-02 NOT IDENT. CF-251 9.295E-02 1.312E-01 2.700E-01 NOT IDENT. Page 276 of 614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:46:25.97 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 234 10.66* 9.670E-01 1.264E+Ol 1.264E+Ol 14.54 CD-109 88.03 28 3.70* 4.279E+OO 9.929E-01 l.541E+OO 208.30 SN-126 64.28 34 9.60 2.216E+OO 8.784E-01 8.784E-01 194.00 86.94 28 8.90 4.279E+OO 4.128E-01 4.128E-01 208.30 87.57 28 37.00* 4.279E+OO 9.929E-02 9.929E-02 208.30 BA-137M 661.66 92 89.90* l.814E+OO 3.158E-01 3.217E-01 33.79 CS-137 661. 66 92 85.10* 1.814E+OO 3.336E-01 3.398E-01 33.79 EU-155 86.55 28 30.70 4.279E+OO 1.197E-Ol l.345E-01 208.30 105.31 28 21.10* 5.159E+OO l.449E-01 1.629E-01 180.40 TL-208 277.37 ------6.60 3. 710E+OO ------Line Not Found ------583.19 101 85.00* 2.007E+OO 3.312E-01 3.312E-01 31. 90 860.56 ------12.50 1.478E+OO ------Line Not Found ------BI-211 72.87 ------1. 23 3.135E+OO ------Line Not Found ------351.06* 174 12.92* 3.046E+OO 2.464E+OO 2.464E+OO 25.83 PB-212 74.82 90 10.28 3.314E+OO 1.478E+OO 1.478E+OO 58.27 77 .11 136 17.10 3.512E+OO 1.263E+OO 1.263E+OO 40.63 238.63 342 43.60* 4.174E+OO l.049E+OO 1.049E+OO 14.02 300.09 ------3.30 3.479E+OO ------Line Not Found ------BI-214 609.32 129 45.49* 1.938E+OO 8.132E-01 8.134E-01 28.23 1120.29 ,19 14.92 1.202E+OO 5.780E-01 5.782E-01 100.70 1764.49 ------15.30 8.180E-01 ------Line Not Found ------PB-214 74.82 90 5.80 3.314E+OO 2.620E+OO 2.621E+OO 58.27 77 .11 136 9.70 3.512E+OO 2.227E+OO 2.227E+OO 40.63 87.09 28 3.41 4.279E+OO 1.077E+06 1.078E+OO '208.30 242.00 92 7.25 4.131E+OO 1. 713E+OO 1.713E+OO 48.37 295.22 99 18.42 3.524E+OO 8.489E-01 8.492E-01 34.78 351. 93 174 35.60* 3.046E+OO 8. 941E-01 8.944E-01 25.83 RN-222 609.32 129 45.49* 1.938E+OO 8 .132E-01 8.134E-01 28.23 1120.29 19 14.92 1.202E+OO 5.780E-01 5.782E-01 100.70 1764.49 ------15.30 8.180E-01 ------Line Not Found ------RA-224 240.99 92 4.10* 4 .131E+OO 3.029E+OO 3.029E+OO 48.37 RA-226 609.32 129 45.49* l.938E+OO 8.132E-01 8 .134E-01 28.23 1120.29 19 14.92 l.202E+00 5.780E-01 5.782E-01 100.70 1764.49 ------15.30 8.180E-01 ------Line Not Found ------AC-228 105.21 28 1.10 5.159E+OO 2.779E+OO 2.779E+OO 180.40 338.32 92 11. 27 3.145E+OO 1. 453E+OO 1.453E+OO 39.44 794.95 ------4.25 l.572E+OO ------Line Not Found ------835.71 ------1. 61 1.512E+OO ------Line Not Found ------911. 20 75 25.80* 1.414E+OO 1.140E+OO 1.140E+OO 26.14 968.97 55 15.80 1.347E+OO l.445E+OO 1.445E+OO 43.78 RA-228 105.21 28 1.10 5.159E+OO 2.779E+OO 2. 779E+.OO 180.40 338.32 92 11. 27 3.145E+OO 1.453E+OO 1.453E+OO 39.44 794.95 ------4.25 1.572E+OO ------Line Not Found ------835. 71 ------1. 61 1.512E+OO ------Line Not Found ------911. 20 75 25.80* 1.414E+OO l.140E+OO l.140E+00 26 .14 968.97 55 15.80 1. 34 7E+OO 1.445E+OO l.445E+OO 43.78 TH-228 74.82 90 10.28 3.314E+OO 1.478E+OO 1.478E+OO 58.27 Page 277 of 614 Nuclide Line Activity Report (continued) Page : 2 Sample ID : R405245011 Acquisition date 3-0CT-2016 04:45:57 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 77 .11 136 17.10 3.512E+OO l.263E+OO 1. 263E+OO 40.63 238.63 342 43.60* 4.174E+OO 1.049E+OO 1. 049E+OO 14.02 300.09 ------3.30 3.479E+OO ------Line Not Found ------TH-230 609.32 129 45.49* l.938E+OO 8 .132E-01 8.132E-01 28.23 1120.29 19 14.92 1. 2 02E+O 0
  • 5.780E-01 5.780E-01 100.70 1764.49 ------15.30 8.180E-01 ------Line Not Found ------TH-232 105.21 28 1.10 5.159E+OO 2. 77.9E+OO 2.779E+OO 180.40 338.32 92 11. 27 3.145E+OO 1.453E+OO l.453E+OO 39.44 835.71 ------1. 61 1.512E+OO ------Line Not Found ------911.20 75 25.80* l.414E+OO l.140E+OO 1.140E+OO 26.14 968.97 55 15.80 1. 34 7E+OO 1.445E+OO 1.445E+OO 43.78 TH-234 63.29 34 3.70* 2.216E+OO 2.279E+OO 2.279E+00 194.00 92.59 36 4.23 4.640E+OO 1.012E+OO 1.012E+OO 173.37 U-234 609.32 129 45.49* 1. 938E+OO 8.132E-01 8.132E-01 28.23 1120.29 19 14.92 l.202E+00 5.780E-01 5.780E-01 100.70 1764.49 ------15.30 8.180E-01 ------Line Not Found ------U-235 89.96 ------3.47 4.467E+OO ------Line Not Found ------93.35 36 5.60 4.640E+OO 7.645E-01 7.645E-01 173.37 143.76 38 10. 96* 5.443E+OO 3.595E-01 3.595E-01 130.91 163.33 ------5.08 5.246E+OO ------Line Not Found ------185.72 87 57.20 4.933E+OO 1. 721E-01 1.721E-01 49.68 205.31 ------5.01 4. 641E+OO ------Line Not Found ------U-238 63.29 34 3.70* 2.216E+00 2.279E+OO 2.279E+OO 194.00 92.59 36 4.23 4.640E+OO 1.012E+OO 1.012E+OO 173.37 AM-243 43.53 ------5.90 2.327E-01 .------Line Not Found ------74.66 90 67.20* 3.314E+OO 2.261E-01 2.262E-01 58.27 ANH-511 511. 00 49 100.00* 2.232E+OO l.225E-01 l.225E-01 77.20 Flag: "*" Key line Page 278 of 614 Summary of Nuclide Activity Sample ID : R405245011 Acquisition date Page : 3 3-0CT-2016 04:45:57 Total number of lines in spectrum 36 Number of unidentified lines 6 Number of lines tentatively identified by NID 30 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 EU-155 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232-TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 4.75Y l.41E+10Y 7.04E+08Y 1. 41E+l0Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+l0Y 1600.00Y 1. 41E+l0Y 1. 41E+l0Y 1. 41E+10Y 7.54E+04Y 1. 41E+l0Y 4.47E+"09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 55 1. 00 1. 02 1. 02 1.12 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.264E+Ol 9.929E-01 9.929E-02 3.158E-01 3.336E-01 1.449E-01 3.312E-01 2.464E+OO 1.049E+OO 8.132E-01 8. 941E-01 8.132E-01 3.029E+OO 8.132E-01 1.140E+OO 1.140E+OO 1.049E+OO 8.132E-01 1.140E+OO 2.279E+OO 8.132E-01 3.595E-01 2.279E+OO 2.261E-01 1.225E-01 3.609E+Ol 3.609E+Ol Decay Corr pCi/GRAM 1.264E+Ol 1.541E+OO 9.929E-02 3.217E-01 3.398E-01 1. 629E-01 3.312E-01 2.464E+OO 1.049E+OO 8.134E-01 8.944E-01 8.134E-01 3.029E+OO 8.134E-01 1.140E+OO 1.140E+OO 1.049E+00 8.132E-01 1.140E+OO 2.279E+OO 8.132E-01 3.595E-01 2.279E+OO 2.262E-01 1.225E-01 3.667E+Ol 3.667E+Ol 83.33% Decay Corr 2-Sigma Error 0.184E+Ol 3.210E+OO 20.68E-02 l.087E-01 l.148E-01 2.938E-01 l.056E-01 0.636E+OO 0.147E+OO 2.296E-01 2.310E-01 2.296E-01 1.465E+00 2. 296E-01 0.298E+OO 0.298E+OO 0.147E+OO 2.295E-01 0.298E+OO 4.422E+OO 2.295E-01 4.706E-01 4.422E+OO 1.318E-01 0.946E-01 "M" Manually accepted* 2-Sigma %Error 14.54 208.30 208.30 33.79 33.79 180.40 31. 9*0 25.83 14.02 28.23 25.83 28.23 48.37 28.23 26 .14 26.14 14.02 28.23 26.14 194.00 28.23 130. 91 194.00 58.27 77.20 Flags: "K" Keyline not found "E" = Manually edited "A"= Nuclide specific abn. limit Page 279of614 Flags Unidentified Energy Lines Page : 4 Sample ID : R405245011 Acquisition date : 3-0CT-2016 04:45:57 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 30.20 17 173 1. 40 60.62 58 10 3.74E-03 **** 2.27E-05 0 117. 30 34 74 0.80 234.91 232 7 8.20E-03 97.5 5.40E+OO T 0 128.15 16 102 1. 56 256.61 255 8 3.81E-03 **** 5.48E+OO T 0 210.21 11 119 0.73 420.80 414 8 2.78E-03 **** 4.57E+OO T 0 463.12 45 34 1. 92 926.82 921 12 1. 20E-02 62.7 2.42E+OO T 0 681.17 8 15 1. 34 1363.10 1355 11 2.28E-03 **** 1.77E+OO 0 727.15 30 18 0.89 1455.08 1448 14 8. 21E-03 73.8 1.69E+OO T 0 734.16 19 9 1. 34 1469.11 1462 12 5.37E-03 76.8 l.67E+OO T 0 990.07 6 15 3.31 1981.10 1973 14 1.71E-03 **** 1.33E+OO 0 1166. 61 14 3 2.84 2334.28 2327 15 3.86E-03 80.3 1.16E+OO 0 1172.34 6 2 0.48 2345.73 2341 8 1. 70E-03 **** l.16E+OO T 3 1235.58 10 4 1. 88 2472.24 2470 13 2.93E-03 72. 7 1. llE+OO. T 3 1238.09 22 8 2.32 2477.27 2470 13 6.45E-03 70.0 l. llE+OO T 0 1288.00 7 8 1. 00 2577.13 2570 11 1. 96E-03 **** 1. 07E+OO 0 1560.44 8 0 3.30 3122.13 3116 11 2.22E-03 70.7 9.14E-01 Flags: "T" = Tentatively associated Page 280of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:46:41.59 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245011.CNF;l *
  • Acquisition date 3-0CT-2016 04:45:57 Sensitivity : 3.000 *
  • Detector ID GAM08 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.63 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:53:00 Nuclide Library : SOLID *
  • Sample ID R405245011 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.3466E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry :*CAN *
  • Eff. File : 'DKA100: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;l4' * ***********************************************x*****x************************* Combined Critical Level Report .NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 EU-155 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234. U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 3.520E-01 1.343E+OO 8.662E-02 4.064E-02 4.293E-02 l.117E-01 3.068E-02 2.036E-01 5. 031E-02 6.956E-02 l.739E-01 6.956E-02 5.395E-01 6.956E-02 l.055E-01 l.055E-01 5. 031E-02 6.954E-02 1.055E-01 1.422E+OO 6.954E-02 1.616E-01 l.422E+OO 6.369E-02. 2.136E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 281of614 Le (pCi/GRAM 1.llSE+Ol 4.200E-02 O.OOOE+OO 3.104E-02 3.918E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG--llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 282of614 O.OOOE+OO 7.232E-02 4.667E-01 O.OOOE+OO 5.234E-02 5.094E-01 5.002E+OO 4.288E-02 l.537E-01 2 .196E+OO l.322E+Ol O.OOOE+OO l.900E-01 O.OOOE+OO O.OOOE+OO 6.213E-01 8.070E+OO 7. 901E-01 O.OOOE+OO 2.177E-01 4.833E+02 3.199E-02 8.826E-01 2.338E+OO 1. 602E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.084E-02 7.026E-02 4.448E+OO 4.456E-01 4.456E-01 3.074E-02 l.058E-01 2.322E-01 O.OOOE+OO O.OOOE+OO 1. 2 90E-01 1.613E+OO l.147E-01 2.549E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.075E-02 O.OOOE+OO 5.330E-02 1.287E-01 O.OOOE+OO 0.000E+OO 1.083E-01 O.OOOE+OO O.OOOE+OO 2.002E+Ol O.OOOE+OO 3.670E-01 4.994E-02 4.322E+00 5.467E-02 O.OOOE+OO 9.044E+02 O.OOOE+OO 2.229E-02 8. 81'6E-02 1. 794E-01 1.020E-01 1.339E+OO 5.270E-02 3.223E+Ol 2.025E-01 7.927E-02 2.648E-02 3.422E+OO SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NdT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 . TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 283of614 1.076E+OO 3. 731E+OO 2.172E+Ol 1.004E+02 5.238E-01 2.090E+OO 5.369E-02 5.876E+OO 7.377E-01 7.160E-01 3.643E-01 5.857E-01 2.590E-01 2.590E-01 4.819E-01 4.558E-01 5.857E-01 6. SllE-02 2.520E-01 4.327E+OO 6. SllE-02 O.OOOE+OO 2.633E-01 3.305E+02 l.929E-01 1.073E-01 6.768E-02 3.226E-02 4.205E-02 1.261E-01 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT . NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN* NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:46:47.07 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245011.CNF;l *
  • Acquisition date 3-0CT-2016 04:45:57 Sensitivity : 3.000 *
  • Detector ID GAM08 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.63 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:53:00 Nuclide Library : SOLID *
  • Sample ID R405245011 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity 1.3466E+02 GRAM *
  • Quantity' Err(%)* 1. 4852E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : *0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;14
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.264E+Ol 1.918E+00 CD-109 3. 2 68E'-01 3.177E+00 SN-126 2.106E-02 2.047E-01 BA-137M 3.217E-01 1.074E-01 CS-137 3.398E-01 l.135E-01 EU-155 1. 629E-01 2.881E-01 TL-208 3.312E-01 l.045E-01 BI-211 1.246E-01 1.022E+OO PB-212 1.049E+OO 1.545E-01 BI-214 8.134E-01 2.277E-01 PB-214 8.944E-01 2.294E-01 RN-222 8.134E-01 2.277E-01 RA-224 l.528E+OO l.530E+OO RA-226 8.134E-01 2.277E-01 AC-228 l.140E+OO 2.978E-01 RA-228 1.140E+00 2.978E-01 TH-228 1.049E+OO 1.545E-01 TH-230 8 .132E-01 -2.276E-01 TH-232 l.140E+OO 2.978E-01 TH-234 2.279E+OO 4.362E+OO U-234 8 .132E-01 2.276E-01 U-235 3.595E-01 4.615E-01 U-238 2.279E+00 4.362E+OO AM-243 1. 529E-01 l.322E-01 ANH-511 l.225E-01 9.282E-02 Non-Identified Nuclides Nuclide BE-7 NA--22 NA-24 AL-26 SC-46 Page 284 of 614 Key-Line Activity (pCi/GRAM -l.330E+OO -4.432E-02 -1.000E+41 l.886E-02 2.636E-01 K.L Act error ( 1. 96-sigma) 1.339E+Ol 6. 098E.-02 l.402E+41 2.933E-02 4.073E-Ol TPU ( 1. 96-sigma) l.918E+OO 3.177E+OO 2.047E-01 1.074E-01 l.135E-01 2. 881E-01 l.045E-01 l.022E+00 1.545E-01 2.277E-01 2.294E-01 2.277E-01 1.530E+OO 2.277E-01 2.978E-01 2.978E-01 l.545E-01 2.276E-01 2.978E-01 4.362E+00 2.276E-01 4.615E-01 4.362E+00 l.322E-01 9.282E-02 TPU (1. 96-sigma) l.340E+Ol 6.417E-02 O.OOOE+OO 3.054E-02 4. 2.42E-01 NOT r'DENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 -9.229E+03 l.363E+04 l.425E+04 SHORT HLIF CR-51 -5.497E+Ol 4.268E+02 4.275E+02 SHORT HLIF MN-54 8.086E-02 7.044E-02 7.931E-02 NOT IDENT. C0-56 3.830E-02 5.338E-01 5.341E-01 FAIL ABUN MN-56 l.OOOE+41 l.560E+42 O.OOOE+OO SHORT HLIF C0-57 8.816E-03 6 .114E-02 6.127E-02 NOT IDENT. C0-58 -8.355E-02 6.033E-01 6.045E-01 NOT IDENT. FE-59 -3.504E+OO 6.773E+OO 6.955E+OO NOT IDENT. C0-60 l.727E-02 4.714E-02 4.778E-02 FAIL ABUN ZN-65 -3.176E-05 2.086E-01 2.086E-01 NOT IDENT. GE-68 -2.089E+OO 3.027E+OO 3.171E+OO NOT IDENT. AS-73 2.129E+OO l.480E+Ol l.483E+Ol NOT IDENT. AS-74 3.144E+03 5 .119E+03 5.312E+03 SHORT HLIF -l.073E-01 2.258E-01 2.309E-01 NOT IDENT. BR-77 2.334E+37 l.972E+38 O.OOOE+OO SHORT HLIF SR-82 l.998E+02 6.101E+02 6.167E+02 SHORT HLIF RB-83 -l.315E-01 7.617E-01 7.640E-01 NOT IDENT. KR-85 l.102E+Ol 8.030E+OO 9.443E+OO NOT IDENT. SR-85 l.077E+OO 7.864E-01 9.242E-01 NOT IDENT. RB-86 -l.403E+04 2.735E+04 2.808E+04 SHORT HLIF Y-88 4.602E-02 _ 2. 413E-01 2.422E-01 NOT IDENT. Y-91 7.625E+OO 5.774E+02 5.774E+02 NOT IDENT. NB-94 l.393E-02 3.427E-02 3.484E-02 NOT IDENT. NB-95 -l.565E-01 l.035E+OO l.037E+OO NOT IDENT. NB-95M 3.007E-01 2. 872E+OO 2.875E+OO NOT IDENT. ZR-95 7.957E-01 1. 721E+OO 1. 758E+OO NOT IDENT. NB-97 l.OOOE+41 l.066E+42 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 l'. 247E+41 O.OOOE+OO SHORT HLIF M0-99 -l.191E+31 3.185E+31 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 l.838E+41-O.OOOE+OO SHORT HLIF RH-101 2.777E-02 6.646E-02 6. 7 63E-02 FAIL ABUN RH-102 7.343E-02 7.287E-02 8.004E-02 NOT IDENT. RU-103 -3.574E-01 5.327E+OO 5.329E+OO FAIL ABUN RH-106 -3.463E-01 6.070E-01 6.268E-01 NOT IDENT. RU-106 -3.463E-01 6.070E-01 6.268E-01 NOT IDENT. AG-108M 3.395E-02 3.122E-02 3.477E-02 NOT IDENT. AG-llOM 7.868E-02 l.083E-01 l.140E-01 NOT IDENT. SN-113 -8.900E-02 2.811E-01 2.840E-01 NOT IDENT. CD-115 -7.267E+37 3.565E+38 O.OOOE+OO SHORT HLIF SN-ll 7M -5.532E+04 8.945E+04 9.286E+04 SHORT HLIF TE-123M l.445E-02 l.541E-01 l.542E-01 NOT IDENT. SB-124 l.202E+00 1. 3 62E-+00 l.466E+OO NOT IDENT. SB-125 9.768E-02 l.210E-01 l.288E-01 FAIL ABUN TE-125M -4.586E+Ol 3. 318E+0*2 3.325E+02 NOT IDENT. I-126 7.514E+03 9.824E+05 9.824E+05 SHORT HLIF SB-126 5.545E+05 8.047E+05 8.427E+05 SHORT HLIF SB-127 -l.126E+20 6.323E+21 O.OOOE+OO SHORT HLIF I-131 5.774E+08 3.350E+09 3.360E+09 SHORT HLIF I-132 -l.000E+41 2.173E+42 O.OOOE+OO SHORT HLIF TE-132 6.515E+25 1. 006E+26 O.OOOE+OO SHORT HLIF BA-133 -3.252E-02 5.776E-02 5.959E-02 NOT IDENT. I-133 l.OOOE+41 3.046E+41 0. OOOE+_OO SHORT HLIF CS-134 3. 421E-02 5.579E-02 5.789E-02 NOT IDENT. cs....:135 --6. 406E-02 l.522E-01 l.550E-01 NOT IDENT. I-135 l.OOOE+41 7.036E+41 O.OOOE+OO SHORT HLIF CS-136 -2. 724E+05 2.939E+05 3.185E+05 SHORT HLIF CE-139-8.620E-03 l.300E-Ol 1. 301E-01 NOT IDENT. BA-140 4.535E+05 l.070E+06 l.089E+06 SHORT HLIF LA.:.140 -6.687E+04 2.502E+05 2.520E+05 SHORT HLIF CE-141 l.307E+Ol 2.434E+Ol 2.505E+Ol NOT IDENT. CE-143 l.000E+41 l.099E+41 0.000E+OO SHORT HLIF CE-144 -7.755E-02 4.498E-01 4. 511E-01 NOT IDENT. PM-144 4.964E-03 5.599E-02 5.604E-02 NOT IDENT. PR-144 4.296E-01 4.846E+OO 4.850E+OO NOT IDENT. PM-146 4.815E-02 5.836E-02 6.227E-02 NOT IDENT. ND-147 3.766E+05 l.954E+07 l.954E+07 SHORT HLIF PM-147 4.691E+02 l.108E+03 l.128E+03 NOT IDENT. PM-149 -7 .116E+39 5.769E+39 O.OOOE+OO SHORT HLIF EU-150 1. 063E-03 2.835E-02 2.835E-02 FAIL ABUN EU-152 l.170E-02 l.045E-01 l.047E-01 NOT IDENT. GD-153 4.474E-02 2.050E-01 2.060E-01 NOT IDENT. EU-154 -l.122E-01 l.494E-01 l.577E-01 NOT IDENT. TB-160 -l.259E+OO l.842E+OO l.927E+OO FAIL ABUN H0-166M -2.834E-03 6.056E-02 6.057E-02 FAIL ABUN TM-171 -6.785E+OO 3.711E+Ol 3.724E+Ol NOT IDENT. HF-172 -2.480E-01 2. 964E-01 3.168E-01 FAIL -ABUN LU-172 l.984E-02 8.759E-02 8.804E-02 FAIL ABUN LU-176 7.158E-03 2.943E-02 2. 961E-02 FAIL ABUN Page 285of614 HF-181 -2.444E+OO 4.464E+00 4.598E+OO NOT IDENT. TA-182 6.995E-01 l.166E+OO l.208E+OO FAIL ABUN. RE-183 -9.270E-01 4.309E+OO 4.329E+OO NOT IDENT. RE-184 -2.450E+Ol 3.095E+Ol 3.286E+Ol NOT IDENT. W-188 -2.303E+Ol 1.305E+02 1.309E+02 FAIL ABUN IR-192 3.943E-01 5.594E-01 5.869E-01 FAIL ABUN HG-203 -2.502E+OO 2.635E+OO 2.866E+OO NOT IDENT. BI-207 -l .114E-02 6.555E-02 6.574E-02 FAIL ABUN PB-210 -1.649E+OO 6.729E+OO 6.770E+OO NOT IDENT. PB-211 3.165E-01 8.199E-01 8.322E-01 NOT IDENT. BI-212 l.480E+OO 1.073E+OO 1. 2 63E+00 FAIL ABUN RN-219 -2.221E-01 4.556E-01 4.665E-01 NOT IDENT. RA-223 -9.873E-03 6.912E-01 6.912E-01 FAIL ABUN AC-227 2.809E-01 2.677E-01 2.962E-01 NOT IDENT. TH-227 2.809E-01 2.677E-01 2.962E-01 NOT IDENT. TH-229 -5.536E-02 5.361E-01 5.367E-01 FAIL ABUN PA-231 9.694E-03 5.179E-01 5.179E-01 NOT IDENT. TH-231 -9.873E-03 6.912E-01 6.912E-01 FAIL ABUN PA-233 2.849E-02 7.126E-02 7.241E-02 NOT IDENT. PA-234 -8.599E-02 3.278E-01 3. 301E-01 FAIL ABUN PA-234M -l.644E+00 5.130E+OO 5.183E+00 NOT IDENT. NP-237 2.849E-02 7.126E-02 7.241E-02 NOT IDENT. NP-238 -5.357E+39 4.612E+40 O.OOOE+OO SHORT HLIF NP-239 4.421E-01 4.241E-01 4.686E-01 FAIL ABUN PU-239 2.529E+02 6.036E+02 6.143E+02 FAIL ABUN AM-241 1. 417E-01 2.220E-01 2.310E-01 NOT IDENT. CM-243 1. 966E-02 l.340E-01 l.343E-01 NOT IDENT. BK-247 -6.146E-02 8. 3'7 9E-02 8.825E-02 FAIL ABUN CM-247 -3.382E-02 4.2Ei5E-02 4.529E-02 NOT IDENT. CF-249 5.843E-03 4 .. 814E-02 4.821E-02 NOT IDENT. CF-251 9.295E-02 1. 317E-01 1.382E-01 NOT IDENT. Page 286 of 614
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 66.6529 87.09 102.4304 136.47 77.5446 45.60 62.0535 87.57 102.5234 140.51 0.0000 46.54 63.2245 88.03 103.7161 143.76 50.6101 49.72 0.0000 88.34 103.7764 144.24 50.6428 51. 35 67 .1196 88.47 103.8015 145.44 45.0881 .51. 87 76.3782 89. 96 104.0905 152.43 85.3221 52.39 61.1868. 1093.63 86.4819 153.25 0.0000 52.97 57.1948 91.11 0.0000 323.87 75.7441 53.44 62.3780 92.59 89.0167 156.02 0.0000 54.07 59.4074 93.35 89.1400 158.56 0.0000 57.36 0.0000 94.56 80.4012 159.00 57. 7696 57.53 74.3975 94.65 80.4139 162.33 58.0106 57.98 68.2737 94*. 67 80.4172 162.66 0.0000 59.27 59.4966 94.87 80.4457 163.33 53.1391 59. 32 59.5040 97.43 58.3643 165.86 57.0234 59.54 59.5357 98.43 76.4564 176.31 66.1074 60.96 80.5798 98.44 76.4580 17 6. 60 0.0000 61.17 73.6702 99.53 52.9464 177.52 51.9549 62.93 66.9990 100 .11 63.1483 181. 07 0.0000 63.29 67.0555 102.03 79.9502 181. 52 51. 7749 63.58 67.1008 103.18 72.5488 184.41 45.6108 64.28 67.2101 103.37 63.5007 143.76 50.7538 66.73 59.1394 62.5602 193.51 59.7269 67.24 77.5334 105.31 62.5707 197.03 60.8127 125.81 80.4323 106.12 62.6551 198.01 65.1641 67.75 69.1540 106.47 62.6916 201.83 58.5433 69.67 82.9143 109.28 56.4925 203.43 56.9182 70.83 90.9395 111. 00 64.3052 205.31 44.0694 72.81 89.9005 111. 76 0.0000 210.85 66.4854 72.87 89.9120 114. 06 63.0815 215.65 66.3755 74.66 106.3703 116. 30 0.0000 222 .11 58.8956 74.82 106.4058 116.74 57.1670 227.09 56.5345 74.97 106.4390 119.76 65.1956 227.38 61.8524 77 .11 106.9126 121.12 59.1087 228.16 0.0000 78.74 88.1268 121. 22 59.1179 228.18 45.0987 79.69 95.5336 121. 78 66.5638 116.74 45.0987 80.12 89.8207 122.06 68.9286 235.69 56 .1139 80.19 0.0000 122.92 66.6786 235. 96 46.3284 80.57 88.4520 123.07 59.6730 238.63 46.4453 81. 00 101. 2263 265.00 64.4124 238.98 0.0000. 81. 07 101.2405 125.81 67.3581 240.99 46.5484 81.75 87.2058 127.23 48.6617 242.00 46.5923 83.79 94.8518 127.91 45.5680 244.70 46.7092 84.00 94.8908 129.30 51. 9579 252.40 0.0000 85.43 98.0805 131. 20 67.8891 252.80 42.5316 86.55 102.3254 133.02 74.3975 254.15 0.0000 86.79 102.3715 133.52 66.5308 256.23 33.5854 86.94 102.4013 136.00 61.9952 260.90 0.0000 Page 287 of 614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY .MDA COUNTS 2 64. 66 42.9820 355.39 0.0000 584.27 15.6782 2 64. 80 44.8160 356.01 39.7733 595.83. 0.0000 265.00 46.6535 364.49 0.0000 427.87 20.3145 2 68. 22 41.2802 366.42 0.0000 602.52 0.0000 269.46 41.3242 372 .. 51 38.7382 604.72 18.6578 270.03 37.6701 375.05 35.8206 607.14 21. 5087 271.23 45.0662 377.52 35.8799 609.32 21.5304 273.65 0.0000 356.01 29.0254 610.33 21.5412 276.40 58.1986 388.16 32 .1191 614.28 20.4441 277.37 37.9062 388.63 0.0000 618.01 18.2038 277.60 38.8384 391. 69 34:2054 620.36 14.8070 278.00 29.6009 264.66 20.2380 621. 93 20.5166 279.20 45.3723 401.81 31.3923 630.19 0.0000 279.54 45.3852 402.40 34.4427 631.29 11. 4465 279.70 53. 7284 404.85 26.3798 633.25 13. 7480 280.46 46.3470 410.95 25.4634 634.78 0.0000 283.69 26.0244 413.71 15.3046 635.95 17.2058 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 39.0922 423. 72 0.0000 645.85 11.5214 2*85. 90 0.0000 427.09 26.7485 657.76 19 .1104 287.50 22.3770 427.87 18.5270 657.90 0.0000 290.67 37.8592 433.94 14.4631 661.'66 24.3641 293.27 0.0000 439.40 20.7292 664.57 0.0000 351. 93 47.8509 453.88 22.9981 666.33 0.0000 295. 96 46.4707 463.37 28.3804 666.50 0.0000 879.38 43.7461 468.07 25.2949 667.71 0.0000 299.98 34.8478 473.00 0.0000 677.62 26.6343 300.09 34.8508 475.06 27. 5118 685.70 0.0000 300.13 32. 9677 476.78 24.3608 695.00 0.0000 301.36 39.6006 477.60 22.2527 696. 49 13.2472 302.85 41.5347 482.18 23. 3719 696. 51 13.2477 256.23 30.2467 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 12.3683 306.78 35.9822 497.08 14.9955 697.49 12.3692 308.46 38.8738 505.52 25.8242 702.65 13.2816 311. 90 33.2739 507.63 0.0000 706.68 15. 9642 316.51 35.3003 511. 00 12.9501 711. 68 14.2197 319.41 0.0000 514.00 12.9707 720. 70 0.0000 320.08 0.0000 514.00 12.9707 721. 93 0.0000 321. 04 33.5075 520.40 21. 6911 722.78 17.1410 323.87 30.7012 520.69 0.0000 722.91 17.1422 325.23 38.4155 522.65 0.0000 723.31 11. 4301 328.76 0.0000 527.90 0.0000 724 .19 10.0047 333.37 34.7838 528.26 15.2458 727. 33 12.8795 '333.97 24.6492 529.59 8.7181 733.00 10.0403 334.37 24.6564 529.87 0.0000 735.93 8.6162 338.28 29.0912 531. 02 0.0000 333.97 4.3107 338.32 29.0918 537.26 0.0000 739.50 0.0000 311. 90 26.2238 546.56 0.0000 747.24 16.2285 340.48 26.2238 552.55 13. 2310 748.06 18.0371 340.55 0.0000 563.25 22 .1696 752.31 18.9710 344.28 25.7114 569.33 21.1237 .753.82 0. 0.000 345.93* 30.2274 946.00 21.1261 756.73 15.3839 351.06 36.2096 569.70 17.7917 756.80 15.3845 351. 93 36.2322 583.19 15.6702 884.68 18.1500* Page 288of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:47:18.80 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245012.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM09.CNF;335 Background date : Z-OCT-2016 11:00:29. Sample date 15-DEC-2015 12:56:00 Acquisition date : 3-0CT-2016 04:46:21. Sample ID R405245012 Sample quantity : 1.32296E+02 GRAM Detector name GAM09 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.50 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596387 Detector SN# Matrix Spike ID : LCS ID 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 4 4 4 4 0 0 0 0 0 0 0 2 2 0 0 0 0 2 2 0 0 0 0 0 0 0 0 0 0 0 Page 290 of 614 Energy 53.28 63.46* 75.03 77.23 87.25 90.02 92.58* 94.65 122.62 125.64 129.05 134.94 154.41 185.94* 209.03 238.65* 241.86 295.26* 299.97 328.69 338.21* 348.66 351.85* 427.55 437.49 464.58 470.16 511. 50* 543.26 582.92* 609.33* 661.41 665.88 72.6. 76 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 25 26 104 182 74 44 61 24 32 22 32 30 33 88 49 362 97 116 33 16 85 19 *214 40 15 23 10 69 11 112 141 248 12 48 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 68 53 76 75 86 83 94 66 58 53 73 72 85 107 70 73 71 54 28 67 49 9 38 23 31 59 26 26 18 19 31 8 10 3 1. 04 0.95 0.91 0.89 1. 28 1. 00 1. 23 0.89 0.59 1.19 1. 26 1. 42 1. 54 1.11 1.13 1.11 1. 33 1.10 2.26 0.58 1. 01 1. 33 1. 26 4.13 0.90 1. 76 1. 50 2.27 1. 34 1. 28 1. 36 1.14 1. 32 1. 28 106.22 126.59 149.73 154.15 174.19 179.73 184.85 189.00 244.96 251.00 257.82 269.62 308.58 371. 65 417.86 477 .13 483.54 590.39 599.82 657.28 676.32 697.24 703.62 855.07 874.97 929.18 .940. 35 1023.07 1086.60 1165. 96 1218.82 1323.02 1331. 96 1453.78 104 124 146 146 171 1n 171 171 241 249 255 267 304 366 413 472 472 586 596 650 672 696 696 849 872 921 934 .1015 1083 1160 1213 1318 1328 1448 6 7.0lE-03 55.3 5 7.lOE-03 50.5 14 2.89E-02 15.8 7.86E-01 14 5.06E-02 10.3 21 2.04E-02 22.7 l.70E+OO 21 1.21E-02 36.9 21 l.71E-02 33.2 21 6.77E-03 59.5 7 8.99E-03 42.7 5 5.97E-03 55.0 6 8.81E-03 46.3 7 8.35E-03 50.5 8 9. 21E-03 51. 3 11 2.46E-02 26.5 9 1. 36E-02 33. 8 16 1.0lE-01 6.5 2.35E+OO 16 2. 68E:-02 19. 0 9 3.21E-02 15.0 8 9.06E-03 33.7 10 4.41E-03 99.9 9 2.35E-02 18.8 20 5.28E-03 24.0 2.38E+OO 20 5.93E-02 8.5 12 1.lOE-02 29.3 9 4.05E-03 72.5 13 6.43E-03 72.6 9 2.69E-03101.8 20 1.91E-02 25.5 8 2.95E-03 76.0 11 3.llE-02 12.4 14 3.91E-02 12.0 11 6.88E-02 6.7 8 3.39E-03 53.1 10 l.34E-02 15.7 Peak Search Report (continued) Page : 2 Sample ID : R405245012 Acquisition date 3-0CT-2016 04:46:21 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 744.22 10 2 1. 47 1488.70 1485 8 2.73E-03 40.7 36 0 768.03 20 15 2.41 1536.36 1532 9 5.45E-03 4'2. 8 37 0 785.46 18 9 1. 48 1571.22 1567 9 5.00E-03 38.2 38 0 7,94.58 34 3 3.57 1589.48 1583 13 9. 41E-03 20.3 39 0 819.46 19 0 0.67 1639.26 1634 11 5.28E-03 22.9 40 0 8 94 .11 22 2 1. 22 1788.64 1784 9 6.05E-03 24.7 41 0 911.21* 76 22 1. 37 1822.85 1815 16 2. llE-02 18.7 42 0 939.05 6 7 0. 86 1878.55 1874 7 1. 78E-03 78.2 43 1 964. 62 27 4 1. 82 1929.72 1923 21 7.48E-03 26.1 8.02E-01 44 1 968. 42 55 2 1. 82 1937.33 1923 21 l.54E-02 15.1 45 0 1017.49 22 5 1. 30 2035.51 2032 8 6.19E-03 28.0 46 0 1069.26 15 3 1. 00 2139.11 2133 11 4.23E-03 33.2 47 0 1111. 42 11 2 i: 07 2223.47 2220 7 3.16E-03 35.2 48 0 1114. 90 8 6 1. 31 2230.44 2227 8 2 .13E-03 66.4 49 0 1119. 93 26 7 2.21 2240.50 2235 10 7.17E-03 27.9 50 0 1154. 06 13 13 0.70 2308.79 2303 11 3.72E-03 59.6 51 0 1168.28 13 10 0.61 2337.26 2331 13 3.53E-03 58.2 52 0 1353.77 6 1 1. 34 2708.41 2705 6 1.55E-03 54.6 53 0 1377. 03 24 0 1.10 2754.96 2749 12 6.67E-03 20.4 54 0 1408.02 8 3 0.93 2816.98 2814 6 2.35E-03 46.6 55 0 1460.27* 314 10 2.23 2921. 52 2915 13 8.73E-02 6 .'1 56 0 1763 .. 74* 24 0 0.73 3528.81 3521 14 6.55E-03 22.6 F,lag: "*" = Peak area was modified by background subtraction ; Page 291 of 614 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 05:47:20 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245012.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 15-DEC-2015 12:56:00 R405245012 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 04:46:21 132.30 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA9 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74. 82 ' PB-214 74.82 PB-214 74.82 HF-172 52.97 HF-172 52.97 HF-172 54.07 HF-172 62.93 HF-172 62.93 HF-172 62.93 HF-172 122.92 HF-172 122.92 PB-214 351. 93 Page 292 of 614 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 AS-73 53.44 HF-172 54. 07 AS-73 53.44 TH-234 63.29 U-238 63.29 SN-126, 64.28 PM-147 121. 22 C0-57 122.06 BI-211 351.06 CAN 0 01:00:00.50 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : R405245012

  • Acquisition date 3-0CT-2016 04:46:21 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.146E+OO 1.392E+Ol 1.392E+Ol 12.14 OK C0-57 122.06 85.60* 6.295E+OO 3.613E-02 7.623E-02 91. 68 OK 136.47 10.68 6.345E+OO Line Not Found Absent ZN-65 1115. 54 50.60* 1.434E+OO 5.845E-02 1.342E-01 132.81 OK CD-109 88.03 3.70* 4.861E+OO 1.843E+OO 2.861E+OO 67.84 OK SN-126 64.28 9.60 2. 28.7E+OO 6.912E-01 6.912E-01 114. 87 OK 86.94 8.90 4.861E:+OO 7.662E-01 7.662E-01 67.84 OK 87.57 37.00* 4.861E+OO 1.843E-01 1.843E-01 67.84 OK BA-137M 661. 66 89.90* 2.157E+OO 7.327E-01 7.464E-01 13.49 OK CS-137 661. 66 85.10* 2.157E+OO 7.740E-01 7.885E-01 13.49 OK CE-144 80.12 1. 36 4.226E+OO Line Not Found Absent 133.52 11. 09* 6.348E+OO 2.734E-01 5.573E-01 101.01 OK PM-147 121. 22 0.00* 6.295E+OO l.085E+03 1. 341E+03 91. 68 OK HF-172 52.97 36.00 9.935E-01 Line Not Found <<INT Reject 54.07 63.00 1.028E+OO l.414E-01 1.903E-01 223.64 OK 61.17 20.30 1.994E+OO Line Not Found Absent 62. 93 4.50 2.219E+OO Line Not Found <<INT Reject 67. 68 5.99 2.822E+00 Line Not Found Absent 81. 75 4.50 4.383E+OO Line Not Found Absent 114. 06 2.60 6.157E+OO Line Not Found Absent 122.92 1.14 6.298E+00 Line Not Found <<INT Reject 125.81 11. 30* 6.322E+OO 1.936E-01 2.605E-01 109.92 OK 127.91 1. 46 6.341E+OO 2.199E+OO 2. 960E+OO 92.54 OK TL-208 277.37 6.60 4.352E+OO Line Not Found Absent 583.19 85.00* 2.383E+00 3.201E-01 3. 201E-01 24.75 OK 860.56 12.50 1.758E+OO Line Not Found Absent BI-211 72. 87 1. 23 3.448E+OO Line Not Found Absent 351.06 12.92* 3.589E+OO 2.263E-01 2.263E-01 394.29 OK BI-212 727.33 6.67* 2.005E+OO 2.055E+00 2.055E+OO 31. 40 OK 785.37 1.10 1. 887E+OO 4.916E+OO 4.916E+OO 76.38 OK 1620.50 1. 47 l.045E+OO Line Not Found Absent PB-212 74.82 10.28 3.692E+OO 1.302E+00 1.302E+OO 45.69 OK 77 .11 17.10 3.931E+OO 1. 799E+OO 1. 799E+OO 20.57 OK 238.63 43.60* 4.882E+OO l.048E+00 1 :.048E+OO 13.02 OK 300.09 3.30 4.088E+OO l.467E+OO 1.467E+OO 67.49 OK BI-214 609.32 45.49* 2.301E+OO 7.766E-01 7.769E-01 23.93 OK 1120.29 14.92 l.429E+OO 6.686E-01 6.689E-01 55.73 OK 1764.49 15.30 9.660E-01 8.510E-01 8.513E-01 45 .11 OK PB-214 74.82 5.80 3.669E+OO Line Not Found <<INT Reject 77 .11 9.70 3. 931E+OO 3. l 72E+OO 3.173E+OO 20.57 OK 87.09 3.41 4.849E+00 Line Not Found <<INT Reject 242.00 7.25 4.832E+OO Line Not Found <<INT Reject 295.22 18.42 4.140E+00 9.212E-01 9.215E-01 29.90 OK 351. 93 35.60* 3.588E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2. 301E+OO 7.766E-01 7.769E-01 23.93 OK 1120.29 14.92 l.429E+OO 6.686E-01 6.6B9E-01 55.73 OK 1764.49 15.30 9.660E-01 8.510E-01 8.513E-01 45 .11 OK RA-224 240.99 4.10* 4.834E+OO 1. 371E+OO 1. 371E+OO 90.49 OK RA-226 609.32 45.49* 2 .'301E+OO 7.766E-01 7.769E:_Ol 23.93 OK Page 293 of 614 Nuclide Line Activity Report (continued) Page : 3 Sample ID : R405245012 Acquisition date 3-0CT-2016 04:46:21 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1120.29 14.92 1.429E+OO 6.686E-01 6.689E-01 55.73 OK 1764.49 15.30 9.660E-01 8.510E-01 8.513E-01 45 .11 OK AC-228 105.21 1.10 5. 896E+OO Line Not Found Absent 338.32 11. 27 3.707E+OO 1.218E+OO 1.218E+OO 37.61 OK 794.95 4.25 1.870E+OO 2.415E+OO 2.415E+OO 40.70 OK 835. 71 1. 61 1. 799E+OO -----* Line Not Found Absent 911. 20 25.80* 1.682E+OO 9.814E-01 9.814E-01 37.46 OK 968. 97 15.80 1.604E+OO 1.218E+OO 1.218E+OO 30.18 OK RA-228 105.21 1.10 5.896E+OO Line Not Found Absent 338.32 11. 27 3.707E+OO 1.218E+OO 1.218E+OO 37.61 OK 794.95 4.25 1. 870E+OO 2.415E+OO 2.415E+OO 40.70 OK 835.71 1. 61 1. 799E+OO Line Not Found Absent 911.20 25.80* 1.682E+OO 9.814E-01 9.814E-01 37.46 OK 968. 97 15.80 1.604E+OO 1.218E+00 1.218E+00 30.18 OK TH-228 74.82 10.28 3.692E+00 1. 302E+OO 1.302E+OO 45.69 OK 77 .11 17.10 3. 931E+OO 1. 799E+OO 1. 799E+OO 20.57 OK 238.63 43.60* 4.882E+OO 1.048E+OO 1.048E+OO 13.02 OK 300.09 3.30 4.088E+OO 1. 467E+OO 1.467E+OO 67.49 OK TH-230 609.32 45.49* . 2. 301E+OO 7.766E-01 7.767E-01 23.93 OK 1120.29 14.92 1.429E+OO 6.686E-01 6.686E-01 55.73 OK 1764.49 15.30 9.660E-01 8.510E-01 8.510E-01 45 .11 OK PA-231 283.69 1. 70 4.275E+OO Line Not Found Absent 301.36 5.35* 4.088E+00 9.047E-01 9.047E-01 67.49 OK TH-232 105.21 1.10 5.896E+OO Line Not Found Absent 338.32 11. 27 3.707E+00 1.218E+OO 1.218E+OO 37.61 OK 835. 71 1. 61 1. 799E+OO Line Not Found Absent 911.20 25.80* 1.682E+OO 9.814E-01 9.814E-01 37.46 OK 968. 97 15.80 1.604E+OO 1.218E+OO 1.218E+OO 30.18 OK TH-234 63.29 3.70* 2.287E+OO 1.794E+OO 1. 794E+OO 114. 87 OK 92.59 4.23 5.249E+OO 1.816E+OO 1.816E+OO 66.35 OK U-234 609.32 45.49* 2. 301E+OO 7.766E-01 7.766E-01 23.93 OK 1120.29 14.92 1. 429E+OO 6.686E-01 6.686E-01 55.73 OK 1764.49 15.30 9.660E-01 8.510E-01 8.510E-01 45 .11 OK U-235 89. 96 3.47 5.072E+00 1.624E+OO 1.624E+OO 73.79 OK 93.35 5.60 5.249E+00 1.372E+OO 1.372E+OO 66.35 OK 143.76 10.96* 6. 311E+OO Line Not Found Absent 163.33 5.08 6. 096E+OO Line Not Found Absent 185.72 57.20 5.741E+OO .1.689E-01 1.689E-01 53.10 OK 205.31 5.01 5.415E+00 Line Not Found Absent U-238 63.29 3.70* 2.287E+OO 1. 794E+OO 1. 794E+00 114. 87 OK 92.59 4.23 5.249E+OO 1.816E+00 1.816E+OO 66.35 OK AM-243 43.53 5.90 1.969E-01 Line Not Found Absent 74.66 67.20* 3.692E+OO 1. 991E-01 1.991E-01 45.69 OK ANH-511. 511.00 100.00* 2.644E+OO 1.519E-01 1.519E-01 51. 05 OK Flag: "*" = Keyline Page 294 of 614 VAX/VMS Nuclide Identification *Report Generated 0*3-0CT-2016 05: 4 7: 21. 96 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245012.CNF;l *
  • Acquisition date 3-0CT-2016 04:46:21 Sensitivity : 3.000 *
  • Detector ID GAM09 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.50 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:56:00 Analyst initials: MXRl *
  • Sample ID R405245012 Sample Quantity l.3230E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* *
  • CALIBRATION INFORMATION * * * *
  • Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;16
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.392E+Ol 1. 656E+OO C0-57 7.623E-02 6.850E-02 ZN-65 l.342E-01 1. 747E-01 CD-109 2.861E+OO 1.902E+OO SN-126 1.843E-01 1.225E-01 BA-137M 7.464E-01 9.867E-02 CS-137 7.885E-01 l.042E-01 CE-144 5.573E-01 5.517E-01 PM-147 1. 341E+03 1. 205E+03 HF-172 2.605E-01 2.806E-01 TL-208 3. 201E-01 7.763E-02 BI-211 2.263E-01 8.744E-01 BI-212 2.055E+OO 6.325E-01 PB-212 1.048E+OO 1.337E-01 BI-214 7.769E-01 l.822E-01 PB-214 1.004E+OO 1.669E-01 RN-222 7.769E-01 1.822E-01 RA-224 1.371E+OO 1.216E+OO RA-226 7.769E-01 1.822E-01 AC-228 9.814E-01 3.603E-01 RA-228 9.814E-01 3.603E-01 TH-228 1.048E+OO 1.337E-01 TH-230 7.767E-Ol 1.822E-01 PA-231 9.047E-01 5.984E-01 TH-232 9.814E-01 :3.603E-01 TH-234 1.794E+OO 2.019E+OO U-234 7.766E-01 1.822E-01 U-235 l.187E-01 l.663E-01 U-238 1. 794E+OO 2.019E+OO AM-243 l.991E-01 8.916E-02 ANH-511 1. 519E-01 7.600E-02 ----Non-Identified Nuclides Nuclide Page 295 of 614 Key-Line Activity (pCi/GRAM K.L. Cnt Uncert ( 1. 96-sigma) MDA (pCi/GRAM 7.249E-01 6.902E-02 3.206E-01 1.974E+OO 6.209E-02 6.559E-02 6.693E-01 1.195E+03 3.489E-01 6.802E-02 3.739E-01 7.675E-01 1.068E-01 l.296E-01 3.332E-01 1. 296E-01 l.146E+OO l.296E-01 1. 788E-01 1. 788E-01 l.068E-01 l.296E-01 6.739E-01 l.788E-01 2.737E+OO 1.296E-01 3.344E-01 2.737E+OO 9.394E-02 4.690E-02 MDA (pCi/GRAM BE-7 -4.246E-01 1.017E+Ol 2.023E+Ol NOT IDENT. NA-22 -1.932E-02 4.686E-02 8.846E-02 NOT IDENT. NA-24 O.OOOE+OO 1.668E+41 O.OOOE+OO SHORT HLIF AL-26 -1.835E-02 3.154E-02 5.588E-02 NOT IDENT. SC-46 2.285E-02 4.0lOE-01 7.063E-01 FAIL ABUN V-48 O.OOOE+OO 1.230E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.348E+02 O.OOOE+OO SHORT HLIF MN-54 -2.640E-02 5.768E-02 1.033E-01 NOT IDENT. C0-56 l.014E-01 4.045E-01 8.338E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF C0-58 2.654E-01 3. 896E-01 9.174E-01 NOT IDENT. FE-59 4.556E-01 5.883E+OO l.155E+Ol NOT IDENT. C0-60 -6.267E-03 3.842E-02 7. 711E-02 NOT IDENT. GE-68 -3.057E+OO 2.575E+OO 3.794E+OO NOT IDENT. AS-73 l.082E+Ol 2.371E+Ol 2 .. 744E+Ol FAIL ABUN AS-74 O.OOOE+OO 4.537E+03 O.OOOE+OO SHORT HLIF SE-75 2. 963E-02 1.928E-01 3.625E-01 FAIL ABUN BR-77 O.OOOE+OO 2.974E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.527E+02 O.OOOE+OO SHORT HLIF RB-83 4.316E-01 6.675E-01 1.406E+OO NOT IDENT. KR-85 4.866E+00 6.507E+OO 1.399E+Ol NOT IDENT. SR-85 4.734E-01 6.371E-01 1.369E+OO NOT IDENT. RB-86 O.OOOE+OO 2.322E+04 0.000E+OO SHORT HLIF Y-88 -4.635E-02 1.853E-01 3.821E-01 NOT IDENT. Y-91 -5.755E+Ol 4.462E+02 8.940E+02 NOT IDENT. NB-94 -8. 791E-05 2.855E-02 5.619E-02 NOT IDENT. NB-95 1.172E-02 9. 423E-'01 l.619E+00 NOT IDENT. NB-95M 1.402E+OO 2.334E+OO 4.240E+OO NOT IDENT. ZR-95 2.865E-01 1.141E+00 2.383E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.598E+31 0.000E+OO SHORT HLIF TC-99M O.OOOE+OO 1. 656E+41 O.OOOE+OO SHORT HLIF RH-101 8.417E-03 3.424E-02 5.629E-02 NOT IDENT. RH-102 2.724E-02 5.616E-02 1.189E-01 FAIL ABUN RU-103 6.090E-01 4.364E+00 8. 962E+OO FAIL ABUN RH-106 -1.405E-01 5.266E-01 9.899E-01 NOT IDENT. RU-106 -l.405E-01 5.266E-01 9.899E-01 NOT IDENT. AG-108M 2.457E-03 2.746E-02 5.053E-02 NOT IDENT. AG-llOM l.905E-04 l.078E-01 2.074E-01 NOT IDENT. SN-113 -7.982E-03 2.148E-01 4.269E-01 NOT IDENT. CD-115 O.OOOE+OO 3.368E+38 O.OOOE+OO SHORT HLIF SN-117M O.ObOE+OO 5.737E+04 0.000E+OO SHORT HLIF TE-123M -4.284E-03 1.084E-01 2.056E-01 NOT IDENT. SB-124 1.060E+OO l.528E+OO 4 .172E+OO NOT IDENT. SB-125 O.OOOE+OO 1.810E-01 2.016E-01 FAIL ABUN TE-125M -5.316E+Ol 2.369E+02 4.503E+02 NOT IDENT. I-126 O.OOOE+OO 6. 728E+05 O.OOOE+OO SHORT HLIF SB-126 0.000E+OO 8.817E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.026E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.796E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 8.209E+25 O.OOOE+OO SHORT HLIF BA-133 l.898E-02 4.834E-02 9.054E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 6.265E-02 1.074E-01 FAIL ABUN CS-135 -9.288E-02 l.469E-01 2.496E-01 NOT IDENT. I.:..135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.128"E+05 O.OOOE+OO SHORT HLIF CE-139 8.757E-02 l.009E-01 2.045E-01 NOT IDENT. BA-140 O.OOOE+OO 8.537E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.481E+05 O.OOOE+OO SHORT HLIF CE-141 -3. 711E+OO 1.892E+Ol 3.536E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF PM-144 5.472E-03 5. 564E-02 1. 096E-01 NOT IDENT. PR-144 5.236E-01 4.823E+OO 9.514E+OO NOT IDENT. PM-146 l.326E-02 4.723E-02 9.562E-02 NOT IDENT. ND-147 O.OOOE+OO l.929E+07 O.OOOE+OO SHORT HLIF PM-149 O.OOOE+OO 5.189E+39 O.OOOE+OO SHOR.T HLIF EU-150 1.351E-02 2.788E-02 5.0lOE-02 FAIL ABUN EU-152 3.668E-02 9.586E-02 1.827E-01 FAIL ABUN GD-153 -1.041E-01 1. 788E-01 3.048E-01 NOT IDENT. EU-154. -5.023E-02 l.147E-01 2.155E-01 FAIL ABUN EU-155 3.595E-03 1. 028E-01 l.999E-01 FAIL ABUN TB-160 -1.069E+OO 2.128E+OO 3. 713E+OO FAIL ABUN H0-166M 2.060E-02 5. 341E-02 l .113E-01 NOT IDENT. TM-171 4.733E+Ol 5.127E+Ol 6.134E+Ol FAIL ABUN Page 296 of 614 LU-172 3.675E-02 6.692E-02 1.470E-01 FAIL ABUN LU-176 6.443E-03 2.092E-02 4.056E-02 FAIL ABUN HF-181 -4. 031E-Ol 3.383E+OO 6.698E+OO NOT IDENT. TA-182 1.015E+OO 9.632E-01 2.189E+OO
  • FAIL ABUN RE-183 -3.628E-02 3.562E+OO 7.172E+OO NOT IDENT. RE-184 -9 .. 14 7E+OO 2.818E+Ol 5.108E+Ol FAIL ABUN W-188 5.274E+Ol 1.149E+02 2.058E+02 FAIL ABUN IR-192 2.434E-01 4.075E-01 8.082E-01 FAIL ABUN HG-203 -5.044E-Ol 2.340E+OO 4.160E+OO NOT IDENT. .BI-207 1. 715E-02 4 .119E-02 8.725E-02 FAIL ABUN PB-210 -1.050E+OO 6.371E+OO 1.270E+Ol NOT IDENT. PB-211 -2.266E-01 6.673E-01 1.277E+OO FAIL ABUN RN-219 3.369E-01 3. 7 51E-01 8.120E-01 NOT IDENT. RA-223 1. 021E-01 6.830E-01 1.165E+OO FAIL ABUN AC-227 -2.948E-02 2.364E-01 4. 282E.:..01 FAIL ABUN TH-227 -2.948E-02 2.364E-01 4.282E-01 FAIL ABUN TH-229 1.114E-01 4. 731E-01 8.976E-01 FAIL ABUN TH-231 1.021E-01 6.830E-01 l.165E+OO FAIL ABUN PA-233 l.835E-02 6.483E-02 l.215E-01 FAIL ABUN PA-234 -6.456E-02 2.728E-01 5.055E-01 FAIL ABUN PA-234M 2.749E-01 *5.435E+OO 1.062E+Ol NOT IDENT. NP-237 l.835E-02 6.483E-02 l.215E-01 FAIL ABUN NP-238 O.OOOE+OO 4.857E+40 O.OOOE+OO SHORT HLIF NP-239 -5.676E-02 2.073E-01 3.928E-01 NOT IDENT. PU-239 5.088E+02 4.615E+02 6.359E+02 FAIL ABUN AM-241 -l.357E-02 1. 679E-01 3.356E-01 NOT IDENT. CM-243 5.228E-02 9.018E-02 1.843E-01 NOT IDENT. BK-247 9.436E-03 7.072E-02 1.324E-01 FAIL ABUN CM-247 3.715E-02 3.424E-02 7.539E-02 NOT IDENT. CF-249 -5.018E-03 4.382E-02 7.710E-02 NOT IDENT. CF-251 4.004E-02 1.046E-01 2.042E-01 NOT IDENT. Page 297of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:47:19.52 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 300 10.66* l.146E+OO l.392E+Ol 1.392E+Ol 12.14 C0-57 122.06 37 85.60* 6.295E+OO 3.870E-02 8.164E-02 85.40 136.47 ------10.68 6.345E+OO ------Line Not Found ------ZN-65 1115. 54 7 50.60* 1.434E+OO 5.845E-02 l.342E-01 132.81 AS-73 53.44 30 10.30* l.028E+OO l.617E+OO 2.023E+Ol 110. 52 CD-109 88.03 85 3.70* 4.861E+OO 2.692E+00 4.178E+OO 45.48 SN-126 64.28 30 9.60 2.287E+OO 7.814E-01 7.814E-01 101.06 86.94 85 8.90 4.861E+OO 1.119E+OO 1.119E+OO 45.48 87.57 85 37.00* 4.861E+00 2.692E-01 2.692E-01 45.48 BA-137M 661. 66 250 89.90* 2.157E+00 7.327E-01 7.464E-01 13.49 CS-137 661. 66 250 85.10* 2.157E+OO 7.740E-01 7.885E-01 13. 49 CE-144 80.12 ------1.36 4.226E+OO ------Line Not Found ------133.52 34 11. 09* 6.348E+OO 2.734E-01 5.573E-01 101.01 PM-147 121.22 37 0.00* 6.295E+OO l.162E+03 l.436E+03 85.40 HF-172 52.97 30 36.00 1.028E+OO 4.627E-01 6.228E-01 110. 52 54.07 30 63.00 1.028E+OO 2.644E-01 3.559E-01 110. 52 61.17 ------20.30 1.994E+OO ------Line Not Found ------62.93 30 4.50 2.287E+00 1.667E+OO 2.244E+00 101.06 67.68 ------5.99 2.822E+OO ------Line Not Found ------81. 75 ------4.50 4.383E+OO ------Line Not Found ------114. 06 ------2.60 6.157E+OO ------Line Not *Found ------122.92 37 1.14 6.295E+OO 2.906E+00 3. 911E+OO 85.40 125.81 24 11. 30* 6.322E+OO l.936E-01 2.605E-01 109.92 127.91 36 1. 46 6.341E+OO 2.199E+OO 2. 960E+OO 92.54 TL-20B 277.37 ------6.60 4.352E+OO ------Line Not Found ------583.19 114 85.00* 2.383E+OO 3.201E-01 3.201E-01 24.75 860.56 ------12.50 1. 758E+00 ------Line Not Found -----,:;-BI-211 72. 87 ------1. 23 3.448E+OO ------Line Not Found ------351. 06 226 12.92* 3.589E+OO 2.765E+OO 2.765E+OO 16.97 BI-212 727. 33 48 6.67* 2.005E+OO 2.0S5E+OO 2.055E+00 31. 40 785.37 18 1.10 1. 887E+OO 4. 91.6E+OO 4.916E+00 76.38 1620.50 ------1. 47 l.045E+OO ------Line Not Found ------PB-212 74.82 122 10.28 3.692E+OO 1. 821E+OO 1. 821E+OO 31. 52 77 .11 213 17.10 3.931E+OO 1. 799E+OO L 799E+00 20.57 238.63 393 43.60* 4.882E+OO l.048E+OO 1.048E+OO 13.02 300.09 35 3.30 4.088E+OO 1.467E+OO 1.467E+OO 67.49 BI-214 609.32 143 45.49* 2.301E+00 7.766E-01 7.769E-01 23.93 1120. 29 25 14.92 1.429E+OO 6.686E-01 6.689E-01 55.73 1764.49 22 15.30 9.660E-01 8.510E-01 8.513E-01 45 .11 PB-214 74.82 122 5.80 3.692E+OO 3.228E+OO 3.229E+OO 31. 52 77 .11 213 9.70 3. 931E+OO 3.173E+OO 20.57 87.09 85 3.41 4.861E+00 2. 921E+OO 2.922E+OO 45.48 242.00 105 7.25 4.834E+OO 1.696E+OO 1.697E+OO 38.03 295.22 124 18.42 4.140E+OO 9.212E-01 9.215E-01 29.90 351. 93 226 35.60*' 3.589E+OO 1.003E+OO 1.004E+OO 16.97 RN-222 609.32 143 45.49* 2. 301E+OO 7.766E-01 7.769E-01 23.93 1120.29 25 14.92 1.429E+OO 6.686E-01 6.689E-01 55.73 Page 298of614 Nuclide Line Activity Report (continued) Page : 2 Sample ID : R405245012 Acquisition date 3-0CT-2016 04:46:21 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 1764.49 22 15.30 9.660E-01 8.510E-01 8.513E-01 45 .11 RA-224' 240.99 105 4.10* 4.834E+OO 3.000E+OO 3.000E+OO 38.03 RA-226. 609.32 143 45.49* 2. 301E+OO 7.766E-01 7.769E-01 23.93 1120.29 25 14.92 l.429E+OO 6.686E-01 6.689E-01 55.73 1764.49 22 15.30 9.660E-01 8.510E-01 8.513E-01 45 .11 AC-228 105.21 ------1.10 5. 896E+OO ------Line Not Found ------338.32 90 11.27 3.707E+OO l.218E+OO 1.218E+OO 37.61 794.95 34 4.25 1.870E+OO 2.415E+OO 2.415E+OO .40. 70 835.71 ------1. 61 1.799E+OO ------Line Not Found ------911. 20 75 25.80* 1.682E+OO 9.814E-01 9.814E-01 37.46 968. 97 54 15.80 1.604E+OO 1. 218E+OO 1.218E+OO 30.18 RA-228 105.21 ------1.10 5.896E+OO ------Line l':Jot Found ------338.32 90 11. 27 3.707E+OO 1.218E+OO l.218E+00 37.61 794.95 34 4.25 1.870E+OO 2.415E+OO 2.415E+OO 40.70 835. 71 ------1. 61 1.799E+OO ------Line Not Found ------911.20 75 25.80* 1.682E+OO 9.814E-01 9 .. 814E-01 37.46 968. 97 54 15.80 1. 604.E+OO 1.218E+OO 1.218E+OO 30.18 TH-228 74.82 122 10.28 3.692E+OO 1.821E+OO 1.821E+OO 31. 52 77 .11 213 17.10 3. 931E+OO 1. 799E+OO 1. 799E+OO 20. 57 238.63 393 43.60* 4.882E+00 1.048E+OO 1.048E+OO 13.02 300.09 35 3.30 4.088E+OO 1.467E+OO 1.467E+OO 67.49 TH-230 609.32 143 45.49* 2. 301E+OO 7.766E-01 7.767E-01 23.93 1120.29 25 14.92 1.429E+OO 6.686E-01 6.686E-01 55.73 1764.49 22 15.30 9.660E-01 8.510E-01 8.510E-01 45 .11 PA-231 283.69 ------1. 70 4.275E+OO ------Line Not Found ------301.36 35 5.35* 4.088E+OO 9.047E-01 9.047E-01 67.49 TH-232 105.21 ------1.10 5. 896E+OO ------Line Not Found ------338.32 90 11. 27 3.707E+OO 1.218E+OO 1.218E+OO 37.61 835. 71 ------*1. 61 1.799E+OO ------Line Not Found ------911. 20 75 25.80* l.682E+OO 9.814E-01 9.814E-01 37.46 968. 97 54 15.80 1.604E+OO 1.218E+OO 1.218E+OO 30.18 TH-234 63.29 30 3.70* 2.287E+OO 2.028E+OO 2.028E+OO 101.06 92.59 71 4. 23. 5.249E+OO 1.816E+OO 1.816E+OO 66.35 U-234 609.32 143 45.49* 2.301E+OO 7.766E-01 7.766E-01 23.93 1120.29 25 14.92 1.429E+OO 6.686E-01 6.686E-01 55.73 1764.49 22 15.30 9.660E-01 8.510E-01. 8.510E-01 45 .11 U-235 89. 96 50 3.47 5.072E+OO 1.624E+OO 1.624E+OO 73.79 93.35 71 5.60 5.249E+OO 1.372E+OO 1. 372E+OO 66.35 143.76 ------10.96* 6. 311E+OO ------Line Not Found ------163.33 ------5.08 6. 096E+OO ------Line Not Found ------185. 72 98 57.20 5.741E+OO l.689E-01 1. 68 9E-01 53.10 205.31 ------5.01 5.415E+OO ------Line Not Found ------U-238 63.29 30 3.70* 2.287E+OO 2.028E+00 2.028E+OO 101.06 92.59 71 4.23 5.249E+OO 1.816E+OO 1.816E+OO 66.35 AM-243 43.53 ------5.90 1. 969E-01 ------Line Not Found ------74.66 122 67.20* 3.692E+OO 2.786E-01 2.786E-01 31. 52 ANH-511 511. 00 71 100.00* 2.644E+OO 1.519E-01 1.519E-01 51. 05 Flag: "*" Key line Page 299 of 614 Summary of Nuclide Activity Sample ID : R405245012 Acquisition date Page : 3 3-0CT-2016 04:46:21 Total number of l.ines in spectrum 56 Number of unidentified lines 13 Number of lines tentatively identified by NID 43 Nuclide Type : Nuclide K-40 C0-57 ZN-65 AS-73 CD-109 SN-126 BA-137M CS-137 CE-144 PM-147 HF-172 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 'l'H-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 271.74D 244.06D 80.30D 461.40D 2.30E+05Y 30.08Y 30.08Y 284. 910 2.62Y 1. 87Y 1. 41E+10Y 7.04E+08Y 1.41E+10Y 1.41E+10Y 1600.00Y 1600.00Y 1600. OOY 1. 41E+l0Y 1600. OOY 1. 41E+10Y 1. 41E+10Y l.41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 2 .11 2.30 12.5 1. 55 1. 00 1. 02 1. 02 2.04 1. 24 1. 35 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.392E+Ol 3.870E-02 5.845E-02 l.617E+OO 2.692E+OO 2.692E-01 7.327E-01 7.740E-01 2.734E-01 1.162E+03 1.936E-01 3.201E-01 2.765E+OO 2.055E+OO 1.048E+OO 7.766E-01 1.003E+OO 7.766E-01 3.000E+OO 7.766E-01 9.814E-01 9.814E-01 1.048E+OO 7.766E-01 9.047E-01 9.814E-01 2.028E+OO 7.766E-01 1.689E-01 2.028E+OO 2.786E-01 1.519E-01 l.206E+03 1.206E+03 Decay Corr pCi/GRAM 1. 392E+Ol 8.164E-02 1.342E-01 2.023E+01 4.178E+OO 2.692E-01 7.464E-01 7.885E-01 5.573E-01 1.436E1;03 2.605E-01 3.201E-01 2.765E+OO 2.055E+OO 1.048E+OO 7.769E-01 1.004E+OO 7.769E-01 3.000E+OO 7.769E-01 9.814E-01 9.814E-01 1.048E+OO 7.767E-01 9.047E-01 9.814E-01 2.028E+OO 7.766E-01 1. 689E-01 2.028E+OO 2.786E-01 1.519E-01 1.501E+03 1. 501E+03 76.79% Decay Corr 2-Sigma Error 0.169E+Ol 6.972E-02 1.782E-01 2.236E+Ol 1.900E+OO 1.224E-01 1.007E-01 1.064E-01 5.629E-01 1.227E+03 2.863E-01 0.792E-01 0.469E+00 0.645E+OO 0.136E+OO 1.859E-01 0.170E+OO 1.859E-01 1.141E+OO 1.859E-01 3.677E-01 3.677E-01 0.136E+OO l.859E-01 6.106E-01 3.677E-01 2.049E+00 l.859E-01 0.897E-01 2.049E+OO 0.878E-01 0.775E-01 "M" Manually accepted 2-Sigma %Error 12.14 85.40 132.81 110. 52 45.48 45.48 13.49 13.49 101.01 85.40 10*9. 92 24.75 16.97 . 31.40 13.02 23.93 16.97 23.93 38.03 23.93 37.46 37.46 13.02 23.93 67.49 37.46 101.06 23.93 53.10 101.06 31. 52 51. 05 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 300 of 614 Flags K Unidentified Energy Lines Page : 4 Sample ID : R405245012 Acquisition date : 3-0CT-2016 04:46:21 It Energy Area Bkgnd FWHM Channel Left *Pw Cts/Sec %Err %Eff Flags 4 94.65 28 76 0.89 189.00 171 21 6.77E-03 **** 5.38E+OO T 0 154.41 37 95 1. 54 308.58 304 8 9.21E-03 **** 6.21E+OO T 0 209.03 54 77 1.13 417.86 413 9 l.36E-02 67. 6 . 5.35E+OO 0 328.69 17 71 0.58 657.28 650 10 4. 41E-03 **** 3.80E+OO T 2 348.66 20 10 1. 33 697.24 696 20 5.28E-03 47. 9 . 3.62E+OO 0 427.55 41 24 4.13 855.07 849 12 1. lOE-02 58.5 3.06E+OO T 0 437.49 15 33 0.90 874.97 872 9 4.05E-03 **** 3.00E+OO 0 464.58 24 61 1. 76 929.18 921 13 6.43E-03 **** 2.86E+OO T 0 470.16 10 27 1. 50 940.35 934 9 2.69E-03 **** 2.83E+OO 0 543.26 11 19 1. 34 1086.60 1083 8 2.95E-03 **** 2.52E+OO 0 665.88 12 10 1. 32 1331. 96 1328 8 3.39E-03 **** 2.15E+OO T 0 744.22 10 2 1. 47 1488.70 1485 8 2.73E-03 81. 4 l.97E+00 0 768.03 20 15 2.41 1536.36 1532 9 5.45E-03 85.5 1.92E+OO T 0 819.46 19 0 0.67 1639.26 1634 11 5.28E-03 45.9 1. 83E+OO T 0 8 94 .11 22 2 1. 22 1788.64 1784 9 6.05E-03 49.5 1. 71E+OO T 0 939.05 6 6 0,86 1878.55 1874 7 1. 78E-03 **** 1. 64E+OO 1 964. 62 27 4 1. 82 1929.72 1923 21 7.48E-03 52.3 1. 61E+OO T 0 1017.49 22 5 1. 30 2035.51 2032 8 6.19E-03 56.1 1.54E+OO 0 1069.26 15 3 1. 00 2139.11* 2133 11 4.23E-03 66.4 l.48E+OO 0 1111. 42 11 2 1. 07 2223.47 2220 7 3.16E-03 70.4 1. 44E+OO T 0 1154.06 13 12 0.70 2308.79 2303 11 3.72E-03 **** 1. 40E+OO 0 1168. 28 12 10 0.61 2337:26 2331 13 3.53E-03 **** l.38E+OO 0 1353.77 5 1 1. 34 2708.41 2705 6 1.55E-03 **** l.22E+OO 0 1377.03 23 0 1.10 2754.96 2749 12 6.67E-03 40.8 1. 21E+OO 0 1408.02 8 2 0.93 2816.98 2814 6 2.35E-03 93.1 l.18E+OO T Flags: "T" = Tentatively associated Page 301of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:47:33.93 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * .*
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245012.CNF;l *
  • Acquisition date 3-0CT-2016 04:46:21 Sensitivity 3.000 *
  • Detector ID GAM09 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.50 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:56:00 Nuclide Library : SOLID *
  • Sample ID R405245012 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.3230E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight :. 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;*16
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 C0-57 ZN-65 CD-109 SN-126 BA-137M CS-137 CE-144 PM-147 HF-172 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2. 996E-01 3.138E-02 1. 359E-01 9.188E-01 5. 960E-02 2.696E-02 2.848E-02 3.116E-01 5.423E+02 1.594E-01 3.016E-02 1.700E-01 3.256E-01 4. 972E-02 5.736E-02 1.605E-01 5.736E-02 5.332E-01 5.736E-02 7.153E-02 7.153E-02 4.972E-02 5.735E-02 3.008E-01 *7 .153E-02 1.273E+00 5.735E-02 '1.557E-01 1. 273E+OO 4.369E-02 2.050E-02 ----Non-Identified Nuclides Nuclide Page 302 of 614 Le (pCi/GRAM BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-58 FE-59 C0-60 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-ll3 CD-ll5 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-U4 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 PM-144 PR-144 PM-146 ND-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M. TM-171 LU-172 Page 303of614 8.905E+OO 3.682E-02 O.OOOE+OO 1. 980E-02 3.023E-01 0.000E+OO O.OOOE+OO 4.338E-02 3.567E-01 O.OOOE+OO 3.845E-01 4.878E+OO 3.166E-02 1. 553E+OO 1. 278E+Ol O.OOOE+OO l.651E-01 O.OOOE+OO O.OOOE+OO 6.332E-01 6.276E+OO 6.142E-01 O.OOOE+OO l.354E-01 3.765E+02 2. 431E-02 7.133E-01 1. 966E+OO l.017E+OO O.OOOE-t-00 0;000E+OO O.OOOE+OO O.OOOE+OO 2. 596E-02 5.225E-02 *3.924E+OO 4.352E-01 4.352E-01 2.240E-02 8.979E-02 l.920E-01 O.OOOE+OO O.OOOE+OO 9.439E-02 l.620E+OO 9.031E-02 2.083E+02 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.152E-02 O.OOOE+OO 4.734E-02 l.138E-01 0.000E+OO O.OOOE+OO 9.513E-02 O.OOOE+OO 0.000E+OO 1. 634E+Ol O.OOOE+OO 4.822E-02 4.187E+OO 4.325E-02 O.OOOE+OO O.OOOE+OO 2.283E-02 8.295E-02. l.408E-Ol 8.950E-02 9.274E-02 1. 6l1E+OO 4.860E-02 2.820E+Ol 6. 218E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT.HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. .NOT I DENT. FAIL ABUN SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 304 of 614 1. 819E-02 2.930E+OO 9.687E-01 3.317E+OO 2.184E+Ol 9.435E+Ol 3.662E-01 1.907E+OO 3.656E-02 5.845E+OO 5.739E-01 3.691E-01 5. 311E-01 1. 962E-01 1. 962E-01 4.169E-01 5. 311E-01 5.560E-02 2.133E-01. 4.723E+OO 5.560E-02 .0. OOOE+OO 1.802E-01 2.981E+02 l.552E-01 8.544E-02 6.039E-02 3. 431E-02 3.496E-02 9.432E-02 FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:47:39.63 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road* *
  • Charleston, SC 29407 * ******************************************************************************* * * * ** DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245012.CNF;l *
  • Acquisition date 3-0CT-2016 04:46:21 Sensitivity : 3.000 *
  • Detector ID GAM09 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.50 Half life ratio : ***** *
  • Sample date 15-DEC-2015 12:56:00 Nuclide Library : SOLID *
  • Sample ID R405245012 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity l.3230E+02 GRAM *
  • Quantity Err(%) 1.5118E-03 % *
  • Wet wt* corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;l6
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.392E+Ol 1.808E+OO C0-57 7.625E-02 6.860E-02 ZN-65 l.342E-01 1.747E-01 CD-109 2.861E+OO l.923E+OO SN-126 1.843E-01 l.235E-01 BA-137M 7.464E-01 l.037E-01 CS-137 7.885E-01 1. 096E-01 CE-144 5.573E-01 5.525E-01 PM-147 1. 341E+03 l.207E+03 HF-172 2.605E-01 2.838E-01 TL-208 3. 201E-01 7.881E-02 BI-211 2.263E-01 8.880E-01 BI-212 2.055E+OO 6.409E-01 PB-212 1.048E+OO 1. 447E-01 BI-214 7.769E-01 1.852E-01 PB-214 1.004E+OO 1. 720E-01 RN-222 7.769E-01 1.852E-01 RA-224 1.371E+OO 1.223E+OO RA-226 7.769E-01 1.852E-01 AC-228 9.814E-01 3.638E-01 RA-228 9.814E-01 3.638E-01 TH-228 1.048E+OO l.447E-01 TH-230 7.767E-01 l.852E-01 PA-231 9.047E-01 6.287E-01 TH-232 9.814E-01 3.638E-01 TH-234 1. 794E+OO 2.059E+OO U-234 7.766E-01 1.852E-01 U-235. 1.187E-01 1.664E:-01 U-238 l.794E+OO 2.059E+OO AM-243 l.991E-01 9.057E:-02 ANH-511 1.519E-01 7.625E-02 Non-Identified Nuclides Nuclide Page 305of614 Key-Line Activity (pCi/GRAM K.L Act error (1.96-sigma) TPU ( 1 . 96-sigma ) 1.808E+OO 6.860E-02 1. 747E-01 1.923E+OO l.235E-01 l.037E-01 l.096E-01 5.525E-01 1.207E+03 2.838E-01 7.881E-02 8.880E-01 6.409E-01 1.447E-01 1.852E-01 1.720E-01 l.852E-01 1.223E+OO 1.852E-Ol. 3.638E-01 3.638E-01 l.447E-01 l.852E-01 6.287E-01 3.638E-01 2.059E+OO l.852E-01 l.664E-01 2.059E+OO 9.057E-02 7.625E-02
  • TPU ( 1. 96-sigma)

BE-7 -4.246E-01 1. 017E+Ol 1.017E+Ol NOT IDENT. NA-22 -1.932E-02 4.687E-02 4.767E-02 NOT IDENT. NA-24 -1.000E+41 1.722E+41 O.OOOE+OO SHORT HLIF AL-26 -l.835E-02 3.157E-02 3.263E-02 NOT IDENT. SC-46 2.285E-02 4.0lOE-01 4.012E-01 FAIL ABUN V-48 2.367E+02 1.230E+04 l.230E+04 SHORT HLIF CR-51 8.983E+Ol 3.349E+02 3.373E+02 SHORT HLIF MN-54 -2.640E-02 5.769E-02 5.890E-02 NOT IDENT. C0-56 1.014E-01 4.045E-01 4. 071E-01 NOT IDENT. MN-56 1.000E+41 3.687E+41 O.OOOE+OO SHORT HLIF C0-58 2.654E-01 3.897E-01 4.077E-01 NOT IDENT. FE-59 4.556E-01 5.883E+OO 5.887E+OO NOT IDENT. C0-60 -6.267E-03 3.842E-02 3.852E-02 NOT IDENT. GE-68 -3.057E+OO 2.578Ef00 2.923E+OO NOT IDENT. AS-73 1.086E+Ol 2.396E+Ol 2.445E+Ol FAIL ABUN AS-74 2.705E+03 4.542E+03 4.703E+03 SHORT HLIF SE-75 2. 963E-02 1.928E-01 l.933E-01 FAIL ABUN BR-77 2.330E+37 1. 968E+38 0.000E+OO SHORT HLIF SR-82 -l.325E+02 5.528E+02 5.560E+02 SHORT HLIF RB-83 4.316E-01 6. 701E-01 6.978E-01 NOT IDENT. KR-85 4.866E+OO 6.510E+OO 6.870E+OO NOT IDENT. SR-85 4.734E-01 6.374E-01 6. 722E-01 .NOT IDENT. RB-86 -l.615E+04 2.323E+04 2.435E+04 SHORT HLIF Y-88 -4.635E-02 l.853E-01 1. 8 65E-01 NOT IDENT. Y-91 -5.755E+Ol 4.462E+02 4.470E+02 NOT IDENT. NB-94 -8.791E-05 2.855E-02. 2.855E-02 NOT IDENT. NB-95 l.172E-02 9.423E-01 9.423E-01 NOT IDENT. NB-95M 1.402E+OO 2.336E+OO 2.420E+00 NOT IDENT. ZR-95 2.865E-01 1.141E+OO l.148E+OO NOT IDENT. NB-97 -1.000E+41 4.144E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.OOOE+41 2.544E+41 O.OOOE+OO SHORT HLIF M0-99 1. 896E+31 2.601E+31 0.000E+OO SHORT HLIF TC-99M l.OOOE+41 1. 659E+41 O.OOOE+OO SHORT HLIF RH-101 8.417E-03 3.428E-02 3.449E-02 NOT IDENT. RH-102 2.724E-02 5.620E-02 5.753E-02 FAIL ABUN RU-103 6.090E-01 4.364E+OO 4. 372E+OO FAIL ABUN RH-106 -1.405E-01 5.267E-01 5.305E-01 NOT IDENT. RU-106 -l.405E-01 5.267E-01 5.305E-01 NOT IDENT. AG-108M 2.457E-03 2.746E-02 2.748E-02 NOT IDENT. 1.905E-04 l.078E-01 l.078E-01 NOT IDENT. SN-113 -7.982E-03 2.148E-01 2.148E-01 NOT IDENT. CD-115 -l.570E+37 3.368E+38 O.OOOE+OO SHORT HLIF SN-117M 7.138E+03 5.738E+04 5.747E+04 SHORT HLIF TE-123M -4.284E-03 1.084E-01 1.084E-01 NOT IDENT. SB-124 1.060E+OO l.529E+OO l.602E+OO NOT IDENT. SB-125 3.157E-01 l.814E-01 2.306E-01 FAIL ABUN TE....:.125M -5.316E+Ol 2.369E+02 2.381E+02 NOT IDENT. I-126 6.465E+05 6.783E+05 7.383E+05 SHORT HLIF SB-126 -1.815E+05 8.823E+05 8. 8 61E+05 SHORT HLIF SB-127 2.634E+21 6.987E+21 O.OOOE+OO SHORT HLIF I-131 l.662E+09 2.797E+09 2. 896E+09 SHORT HLIF I-132 1. OOOE+41 2.093E+42 O.OOOE+OO SHORT HLIF TE-132 4.788E+25 8.426E+25 0.000E+OO SHORT HLIF BA-133 1. 898E-02 4.834E-02 4.910E-02 NOT IDENT. I-133 -l.OOOE+41 4.311E+41 O.OOOE+OO SHORT HLIF CS-134 1. 571E-01 6.301E-02 9.479E-02 FAIL ABUN CS-135 .-9. 288E-02 1.471E-01 1.529E-01 NOT IDENT. I-135 l.000E+41 l.188E+42 O.OOOE+OO SHORT HLIF CS-136 -4.293E+03 2.128E+05 2.128E+05 SHORT HLIF CE-139 8.757E-02 1.024E-01 l.098E-01 NOT IDENT. BA-140 -1.932E+05 8.538E+05 8.582E+05 SHORT HLIF LA-140 -9.831E+04 2.481E+05 2.521E+05 SHORT HLIF CE-141 -3. 711E+OO 1.892E+Ol 1.899E+Ol NOT I DENT*. CE-143 -1.000E+41 5.630E+41 O.OOOE+OO SHORT HLIF PM-144 5.472E-03 5.564E-02 5.569E-02 NOT IDENT. PR-144 5.236E-01 4.823E+OO 4.829E+OO . NOT IDENT. PM-146 1. 326E-02 4. 724E-02 4.762E-02 NOT IDENT. ND-147 7. 518E+06 . 1.929E+07 l.959E+07 SHORT HLIF PM-149 l.079E+39 5.194E+39 O.OOOE+OO SHORT HLIF EU-150 1.351E-02 2.789E-02 2.855E-02 FAIL ABUN EU-152 3.668E-02 9.588E-02 9.730E-02 FAIL ABUN GD-153 -1.041E-01 1. 789E-01 l.849E-01 NOT IDENT. EU-154 -5.023E-02 l.147E-01 l.169E-01 FAIL ABUN EU-155 3.595E-03 1.028E-01 1.028E-01 FAIL ABUN TB-160 -l.069E+00 2.129E+OO 2.183E+OO FAIL ABUN H0-166M 2.060E-02 5.342E-02 5.422E-02 NOT IDENT. TM-171 4.733E+Ol *5.144E+Ol 5.569E+Ol FAIL ABUN Page 306of614 LU-172 3.675E-02 6.703E-02 6.905E-02 FAIL ABUN LU-176 6.443E-03 2.092E-02 2 .112E-02 FAIL ABUN HF-181 -4.031E-01 3.383E+OO 3.388E+OO NOT IDENT. TA-182 1. 015E+OO 9.639E-01 l.067E+00 FAIL ABUN RE-183 -3.628E-02 3.562E+00 3.562E+00 NOT IDENT. RE-184 -9.147E+OO 2.826E+Ol 2.856E+Ol FAIL ABUN W-188 5. 2,74E+Ol l.150E+02 1.17 5E+02 FAIL ABUN IR-192 2.434E-01 4.076E-01 4.221E-01 FAIL ABUN HG-203 -5.044E-01 2. 341E+OO 2.352E+OO NOT IDENT . . BI-207 1. 715E-02 4.120E-02 4.192E-02 FAIL ABUN PB-210 -1.050E+OO 6. 372E+OO 6.389E+OO NOT IDENT. PB-211 -2.266E-01 6.674E-01 6.751E-01 FAIL ABUN RN-219 3.369E-01 3.774E-01 4.068E-01 NOT 'IDENT. RA-223 1. 021E-01 6.830E-01 6.846E-01 FAIL ABUN AC-227 -2.948E-02 2.364E-01 2.368E-01 FAIL ABUN TH-227 -2.948E-02 2.364E-01 2.368E-01 FAIL ABUN TH-229 1.114E-01 4.732E-01 4.758E-01 FAIL ABUN TH-231 1. 021E-01 6.830E-01 6.846E-01 FAIL ABUN PA-233 l.835E-02 6.484E-02 6.537E-02 FAIL ABUN PA.:.234 -6.456E-02 2.826E-01 2.841E-01 FAIL ABUN PA-234M 2.749E-01 5.435E+OO 5.437E+OO NOT IDENT. NP-237 l.835E--'02 6.484E-02 6.537E-02 FAIL ABUN NP-238 -2.647E+40 4.858E+40 O.OOOE+OO *SHORT HLIF NP-239 -'-5.676E-02 2.074E-01 2.089E-01 NOT IDENT. PU-239 5.088E+02 4.620E+02 5.158E+02 FAIL ABUN AM-241 -l.357E-02 1.679E-01 1.680E-01 NOT IDENT. CM-243 5.228E-02 9.031E-02 9.333E-02 NOT IDENT. BK-247 9.436E-03 7.074E-02 7.087E-02 FAIL ABUN CM-247 3.715E-02 3.481E-02 3.863E-02 NOT IDENT. CF-249 -5.018E-03 4.382E-02 4.388E-02 NOT IDENT. CF-251 4.004E.:.02 1. 047E-01 1. NOT IDENT. Page 307of614

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 36.4763 87.09 60.3487 136.47 40.9297 45.60 44.5556 87.57 60.4129 140.51 0.0000 46.54 38.4244 88.03 60.4734 143.76 40.7561 49.72 0.0000 88.34 60.5145 144.24 42.7284 51. 35 45. 6696 88.47 60.5319 145.44 53.5095 51. 87 52.1273 89. 96 60. 7282 152.43 51.1280 52.39 49.0154 1093.63 60.8172 153.25 0.0000 52.97 43.2327 91.11 0.0000 323.87 51.2621 53.44 43.2953 92;59 61.0704 156.02 0.0000 54.07 43.3790 93.35 61.1683 158.56 0.0000 57.36 0.0000 94.56 61.3236 159.00 42.6864 57.53 49.5115 94.65 61.3347 162.33 42.8898 57.98 51.2017 94.67 61. 3373 162.66 0.0000 59.27 52.2087 94.87 61. 3631 163.33 60.9302 59.32 52.2163 97.43 57.2173 165.86 42.1013 59.54 52.2490 98.43 54.6465 176.31 54.9072 60.96 46.9954 98.44 54.6474 176.60 0.0000 61.17 51.3974 99.53 49.3809 177.52 41.7564 62. 93 58.5182 100 .11 51.2362 181.07 0.0000 63.29 58.5761 102.03 55.9439 181.52 53.2386 63.58 58.6226 103.18 47.9314 184.41 40.0789 64.28 48*. 5319 103.37 43.4257 143.76 40.1467 66.73 59.9546 105.21 59.9248 193.51 51.9798 67.24 62.5368 105.31 54.4876 197.03 57.4271 125.81 55. 9311 106.12 53.6632 198.01 53.3151 67.75 57.6107. 106.47 57.3398 201.83 47.2618 69.67 52.0254 109.28 55.8169 203.43 47.3531 70.83 63. 9621 111. 00 57.8330 205.31 44.9987 72.81 50.7491 111. 76 0.0000 210.85 52.3707 72. 87 50.7568 114.06 48.0053 215.65 42. 6996 74.66 59.4791 116. 30 0.0000 222 .11 37.6377 74.82 59.5026 116.74 46.3837 227.09 60.5553 74.97 59.5245 119. 7 6 36.0636 227.38 56.2482 77 .11 59.8337 121.12 32.4103 228.16 0.0000 78.74 60.0665 121. 22 32.4159 228.18 38.9756 79.69 52.7476 121.78 33.6956 116.74 38.9756 80.12 51.6531 122.06 33.7121 235.69 42.2061 80.19 0.0000 122.92 33.7625 235. 96 43.6743 80.57 56.3033 123.07 39.3997 238.63 60.2234 81. 00 57.5099 265.00 33_. 8069 238.98 0.0000 81. 07 64.4219 125.81 37.7005 240.99 60.3745 81. 75 64.5233 127.23 41. 5706 242.00 60.4391 83.79 59.0367 127.91 39.7268 244.70 44.0802 84.00 59.0647 129.30 54.3563 *252.40 0.0000 85.43 67.3882 131.20 43 .1156 252.80 35.5605 .* 86. 55 60.2766 133.02 53.4203 254.15 0.0000 86.79 60.3087 133. 52 61.1016 256.23 42.3754 86.94 60.3287 136. 00 47.2892 260.90 0.0000 Page 308 of 614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 32. 6117 355.39 0.0000 584.27 16. 9116 264.80 33.7408 356.01 34 .1105 595.83 0.0000 265.00 33.7473 364.49 0.0000 427.87 17.0566 268.22 47.3961 366.42 0.0000 602.52 0.0000 269.46 '42.9344 372. 51 19.7407 604.72 11.3955 270.03 39.5662 375.05 32.1406 607.14 18.5407 271.23 35.0850 377.52 28.4847 609.32 19.9891 273.65 0.0000 356.01 18.6644 610.33 19.9994 276.40 44.3594 388.16 33.7030 614.28 17.1768 277.37 30.7384 388.63 0.0000 618.01 22.9463 277.60 30.7450 391.69 27.5329 620.36 16. 2723 278.00 36.4521 264.66 29.3910 621.93 21. 0753 279.20 44.4772 401.81 21.0103 630.19 0.0000 279.54 .35. 3651 402.40 19.3379 631.29 12. 5118 279.70 33.0879 404.85 31.1630 633.25 21.1943 280.46 37.6789 410.95 27.9136 634.78 0.0000 283.69 28.6316 413.71 20.3398 635.95 10. 6115 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41' 41. 2954 423.72 0.0000 645.85 22.2953 285.90 0.0000 427.09 23.0944 657.76 17.5496 287.50 28.7331 427.87 23.1064 657.90 0.0000 290.67 32.2750 433.94 19.3346 661.66 14.6521 293.27 0.0000 439.40 24.5797 664.57 0.0000 351. 93 26.2360' 453.88 26.1200 666.33 0.0000 295. 96 26.2533 463.37 21. 0239 666.50 0.0000 879.38 25.5416 468.07 22.4043 667. 71 0.0000 299.98 30.9985 473.00 0.0000 677.62 10.8263 300.09 31.0010 475.06 24. 7096 685.70 0.0000 300 .13 31. 002 6 476.78 19.4353 695.00 0.0000 301.36 23.2776 477.60 16.7935 696. 49 16.8789 302.85 13.9849 482.18 17.7279 696. 51 16.8789 256.23 30.3450 487.02 0.0000 697.00 0.0000 304.85 -0.0000 492.35 0.0000 697.30 14.8987 306.78 21.0504 497.08 15.2060 697.49 14.8999 308.46 26.9377 505.52 12.1366 702.65 13. 9390 311. 90 34.0667 507.63 0.0000 706.68 11. 9697 316.51 22.4088 511. 00 16.2345 711. 68 11. 9971 319.41 0.0000 514.00 16.2634 720*. 70 0.0000 320.08 0.0000 514.00 16.2634 721.93 0.0000 321. 04 34.3348 520.40 19.0449 722.78 13.5637 323.87 33.2303 520.69 0.0000 722.91 13.5643 325.23 34.8530 522.65 0.0000 723.31 13.5670 328.76 0.0000 527.90 0.0000 724.19 12.0640 333.37 33.4952 528.26 20.0422 727. 33 10.5709 333.97 27.1283 529.59 19.1458 733.00 18.1670 334.37 39.9078 529.87 0.0000 735.93 18.1904 338.28 33.6302 531 .. 02 0.0000 333.97 20.2246 338.32 33. 6311 537.26 0.0000 739.50 0.0000 311. 90 27.2729 546.56 0.0000 747.24 6.0933 340.48 27.2729 552.55 12.9302 748.06 3.0477 340.55 0.0000 563.25 23.2249 752.31 7.1245 344.28 26.5527 569.33 19.5739 753.82 0.0000 345.93 38.6729 '946.00 19.5756 756.73 9.1772 351. 06 33. 9772 569.70 16. 7805. 756.80 9.1776 351.93 34. 0011 583.19 20.6581 884.68 9.2058 Page 309 of 614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 18.4255 1274.44 15. 6395 1620.50 0.0000 766.42 19. 9666 1001.03 15.6651 1621.92 3.9790 766.84 16.8975 1002.74 15.6742 1678.03 0.0000 772.60 0.0000 1004.73 16.8048 1690.97 1.0100 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 2.0519 778.90 10.2934 1028.54 0.0000 1063.66 0.0000 783.70 0.0000 1037.84 15.8594 1771. 35 1.0274 785.37 11. 3531 1038.76 0.0000 1791.20 0.0000 792.07 1.5524 631.29 9.0885 1808.65 3.1062 794.95 14.5064 1048.07 0.0000 1810.72 0.0000 795.86 14.5121 1049.04 17.0544 1836.06 3.1234 810.06 6.2556 1050.41 11. 3745 810.29 6.2561 1063.66 3.4270 344.28 6.2566 1077.00 0.0000 810.76 4.1715 1077.34 17.2107 815.77 0.0000 1085.87 10.3542 1048.07 0.0000 1093.63 5.7666 832.01 11. 5698 1099.45 9.2435 834.85 13.6887 1112. 07 0.0000 835.71 8.4268 1112. 84 0.0000 836.80 0.0000 1115. 54 10.4509 846.75 0.0000 1120.29 8.7219 846.77 9. 5211 1120. 55 8.7225 856.80 0.0000 1221.41 17.4487 860.56 9. 5724 1129. 67 13. 9951* 871.09 12.8145 1131.51 0.0000 873.19 10.6873 1147.95 0.0000 875.33 0.0000 1173.23 7.0903 879.38 20.3537 1177.95 9. 7626 880.51 11. 7887 1189.05 12.4662 883.24 17.1647 1204.77 10.7344 884.68 13.9543 1221. 41 8.9880 889.28 11.2900 1231. 02 17.1248 894.76 9. 6969 1235.36 0.0000 898.04 12.9453 1238.28 10.8376 900.72 15.1177 1260.41 0.0000 903.28 15 .1319 1271.87 10.9402 911.20 5.4201 1274.44 11. 8606 912.08 5.4220 1274.54 11. 8 606 923.98 0.0000 1291.59 4.5834 926.50 11. 9910 1298.22 0.0000 929 .11 9.8199 1312 .11 0.0000 937.49 9. 8496 1332.49 8.3414 944.13 0.0000 1362.66 0.0000 946.00 12.0751 1365.19 3.7395 949.00 6.5935 1368.63 0.0000 667. 71 0.0000 1384.29 0.9395 962. 31 8.2806 1408.01 5. 6711 964. 08 6.6287 1457.56 0.0000 966 .17 6.6335 1460.82 7.6621 911.20 6.6399 1489.16 4.8221 968. 97 6..6399 1505.03 9.6814 983.53 0.0000 1584.12 6.9039 984.45 0.0000 1596.21 0.0000 Page 310 of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:48:10.80 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Conf igura ti on DKAl 0 0: [CANBERRA. GAMMA. ARCHIVE. GAMMA] R40524.5013 . CNF; 1 Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM19.CNF;561 Background date : 2-0CT-2016 11:01:07. Sample date 15-DEC-2015 11:04:00 Acquisition date : 3-0CT-2016 04:46:48. Sample ID R405245013 Sample quantity l.36095E+02 GRAM Detector name : GAM19 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.74 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596387 Detector SN# Matrix Spike ID : . LCS ID : 1556 ******************************************************************************** Pk It 1 0 2 0 3 3 4 3 5 0 6 0 7 0 8 0 9 0 10 0 11 0 12 0 13 3 14 3 15 0 16 0 17 0 18 0 19 0 20 0 21 3 22 3 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Page 311 of 614 Energy 46.17* 61. 41 74.72* 76.93* 83.92 87 .11 92. 96* 108.15 128.25 169.23 185.98* 209. 96 238.49* 241.56 270.47 295.29* 302.05 328.16 338 .11 351.85* 415.91 419.18 463.30 510.36* 545.61 551.59 569.74* 583.26* 609.19* 618.51 663.92 728.53 786.07 795.26 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 26 37 121 211 38 69 75 36 38 21 75 56 422 69 64 116 74 27 68 189 18 24 10 39 15 44 6 102 151 22 32 16 12 14 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 89 247 160 160 198 128 186 86 98 57 118 110 62 80 51 92 83 60 73 50 10 20 34 62 53 28 33 60 32 36 54 48 17 31 0.73 93.12 3.94 123.59 1.21 150.24 1.33 154.67 0.98 168.64 1.25 175.02 1.29 186.74 0.94 217.13 1.36 257.35 1.33 339.34 0.89 372.85 1.11 420.83 1.53 477.91 1.89 484.06 2.24 541.90 1.17 591.57 6.44 605.09 2.12. 657.34 1.27 677.25 1.36 704.72 1.38 832.91 1.90 839.44 1.23 927. 72 2.55 1021.89 4.65 1092.41 5.29 1104.38 1. 51 1140. 69 1.37* 1167. 75 1.22 1219.64 2.37 1238.28 6.86 1329.14 1. 98 1458. 42 1.33 1573.55 1.41 1591.93 90 120 147 147 163 172 183 214 254 336 368 416 471 471 538 585 597 652 673 700 831 831 926 1013 1079 1097 1136 1160 1213 1229 1323 1449 1566 1586 7 7.35E-03 63.9 13 1.03E-02 88.2 13 3.37E-02 19.4 2.48E+OO 13 5.85E-02 13.0 10 1.07E-02 70.5 6 1.91E-02 28.6 10 2.07E-02 37.5 7 1. OOE-02 45. 8 7 1. 07E-02 45. 6 .6 5.79E-03 61.8 8 2.09E-02 28.6 10 l.57E-02 37.5 20 1.17E-01 5.9 5.75E+OO 20 l.92E-02 37.6 9 1. 77E-02 23. 9 12 3.23E-02 19.3 17 2.05E-02 30.8 9 7.37E-03 56.3 9 1.90E-02 25.5 10 5.25E-02 10.3 12 5.02E-03 32.8 2.81E+OO 12 6.55E-03 37.1 6 2.85E-03 9(.7 19 l.07E-02 57.8 19 4.21E-03117.3 16 l.23E-02 30.6 14 1.78E-03271.6 16 2.82E-02 19.9 13 4.20E-02 11.5 16 6.llE-03 69.6 17 8.97E-03 59.9 15 4.33E-03100.7 10 3.21E-03 73.8 14 3.98E-03 87.1 Peak Search Report (continued) Page : 2 Sample ID : R405245013 Acquisition date : 3-0CT-2016 04:46:48 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 809.29 4 22 0.62 1620.00 l611 11 l. llE-03232. 5 36 0 815.04 18 18 3'. 7 8 1631. 5 0 1624 14 5.02E-03 54.5 37 0 911.16* 86 16 1. 63 1823. 8*4 1815 16 2.38E-02 15.5 38 0 952.18 10 17 4.66 1905.90 1897 14 2. 70E-03 96. 6 39 0 .969. 22 48 15 1.70 1939.99 1935 11 l.35E-02 21.5 40 0 1063.66* 24 18 1.90 2128.96 2121 18 6.61E-03 65.5 41 0 1120 .11 31 22 1. 04 2241. 92 2238 *11 8. 74E-03 32. 7 42 0 1196. 65 23 7 0.96 2395.06 2387 16 6.30E-03 34.7 43 0 1210.97 14 27 6.38 2423.70 2407 22 4.00E-03 96.2 44 0 1238.91 36 13 4.27 2479.62 2470 18 l.OlE-02 .28.8 45 0 1377. 92 13 12 1. 56 2757. 77 2750 12 3. 61E-03 60.1 46 0 1460.66 320 7 1.79 2923.32 2917 13 8.87E-02 5.8 47 0 1764.19* 33 0 2.05 3530.65 3525 11 9.12E-03 18.7 Flag: "*"=Peak* area was modified by.background subtraction Page 312of614 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 05:48:13 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245013.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 15-DEC-2015 11:04:00 R405245013 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 04:46:48 136.10 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA19 0 01:00:00.00 1. 50 keV No Linear 75.00 Report Interfering Page 313of614 Nuclide PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 74.82 351.93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-207 BI-211 Line 240.99 86.94 87.57 88.03 7'4. 66 74.82 74.82 74.97 351.06 CAN 0 01:00:00.74 10.00 o,oo % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : R405245013 Acquisition date 3-0CT-2016 04:46:48 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM. %Error Status K-40 1460.82 10.66* l.161E+OO 1.362E+Ol 1.362E+Ol 11. 66 OK C0-58 810.76 99.45* 1. 849E+OO 1.204E-02 2. llOE-01 465.03 OK CD-109 88.03 3.70* 5.479E+OO 1.384E+OO 2.149E+OO 94.43 OK TE-125M 109.28 0.27* 6.331E+OO 1. 354E+Ol 4.644E+02 91. 56 OK SN-126 64.28 9.60 3.426E+OO Line Not Found Absent 86.94 8.90 5.479E+OO 5.754E-01 5.754E-01 94. 43 OK 87.57 37.00* 5.479E+OO 1.384E-01 1.384E-01 94.43 OK BI-207 72. 81 21. 40 4.355E+OO Line Not Found Absent 74.97 35.70 4.535E+OO 3.481E-:-01 3.540E-01 57.46 OK 569.70 97.76 2.437E+OO l.529E-02 1.555E-02 543.18 OK 1063.66 74.60* 1. 496E+OO 1.154E-01 1.174E-01 131. 01 OK 1770.23 6.87 9.833E-01 Line Not Found Absent TL-208 277.37 6.60 4.415E+00 Line Not Found Absent 583.19 85.00* 2.392E+OO 2.839E-01 2.839E-01 39.85 OK 860.56 12.50 1. 763E+OO Line Not Found Absent PB-210 46.54 4.25* 8.614E-01 4.914E+00 5.038E+00 127. 72 OK BI-212 727. 33 6.67* 2.006E+OO 6.507E-01 6.507E-01 201.39 OK 785.37 1.10 1. 891E+00 3.081E+OO 3.081E+00 147.67 OK 1620.50 1. 47 1.063E+OO Line 'Not Found Absent PB-212 74.82 10.28 4.535E+00 1.209E+OO 1.209E+00 57.46 OK 77 .11 17*.10 4.732E+OO 1. 712E+OO 1.712E+OO 26.03 OK 238.63 43.60* 4. 962E+OO 1.184E+OO 1.184E+OO 11. 79 OK 300.09 3.30 4.142E+OO Line Not Found Absent BI-214 609.32 45.49* 2.310E+OO 8.145E-01 8.148E-01 22.97 OK 1120.29 14.92 1.437E+OO 7.910E-01 7.913E-01 65.43 OK 1764.49 15.30 9.863E-01 1.129E+OO 1.129E+OO 37.33 OK PB-214 74.82 5.80 4.544E+OO Line Not Found <<INT Reject 77 .11 9.70 4.732E+OO 3.018E+OO 3.019E+OO 26.03 OK 87.09 3.41 5.478E+OO Line Not Found <<INT Reject 242.00 7.25 4.908E+OO Line Not Found <<INT Reject 295.22 18.42 4.197E+OO 8.991E-01 8.994E-01 38.65 OK 351. 93 35.60* 8.637E-01 8.640E-01 20.51 OK RN-222 609.32 45.49* 2.310E+OO 8.145E-01 8.148E-01 . 22. 97 OK 1120.29 14.92 1.437E+OO 7.910E-01 7.913E-01 65.43 OK 1764.49 15.30 9.863E-01 1.129E+oo* 1.129E+OO 37.33 OK RA-224 240.99 4.10* 4. *915E+OO 4.899E-01 4.899E-01 343.10 OK RA-226 609.32 45.49* 2.310E+OO . 8 .145E-01 8.148E-01 22.97 OK 1120.29 14.92 1.437E+OO 7.910E-01 7. 913E-01 65.43 OK 1764.49 15.30 9.863E-01 1.129E+OO 1.129E+OO 37.33 OK AC-228 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11.27 3.752E+OO 9.555E-01 9.555E-01 51. 01 OK 794.95 4.25 1.874E+00 9.958E-01 9.958E-01 174 .13 OK 835.71 1. 61 1.803E+OO Line Not Found Absent 911.20 25.80* 1.687E+OO 1.078E+OO 1.078E+OO 30.96 OK 968.97 15.80 1.608E+OO 1.040E+OO 1.040E+OO 42.97 OK RA-228 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11. 27 3.752E+OO 9.555E-01 9.555E-01 51. 01 OK 794.95 4.25 1.874E+OO 9.958E-01 9.958E-01 174.13 OK 835. 71 1. 61 1. 803E+OO Line Not Found Absent Page 314of614 Nuclide Line Activity Report (continued) Page : 3 Sample ID : R405245013 Acquisition date 3-0CT-2016 04:46:48 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 911.20 25.80* l.687E+OO 1.078E+OO l.078E+OO 30. 96 OK 968. 97 15.80 l.608E+OO l.040E+OO 1.040E+OO 42.97 OK TH-228 74.82 10.28 4.535E+OO 1.209E+OO 1.209E+OO 57.46 OK 77 .11 17.10 4.732E+00 1. 712E+OO 1. 712E+OO 26.03 OK 238.63 43.60* 4. 962E+OO 1.184E+OO l.184E+OO 11. 79 OK 300.09 3.30 4.142E+OO Line Not Found Absent TH-230 609.32 45.49* 2.310E+OO 8.145E-01 8.145E-01 22. 97 OK 1120.29 14.92 l.437E+OO 7.910E-01 7.910E-01 65.43 OK 1764.49 15.30 9.863E-01 1.129E+OO 1.129E+OO 37.33 OK PA-231 283.69 1. 70 4.336E+OO Line Not Found Absent 301.36 5.35* 4.120E+OO 2.000E+OO 2.000E+OO 61. 66 OK TH-232 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11.27 3.752E+OO 9.555E-01 9.555E-Ol 51. 01 OK 835. 71 1. 61 1. 803E+OO Line Not Found Absent 911. 20 25.80* 1.687E+OO 1. 078E+OO 1.078E+OO 30.96 OK 968. 97 15.80 1.608E+OO l.040E+OO 1.040E+OO 42.97 OK U-234 609.32 45.49* 2.310E+OO 8.145E-01 8.145E-01 22.97 OK 1120.29 14.92 1.437E+OO 7.910E-01 7.910E-01 65.43 OK 1764.49 15.30 9.863E-01 l.129E+OO 1.129E+OO 37.33 OK AM-243 43.53 5.90 5.190E-01 Line Not Found Absent 74.66 67.20* 4.535E+OO l.849E-01 1. 849E-01 57.46 OK ANH-511 511. 00 100.00* 2.665E+00 8.292E-02 8.292E-02 115. 62 OK Flag: "*" = Keyline Page 315 of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:48:14.27 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245013.CNF;l *
  • Acquisition date 3-0CT-2016 04:46:48 Sensitivity : 3.000 *
  • Detector ID GAM19 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.74 Half life ratio : ***** *
  • Sample date 15-DEC-2015 11:04:00 Analyst initials: MXRl *
  • Sample ID R405245013 Sample Quantity 1.3610E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 15-JUN-2016 10:35:16 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;17
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pC;i./GRAM K-40 1.362E+Ol 1.556E+OO 6.062E-01 C0-58 2. llOE-01 9.617E-01 l.lOOE+OO CD-109 2.149E+OO 1.988E+OO 2.365E+OO TE-125M 4.644E+02 4.167E+02 4.982E+02 SN-126 1.384E-01 1.281E-01 l.588E-01 BI-207 l.174E-01 l.507E-01 1.135E-01 TL-208 2.839E-01 l.108E-01 6.412E-02 PB-210 5.038E+OO 6.307E+OO 5.515E+OO BI-212 6.507E-01 l.284E+OO l.036E+OO PB-212 1.184E+00 l.368E-01 9. 661E-02 BI-214 8.148E-01 1.834E-01 1.369E-01 PB-214 8.640E-01 l.737E-01 l.440E-01 RN-222 8.148E-01 1.834E-01 1.369E-01 RA-224 4.899E-01 1.647E+OO 1.036E+OO RA-226 8.148E-01 1.834E-01 1.369E-01 AC-228 1.078E+OO 3.270E-01 2.527E-01 RA-228 l.078E+00 3.270E-01 2.527E-01 TH-228 1.184E+OO l.368E-01 9.661E-02 TH-230 8.145E-01 l.833E-01 1.368E-01 PA-231 2.000E+OO 1.208E+OO 6.890E-01 TH-232 1.078E+OO 3.270E-01 2.527E-01 U-234 8.145E-01 l.833E-01 l.368E-01 AM-243 1. 849E-01 1.041E-01 1.034E-01 ANH-511 8.292E-02 9.395E-02 5.751E-02 Non-Identified *Nuclides ----Key-Line Activity . K.L. Cnt Uncert MDA Nuclide (pCi/GRAM (1.96-sigma) (pCi/GRAM BE-7 -1. 611E+OO 1.284E+Ol 2.358E+Ol NOT IDENT. NA-22 -7.674E-03 3.141E-02 06. 220E-02 NOT IDENT. NA-24 O.OOOE+OO 1.960E+41 0.000E+OO SHORT HLIF AL-26 -8.582E-03 2.214E-02 4.575E-02 NOT IDENT. SC-46 l.079E-01 3.422E-01 7.226E-01 FAIL ABUN V-48 O.OOOE+OO 1. 224E+04. O.OOOE+OO SHORT HLIF Page 316 of 614 CR-51 O.OOOE+OO 4.282E+02 O.OOOE+OO SHORT HLIF MN-54 3.093E-02 7.381E-02 1. 511E-01 NOT IDENT. C0-56 2.480E-01 4.544E-01 9.720E-01 FAIL ABUN MN-56 O.OOOE+OO l.856E+41 O.OOOE+OO SHORT HLIF C0-57 3.47JE-02 5.070E-02 1. 031E-01 NOT IDENT. FE-59 -1.243E+OO 6.901E+OO l.302E+Ol NOT IDENT. C0-60 -7.556E-03 4.086E-02 7.803E-02 NOT IDENT. ZN-65 -6.258E-02 1. 868E-01 2.956E-01 NOT IDENT. GE-68 2.608E+OO 2.178E+OO 5.206E+OO NOT IDENT. AS-73 -6.535E-01 7.699E+OO l.418E+Ol NOT IDENT. AS-74 0.000E+OO 5.739E+03 O.OOOE+OO SHORT HLIF SE-75 -1.800E-01 2.208E-01 3.880E-01 NOT IDENT. BR-77 O.OOOE+OO 3.111E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.532E+02 O.OOOE+OO SHORT HLIF RB-83 -1.429E-01 7.184E-01 l.302E+OO FAIL ABUN KR-85 -1.549E+OO 8.898E+OO l.422E+Ol NOT IDENT. SR-85 -1.522E-01 8.726E-01 l.395E+OO NOT IDENT. RB-86 O.OOOE+OO l.982E+04 O.OOOE+OO SHORT HLIF Y-88 -1.167E-01 2.153E-:-01 4.008E-01 NOT IDENT. Y-91 -2.761E+02 5.925E+02 1.049E+03 NOT IDENT. NB-94 -3.633E-03 3.142E-02 6.152E-02 NOT IDENT. NB-95 -2.993E-01 9.413E-01 1. 759E+OO NOT IDENT. NB-95M -5.508E-01 2.462E+OO 4.097E+OO NOT IDENT. ZR-95 9.471E-01 1.706E+OO 3.517E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 7.793E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.977E+31 O.OOOE+OO SHORT HLIF TC-99M 'O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF RH-101 6.494E-02 5.807E-02 7.235E-02 FAIL ABUN RH-102 -3.704E-02 7.075E-02 1.202E-01 NOT IDENT. RU-103 -1.862E+OO 6.567E+OO 1.170E+Ol FAIL ABUN RH-106 -l.765E-01 5.725E-01 8.879E-01 NOT IDENT. RU-106 -1. 7 65E-01 5.725E-01 8.879E-01 NOT IDENT. AG-108M 2.374E-02 3.461E-02 6. 881E-02 NOT IDENT. AG-llOM -3.029E-02 1.129E-01 2 .131E-01 NOT IDENT. SN-113 6.323E-02 2.295E-01 4.473E-01 NOT IDENT. CD-115 O.OOOE+OO 3.743E+38 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 7.459E+04 O.OOOE+OO SHORT HLIF TE-123M 1.309E-02 1.375E-01 2.666E-01 NOT IDENT. SB-124 -3.819E-01 1. 773E+OO 3. 714E+OO NOT IDENT. SB-125 5.360E-02 l.153E-01 2.274E-01 FAIL ABUN I-126 O.OOOE+OO 6.639E+05 O.OOOE+OO .SHORT HLIF SB-126 O.OOOE+OO 9.308E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.705E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3. 321E+09 O.OOOE+OO SHORT HLIF i-132 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 8. 881E+25 O.OOOE+OO SHORT HLIF BA-133 2.025E-02 5.027E-02 8. 911E_.:.02 FAIL ABUN I-133 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 6.477E-02 l.105E-01 l.283E-01 FAIL ABUN CS-135 -2.828E-02 1. 771E-01 2.942E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 2.524E+05 O.OOOE+OO SHORT HLIF BA-137M O.OOOE+OO 5.054E-02 1.102E-01 NOT IDENT. CS-137 O.OOOE+OO 5.339E-02 1.164E-01 NOT IDENT. CE-139 -2.430E-03 1.210E-01 2.099E-01 NOT IDENT. BA-140 O.OOOE+OO 1.053E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.915E+05 O.OOOE+OO SHORT HLIF CE-141 5.602E+OO 2.235E+Ol 4.388E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.101E+41 O.OOOE+OO SHORT HLIF CE-144 -9.145E-02' 3.862E-01 7.381E-01 NOT IDENT. PM-144 -l.497E-02 6.151E-02 1.184E-01 FAIL ABUN PR-144 -1.263E+OO 5.328E+OO 1.026E+Ol NOT IDENT. PM-146 6.939E-03 4.580E-02 8. 7 91E-02 NOT IDENT. ND-147 O.OOOE+OO 2.245E+07 O.OOOE+OO SHORT HLIF PM-147 -4.029E+Ol 8.947E+02 1. 7 41E+0'3 NOT IDENT. PM-149 O.OOOE+OO 5.951E+39 O.OOOE+OO SHORT HLIF EU-150 1.774E-02 3.270E-02 5.840E-02 FAIL ABUN EU-152 -2.646E-02 1.070E-01 1.958E-01 FAIL ABUN GD-153 6.049E-03 2.129E-01 3.530E-01 NOT IDENT. EU-154 -l.629E-02 7.811E-02 l.561E-01 NOT IDENT. EU-155 5.927E-02 1.334E-01 2.278E-01 FAIL ABUN TB-160 -7.928E-01 2.108E+OO 3.898E+OO FAIL ABUN H0-166M 2.147E-03 6.533E-02 l.287E-01 FAIL ABUN TM-171 -3.765E+OO 2.081E+Ol 3.790E+Ol NOT IDENT. HF-172 2.343E-02 2.614E-01 4.639E-01 FAIL ABUN LU-172 1.259E-02 8.594E-02 l.710E-01 FAIL ABUN LU-17.6 -2.969E-03 2.804E-02 4.695E-02 FAIL ABUN Page 317of614 HF-181 1.900E-02 4.525E+OO 8.428E+OO NOT IDENT. TA-182 6 .. 860E-01 9.752E-01 2.074E+OO FAIL ABUN RE-183 1.865E+OO 2.884E+OO 5.222E+OO NOT IDENT. RE-184 1.937E+Ol 2.706E+Ol 5. 713E+Ol NOT IDENT. W-188 -5.483E+Ol l.360E+02 2.173E+02 NOT IDENT. IR-192 -1.690E-Ol 5.273E-01 9.592E-01 FAIL ABUN HG-203 -6.756E-01 2.524E+OO 4.640E+OO NOT IDENT. BI-211 O.OOOE+OO 4.784E-01 8.498E-01 FAIL ABUN PB-211 1.088E-01 8.622E-01 l.614E+OO NOT IDENT. RN-219 1.717E-01 4.731E-01 9.094E-01 FAIL ABUN RA-223 -5.957E-01 8.043E-01 1.221E+OO FAIL ABUN AC-227 2.755E-01 2.498E-01 5.158E-01 NOT IDENT. TH-227 2.755E-01 2.498E-01 5.158E-01 NOT IDENT. TH-229 -4.613E-02 5.176E-01 9.813E-01 FAIL ABUN TH-231 -5.957E-01 8.043E-01 1.221E+OO FAIL ABUN PA-233 -6. 571E-02 6.202E-02 l.042E-01 NOT IDENT. PA-234 -2.264E-01 3.256E-01 4.702E-01 FAIL ABUN PA-234M l.319E+OO 4.645E+OO 9.639E+OO NOT IDENT. TH-234 3.201E-01 1.416E+OO 2.650E+OO FAIL ABUN U-235 1.365E-01 2.026E-01 3.984E-01 FAIL ABUN NP-237 -6.571E-02 6.202E-02 l.042E-01 NOT IDENT. NP-238 O.OOOE+OO 5.386E+40 O.OOOE+OO SHORT HLIF U-238 3.201E-01 1. 416E+OO 2.6SOE+oo* FAIL ABUN NP-239 -2.922E-01 2.429E-01 4.370E-01 NOT IDENT. PU-239 5.914E+02 5.289E+02 6. 991E+02 FAIL ABUN AM-241 6.989E-02 1.530E-01 2.693E-01 NOT IDENT. CM-243 9.628E-02 l.140E-01 2.168E-01 NOT IDENT. BK-247 -4.885E-02 7.917E-02 1.419E-01 FAIL ABUN CM-247 2.083E-02 4.448E-02 8.607E-02 NOT IDENT. CF-249 3.145E-02 3.774E-02 7.821E-02 NOT IDENT. CF-251 1.150E-02 l.141E-01 2.218E-01 NOT IDENT. Page 318of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:48:11.78 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 305 10.66* 1.161E+OO l.362E+Ol l.362E+Ol 11. 66 C0-58 810.76 4 99.45* l.849E+OO 1.204E-02 2. llOE-01 465.03 CD-109 88.03 81 3.70* 5.479E+OO 2.213E+OO 3.435E+OO 57.27 TE-125M 109.28 42 0.27* 6.331E+OO 1.354E+Ol 4.644E+02 91. 56 SN-126 64.28 ------9.60 3.426E+OO ------Line Not Found ------86.94 81 8.90 5. 479E+O.O 9.199E-01 .9.199E-01* 57.27 87. 57 81 37.00* 5.479E+OO 2.213E-01 2.213E-01 57.27 BI-207 72.81 ------21. 40 4.355E+OO ------Line Not Found ------74.97 145 35.70 4.535E+OO 4.941E-01 5.025E-01 38.83 569.70 7 97.76 2.437E+OO 1.529E-02 l.555E-02 543.18 1063.66 23 74.60* 1. 496E+OO 1.154E-01 1. l 74E__.01 131. 01 1770.23 ------6*. 87 9.833E-01 ------Line Not Found ------TL-208 277.37 ------6.60 4.415E+OO ------Line Not Found ------583.19 105 85.00* 2.392E+OO 2.839E-01 2.839E-01 39.85 860.56 ------12.50 1. 763E+OO ------Line Not Found ------PB-210 46.54 33 4.25* 8.614E-01 4.914E+OO 5.038E+OO 127.72 BI-211 72.87 ------1. 23 4.361E+OO ------Line Not Found ------351.06 202 12.92* 3.630E+OO 2.380E+OO 2.380E+OO 20.51 BI-212 727. 33 16 6.67* 2.006E+OO 6.507E-01 6.507E-01 201.39 785.37 12 1.10 1.891E+OO 3.081E+OO 3. 081E+OO 147.67 1620.50 ------1. 47 1.063E+OO ------Line Not Found ------PB-212 74.82 145 10.28 4.535E+OO 1. 716E+OO l.716E+OO 38.83 77 .11 251 17.10 4.732E+OO l.712E+00 1.712E+OO 26. 03 238.63 464 43.60* 4. 962E+OO 1.184E+OO 1.184E+OO 11. 79 300.09 ------3.30 4.142E+OO ------Line Not Found ------BI-214 609.32 155 45.49* 2.310E+OO 8.145E-01 8.148E-01 22.97 1120.29 31 14.92 l.437E+OO 7.910E-01 7.913E-01 65.43 1764.49 31 15.30 9.863E-01 1.129E+OO 1.129E+OO 37.33 PB-214 74.82 145 5.80 4.535E+OO 3.041E+OO 3.042E+OO 38.83 77 .11 251 9.70 4.732E+OO 3.018E+OO 3.019E+OO 26.03 87.09 81 3.41 5.479E+OO 2.401E+OO 2.402E+OO 57.27 242.00 76 7.25 4. 915E+oo* l.176E+OO 1.177E+OO 75.23 295.22 126 18.42 4 .1.97E+OO 8.99lE-01 8.994E-01 38.65 351.93 202 35.60* 3.630E+OO 8.637E-01 8.640E-01 20.51 RN-222 609.32 155 45.49* 2.310E+OO 8.145E-01 8.148E-01 22.97 1120.29 31 14.92 1.437E+OO 7.910E-01 7.913E-01 65.43 1764.49 31 15.30 9.863E-01 1.129E+OO 1.129E+OO 37.33 RA-224 240.99 76 4.10* 4.915E+OO 2.080E+OO 2.080E+OO 75.23 RA-226 609.32 155 45.49* 2.310E+OO 8.145E-01 8.148E-01 22.97 1120.29 31 14.92 1.437E+OO 7.910E-01 7.913E-01 65.43 1764.49 31 15.30 9.863E-01 1.129E+OO 1.129E+OO 37.33 AC-228 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 73 11. 27 3.752E+OO 9.555E-01 9.555E-01 51. 01 794.95 14 4.25 1.874E+OO 9.958E-01 9.958E-01 174.13 835.71 ------1. 61 l.803E+OO ------Line Not Found ------911.20 85 25.80* 1.687E+OO 1. 078E+OO 1.078E+OO 30. 96 968. 97 48 15.80 1.608E+OO 1.040E+OO 1.040E+OO 42.97 Page 319of614 Nuclide Line Activity Report (continued) Page : 2 Sample ID : R405245013 Acquisition date 3-0CT-2016 04:46:48 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff *pCi/GRAM pCi/GRAM %Error RA-228 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 73 11.27 3.752E+OO 9.555E-01 9.555E-01 51. 01 794.95 14 4.25 1. 874E+OO 9.958E-01 9.958E-01 174 .13 835. 71 ------1. 61 l.803E+OO ------Line Not Found ------911. 20 85 25.80* l.687E+OO l.078E+OO l.078E+OO 30. 96 968. 97 48 15.80 l.608E+OO l.040E+OO l.040E+OO 42.97 TH-228 74.82 145 10.28 4.535E+OO 1. 716E+OO 1. 716E+OO 38.83 77 .11 251 17.10 4.732E+OO l.712E+00 1. 712E+00 26.03 238.63 464 43.60* 4. 962E+OO l.184E+OO l.184E+OO 11. 79 300.09 ------3.30 4.142E+00 ------Line Not Found ------TH-230 609.32 155 45.49* 2.310E+OO 8.145E-01 8.145E-01 22.97 1120.29 31 14.92 1.437E+OO 7.910E-01 7.910E-01 65.43 1764.49 31 15.30 9.863E-01 l.129E+OO l.129E+OO 37.33 PA-231 283.69 ------1. 70 4.336E+OO ------Line Not Found ------301.36 80 5.35* 4.120E+00 2.000E+OO 2.000E+OO 61. 66 TH...:232 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 73 11. 27 3.752E+OO 9.555E-01 9.555E-01 51. 01 835. 71 ------1. 61 l.803E+OO ------Line Not Found ------911.20 85 25.80*. 1.687E+OO 1.078E+OO 1.078E+OO 30. 96 968. 97 48 15.80 l.608E+00 l.040E+00 l.040E+OO 42.97
  • U-234 609.32 155 45.49* 2.310E+OO 8.145E-01 8.145E-01 22.97 1120.29 31 14.92 1.437E+OO 7.910E-01 7.910E-01 65 .43 1764.49 31 15.30 9.863E-01 l.129E+00 1.129E+OO 37.33 AM-243 43.53 ------5.90 5.190E-01 ------Line Not Found ------74.66 145 67.20* 4.535E+00 2.625E-01 2.625E-01 38.83 ANH-511 511. 00 40 100.00* 2.665E+OO 8.292E-02 8.292E-02 115.62 Flag: "*" Key line *Page 320of614 Summary of Nuclide Activity Sample ID : R405245013 Acquisition date Page : 3 3-0CT-2016 04:46:48 Total number of lines in spectrum 47 Number of unidentified lines 6 Number of lines tentatively identified by NID 41 Nuclide Type : Nuclide K-40 C0-58 CD-109 TE-125M SN-126 BI-207 TL-208 PB-210 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 Hlife l.25E+09Y 70.86D 461.40D 57.40D 2.30E+05Y 32.90Y l.41E+l0Y 22.20Y 7.04E+08Y 1. 41E+l0Y 1. 41E+l0Y 1600.00Y 1600. OOY 1600.00Y 1. 41E+l0Y 1600.00Y l.41E+l0Y 1. 4lE+lOY 1. 41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 2.45E+05Y 7-370.00Y l.OOE+09Y Decay l. 00 17.5 l. 55 34.3 l. 00 l. 02 l. 00 l. 03 l. 00 l. 00 l. 00 l. 00 l. 00 l. 00 l. 00 i. oo* l. 00 l. 00 l. 00 l. 00 l. 00 l. 00 l. 00 l. 00 l. 00 Uncorrected pCi/GRAM l.362E+Ol l.204E-02 2. 213E+OO l.354E+Ol 2. 213E-01 l.154E-Ol 2.839E-Ol 4.914E+OO 2.380E+00 6.507E-01 l.184E+OO 8.145E-01 8.637E-01 8.145E-01 2.080E+OO 8.145E-01 l.078E+OO l. 078E+OO l.184E+OO 8.145E-01 2.000E+OO l.078E+OO 8.145E-01 2.625E-01 8.292E-02 Total Activity : 5.291E+Ol Grand Total Activity : 5.291E+Ol Decay Corr pCi/GRAM l.362E+Ol 2. llOE-01 3.435E+OO 4.644E+02 2. 213E-01 l.174E-01 2.839E-01 5.038E+OO 2.380E+OO 6.507E-01 l.184E+OO 8.148E-01 8.640E-01 8 .148E-0*1 2.080E+OO 8.148E-01 l.078E+00 l.078E+OO l.184E+OO 8.145E-01 2.000E+OO 1. 078E+OO 8.145E-Ol 2.625E-Ol 8.292E-02 5.053E+02 5.053E+02 87.23% Decay Corr 2-Sigma Error 0.159E+Ol 9.814E-01 l. 967E+OO 4.252E+02 l.267E-01 1.538E-01 l.131E-01 6.435E+OO 0.488E+OO 13.lOE-01 0.140E+00 l. 871E-01 l.772E-01 1. 871E-01 l.565E+OO 1. 871E-01 0.334E+OO 0.334E+OO 0.140E+00 1. 871E-01 l.233E+00 0.334E+OO 1. 871E-01 l.019E-01 9.587E-02 Manually accepted 2-Sigma %Error 11. 66 465.03 57.27 91. 56 57.27 131.01 39.85 127.72 20.51 201.39 11. 79 22.97 20.51 22.97 75.23 22:97 . 30. 96 30. 96 11. 79 22.97 61. 66 30. 96 22.97 38.83 115. 62 Flags: "K" "E" Keyline not found Manually edited "M" "A" Nuclide specific abn. limit Page 321 of 614 Flags Unidentified Energy Lines Page : 4 Sample ID : R405245013 Acquisition date : 3-0CT-2016 04:46:48 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 61. 41 45 299 3.94 123.59 120 13 l.03E-02 **** 3.07E+OO T 0 83.92 46 234 0.98 168.64 163 10 1.07E-02 **** 5.27E+OO T 0 92. 96 88 219 1. 29 186.74 183 10 2.07E-02 75.1 5.80E+OO T 0 128.25 44 112 1. 36 257.35 254 7 1.07E-02 91. 3 6.54E+OO T 0 169.23 24 64 1. 33 339.34 336 6 5.79E-03 **** 6.12E+OO 0 185.98 84 132 0.89 372. 85 368 8 2.09E-02 57.3 5.84E+OO T 0 209. 96 63 122 1.11 420.83 416 10 1.57E-02 75.0 5.43E+OO T 0 270.47 69 56 2.24 541.90 538 9 1.77E-02 47.9 4.50E+OO T 0 328.16 29 65 2.12 657.34 652 9 7.37E-03 **** 3.85E+OO T 3 415.91 19 11 1. 38 832.91 831 12 5.02E-03 65.5 3.16E+OO T 3 419.18 25 21 1. 90 839.44 831 12 6.55E-03 74.2 3.13E+OO 0 463.30 11 35 1. 23 927.72 926 6 2.85E-03 **** 2.88E+OO T 0 545.61 16 55 4.65 1092.41 1079 19 4.21E-03 **** 2.52E+OO T 0 551.59 46 29 5.29 1104. 38 1097 16 1. 23E-02 61.1 2.50E+OO T 0 618.51 23 37 2.37 1238.28 1229 16 6. llE-03 **** 2.28E+OO T 0 663.92 33 55 6.86 1329.14 1323 17 8.97E-03 **** 2.16E+OO T 0 815.04 18 18 3.78 1631.50 1624 14 5.02E-03 **** 1.84E+OO T 0 952.18 10 17 4.66 1905.90 1897 14 2.70E-03 **** l.63E+OO 0 1196. 65 22 7 0.96 2395.06 2387 16 6.30E-03 69.5 1.36E+00 0 1210.97 14 26 6.38 2423.70 2407 22 4.00E-03 ***** 1.35E+OO 0 1238.91 35 12 4.27 2479.62 2470 18 l.OlE-02 57.5 l.33E+OO T 0 1377.92 12 12' 1. 56 2757.77 2750 12 3.61E-03 **** 1.22E+OO Flags: "T" = Tentatively associated Page 322 of 614 Nuclide Identification Report Generated 05:48:28.17 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245013.CNF;l *
  • Acquisition date 3-0CT-2016 04:46:48 Sensitivity 3.000 *
  • Detector ID GAM19 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.74 Half life ratio : ***** *
  • Sample date 15-DEC-2015 11:04:00 Nuclide Library : SOLID *
  • Sample ID R405245013 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.3610E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 15-JUN-2016 10: 35: 16 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;17
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis.* Identified Nuclides Nuclide K-40 C0-58 CD-109 TE-125M SN-126 BI-207 TL-208 PB-210 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 Le (pCi/GRAM 2.427E-01 4.781E-01 1.123E+OO 2.335E+02 7.559E-02 4.991E-02 2.832E-02 2.548E+OO 4.618E-01 4.474E-02 6 .121E-02 6.610E-02 6 .121E-02 4.797E-01 6 .121E-02 1.091E-01 1.091E-01 4.474E-02 6 .119E-02 3.09'7E-01 1.091E-01 6 .119E-02 4. 913E-02 2.590E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 323of614 Le (pCi/GRAM l.061E+Ol 2.394E-02 O.OOOE+OO 1.513E-02 3 .119E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57
  • FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-:-134 CS-135 I-135
  • CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD_.:.153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 324 of 614 6.756E-02 4.275E-01 O.OOOE+OO 4.860E-02 5. 641E+OO 3.237E-02 l.242E-01 2.270E+OO 6.597E+OO O.OOOE+OO 1. 785E-01 O.DOOE+OO 0.000E+OO 5.829E-01 6.415E+OO 6.291E-01 O.OOOE+OO l.475E-01 4.563E+02 2.709E-02 7.864E-01 1. 901E+OO 1.589E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.410E-02 5.312E-02 5. 311E+OO 3". 859E-01 3.859E-01 3.164E-02 9.299E-02 2.030E-01 O.OOOE+OO O.OOOE+OO l.252E-01 l.412E+OO l.036E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.094E-02 O.OOOE+OO 5. 801E-02 l.365E-01 O.OOOE+OO O.OOOE+OO 5 .114E-02 5.403E-02 9.810E-02 O.OOOE+OO O.OOOE+OO 2.066E+Ol O.OOOE+OO 3.472E-01 5.279E-02 4.576E+OO 3.954E-02 O.OOOE+OO 8 .188E+o2 O.OOOE+OO 2.707E-02 8.977E-02 1. 661E-01 6.044E-02 l.073E-01 1.710E+OO 5.750E-02 1.770E+01 2.178E-01 7.457E-02 2.146E-02 3.807E+OO NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 . U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 325 of 614 9.154E-01 2.451E+OO 2.497E+Ol 1.004E+02 4.431E-01 2.153E+OO 4.087E-01 7.445E-01 4.191E-01 5.610E-01 2.407E-01 2.407E-01 4.600E-01 5.610E-01 4. 716E-02 1. 968E-01 4.249E+OO 1. 261E+OO l.883E-01 4.716E-02 O.OOOE+OO 1.261E+OO 2.033E-01 3.307E+02 1. 2 68E-01 1.023E-01 6.533E-02 3.977E-02 3.564E-02 l.034E-01 FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL .ABUN NOT IDENT: NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Ident'ificati.on Report Generated 03-0CT-2016 05 :'48: 33. 66 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245013.CNF;l *
  • Acquisition date 3-0CT-2016 04:46:48 Sensitivity : 3.000 * *
  • Detector ID GAM19 Energy tolerance: 1. 500 *
  • Elapsed live 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.74 Half life ratio : ***** *
  • Sample date 15-DEC-2015 11:04:00 Nuclide Library : SOLID *
  • Sample ID R405245013 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : l.3610E+02 GRAM *
  • Quantity Err(%) : 1.4696E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION .INFORMATION *
  • Eff. Cal. date 15-JUN-2016 10:35:16 Eff. Geometry : CAN *.
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;l7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide* (pCi/GRAM (1. 96-sigma) (1.96-sigma) K-40 1. 362E+Ol 1.712E+OO 1. 712E+OO C0-58 2. llOE-01 9.618E-01 9.618E-01 CD-109 2.149E+OO 2.003E+OO 2.003E+OO TE-125M 4.644E+02 4.176E+02 4.176E+02 SN-126 1.384E-01 1. 288E-01 l.288E-01 BI-207 1.174E-01 l.508E-01 1.508E-01 TL-208 2.839E-01 l.115E-01 1.115E-Oi PB-210 5.038E+OO 6.326E+OO 6.326E+00 BI-212 6.507E-01 1.285E+OO l.285E+OO PB-212 1.184E+OO 1.505E-01 l.505E-01 BI-214 8.148E-01 1. 867E-01 1. 8 67E-01 PB-214 8.640E-01 1. 774E-01 1.774E-01 RN-222 8.148E-01 1.867E-01 l.867E-01 RA-224 4.899E-01 1.651E+OO 1.651E+OO RA-226 8.148E-01 1. 867E-01 1. 867E-01 AC-228 1.078E+OO 3.316E-01 3.316E-01 RA-228 1.078E+OO 3.316E-01 3.316E-01 TH-228 1.184E+OO 1.505E-01 l.505E-01 TH-230 8.145E-01 1. 867E-01 l.867E-01 PA-231 2.000E+OO 1.282E+OO l.282E+OO TH-232 1.078E+OO 3.316E-01 3.316E-01 U-234 8.145E-01 l.867E-01 1. 867E-01 AM-243 1.849E-01 l.052E-01 1.052E-01 ANH-511 8.292E-02 9 .. 4 OlE-02 9. 401E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1.96-sigma) (1.96-sigma) BE-7 -1.611E+OO 1.284E+Ol l.286E+Ol NOT IDENT. NA-22 -7.674E-03 3.141E-02* 3 .1°60E-02 NOT IDENT. NA-24 -l.OOOE+41 2.818E+41 O.OOOE+OO SHORT HLIF AL-26 -8.582E-03 2.214E-02 2.248E-02 NOT IDENT. SC-46 1.079E-01 3.422E-01 3.457E-01 FAIL ABUN V-48 -l.217E+04 1.225E+04 l.342E+04 SHORT HLIF Page 326 of 614 CR-51 3.290E+02 4.284E+02 4.534E+02 SHORT HLIF MN-54 3.093E-02 7.383E-02 7.513E-02 NOT IDENT. C0-56 2.480E-01 4.546E-01 4.681E-01 FAIL ABUN MN-56 1.000E+41 1.856E+41 0.000E+OO SHORT HLIF C0-57 3.473E-02 5.073E-02 5.309E-02 NOT IDENT. FE-59 -1.243E+OO 6. 901E+OO 6.924E+OO NOT IDENT. C0-60 -7.556E-03 4.086E-02 4.lOOE-02 NOT IDENT. ZN-65 -6.258E-02 1.868E-01 l.889E-01 NOT IDENT. GE-68 2.608E+OO 2.180E+OO 2.477E+OO NOT IDENT. AS-73 -6.535E-01 7.701E+OO 7.706E+OO NOT IDENT. AS-74 -2.933E+02 5.740E+03 5.741E+03 SHORT HLIF SE-75 -1..800E-01 2.210E-01 2.354E-01 NOT IDENT. BR-77 2.692E+37 2.275E+38 O.OOOE+OO SHORT HLIF SR-82 -8.498E+02 7.543E+02 8.460E+02 SHORT HLIF RB-83 -1.429E-01 7.187E-01 7.216E-01 FAIL ABUN KR-85 -1.549E+OO 8.898E+OO 8.925E+OO NOT IDENT. SR-85 -1.522E-01 8.726E-01 8.753E-01 NOT IDENT. RB-86 2.143E+04 l.984E+04 2.207E+04 SHORT HLIF Y-88 -1.167E-01 2.155E-01 2.218E-01 NOT IDENT. Y-91 -2. 761E+02 5.926E+02 6.055E+02 NOT IDENT. NB-94 -3.633E-03 3.142E-02 3.146E-02 NOT IDENT. NB-95 -2.993E-01 9.414E-01 9.510E-01 NOT IDENT. NB-95M -5.508E-01 2.462E+OO 2.475E+OO NOT IDENT. ZR-95 9.471E-01 1.706E+OO 1. 759E+OO NOT IDENT. NB-97 -1.000E+41 4.230E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 7.804E+40 0.000E+OO SHORT HLIF M0-99 -1.442E+31 2.978E+31 0.000E+OO SHORT HLI"F TC-99M 1. OO'OE+41 5.689E+42 O.OOOE+OO SHORT HLIF RH-101 6.494E-02 5.925E-02 6.609E-02 FAIL ABUN RH-102 -3.704E-02 7.082E-02 7.276E-02 NOT IDENT. RU-103 -1. 8 62E+OO 6.568E+OO 6.621E+OO FAIL ABUN RH-106 -1. 7 65E-01 5.726E-01 5.781E-01 NOT IDENT. RU-106 -1.765E-01 5.726E-01 5. 781E-01 NOT IDENT. AG-108M 2.374E-02 3.463E-02 3.624E-02 NOT IDENT. AG-110M -3.029E-02 l.129E-01 l .138E-01 NOT IDENT. SN-113 6.323E-02 2.296E-01 2. 313E-01 NOT IDENT. CD-115 -1. 788E+38 3.757E+38 O.OOOE+OO SHORT HLIF SN-117M -l.469E+04 7.461E+04 7.490E+04 SHORT HLIF TE-123M l.309E-02 1. 375E-01 1. 37 6E-01 NOT IDENT. SB-124 -3.819E-01 1. 773E+OO 1. 781E+OO NOT IDENT. SB-125 5.360E-02 l.153E-01 1.178E-01 FAIL ABUN I-126 3.901E+05 6.659E+05 6.888.E+05 SHORT HLIF SB-126 -7.610E+05 9.413E+05 1.002E+06 SHORT HLIF SB-127 -5.786E+21 1.026E+22 O.OOOE+OO SHORT HLIF I-131 -l.468E+09 3.322E+09 3.387E+09 SHORT HLIF I-132 l.000E+41 l.827E+42 O.OOOE+OO SHORT HLIF TE-132 -l.595E+25 8.904E+25 O.OOOE+OO SHORT HLIF BA-133 2.025E-02 5.028E-02 5.llOE-02 FAIL ABUN I-133 1. 000,E+41 3. 441E+41 O.OOOE+OO SHORT HLIF CS-134 6.477E-02 1.106E-01 l.144E-01 FAIL ABUN CS-135 -2.828E-02 1. 772E-01 1. 776E-01 NOT IDENT. I-135 1. OOOE+41 8.680E+41 O.OOOE+OO SHORT HLIF CS-136 -7.288E+04 2.526E+05 2.547E+05 SHORT HLIF BA-137M 1.127E-01 5.077E-02 7.181E-02 NOT IDENT. CS-137 1.190E-01 5.363E-02 7.586E-02 NOT IDENT. CE-139 -2.430E-03 l.210E-01 l.210E-01 NOT IDENT. BA-140 4.322E+05 l.053E+06 1.071E+06 SHORT HLIF LA-140 -1.188E+05 2.916E+05 2. 965E+05 SHORT HLIF CE-141 5.602E+OO 2.235E+Ol 2.249E+Ol NOT IDENT. CE-143 1. 000E+41 1.105E+41 O.OOOE+OO SHORT HLIF CE-144 -9.145E-02 3.862E-01 3.884E-01 NOT IDENT. PM-144 -1.497E-02 6.151E-02 6.188E-02 FAIL ABUN PR-144 -1. 263E+OO 5.328E+OO 5.358E+OO NOT IDENT. PM-146 6.939E-03 4.581E-02 4.591E-02 NOT IDENT. ND-147 1.854E+07 2.247E+07 2.398E+07 SHORT HLIF PM-147 ....:4. 029E+Ol 8.947E+02 8.949E+02 NOT IDENT. PM-149 2.012E+39 5. 966E+39 O.OOOE+OO SHORT HLIF EU-150 1. 774E-02 3. 271E-02 3.367E-02 FAIL ABUN EU-152 :..._2. 646E-02 1.070E-01 1.077E-01 'FAIL ABUN GD-153 6.049E-03 2.129E-01 2.129E-01 NOT IDENT. EU-154 -l.629E-02 7.811E-02 7.846E-02 NOT IDENT. EU-155 5.927E-02 l.335E-01 l.361E-01 FAIL ABUN TB-160 -7.928E-01 2.109E+OO 2.139E+OO FAIL ABUN H0-166M 2.147E-03 6. 533E--02 6.534E-02 FAIL ABUN TM-171 -3.765E+OO 2.082E+Ol 2.089E+Ol NOT IDENT. HF-172 2.343E-02 2.614E-01 2.616E-01 FAIL ABUN LU-172 1.259E-02 8.595E-02 8.614E-02 FAIL ABUN LU-176 -2. 969E-03 2.804E-02 2.807E-02 FAIL ABUN Page 327of614 HF-181 1.900E-02 4.525E+OO 4.525E+OO NOT IDENT. TA-182 6.860E-01 9.755E-01 1.023E+00 FAIL ABUN RE-183 1.865E+OO 2.899E+OO 3.018E+OO NOT IDENT. RE-184 1.937E+Ol 2.744E+Ol 2.880E+Ol NOT IDENT. W-188 -5.483E+Ol l.362E+02 1. 3.84E+02 NOT IDENT. IR-192 -1.690E-01 5.274E-01 5.329E-01 FAIL ABUN HG-203 -6.756E-01 2.524E+OO 2.543E+OO NOT IDENT. BI-211 2.380E+OO 4.901E-01 1.179E+OO FAIL ABUN PB....:211 1.088E-01 8.622E-01 8.636E-01 NOT IDENT. RN-219 1.717E-01 4.736E-01 4.799E-01 FAIL ABUN RA-223 ..:.5.957E-01 8. 051E-01 8.487E-01 FAIL ABUN AC-227 2.755E-01 2.525E-01 2.814E-01 NOT IDENT. TH-227 2.755E-01 2.525E-01 2.814E-01 NOT IDENT. TH-229 -4.613E-02 5.176E-01 5.180E-01 FAIL ABUN TH-231 -5.957E-01 8.051E-01 8.487E-01 FAIL ABUN PA-233 -6.571E-02 6.210E-02 6.880E-02 NOT IDENT. PA-234 * -2.264E-01 4.160E-01 4.283E-01 FAIL ABUN PA-234M l.319E+00 4.645E+OO 4.683E+OO NOT IDENT. TH-234 3.201E-01 1.418E+OO 1.425E+OO FAIL ABUN U-235 l.365E-01 2.027E-01 2 .119E-01 FAIL ABUN NP-237 -6.571E-02 6.210E-02 6.880E-02 NOT IDENT. NP-238 -3.009E+40 5.387E+40 O.OOOE+OO SHORT HLIF U-238 3.201E-01 1.418E+OO 1.425E+OO FAIL ABUN NP-239 -2.922E-01 2.441E-01 2.773E-01 NOT IDENT. PU-239 5.914E+02 5.295E+02 FAIL ABUN AM-241 6.989E-02 l.531E-01 1. 563E-01 NOT IDENT. CM-243 9.628E-02 l.144E-01 l.223E-01 NOT IDENT. BK-247 -4. 885E'-02 7.978E-02 8.277E-02 FAIL ABUN CM-247 2.083E-02 4.462E-02 4.559E-02 NOT IDENT. CF-249 3.145E-02 3.782E-02 4.039E-02 NOT IDENT. CF-251 l.150E-02 1.141E-01 1.142E-01 NOT IDENT. Page 328 of 614
                                                                                                                                                              • '* GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 68.5676 87.09 125.8018 136.47 85.0358 45.60 49.4184 87.57 129 .1195 140.51 0.0000 46.54 49.5206 88.03 119. 5168 143.76 77.0593 49.72 0.0000 88.34 117.9552 144.24 68.4363 51. 35 80.7268 88.47 117.9782 145.44 80.6674 51. 87 72.8457 89. 96 114.1860 152.43 80.3886 52.39 70.6440 1093.63 128.0801 153.25 0.0000 52. 97 61.6010 91.11 0.0000 323.87-87.5397 53.44 61.6593. 92.59 97.5488 156.02 0.0000 54.07 64.0237 93.35 97.6544 158.56 0.0000 57.36 0.0000 94.56 97.8223 159.00 78.2915 57.53 78.2714 94.65 79.8982 162.33 78.5531 57.98 61. 4421 94.67 79.9007 162.66 0.0000 59.27 81.6103 94.87 79.9231 163.33 79.5145 59.32 81. 6180 97.43 76.9349 165.86 69.0839 59.54 75.4893 98.43 78.6802 176.31 67. 0967 '60.96 100.7909 98.44 78.6816 17 6. 60 0.0000 61.17 100.8304 99.53 75.1051 177.52 61. 7992 62.93 101.1561 100 .11 88.7190 181.07 0.0000 63.29 101.2223 102.03 98.8330 181.52 80.9079 63.58 101. 27 54 103.18 70.5268 184.41 78.4189 64.28 101.4029 103.37 70.5446 143.76 67.6834 66.73 127.9882 105.21 74.4388 193.51 77.2448 67.24 99.9824 105.31 74.4484 '197. 03 76.5728 125.81 131.3278 106.12 96.0584 198.01 83.9375 67.75 123.5251 106.47 96 .1020 201.83 77.8069 69.67 110. 6002 109.28 74.8343 203.43 82.4973 70.83 122.6074 111. 00 81.6657 205.31 77.1205 72.81 116. 7060 111.76 0.0000 210.85 70.1019 72.87 116. 7180 114. 06 71.9431 215.65 72.2339 74.66 121.0176 116. 30 0.0000 222 .11 67.0283 74.82 121.0487 116.74 87.2909 227.09 57.9490 74.97 121. 0783 119.76 74.9770 227.38 60.7676 77 .11 121.4985 121.12 84.3821 228.16 0.0000 78.74 90.7632 121. 22 84.3923 228.18 60.8059 79.69 90.8994 121.78 74.3154 116.74 60.8059 80.12 90. 9609 122.06 74.3404 235.69 60.6938 80.19 0.0000 122.92 78.6452 I 235.96 62.1180 80.57 91. 024 7 123.07 76. 9673 238.63 52.8145 81. 00 91.0855 265.00 85.3181 238.98 0.0000 81. 07 91.0954 125.81 76.3687 240.99 52.9102 81. 75 107.1902 127.23 73.9454 242.00 52.9506 83.79 110.7352 127.91 88.4652 244.70 59.6912 84.00 110. 7710 129.30 85.6250 252.40 0.0000 85.43 72.3981 131.-20 78.1274 252.80 50.5210 86.55 72. 5198 133.02 92.4071 254.15 0.0000 86.79 117.6849 133.52 89.8915 256.23 43.0032 86.94 1.17. 7116 136. 00 82.4160 260.90 0.6000 Page 329 of 614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 60.5724 355.39 0.0000 584.27 19.3484 264.80 65.3866 356.01 35.1752 595.83 0.0000 265.00 57.7014 364.49 0.0000 427.87 34.3689 268.22 59. 28-03 366.42 0.0000 602.52 0.0000 269.46 63.6730 372. 51 48.3741 604. 72 20.6550 270.03 54.0472 375.05 41. 2280 607.14 20.6748 271.23 54.0928 377.52 41.2850 609.32 24 .1411 273.65 0.0000 356.01 35.2161 610.33 24.1505 276.40 59.1359 388.16 22.8406 614.28 17.2772 277.37 50.4448 388.63 0.0000 618.01 24.2240 277.60 50.4533 391.69 28.0854 620.36 17.3181 278.00 47.5555 264.66 40.7646 621.93 19.0620 279.20 56.3362 401. 81 39.7434 630.19 0.0000 279.54 64.1215 402.40 40.8027 631. 29 26.6667 279.70 64.1295 404.85 . 45.0462 633.25 22.0461 280.46 65.1353 410.95 42.0378 634.78 0.0000 283.69 51.6381 413.71 31. 5741 635.95 22.0685 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 55.6003 423.72 0.0000 645.85 20.9861 285.90 0.0000 427.09 27.5541 657.76 23.4220 287.50 48.8413 427.87 27.5647 657.90 0.0000 290.67 52.8618 433.94 31.*9037 661. 66 16.8885 293.27 0.0000 439.40 28.7919 664.57 0.0000 351. 93 51.5494 453.88 24.7028 666.33 0.0000 295. 96 51.5739 463.37 29.1324 666.50 0.0000 879.38 35.4265 468.07 32.4426 667.71 0.0000 299.98 26.5941 473.00 0.0000 677.62 23.0039 300.09 26.5963 475.06 27.1255 685.70 0.0000 300.13 26.5968 476.78 29.3192 695.00 0.0000 301.36 26.6182 477.60 29.3307 696. 49 23.1610 302.85 26.6440 482.18 29.3939 696. 51 23.1610 256.23 26.6726 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.8210 306.78 40.0682 497.08 37.2698 697.49 16.0400 308.46 35.6543 505.52 31.3615 702. 65 19.6407 311. 90 48.6371 507.63 .0.0000 706.68 23.2443 316.51 55.7471 511. 00 27.5777 711. 68 23.2856 319.41 0.0000 514.00 31. 4803 720.70 0.0000 320.08 0.0000 514.00 31. 4803 721. 93 0.0000 -321. 04 41.9299 520.40 27.6937 722.78 18.7008 323.87 60.0049 520.69 0.0000 722.91 18.7015 325.23 43.5407 522.65 0.0000 723.31 18.7040 328.76 0.0000 527.90 0.0000 724.19 20.1489 333.37 49.7941 528.26 22.2314 727.33 22.5121 333.97 42.2649 529.59 24.4689 733.00 17.3232 334.37 39.2555 529.87 0.0000 735.93 11. 7412 338.28 55.4912 531. 02 0.0000 333.97 19.8798 338.32 55.4935 537.26 0.0000 739.50 0.0000 311. 90 42.4315 546.56 0.0000 747.24 11. 7864 340.48 42.4315 552.55 21. 9034 748.06 11. 7896 340.55 0.0000 563.25 40.6187 752.31 23.6125 344.28 45.5658 569.33 23.7549 753.82 0.0000 345.93 40.5428 946.00 23.7566 756.73 21. 8291 351.06 41.6823 569.70 23.7583 756.80 19.1005 351. 93 41.7032 583.19 19.3394 884.68 20.0583 Page 330of614
  • ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 28.2811 1274.44 11.7301 1620.50 3.3697 766.42 22.8119 1001.03 10.7667 1621. 92 3.3706 766.84 18.2520 1002.74 9.7922 1678.03 0.0000 772.60 0.0000 1004.73 17.6358 1690.97 4.5510 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 4.6104 778.90 12.2164 1028.54 0.0000 1063.66 0.0000 783.70 0.0000 1037.84 12.8500 1771. 35 0.9231 785.37 8.8146 1038.76 0.0000 1791.20 0.0000 792.07 11.7785 631.29 14.8608 1808.65 2.7872 794.95 19.3421 1048.07 0.0000 1810.72 0.0000 795.86 19.3472 1049.04 14.8700 1836.06 5.6001 810.06 14.8081 1050.41 9.9170 810.29 14.8091 1063.66 17.9121 344.28 14.8101 1077.00 0.0000 810.76 14.8115 1077.34 4.9930 815.77 0.0000 1085.87 12.0095 1048.07 0.0000 1093.63 14.0385 832.01 25.1625 1099.45 16.0684 834.85 18.6554 1112. 07 15.1117 835.71 25.1914 1112.84 11. 0839 836.80 0.0000 1115. 54 12.9063 846.75 0.0000 1120. 29 18.1703 846.77 12.1704 1120.55 18.1714 856.80 0.0000 1221. 41 18.1758 860.56 11.2819 1129. 67 10 .1184 871.09 19.8061 1131.51 0.0000 873.19 16.9876 1147.95 0.0000 875.33 0.0000 1173.23 10.2258 879.38 21.7464 1177.95 11.2612 880.51 20.8083 1189.05 9.5800 883.24 12.3057 1204.77. 20.6055 884.68 18.9398 1221.41 11.3766 889.28 10.4313 1231.02 13.2680 894.76 14.2474 1235.36 0.0000 898.04 17.1134 1238.28 12.4592 900. 72 19.9817 1260.41 0.0000 903.28 8.8873 1271. 87 5.2313 911.20 13.3617 1274.44 5.2344 912.08 13.3651 1274.54 5.2344 923.98 0.0000 1291.59 7.3559 926.50 15.3384 1298.22 0.0000 929 .11 15.3501 1312 .11 0.0000 937.49 24.0417 1332. 49 9.5427 944 .13 0.0000 1362.66 0.0000 946.00 16.9662 1365.19 6.4069 949.00 7. 7185 1368.63 0.0000 667.71 0.0000 1384.29 11.7929 962. 31 23.2419 1408.01 5.3873 964.08 15.5024 1457.56 0.0000 966 .17 24.8180 1460.82 5.4456 911.20 22.3149 1489.16 3.2858 968.97 22.3149 1505.03 1. 0988 983.53 0.0000 1584.12 13.3872 984.45 0.0000 1596.21 0.0000 Page 331of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:49:12.16 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245014.CNF;l Background file DKAl.00: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM20.CNF;515 Background date : Z-OCT-2016 11:01:13. Sample date 15-DEC-2015 11:08:00 Acquisition date : 04:47:25. Sample ID R405245014 Sample quantity : 1.54135E+02 GRAM Detector name : GAM20 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:15.40 0.4% Energy tolerance 1. 50000 keV Analyst Initials. MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596387 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It ,1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 3 3 3 3 0 0 0 0 2 2 6 6 6 6 0 0 0 0 4 4 0 0 0 0 0 2 2 0 0 0 0 0 0 0 Page 332of614 Energy 26.73* 28.06* 30.06* 31.78* 42.92 46.97* 57.93 63.98* 74.93 77.14 84.14* 87.26 90.01* 92.91* 151.08 170.22 186.05* 209.04 238.59* 241.53 270.35 295.21* 300.61 329.31 338.97* 351. 81* 354.77* 462.75 490.71 510.66* 541.32 583.02* .609.47* 662.09* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 16 30 34 19 33 38 36 40 196 246 78 116 71 117 44 13 47 41 404 91 41 148 14 61 82 265 15 41 10 55 15 149 182 60 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 6 17 36 55 62 142 88 227 179 141 181 159 108 124 69 99 171 97 57 71 60 86 62 81 89 20 17 25 27 41 23 25 27 25 1. 36 1. 37 1. 37 1. 38 1.34 1. 55 1. 29 1. 04 L22 0.95 1. 98 1. 30 0.97 1. 37 1. 27 0.92 1. 01 1.13 1.13 1. 39 1. 72 1. 26 1. 46 0.86 1.18 1. 24 1. 71 1. 50 0.87 2.08 0. 96 1. 50 1. 31 1. 41 53.68 56.32 60.32 63.75 86.02 94.12 116. 02 128.12 150.00 154.42 168.39 174.65 180.13 185.94 302.20 340.46 372.10 418.05 477.13 483 .. 01 540.63 590.32 601.12 658.51 677.82 703.48 709.41 925.34 981.25 1021.15 1082.48 1165. 87 1218.78 1324.05 51 51 51 51 84 90 113 123 146 146 164 164 164 164 299 334 366 414 472 472 536 586 596 652 671 698 698 921 976 1013 1079 1158 1213 1318 22 4.54E-03 70.5 3.85E+OO 22 8.29E-03 51.9 22 9.54E-03 47.1 22 5.17E-03 87.2 5 9.06E-03 40.5 10 1. 07E-02 61. 6 7 9.91E-03 46.7 10 1.12E-02 73.3 14 5.46E-02 13.1 1.66E+OO 14 6.83E-02 10.l 28 2.17E-02 30.1 l.74E+00 28 3.22E-02 20.5 28 1.97E-02 26.6 28 3.24E-02 21.4 7 1.24E-02 34.3 8 3.55E-03139.9 12 1.31E-02 59.2 9 1.14E-02 46.0 15 1.12E-01 6.0 1.28E+OO 15 2.52E-02 19.6 8 1.13E-02 36.9 10 4.llE-02 14.6 8 3.76E-03104.4 14 1. 68E-02 34. 5 14 2.29E-02 27.4 15 7;37E-02 6.8 2.36E+OO 15 4.16E-03 77.7 9 1.14E-02 26.9 8 2.70E-03 97.2 15 1.54E-02 33.2 8 4.19E-03 60.0 14 4.15E-02 10.9 14 5.06E-02 9.8 10 1. 68E-02 20. 5 Peak Search Report (continued) Page : 2 Sample ID : R405245014 Acquisition date : 3-0CT-2016 04:47:25 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 727. 66 31 38 2.03 1455.23 1446 15 8.47E-03 47.4 36 0 732.73 10 18 0.80 1465.37 1461 7 2.64E-03 79.9 37 0 768.15 24 33 1. 30 1536. 24 1529 12 6. 69E-03 51. 9 38 0 787.21 21 14 1.63 1574.37 1568 12 5.87E-03 42.4 39 0 794.42 41 18 3.39 1588.81 1580 18 1.14E-02 28.8 40 0 862.45 13 30 1.47 1724.95 1717 14 3.60E-03 99.3 41 0 889.92 8 5 2.97 1779.90 1772 10 2.16E-03 65.0 42 0 911.40* 72 22 1. 37 1822. 90 1817 11 1.99E-02 17.6 43 0 924.18 5 12 3.57 1848.48 1841 9 l.52E-03132.4 44 1 965. 06 43 5 1. 94 1930. 30 1921 27 1.20E-02 16.1 1.65E+OO 45 1 969. 09 82 2 1.88 1938.35 1921 27 2.27E-02 11.2 46 0 1001.50* 20 6. 2.18 2003.24 1998 12 5.66E-03 34.4 47 0 1057.29 12 5 1.17 2114.90 2111 7 3.30E-03 43.1 48 0 1120.58 50 3 1. 65 2241. 62 2236 12 l.39E-02 15.8 49 4 1155. 74 20 11 1. 85 2312. 00 2306 16 5.44E-03 40.0 2.42E+00 50 4 1158. 68 13 8. 2.26 2317.89 2306 16 3.56E-03 45.5 51 0 1164.73 15 12 4.40 2330.00 2323 12 4.17E-03 52.9 52 0 1238.30 16 5 1.45 2477.30 2475 6 4.47E-03 32.7 53 0 1281.08 10 14 . L24 2562.98 2557 11 2.82E-03 77.5 54 0 1316.37* 4 5 0.92 2633.64 2626 10 1.08E-03131.8 55 0 1353 .'87 8 11 0.59 2708.75 2701 9* 2.14E-03 86.3 56 0 1377.43 11 7 3.03 2755.92 2751 9 3.17E-03 50.5 57 0 1460.95* 393 15 1.99 2923.21 2916 15 1.09E-01 5.5 58 0 1568.64 4 7 0.83 3138.95 3131 9 1.19E-03119.8 59 0 1588.36 9 2 0,63 3178.46 3174 8 2.51E-03 42.8 60 0 1764.80 34 . 2 1. 90 3532. 02 3527 11 9.33E-03 19.6 Flag: "*" = Peak area was modified by background subtraction Page 333of614 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 05:49:14 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245014.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID *15-DEC-2015 11:08:00 R405245014 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 04:47:25 154.13 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA20 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Page 334of614 Nuclide PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 TH-229 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 88.47 74.66 74.82 74.82 351.06 CAN 0 01:00:15.40 10.00 0.00 % Peak Energy 0.4%

Nuclide Line Activity Report Page : 2 Sample ID : R405245014 Acquisition date 3-0CT-2016 04:47:25 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.312E+OO l.325E+Ol l.325E+Ol 11. 03 OK SC-46 889.28 99.98* l.959E+OO 1. 97 6E-02 2.226E-01 129.99 OK 1120.55 99.99 l.635E+OO 1.481E-01 l.669E+OO 31. 57 OK CD-109 88.03 3.70* 6.845E+OO l.984E+OO 3.079E+OO 60.60 OK SN-126 64.28 9.60 4.873E+OO 5.550E-01 5.550E-01 146.68 OK 86.94 8.90 6.845E+OO 8.247E-01 8.247E-01 60.60 OK 87.57 37.00* 6.845E+OO l.984E-01 l.984E-01 60.60 OK BA-137M 661. 66 89.90* 2.463E+OO l.404E-01 l.430E-01 40.97 OK CS-137 661. 66 85.10* 2.463E+OO l.483E-01 1. 511E-01 40.97 OK TL-208 277.37 6.60 4.947E+OO Line Not Found Absent 583.19 85.00* 2.720E+OO 3.366E-01 3.366E-01 21. 88 OK 860.56 12.50 2. OllE+OO Line Not Found Absent PB-210 46.54 4.25* 2.044E+OO 2.917E+OO 2.991E+OO 123.18 OK BI-211 72.87 1. 23 5.823E+OO Line Not Found Absent 351.06 12.92* 4.084E+OO l.344E-01 l.344E-01 634. 96 OK PB-212 74.82 10.28 6.006E+OO l.478E+OO l.478E+OO 37. 22' OK 77 .11 17.10 6.187E+OO l.469E+OO l.469E+OO 20.12 OK 238.63 43.60* 5.553E+OO 9.503E-01 9.503E-01 12.01 OK 300.09 3.30 4.640E+OO 4:932E-01 4.932E-01 208.80 OK BI-214 609.32 45.49* 2.627E+OO 7.914E-01 7.917E-01 19.52 OK 1120.29 14.92 l.635E+OO 9.926E-01 9.930E-01 31. 57 OK 1764.49 15.30 l.106E+OO 9.146E-01 9.149E-01 39.29 OK PB-214 74.82 5.80 5. 996E+OO Line Not Found <<INT Reject 77.11 9.70 6.187E+OO 2.590E+OO 2.591E+OO 20.12 OK 87.09 3.41 6.836E+OO Line Not Found <<INT Reject 242.00 7.25 5.495E+OO Line Not Found <<INT Reject 295.22 18.42 4.708E+OO 9.522E-01 9.525E-01 29.20 OK 351.93 35.60* 4.083E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.627E+OO 7.914E-01 7.917E-01 19.52 OK 1120.29 14.92 l.635E+OO 9.926E-01 9.930E-01 31. 57 OK 1764.49 15.30 l.106E+OO 9.146E-01 9.149E-01 39.29 OK RA-224 240.99 4.10* 5.503E+OO 6.082E-01 6.082E-01 168.44 OK RA-226 609.32 45.49* 2.627E+OO 7.914E-01 7.917E-01 19.52 OK 1120.29 14.92 l.635E+OO 9.926E-01 9.930E-01. 31.57 OK 1764.49 15.30 l.106E+OO 9.146E-01 9.149E-01 39.29 OK AC-228 105.21 1.10 7.453E+OO Line Not Found Absent 338.32 11. 27 4.210E+OO 9.554E-01 9.554E-01 54.85 OK 794.95 4.25 2.139E+OO 2.280E+OO 2.280E+OO 57.58 OK 835.71 1. 61 2.057E+OO Line Not Found Absent 911. 20 25.80* l.923E+OO 7 .181E-01 7.181E-01 35.17 OK 968.97 15.80 l.834E+OO l.394E+OO l.394E+OO 22.34 OK RA-228 105.21 1.10 7.453E+OO Line Not Found Absent 338.32 11. 27 4.210E+OO 9.554E-01 9.554E-01 54.85 OK 794.95 4.25 2.139E+OO 2.280E+OO 2.280E+OO 57.58 OK 835.71 1. 61 2.057E+OO Line Not Found Absent 911.20 25.80* l.923E+OO 7.181E-01 7.181E-Ol 35.17 OK 968. 97 15.80 l.834E+OO l.394E+OO l.394E+OO 22.34 OK TH-228 74.82 10.28 6.006E+OO l.478E+OO 1. 4 78E+OO 37.22 OK 77 .11 17.10 6.187E+OO l.469E+OO l.469E+OO 20.12 OK Page 335of614.

Nuclide Line Activity Report (continued) Page : 3 Sample ID : R405245014 Acquisition date 3-0CT-2016 04:47:25 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status 238.63 43.60* 5.553E+OO 9.503E-01 9.503E-01 12.01 OK 300.09 3.30 4.640E+OO 4.932E-01 4.932E-01 208.80 OK TH-229 85.43 14.70 6.670E+OO 5.003E-01 5.004E-01 60.20 OK 88.47 24.00 6.845E+OO 3.058E-01 3.058E-01 60.60 OK 193.51 4.41* 6.409E+OO Line Not Found Absent 210.85 2.80 6.063E+OO Line Not Found Absent TH-230 609.32 45.49* 2.627E+OO 7.914E-01 7. 914E-.Ol 19.52 OK 1120.29 14.92 1.635E+OO 9.927E-01 9.927E-01 31. 57 OK 1764.49 15.30 1.106E+OO 9.146E-01 9.146E-01 39.29 OK PA-231 283.69 1. 70 4.860E+OO Line Not Found Absent 301.36 5.35* 4.640E+00 3.042E-01 3.042E-01 208.80 OK TH-232 105.21 1.10 7.453E+OO Line Not Found Absent 338.32 11. 27 4.210E+OO 9.554E-01 9.554E-01 54.85 OK 835. 71 1. 61 2.057E+OO Line Not Found Absent 911.20 25.80* 1.923E+OO 7 .181E-01 7.181E-01 35.17 OK 968. 97 15.80 1.834E+OO 1.394E+OO 1.394E+OO 22.34 OK TH-234 63.29 3.70* 4.873E+OO 1.440E+OO 1.440E+OO 146.68 OK 92.59 4.23 7.105E+OO 2. 411E+OO 2. 411E+OO 42.70 OK U-234 609.32 45.49* 2.627E+OO 7.914E-01 7.914E-01 19.52 OK 1120. 29 14.92 1.635E+OO 9.927E-01 9.927E-01 31. 57 OK 1764.49 15.30 1.106E+00 9.146E-01 9.146E-01 39.29 OK U-235 89. 96 3.47 6.980E+OO 1.823E+OO 1.823E+OO 53.22 OK 93.35 5.60 7.105E+OO 1.821E+OO 1. 821E+OO 42.70 OK 143.76 10. 96* 7.370E+OO Line Not Found Absent 163.33 5.08 7.024E+OO Line Not Found Absent 185.72 57.20 6.562E+OO 7.333E-02 7.333E-02 118. 40 OK 205.31 5.01 6.171E+OO Line Not Found Absent U-238 63.29 3. 70.* 4.873E+OO 1.440E+OO 1.440E+OO 146.68 OK 92.59 4.23 7.105E+OO 2. 411E+OO 2. 411E+OO 42.70 OK AM-243 43.53 5. 90 . 1.188E+OO 3. 091E+OO 3. 091E+OO 81. 01 OK 74.66 67.20* 6.006E+OO 2. 261E-01 2.261E-01 37.22 OK ANH-511 511. 00 100.00* 3. 021E+OO 9.698E-02 9.698E-02 66.34 OK Flag: "*" = Keyline Page 336 of 614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:49:15.33 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* I * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245014.CNF;l *
  • Acquisition date 3-0CT-2016 04:47:25 Sensitivity : 3.000 *
  • Detector ID GAM20 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real 0 01:00:15.40 Half life ratio : ***** *
  • Sample date 15-DEC-2015 11:08:00 Analyst initials: MXRl *
  • Sample ID R405245014 Sample Quantity 1.5413E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN. *
  • Eff. File : D'KAlOO: [CANBERRA. GAMMA] EFF GAM20 CAN. CNF; 15
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.325E+Ol 1.432E+OO SC-46 2.226E-01 2.835E-01 CD-109 3.079E+OO 1. 829E+OO SN-126 1.984E-01 l.178E-01 BA-137M 1.430E-01 5. 741E-02 CS-137 1. 511E-01 6. 065E-02 TL-208 3.366E-01 7.218E-02 PB-210 2.991E+OO 3.610E+OO BI-211 1.344E-01 8.360E-01 PB-212 9.503E-01 1.118E-01 BI-214 7.917E-01 l.515E-01 PB-214 1.00lE+OO l.336E-01 RN-222 7.917E-01 1.515E-01 RA-224 6.082E-01 1.004E+OO RA-226 7.917E-01 1.515E-01 AC-228 7.181E-01 2.475E-01 RA-228 7.181E-01 2.475E-01 TH-228 9.503E-01 1.118E-01 TH-229 -2.266E-01 3.844E-01 TH-230 7.914E-01 1.514E-01 PA-231 3.042E-01 6.225E-01 TH-232-7.181E-01 2.475E-01 TH-234 1.440E+OO 2.070E+OO U-234 7.914E-01 l.514E-01 U-235 -5.5Cl6E-02 1.582E-01 U-238 l.440E+00 2.070E+OO AM-243 2.261E-01 8.248E-02 ANH-511 9.698E-02 6.305E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 Page 337of614 Key-Line Activity (pCi/GRAM -3.933E+OO l.832E-02 K.L. Cnt Oncert (1. 96-sigma) 8.818E+OO 4.201E-02 MDA (pCi/GRAM 5.809E-01 5.059E-01 1.526E+OO 9.864E-02 4.931E-02 5.209E-02 5.217E-02 2.560E+OO 2.944E-01 7.261E-02 9.175E-02 2.815E-01 9.175E-02 7.782E-01 9.175E-02 1.691E-01 1.691E-01 7.261E-02 7.315E-01 9.172E-02 7.122E-01 l.691E-01 1. 569E+OO 9.172E-02 2.813E-01 1.569E+OO 6.946E-02 4.128E-02 MDA (pCi/GRAM 1.621E+Ol 8.486E-02 NOT IDENT. NOT IDENT.

NA-24 O.OOOE+OO 1. 67 5E+41 O.OOOE+OO SHORT HLIF AL-26 -2.120E-02 2.528E-02 3.878E-02 NOT IDENT. V-48 O.OOOE+OO 8.674E+03 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 2. 831E+02 O.OOOE+OO SHORT HLIF MN-54 2.880E-02 5.104E-02 l.062E-01 NOT IDENT. C0-56 2.136E-02 3.547E-01 6.880E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -4 .. 406E-03 3.819E-02 6.973E-02 NOT IDENT. C0-58 -4.540E-01. 5.000E-01 8.002E-01 NOT IDENT. FE-59 2.053E+OO 5.198E+OO 1.lOlE+Ol NOT IDENT. C0-60 -8.137E-03 3.818E-02 7.322E-02 NOT IDENT. ZN-65 l.280E-01 1.474E-01 3.092E-01 NOT IDENT. GE-68 8.738E-01 1. 739E+OO 3.837E+OO NOT IDENT. AS-73 -3.753E-01 4.442Et00 8.482E+OO NOT IDENT. AS-74 O.OOOE+OO 3.081Et03 O.OOOE+OO SHORT HLIF SE-75 -1. llOE-01 l.588E-01 2.941E-01 NOT IDENT. BR-77 O.OOOE+OO 2.541E+36 O.OOOE+OO SHORT HLIF SR-82 0.000E+.00 4.717E+02 O.OOOE+OO SHORT HLIF RB-83 2.903E-01 5. OllE-01 1. 047E+OO NOT IbENT. KR-85 6.028E+OO 5.855E+OO 1.185E+Ol NOT IDENT. SR-85 5.900E-01 5.741E-01 1.162E+OO NOT IDENT. RB-86 O.OOOE+OO 1.655E+04 O.OOOE+OO SHORT HLIF Y-88 4.607E-02 l.157E-01 3.135E-01 NOT IDENT. Y-91 '--7. 005E+Ol 4.233E+02 8.185E+02 NOT IDENT. NB-94 8.724E-04 2.889E-02 5.477E-02 NOT IDENT. NB-95 l.549E-01 7.443E-01 1.307E+OO NOT IDENT. NB-95M -6 .112E-01 1. 747E+00 2.997E+OO NOT IDENT. ZR-95 1.130E+OO 2.195E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 96.0E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.939E+41 O.OOOE+OO SHORT HLIF . M0-99 O.OOOE+OO 2.318E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 3.548E-03 3 .135E-02 5.766E-02 NOT IDENT. RH-102 -8.877E-03 4.126E-02 7. 831E-02 FAIL ABUN RU-103 -2.973E-01 3.454E+00 6.768E+OO FAIL ABUN RH-106 1.981E-01 3.763E-01 7.907E-01 NOT IDENT. RU-106 1. 981E-01 3.763E-01 7.907E-01 NOT IDENT. AG-108M 8.354E-03 2.083E-02 4. 301E-02 NOT IDENT. AG-llOM -9:344E-02 1.000E-01 l.277E-01 NOT IDENT. SN-113 -9.822E-02 1. 793E-01 3.287E-01 NOT IDENT. CD-115 O.OOOE+OO 3.040E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 5.497E+04 O.OOOE+OO SHORT HLIF TE-123M 2.892E-03 1.075E-01 1.956E-01 NOT IDENT. SB-124 2.321E-01 1.540E+OO 3.407E+OO NOT IDENT. SB-125 -4.652E-02 8.540E-02 l.556E-01 FAIL ABUN TE-125M l.127E+02 2.253E+02 4.307E+02 NOT IDENT. I-126 O.OOOE+OO 5.847E+05 O.OOOE+OO SHORT HLIF SB-126-O.OOOE+OO 6.854E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 5.325E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.282E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 6.968E+25 O.OOOE+OO SHORT HLIF BA-133 3.444E-02 5.244E-02 6.603E-02 FAIL"ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 8.368E-02 1.038E-01 FAIL'ABUN CS-135 7.581E-02 1.268E-01 2.389E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO l.674E+05 O.OOOE+OO SHORT HLIF CE-139 6.095E-03 1.009E-01 1.688E-01 NOT IDENT. BA-140 O.OOOE+OO 8 ._201E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.182E+05 O.OOOE+OO SHORT HLIF CE-141 *-5. 901E+OO 1.759E+Ol 3 .121E+Ol NOT IDENT. CE-143 O.OOOE+OO 5.877E+40 O.OOOE+OO SHORT HLIF CE-144 -2.462E-02 3.056E-01 5.548E-01 NOT IDENT. PM-144 4.lOOE-03 4.712E-02 9.079E-02 NOT IDENT. PR-144 3.800E-Ol 4.082E+OO 7.870E+OO NOT IDENT. PM-146 -2.816E-03 3.722E-02 7.154E-02 NOT IDENT. ND-147 O.OOOE+OO 1. 800E+07 O.OOOE+OO SHORT HLIF PM-147 2.628E+02 6.577E+02 l.258E+03 NOT" IDENT. PM-149 O.OOOE+OO 4.122E+39 O.OOOE+OO SHORT HLIF EU-150 1.305E-02 2.442E-02 3.877E-02 FAIL ABUN EU-152 9.722E-04 7.590E-02 1. 349E-01 FAIL ABUN GD-153 -1.173E-01 1.602E-01 2.554E-01 NOT IDENT. EU-154 4.801E-02 9.895E.:.02 2.084E-01 NOT IDENT. EU-155 -7.910E-03 9.470E-02 1. 737E-01 FAIL ABUN TB-160 6.049E-02 1.625E+OO 3.083E+OO FAIL ABUN H0-166M 2.627E-02 4.858E-02 9.978E-02 NOT IDENT. TM-171 4.654E+OO 1.143E+Ol 2.260E+Ol NOT IDENT. Page 338of614 HF-172 -1.600E-02 2.042E-01 3.712E-01 FAIL ABUN LU-172 2.362E-02 5.394E-02 1.193E-01 FAIL ABUN LU-176 -7.322E-03 l.973E-02 3.740E-02 FAIL ABUN HF-181 3.012E+OO 5.569E+OO FAIL ABUN TA-182 8.490E-02 8.367E-01 1.658E+OO FAIL ABUN RE-183 3.022E+OO 2.765E+OO 3.317E+OO FAIL ABUN RE-184 -2.013E+Ol 2.363E+Ol 3.765E+Ol NOT IDENT. W-188 -l.063E+02 9.535E+Ol l.443E+02 FAIL ABUN IR-192 -1.279E-01 3.214E-01 6.094E-01 FAIL ABUN HG-203 7.390E-01 -1.809E+OO 3.666E+OO NOT IDENT. BI-207 -l.803E-04 3.745E-02 7.616E-02 FAIL ABUN PB-211 3.833E-01 5.032E-01 l.072E+OO NOT IDENT. BI-212 1.017E+OO 9. 441E-01 1.139E+OO FAIL'ABUN RN-219 -l.313E-Ol 2.956E-01 5.488E-01 FAIL ABUN RA-223 l.331E-01 5.032E-01 9.211E-01 FAIL ABUN AC-227 -1.080E-01 1.824E-01 3.419E-01 FAIL ABUN TH-227 -1.080E-01 1.824E-01 3.419E-01 FAIL ABUN TH-231 1. 331E-01 5.032E-01 9.211E-01 FAIL ABUN PA-233 8.258E-03 4.608E-02 9.245E-02 FAIL ABUN PA-234 -1.137E-01 2.307E-01 4.344E-01 FAIL ABUN PA-234M 6.675E+OO 4.501E+OO 8.495E+OO FAIL ABUN NP-237 8.258E-03 4.608E-02 9.245E-02 FAIL ABUN -..l NP-238 O.OOOE+OO 3.223E+40 O.OOOE+OO SHORT HLIF NP-239 -3.309E-03 2.008E-01 3.701E-01 NOT IDENT. PU-239 -1.032E+02 2.974E+02 S.263E+02 NOT IDENT. AM-241 -3.443E-02 1. 058E-01 1.567E-01 NOT IDENT. CM-243 -1.479E-02 8. llOE-02 l.482E-01 NOT IDENT. BK-247 -5.213E-02 6.318E-02 1. 091E-01 FAIL ABUN CM-247 -l.954E-02 2.707E-02 4.844E-02 NOT IDENT. CF-249 1.460E-02 3.114E-02 6.361E-02 NOT IDENT. CF-251 -1.569E-02 8.892E-02 1. 757E-01 NOT IDENT. Page 339 of 614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:49:12.92 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 380 10.66* l.312E+OO 1.325E+Ol 1.325E+Ol 11. 03 SC-46 889.28 8 99.98* l.959E+00 1.976E-02 2.226E-01 129.99 1120. 55 50 99.99 1.635E+OO l.481E-01 1.669E+OO 31. 57 CD-109 88.03 149 3.70* 6.845E+OO 2.861E+OO 4.442E+OO 41. 05 SN-126 64.28 53 9.60 4.873E+00 5.550E-01 5 .*550E-01 146.68 86. 94 149 8.90 6.845E+OO l.190E+OO l.190E+OO . 41. 05 87.57 149 37.00* 6.845E+OO 2.861E-01 2.861E-01 41. 05 BA-137M 661.66 64 89.90* 2.463E+OO 1.404E-01 l.430E-01 40.97 CS-137 661.66 64 85.10* 2.463E+OO l.483E-01 1. 511E-01 40.97 TL-208 277.37 ------6.60 4.947E+OO ------Line Not Found ------583.19 160 85.00* 2.720E+OO 3.366E-01 3.366E-01 21. 88 860.56 ------12.50 2. OllE+OO ------Line Not Found ------PB-210 46.54 52 4.25* 2.044E+OO 2.917E+00 2.991E+OO 123.18 BI-211 72. 87 ------1. 23 5.823E+OO ------Line Not Found ------351.06 299 12.92* 4.084E+OO 2.758E+OO 2.758E+OO 13.62 PB-212 74.82 255 10.28 6.006E+OO 2.015E+OO 2.015E+OO 26.17 77 .11 319 17.10 6.187E+OO l.469E+00 1.469E+OO 20.12 238.63 472 43.60* 5.553E+OO 9.503E-01 9.503E-01 12.01 300.09 16 3.30 4.640E+OO 4.932E-01 4.932E-01 208.80 BI-214 609.32 194 45.49* 2.627E+00 7.914E-01 7.917E-01 19.52 1120.29 50 14.92 1.635E+OO 9.926E-01 9.930E-01 31. 57 1764.49 32 15.30 1.106E+OO 9.146E-01 9.149E-01 39.29 PB-214 74.82 255 5. 80 6.006E+OO 3.572E+OO 3.573E+OO 26 .17 77 .11 319 9.70 6.187E+OO 2.590E+OO 2: 591E+OO 20.12 87.09 149 3.41 6.845E+OO 3.105E+OO 3.106E+OO 41. 05 242.00 106 7.25 5.503E+OO 1. 296E+OO 1.297E+OO 39.22 295.22 170 18.42 4.708E+OO 9.522E-01 9.525E-01 29.20 351. 93 299 35.60* 4.084E+OO 1.00lE+OO l.OOlE+OO 13.62 RN-222 609.32 194 45.49* 2.627E+OO 7.914E-01 7.917E-01 19.52 1120.29 50 14.92 l.635E+OO 9.926E-01 9.930E-01 31. 57 1764.49 32 15.30 1.106E+OO 9.146E-01 9.149E-01 39.29 RA-224 240.99 106 4.10* 5.503E+OO 2.292E+OO 2.292E+00 39.22 RA-226 609.32 194 45.49* 2.627E+OO 7.914E-01 7.917E-01 19.52 1120.29 50 14.92 1.635E+OO 9.926E-01 9.930E-01 31. 57 1764.49 '32 15.30 1.106E+OO 9.146E-01 9.149E-01 39.29 AC-228 105.21 ------1.10 7.453E+OO ------Line Not Found ------338.32 93 11. 27 4.210E+00 9.554E-01 9.554E-01 54.85 794.95 43 4.25 2.139E+OO 2.280E+OO 2.280E+OO 57.58 835. 71 ------1. 61 2.057E+OO ------Line Not Found ------911.20 73 25.80* 1.923E+OO 7 .181E-01 7 .181E-01 35.17 968.97 83 15.80 l.834E+00 1.394E+OO 1.394E+OO 22.34 RA-228 105.21 ------1.10 7.453E+OO ------Line Not Found ------338.32 93 11. 27 4.210E+OO 9.554E-01 9.554E-01 54.85 794.95 43 4.25 2.139E+OO 2.280E+OO 2.280E+00 57.58 835.71 ------1. 61 2.057E+OO ------Line Not Found ------911. 20 73 25.80* 1.923E+OO 7 .181E-01 7.181E-01 35.17 968.97 83 15.80 1.834E+OO 1.394E+OO l.394E+00 22.34 Page 340of614 Nuclide Line Activity Report (continued) Page : 2 Sample ID : R405245014 Acquisition date 3-0CT-2016 04:47:25 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error TH-228 74.82 255 10.28 6.006E+OO 2.015E+OO 2.015E+OO 26.17 77 .11 319 17.10 6.187E+OO 1. 469E+OO l.469E+OO 20.12 238.63 472 43.60* 5.553E+OO 9.503E-01 9.503E-01 12.01 300.09 16 3.30 4.640E+OO 4.932E-01 4.932E-01 208.80 TH-229 85.43 101 14.70 6.670E+OO 5.003E-01 5.004E-01 60.20 88.47 149 24.00 6.845E+OO 4. 411E-01 4. 411E-01 41. 05 193.51 ------4.41* 6.409E+OO ------Line Not Found ------210.85 ------2.80 6.063E+OO ------Line Not Found ------TH-230 609.32 194 45.49* 2.627E+OO 7.914E-01 7.914E-01 19.52 1120.29 50 14.92 1.635E+OO 9.927E-01 9.927E-01 31. 57 1764.49 32 15.30 1.106E+OO 9.146E-01 9.146E-01 39.29 PA-231 283.69 ------1. 70 4.860E+OO ------Line Not Found ------301.36 16 5.35* 4.640E+OO 3.042E-01 3.042E-01 208.80 TH-232 105.21 ------1.10 7.453E+OO ------Line Not Found ------338.32 93 11. 27 4.210E+OO 9.554E-01 9.554E-01 54.85 835. 71 ------1. 61 2.057E+OO ------Line Not Found. ------911. 20 73 25.80* 1.923E+OO 7.181E-01 7 .181E-0.l 35.17 968. 97 83 15.80 l.834E+OO l.394E+00 1.394E+OO 22.34 TH-234 63.29 53 3.70* 4. 873.E+OO 1.440E+OO l.440E+OO 146.68 92.59 149 4.23 7.105E+OO 2. 411E+OO 2. 411E+00 42.70 U-234 609.32 194 45.49* 2.627E+OO 7.914E-01 7. 914E-0.l 19.52 1120.29 50 14.92 l.635E+00 9.927E-01 9.927E-01 31. 57 1764.49 32 15.30 1.106E+OO 9.146E-01 9.146E-01 39.29 U-235 89.96 91 3.47 6.980E+OO 1.823E+OO 1.823E+OO 53.22 93.35 149 5.60 7.105E+OO 1. 821E+OO 1.821E+OO 42.70 143.76 ------10.96* 7.370E+OO ------Line Not Found ------163.33 ------5.08 7.024E+OO ------Line Not Found ------185. 72 57 57.20 6.562E+OO 7.333E-02 7.333E-02 118. 40 205.31 ------5.01 6.171E+00 ------Line Not Found ------U-238 63.29 53 3.70* 4.873E+OO l.440E+OO l.440E+OO '146. 68 92.59 149 4.23 7.105E+OO 2. 411E+OO 2. 411E+OO 42.70 AM-243 43.53 44 5.90 1.188E+OO 3.091E+OO 3.091E+OO 81. 01 74.66 255 67.20* 6.006E+OO 3.083E-01 3.083E-01 26.17 ANH-511 511. 00 60 100.00* 3.021E+OO 9.698E-02 9.698E-02 66.34 Flag: "*" Key line Page 341 of 614 Page : 3 Summary of Nuclide Activity Sample ID : R405245014 Acquisit"ion date 3-0CT-2016 04:47:25 Total number of lines in spectrum 60 Number of unidentified lines 20 Number of lines tentatively identified by NID 40 Nuclide Type : Nuclide Hlife K-40 l.25E+09Y SC-46 83.79D CD-109 461.40D SN-126 2.30E+05Y BA-137M 30.08Y CS-137 30.08Y TL-208 l.41E+l0Y PB-210 22.20Y BI-211 7.04E+08Y PB-212 1.41E+l0Y BI-214 1600.00Y PB-214 1600.00Y RN-222 1600.00Y RA-224 l.41E+10Y RA-226 1600.00Y AC-228 1.41E+10Y RA-228 1.41E+10Y TH-228 l.41E+l0Y TH-229 7340.00Y TH-230 7.54E+04Y PA-231 7.04E+08Y TH-232 l.41E+l0Y TH-234 4.47E+09Y U-234 2.45E+05Y U-235 7.04E+08Y U-238 4.47E+09Y AM-243 7370.00Y ANH-511 l.OOE+09Y Decay 1. 00 11. 3 1. 55 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.325E+Ol 1. 976E-02 2.861E+OO 2.861E-01 l.404E-01 l.483E-01 3.366E-01 2.917E+OO 2.758E+OO 9.503E-01 7.914E-01 1.00lE+OO 7.914E-01 2.292E+OO 7.914E-01 7 .181E-01 7 .181E-01 9.503E-01 4.411E-01 7.914E-01 *3.042E-01 7.181E-01 1. 440E+OO 7.914E-01 7.333E-02 l.440E+00 3.083E-01 9.698E-02 3.812E+Ol 3.812E+Ol Decay Corr pCi/GRAM 1.325E+Ol 2.226E-01 4.442E+OO 2.S61E-01 l.430E-01 1. 511E-01 3.366E-01 2.991E+OO 2.758E+OO 9.503E-01 7.917E-01 1.00lE+OO 7.917E-01 2.292E+OO 7.917E-01 7.181E-01 7 .181E-01 9.503E-01 4. 411E-01 7.914E-01 3.042E-01 7.181E-01 1. 440E+OO 7.914E-01 7.333E-02 l.440E+00 3.083E-01 9.698E-02 3.999E+Ol 3.999E+Ol 66.67% Decay Corr 2-Sigma Error 0.146E+Ol 2.893E-01 1.823E+OO. 1.174E-01 0.586E-01 0.619E-01 0.737E-01 3.684E+OO 0.376E+OO l.141E-01 l.546E-01 0.136E+OO 1. 546E-01 0.899E+OO 1.546E-01 2.525E-01 2.525E-01 1.141E-01 1.811E-01 l.545E-01 6.352E-01 2.525E-01 . 2 .112E+OO l.545E-01 8.682E-02 2 .112E+00 0.807E-01 6.434E-02 2-Sigma %Error 11. 03 129.99 41. 05 41. 05 40.97 40.97 21. 88 123.18 13.62 12.01 19.52 13.62 19.52 39.22 19.52 35.17 35.17 12.01 41. 05 19.52 208.80 35.17 146.68 19.52 118. 40 146.68 26.17 66.34 Flags: "K" Keyline not found "E" = Manually edited "M" Manually accepted "A" = Nuclide specific abn. limit Page 342 of 614 Flags K K Unidentified Energy Lines Page : 4 Sample ID : R405245014 Acquisition date : 3-0CT-2016 04:47:25 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 3 26. 73 23 8 1. 36 ' 53. 68 51 22 4.54E-03 **** 1. 62E-07 3 28.06 42 24 1. 37 56.32 51 22 8.29E-03 **** 8.18E-06 3 30.06 ' 48 50 1. 37 60.32 51 22 9.54E-03 94.1 4.93E-04 3 31.78 26 77 1. 38 63.75 51 22 5.17E-03 **** 5.25E-03 0 57.93 47 117 1. 29 116. 02 113 7 9.91E-03 93.4 4.04E+OO T 0 151. 08 54 84 1. 27 302.20 299 7 1.24E-02 68.5 7.25E+OO T 0 170.22 15 120 0.92 340.46 334 8 3.55E-03 **** 6.89E+OO 0 209.04 49 115 1.13 418.05 414 9 1.14E-02 91. 9 6.lOE+OO 0 270.35 47 70 1. 72 540.63 536 8 1.13E-02 73.9 5.05E+OO T 0 329.31 69 92 0.86 658.51 652 14 1. 68E-02 68.9 4.31E+OO T 2 354.77 17 19 1. 71 709.41 698 15 4.16E.-03 **** 4.06E+OO T 0 462.75 45 27 1. 50 925.34 921 9 1.14E-02 53.8 3.27E+OO T 0 490.71 11 30 0.87 981.25 976 8 2.70E-03 **** 3.12E+OO 0 541.32 16 25 0. 96 1082.48 1079 8 4.19E-03 **** 2.88E+OO 0 727.66 32 39 2.03 1455.23 1446 15 8.47E-03 94.7 2.29E+OO T 0 732.73 1.0 18 0.80 1465.37 1461 7 2.64E-03 **** 2.28E+OO T 0 768.15 25 34 1. 30 1536.24 1529 12 6.69E-03 **** 2.20E+OO T 0 787.21 22 14 1. 63 1574.37 1568 12 5.87E-03 84.7 2.15E+OO 0 862.45 13 31 1. 47 1724.95 1717 14 3.60E-03 **** 2.0lE+OO 0 924.18 6 12 3.57 1848.48 1841 9 1.52E-03 **** 1.90E+OO T 1 965.06 44 5 1. 94 1930.30 1921 27 l.20E-02 32.2 l.84E+OO T 0 1001.50 '21 6 2.18 2003.24 1998 12 5. 66E-03 '68 *. 8 1. 79E+OO T 0 1057.29 12 5 1.17 2114. 90 2111 7 3.30E-03 86.1 1.71E+OO 4 1155.74 19 11 1. 85' 2312.00 2306 16 5.44E-03 80.0 1. 60E+OO 4 1158. 68 13 8 2.26 2317.89 2306 16 3.56E-03 90.9 1.59E+OO 0 1164.73 15 12 4.40 2330.00 2323 12 4.17E-03 **** l.59E+00 0 1238.30 16 5 1. 45 2477.30 2475 6 4.47E-03 65.5 1. 51E+OO T 0 1281. 08 10 14 1. 24 2562.98 2557 11 2.82E-03 **** l.47E+00 0 1316.37 4 5 0.92 2633.64 2626 10 l.08E-03 **** 1. 43E+OO. 0 1353.87 8 11 0.59 2708.75 2701 9 2.14E-03 **** 1.40E+OO 0 1377.43 11 6 3.03 2755.92 2751 9 3.17E-03 **** 1.38E+OO 0 1568.64 4 6 0.83 3138. 95 3131 9 l.19E-03 **** 1.23E+OO 0 1588-. 36 9 2 0.63 3178.46 3174 8 2. 51E-03 85.6 l.22E+OO Flags: "T" = Tentatively associated Page 343 of 614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:49:29.11 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245014.CNF;l *
  • Acquisition date 3-0CT-2016 04:47:25 Sensitivity 3.000 *
  • Detector ID GAM20 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:15.40 Half life ratio : ***** *
  • Sample date 15-DEC-2015 11:08:00 Nuclide Library : SOLID *
  • Sample ID R405245014 Analys"t initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.5413E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;15
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 SC-46. CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-'228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.430E-01 2.143E-01 7.200E-01 4.653E-02 2.154E-02 2.275E-02 2.315E-02 l.191E+OO l.342E-01 3.344E-02 4.020E-02 1. 361E-01 4.020E-02 3.584E-01 4.020E-02 7.099E-02 7.099E-02 3.344E-02 3. 411E-01 4.019E-02 3.283E-01 7.099E-02 7.445E-01 4.019E-02 . 1. 320E-01 7.445E-01 3.296E-02 l.839E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 344of614 Le (pCi/GRAM 7.177E+OO 3.683E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL.:..26 '"V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 , NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M 'TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 . PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 345 of 614 1.326E-02 O.OOOE+OO O.OOOE+OO 4.686E-02 2.982E-01 0.000E+OO 3.257E-02 3.437E-01 4.824E+OO 3 .140E-02 , 1. 361E-Ol 1.658E+OO 3.977E+OO O.OOOE+OO 1. 346E-Ol O.OOOE+OO O.OOOE+OO 4.701E-01 5.377E+OO 5. 271E-01 O.OOOE+OO 1.149E-Oi 3.560E+02 2. 451E-02 5.807E-01 1. 380E+OO 9.645E-01 0.000E+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 2.721E-02 3.366E-02 2.958E+OO 3.498E-01 3.498E-01 1. 931E-02 5.326E-02 1. 479E-01 0.000E+OO O.OOOE+OO 9.138E-02 1.352E+OO 6.975E-02 2.034E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3. 013E-02 O.OOOE+OO 4.708E--'02 l .110E-01 O.OOOE+OO O.OOOE+OO 7.895E-02 O.OOOE+OO O.OOOE+OO 1.459E+Ol O.OOOE+OO 2.602E-01 4.038E-02 3.501E+OO 3.227E-02 O.OOOE+OO 5.890E+02 O.OOOE+OO 1.768E-02 6.099E-02 l.199E-01 9.041E-02 8 .181E-02 1.355E+OO 4.453E-02 1.065E+Ol l.745E-01 NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF. NOT !DENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT . . SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 346 of 614 5.107E-02 1.709E-02 2.463E+OO 7.338E-Ol 1.565E+OO 1.601E+Ol 6.553E+Ol 2.755E-01 1.699E+OO 3.273E-02 4.865E-01 5.255E-01 2.461E-01 4. 211E-01 1.571E-Ol 1. 571E-01 4. 211E-01 4.225E-02 1. 873E-01 3.802E+OO 4.225E-02 O.OOOE+OO 1. 733E-01 2.484E+02 7.370E-02 6.947E-02 5.004E-02 2.162E-02 2.905E-02 8.184E-02 FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABl::JN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:49:34.69 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 . * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * ' *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245014.CNF;l *
  • Acquisition date 3-0CT-2016 04:47:25 Sensitivity : 3.000 *
  • Detector ID GAM20 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:15.40 Half life ratio : ***** *
  • Sample date 15-DEC-2015 11:08:00 Nuclide Library : SOLID *
  • Sample ID R405245014 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.5413E+02 GRAM *
  • Quantity Err(%) : 1.2976E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 . * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. *Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (1.96-sigma) K-40 1.325E+Ol 1.590E+OO SC-46 2.226E-01 2.837E-01 CD-109 3.079E+00 1.854E+OO SN-126 1.984E-01 1.189E-01 BA-137M 1.430E-01 5.774E-02 CS-137 1. 511E-01 6.lOOE-02 TL-208 3.366E-01 7.358E-02 PB-210 2. 991E+OO 3.618E+OO BI-211 1.344E-01 8.512E-01 PB-212 9.503E-01 1.226E-01 BI-214 7.917E-01 l.552E_:_Ol PB-214 1. OOlE+OO 1.399E-01 RN-222 7.917E-01 1.552E-01 RA-224 6.082E-01 1. OllE+OO RA-226 7.917E-01 1.552E-01 AC-228 7 .181E-01 2.502E-01 RA-228 7.181E-01 2.502E-01 TH-228 9.503E-01 1. 22 6E-01 TH-229 -2.266E-01 3.846E-01 TH-230 7.914E-01 1.552E-01 PA-231 3. 042E-01* 6.259E-01 TH-232 7.181E-01 2.502E-01 TH-234 1.440E+OO 2.094E+OO U-234 7.914E-01 l.552E-01 U-235 -5.506E-02 l.582E-01 U-238 l.440E+00 2.094E+OO AM-243 2.261E-01 8.428E-02 ANH-511 9.698E-02 6.317E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 Page 347 of 614 Key-Line Activity (pCi/GRAM -3 .. 933E+OO 1.832E.,-02 K.L Act error ( 1. 96-sigma) 8.820E+OO 4.202E-02 TPU ( 1. 96-sigma) 1.590E+OO 2.837E-01 1.854E+OO l.189E-01 5.774E-02 6.lOOE-02 7.358E-02 3.618E+OO 8.512E-01 1.226E-01 l.552E-01 l.399E-01 1.552E-01 1. OllE+OO 1.552E-01 2.502E-01 2.502E-01 l.226E-01 3.846E-01 l.552E-01 6.259E-01 2.502E-01 2.094E+OO l.552E-01 1.'582E-01 2.094E+OO 8.428E-02 6.317E-02 TPU ( 1. 96-sigma) 8.996E+00 NOT IDENT. 4.282E-02 NOT IDENT.

NA-24 1.000E+41 1.728E+41 0.000E+OO SHORT HLIF AL-26 -2.120E-02 2.532E-02 2.706E-02 NOT IDENT. V-48* -4.581E+03 8.676E+03 8.919E+03 SHORT HLIF CR-51 2. 696E+02 2.834E+02 3.083E+02 SHORT HLIF MN-54 2.880E-02 5.106E-02 5.268E-02 NOT IDENT. C0-56 2.136E-02 3.547E-01 3.549E-01 FAIL ABUN MN-56 l.OOOE+41 1. 770E+42 O.OOOE+OO SHORT HLIF C0-57* -4.406E-03 3.820E-02 3.825E-02 NOT IDENT. C0-58 -4.540E-01 5.004E-01 5.406E-01 NOT IDENT. FE-59 2.053E+OO 5.200E+OO 5.282E+OO NOT IDENT. C0-60 -8.137E-03 3.818E-02 3.835E-02 NOT IDENT. ZN-65 l.280E-01 1. 4 75E-.Ol l.584E-01 NOT IDENT. GE-68 8.738E-01 1. 740E+OO l.784E+OO NOT IDENT. AS-73 -3.753E-01 4.443E+OO 4.446E+OO NOT IDENT. AS-74 -2.748E+02 3. 081E+03 3.083E+03 SHORT HLIF SE-75 -1. llOE-01 1.589E-01 l.666E-01 NOT IDENT. BR-77 2.160E+37 l.825E+38 O.OOOE+OO SHORT HLIF SR-82 4.648E+02 4. 722E+02 5.166E+02 SHORT HLIF RB-83 2.903E-01 5.027E-01 5.195E-01 NOT IDENT. KR-85 6.028E+OO 5.860E+OO 6.460E+OO NOT IDENT. SR-85 5.900E-01 5.746E-01 6. 331E-01 NOT IDENT. RB-86 2.867E+03 1.655E+04 l.660E+04 SHORT HLIF Y-88 4.607E-02 1.157E-01 l.176E-01 NOT IDENT. Y-91 -7.005E+Ol 4.233E+02 4.244E+02 NOT IDENT. NB-94 8. 724E-04 2.889E-02 2.889E-02 NOT IDENT. NB-95 l.549E-01 7.444E-01 7.476E-01 NOT IDENT. NB-95M -6 .112E-01 1. 748E+OO 1. 769E+OO NOT IDENT. ZR-95 l.064E-01 1.130E+OO l .131E+OO NOT IDENT. NB-97 -1.000E+41 2.701E+41 O.OOOE+OO SHORT HLIF ZR-97

  • 1. OOOE+41 1. 940E+41 O.OOOE+OO SHORT HLIF M0-99 -2.446E+30 2.318E+31 O.OOOE+OO SHORT HLIF TC-99M -l.000E+41 3.087E+41 O.OOOE+OO SHORT HLIF RH-101 3.548E-03 3.135E-02 3 .139E-02 NOT IDENT. RH-102 -8.877E-03 4.126E-02 4.146E-02 FAIL ABUN RU-103 -2.973E-01 3.454E+OO 3.456E+OO FAIL ABUN RH-106 1. 981E-01 3.765E-01 3.870E-01 NOT IDENT. RU-106 1. 981E-01 3.765E-01 3.870E-01 NOT IDENT. AG-108M 8.354E-03 2.083E-02 2. ll 7E-02 NOT IDENT. AG-llOM -9.344E-02 1. OOlE-01 l.086E-01 NOT IDENT. SN-113 -9.822E-02 1.794E-01 l.847E-01 NOT IDENT. CD-115 -2.748E+38 3.079E+38 O.OOOE+OO SHORT HLIF SN-ll 7M 2.416E+04 5.504E+04 5. 611E+04 SHORT HLIF TE-123M 2.892E-03 1. 075E-01 1.075E-01 NOT IDENT. SB-124 2.321E-01 1.540E+OO 1.543E+OO NOT IDENT. SB-125 -4.652E-02 8.542E-02 8. 7 96E-02 FAIL ABUN TE-125M 1.127E+02 2.254E+02 2.310E+02 NOT IDENT. I-126 2.512E+05 5.857E+05 5. 965E+05 SHORT HLIF SB-126 l.802E+05 6.862E+05 6.910E+05 SHORT HLIF SB-127 -3.124E+21 6.778E+21 0.000E+OO SHORT HLIF I-131 1. 935E+09 2.284E+09 2.445E+09 SHORT HLIF I-132 l.OOOE+41 l.822E+42 O.OOOE+OO SHORT HLIF TE-132 6.798E+24 6.973E+25 O.OOOE+OO SHORT HLIF BA-133 3.444E-02 5.246E-02 5.471E-02 FAIL ABUN I-133 1.000E+41 3.218E+41 O.OOOE+OO SHORT HLIF CS-134 1.483E-01 8.392E-02 1.073E-01 FAIL ABUN CS-135 7.581E-02 1.269E-01 l.314E-01 NOT IDENT. I-135 1. OOOE+41 l.422E+42 O.OOOE+OO SHORT HLIF CS-136 -5.276E+03 1.674E+05 1. 67 5E+05 SHORT HLIF CE-139 6.095E-03 1.009E-01 l.009E-01 NOT IDENT. BA-140 4.345E+04 8. 201E+05 8.204E+05 SHORT HLIF LA-140 -1.967E+05 2.184E+05 2.357E+05 SHORT HLIF CE-141 -5.901E+OO 1. 759E+Ol l.779E+Ol NOT IDENT. CE-143 l.000E+41 5. 961E+40 O.OOOE+OO SHORT HLIF CE-144 -2.462E-02 3.056E-01 3.058E-01 NOT IDENT. PM-144 4.lOOE-03 4.713E-02 4.716E-02 NOT I DENT .. PR-144 3.800E-01 4.082E+OO 4.086E+OO NOT IDENT. PM-146 -2.816E-03 3. 723E-02 3. 725E-02 NOT IDENT. ND-147 1.787E+07 l.803E+07 1.974E+07 SHORT HLIF PM-147 2. 628E+02' 6.579E+02 6.684E+02 NOT I DENT'. PM-149 -1.189E+39 4.130E+39 O.OOOE+OO SHORT HLIF EU-150 1.305E-02 2.443E-02 2.512E-02 FAIL ABUN EU-152 9. 722E-04 7.590E-02 7.590E-02 FAIL ABUN GD-153 -1.173E-01 1.604E-01 1. 688E-01 NOT IDENT. EU-154 4.801E-02 9.897E-02 l.013E-01 NOT IDENT. EU-155 -7.910E-03 9.470E-02 9.477E-02 FAIL ABUN TB-160 6.049E-02 1.625E+OO l.626E+OO FAIL ABUN H0-166M 2.627E-02 4.860E-02 5.002E-02 NOT IDENT. TM-171 4.654E+OO l.143E+Ol l.162E+Ol NOT IDENT. Page 348 of 614 HF-172 -1.600E-02 2.042E-01 2.043E-01 FAIL ABUN LU-172 2.362E-02 5.399E-02 5.503E-02 FAIL ABUN LU-176 -7.322E-03 1.973E-02 2.00lE-02 FAIL ABUN HF-181 -1.220E+OO 3.012E+00 3.062E+OO FAIL ABUN TA-182 8.490E-02 8.367E-01 8.376E-01 FAIL ABUN RE-183 3.022E+OO 2.804E+OO 3 .118E+00 FAIL ABUN RE-184 -2. 013E+Ol 2.410E+Ol 2.575E+Ol NOT IDENT. W-188 -l.063E+02 9.609E+Ol 1. 074E+02 FAIL ABUN IR-192 -l.279E-01 3.214E-01 3.266E-01 FAIL ABUN HG-203 7.390E-01 l.809E+OO 1. 839E+OO NOT IDENT. BI-207 . -1.803E-04 3.745E-02 3.745E-02 FAIL ABUN PB-211 3.833E-01 5.036E--'01 5.324E-01 NOT IDENT. BI-212 1. Ol 7E+OO 9.455E-01 1. 051E+OO FAIL ABUN RN-219 -1.313E-01 2. 961E-01 3.019E-01 FAIL ABUN RA.-223 1.331E-01 5.033E-01* 5.069E-01 FAIL ABUN AC-227 -1.080E-01 l.830E-01 1.893E-01 FAIL ABUN TH-227 -1.080E-01 l.830E-01 1. 893E-01 FAIL ABUN TH-231 1.331E-01 5.033E-01 5.069E-01 FAIL ABUN PA-233 8.258E-03 4.608E-02 4.623E-02 FAIL ABUN PA-234 -l.137E-01 2.648E-01 2.697E-01 FAIL ABUN PA-234M 6.*675E+OO 4.510E+OO 5.422E+OO FAIL ABUN NP-237 8.258E-03 4.608E-02 4.623E-02 FAIL ABUN NP-238 1.848E+39 3.223E+40 O.OOOE+OO SHORT HLIF NP-239 -3.309E-03 2.008E-01 2.008E-01 NOT IDENT. PU-239 -l.032E+02 2.974E+02 3.010E+02' NOT IDENT. AM-241 -3.443E-02 l.059E-01 1.070E-01 NOT IDENT. CM-243 -1. 479E-02 8. lllE-02 8.138E-02 NOT IDENT. BK-247 -5. 213E-02 6.404E-02 6. 822E..:.02 FAIL ABUN CM-247 -l.954E-02 2.727E-02 2.866E-02 NOT IDENT. CF-249 1. 460E-02 3. ll 7E-02 3.185E-02 NOT IDENT. CF-251 -1.569E-02 8.894E-02 8.922E-02 NOT IDENT. Page 349 of 614
  • GEL Laboratories LLC *
  • 2040 Savage Road * * . Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************** ENERGY MDA COUNTS ENERGY MDA .COUNTS ENERGY MDA COUNTS 43.53 70.1585 87.09 92.4462 136.47 74.9334 45.60 49.1026 87.57 92.5056 i40.51 0.0000 46.54 59.8882 88.03 92.5630 143.76 80.3499 49.72 0.0000 88.34 92.6014 144.24 70.6432 51. 35 70.5128 88.47 92.6171 145.44 73.1653 51. 87 65.8992 89. 96 92.8003 152.43 63.8360 52.39 77.8568 1093.63 92.8832 153.25 0.0000 52.97 74.6917 91.11 0.0000 323.87 39.3496 . 53. 44 78.0057 92.59 93 .1192 156.02 0.0000 54.07 81.3480 93.35 93.2107 158.56 0.0000 57.36 0.0000 94.56 69.1521 159.00 62.9936 57.53 82.9371 94.65 69.1603 162.33 66.9018 57.98 83.0012 94.67 69.1621 162.66 0.0000 59.27 94.1301 94.87 69.1795 163.33 60.7625 59.32 94.1380 97.43 95.6231 165.86 67.9438 59.54 94.1731 98.43 66.0163 176.31 70.2410 60. 96 79.0313 98.44 66.0171 176.60 0.0000 61.17 79.0590 99.53 77.7039 177.52 66.1291 62.93 113.4275 100 .11 74.2778 181. 07 0.0000 63.29 113.4945 102.03 79.1064 181. 52 68.0339 63.58 113.5482 103.18 83.8768 184.41 63.1470 64.28 113. 6772 103.37 79.2351 143*. 76 63.2164 66.73 106.3682 105.21 89.9207 193.51 77.1941 67.24 107.9316 105.31 89.9312 197.03 77.4126 125.81 103.5680 106.12 95.8635 198.01 66.4052 67.75 103.5794 106.47 92.3949 201.83 73.4382 69.67 120.2146 109.28 83.3134 203.43 61.5601 70.83 121. 9148 111. 00 112.8743 205.31 51. 3757 72. 81 102.8950 111. 76 0.0000 210.85 65.7842 72. 87 102.9041 114.06 89.6725 215.65 62.1409 74.66 115. 5151 116. 30 0.0000 222 .11 61.5732 74.82 115.5426 116.74 73.3757 227.09 61.7985 74.97 115.5677 119.76 71.2473 227.38 61.8115 77 .11 115. 9300 121.12 61.8397 228.16 0.0000 78.74 93.2630 121.22 61. 8464 228.18 59.2344 79.69 117.4896 121. 78 77.3556 116.74 59.2344 80.12 94.9531 122.06 70.2363' 235.69 52.5482 80.19 0.0000 122.92 85.7922 235. 96 52.5580 80.57 117.6356 123.07 84.6148 238.63 45.6365 81. 00 115. 4434 265.00 63.2048 238.98 0.0000 81. 07 115.4550 125.81 84.8645 240.99 45.7121 81. 75 117.8307 127.23 90.9777 242.00 47.5038 83.79 92.0322 127.91 75.4703 244.70 50.2368 84.00 92.0588 129.30 104.3732 252.40 0.0000 85.43 92.2392 131. 20 93.7616 252.80 46.0850 86.55 92.3789 133.02 81. 8955 254.15 0.0000 86.79 92.4085 133. 52 78.3231 *256. 23 54.1866 86.94 92.4277 136.00 83.3536 260.90 0.0000 Page 350 of 614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 51. 8108 355.39 0.0000 584.27 23.4943 264.80 51.8156 356.01 16.9728 595.83 0.0000 265.00 57.8984 364.49 0.0000 427.87 19. 9610 268.22 44.3206 366.42 0.0000 602.52 0.0000 269.46 41.2205 372.51 32.3398 604.72 28.4084 270.03 41.2355 375.05 23.8108 607.14 28.4337 271.23 45.7529 377.52 43.8681 609.32 16.8633 273.65 0.0000 356.01 34.4429 610.33 16.8698 276.40 53.1062 388.16 29.7241 614.28 17.4218 277.37 51. 3373 388.63 0.0000 618.01 22.2031 277.60 47.742,3 391.69 35.5404 620. 36 14.8152 278.00 48.6552 264.66 28.9453 621. 93 13.7644 279.20 45.9874 401.81 31.8580 630.19 .0. 0000 279.54 51. 4081 402.40 33.7987 631.29 14.8733 279.70 50. 5119 404.85 21. 2704 633.25 13.8204 280.46 56.8528 410.95 36.8496 634.78 0.0000 283.69 36.1702 413.71 24.2757 635.95 13.8337 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 51. 5983 423.72 0.0000 645.85 14.9502 285.90 0.0000 427.09 25.4086 657.76 24.1278 287.50 29.9116 427.87 33.2384 657.90 0.0000 290.67 55.8545 433.94 20.5886 661. 66 16.1066 293.27 0.0000 439.40 24. 5722 -664.57 0.0000 351. 93 58.7418 453.88 29.6832 666.33 0.0000 295. 96 58.7694 463.37 37.2627 666.50 0.0000 879.38 38.3291 468.07 28.8767 667.71 0.0000 299.98 42.4717 473.00 0.0000 677.62 17.2747 300.09 42.4746 475.06 21. 9740 685.70 0.0000 300 .13 42.4755 476.78 34.9850 695.00 0.0000 301.36 46.6203 477.60 25.9979 696.49 20.6444 302.85 43.9170 482.18 25.0478 696. 51 20.6444 256.23 39.5648 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 22.8235 306.78 44.0205 497.08 17.1418 697.49 23.9121 308.46 39.4744 505.52 27.3224 702.65 23.9524 311. 90 34.9555 507.63 0.0000 706.68 20.7140 316.51 35.9722 511. 00 22.3138 711. 68 16.3800 319.41 0.0000 514.00 16.7565 720. 70 0.0000 320.08 0.0000 514.00 16.7565 721. 93 0.0000 321. 04 42.5401 520.40 18.3281 722. 78 18.0831 323.87 33.3464 520.69 0.0000 722. 91 18.0838 325.23 30.5911 522.65 0.0000 723.31 16.4423 328.76 0.0000 527.90 0.0000 724.19 '16.4471 333.37 25.1444 528.26 30.6445 727.33 18 .1100 333.97 25.1532 529.59 18.3970 733.00 16.4935 334.37 44.7266 529.87 0.0000 735.93 13.2075 338.28 37.3535 531. 02 0.0000 333.97 11. 0116 338.32 37.3543 537.26 0.0000 739.50 0.0000 311.90 37.3991 546.56 0.0000 747.24 14.3595 340.48 37.3991 552.55 22.6920 748.06 12.1534 340.55 0.0000 563.25 19.6803 752.31 8.8506 344.28 29.5133 569.33 15.5737 753.82 0.0000 345.93 28.1335 946.00 16.6126 756.73 16.6180 351.06 35.7356 569.70 16. 6139 756.80 16.6187 351. 93 35.7526 583.19 20.8748 884.68 13.3247 Page 351of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 18.3315 1274.44 12.8013 1620.50 4.0537 766.42 18.8912 1001.03 10.6805 1621.92 5.0684 766.84 18.8933 1002.74 10.6853 1678.03 0.0000 772.60 0.0000 1004.73 8.5523 1690.97 4.1033 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 2.0769 778.90 22.3104 1028.54 0.0000 1063.66 4.1577 783.70 0.0000 1037.84 11. 6781 1771. 35 2.0793 785.37 16.7657 1038.76 0.0000 1791.20 0.0000 792.07 10.0800 631. 29 11.7035 1808.65 6.2758 794.95 10.0887 1048.07 0.0000 1810. 72 0.0000 795.86 10.0917 1049.04 9.0076 1836.06 1.0505 810.06 21. 3951 1050.41 9. 9117 810.29 21. 3966 1063.66 12.6559 344.28 19.1451 1077.00 0.0000 810.76 23.6523 1077.34 9.0698 815.77 0.0000 1085.87 10.9065 1048.07 0.0000 1093.63 8.1947 832.01 18 .1341 1099.45 12.7653 834.85 12.4775 1112. 07 19.2043 835.71 11. 3460 1112. 84 17.3788 836.80 0.0000 1115. 54 8.7867 846.75 0.0000 1120. 29 13.7439. 846.77 13. 6587 1120. 55 13.7448 856.80 0.0000 1221.41 13.7476 860.56 15.9984 1129. 67 7.3462 871.09 8.0231 1131.51 0.0000 873.19 16.0559 1147.95 0.0000 875.33 0.0000 1173.23 15.7673 879.38 17.2327 1177.9$ 11.1416 880.51 18.3874 1189.05 15.8234 883.24 12.0757 1204.77 16.8124 884.68 20.7100 1221.41 18.7488 889.28 10.3682 1231.02 15. 9697 894.76 16.1528 1235.36 0.0000 898.04 9.2386 1238.28 16.9354 900.72 18.4909 1260.41 0.0000 903.28 20.8169 1271.87 19.9016 911.20 9.2718 1274.44 9.7527 912.08 1274.54 10 .1139 923.98 0.0000 1291.59 12.3708 926.50 10.4744 1298.22 0.0000 929.11 15.1402 1312 .11 0.0000 937.49 14.8823 1332.49 14.3958 944.13 0.0000 1362.66 0.0000 946.00 18 .4256 1365.19 4.8303 949.00 14.9279 1368.63 0.0000 667.71 0.0000 1384.29 3.8789 962. 31 8.8120 1408.01 4.8715 964.08 8.8159 1457.56 0.0000 966 .17 8.8208 1460.82 8.8583 911.20 8. 8272 1489.16 5.9374 968.97 8.8272. 1505.03 7.9399 983.53 0.0000 1584.12 4.8331 984.45 0.0000 1596.21 0.0000 Page 352of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:50:03.29 ********************************************************************************
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245015.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM28.CNF;265 Background date : 2"-0CT-'-2016 11:01:35. Sample date 15-DEC-2015 14:02:00 Acquisition date : 3-0CT-2016 04:47:45. Sample ID R405245015 Sample quantity 1.20577E+02 GRAM Detector name : GAM28 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.43 0.0% Energy tolerance : 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596387 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 -4 2 4 3 0 4 3 5 3 6 0 7 0 8 0 9 0 10 0 11 2 12 2 13 0 14 0 15 0 16 0 17 0 18 0 19 0 20 0 21* 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Page 353 of614. Energy 74.81* 77.19 87.12 90.05 92.86* 128.53 133.01 162.68* 186.01* 209.42 238.85* 242.07 252.99 272 .11 295.54 302.85 328.79 338.40 352.31* 412.44 463.75 511.24* 573.84 583.33* 609.85* 616.91 662.46* 717. 59 728.28 741.84 757.99 795.48 823.27 862.19 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 145 224 33 55 87 37 42 17 119 34 400 84 33 58 184 52 22 97 228 28 26 56 11 146 187 14 94 17 40 . 14 9 32 4 34 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 177 1.49 149.72 174 1.31 154.48 155 0.95 174.34 114 1.23 180.21 166 1.52 185.84 155 2.26 257.23 68 2.03 266.19 97 0.88 325.59 120 1.25 372.27 76 0.61 419.12 91 1.36 478.03 107 1.63 484.48 45 2.30 506.34 140 0.66 544.60 84 1. 40 591. 50 108 4.73 606.13 62 0.79 658.05 61 1.02 677.28 84 1.37 705.12 60 3. 77 825 ."48 32 1.86 928.17 80 2.29 1023.23 22 0.80 1148.52 39 1. 65 1167. 51 41 1.50 1220.59 20 0.98 1234.71 65 1.51 1325.89 16 5.03 1436.23 19 1. 93 1457. 63 13 1.08 1484.76 12 1. 38 1517. 08 12 1. 05 1592 .13 16 0.99 1647.74 2 6 0 . 7 4 -172 5 . 6 4 145 145 173 178 178 252 263 322 366 415 473 473 503 537 585 598 652 673 698 814 923 1014 1144 1160 1213 1229 1319 1428 1451 1480 1512 1586 1642 1719 15 4.04E-02 19.4 1.35E+OO 15 6.23E-02 12.2 6 9. 20E-03 61. 5 15 1.53E-02 30.3 1.40E+OO 15 2.42E-02 31.5 12 l.02E-02 70.2 7 1.15E-02 36. 5 8 4.84E-03103.4 12 3.29E-02 21.5 8 9.33E-03 48.2 17 1.llE-01 6.6 1.29E+OO 17 2.32E-02 7 9.24E-03 37.4 16 l.60E-02 47.9 13 5.llE-02 12.7 19 1.44E-02 50.3 10 6.16E-03 69.9 10 2.68E-02 18.2 14 6.32E-02 11.0 16 7.81E-03 64.4 9 7.21E-03 44.6 20 l.54E-02 45.6 7 3.08E-03 76.9 17 4.06E-02 12.9 15 5.20E-02 10.7 9 3.84E-03 64.5 16 2. 62E-02 21. 9 13 4.76E-03 54.1 13 1.llE-02 27.7 8 3.80E-03 54.3 8 2.44E-03 79.7 12 8.89E-03 28.0 9 1.06E-03194.7 14 9.55E-03 36.6 Peak Search Report (continued) Page : 2 Sample ID : R405245015 Acquisition date 3-0CT-2016 04:47:45 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 911. 85* 95 14 1. 52 1825.04 1818 14 2.65E-02 13.4 36 0 969. 85 45 26 2.58 1941.13 1934 12 l.24E-02 27.6 37 0 1002.02* 5 5 1.14 2005.51 2002 7 1. 25E-03113. 9 38 0 1121. 91* 40 18 1. 53 2245.47 2238 16 1. lOE-02 30.0 39 0 1165.75 7 13 0.62 2333.22 2328 9 2.03E-03 97.2 40 0 1274.19 12 9 0.63 2550.25 2543 12 3.29E-03 58.5 41 0 1377.98 19 0 2.50 2758.00 2750 15 5.28E-03 22.9 42 0 1384.86 17 4 2.45 2771.76 2765 14 4.79E-03 33.5 43 0 1461.61* 394 7 2.10 2925.38 2917 15 l.lOE-01 5.3 44 0 1501.25 6 3 0.64 3004. 72 2995 13 l.57E-03 78.1 45 0 1765.66* 15 4 0. 71 3533.94 3526 13 4.09E-03 39.2 Flag: "*" = Peak area was modified by background subtraction Page 354 of 614 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 05:50:05 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245015.CNF;l PEAK Vl6.9,PEAKEFF V2:2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl . Configuration Analyses by Sample title Sample date Sample ID 15-DEC-2015 14:02:00 Acquisition date : 3-0CT-2016 04:47:45 R405245015 Sample quantity 120.58 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID Sample geometry : GAMMA28 Detector geometry: 0 01:00:00.00 Elapsed real time: 1.50 keV Half life ratio No Linear 75.00 Systematic Error Efficiencies at
  • Interference Report Interfering Interfered Nuclide Line Nuclide Line PB-214 242.00. RA--'224 240.99 PB-214 87.09 SN-126 86.94 PB-214 87.09 SN-126 87.57 PB-214 87.09 CD-109 88.03 PB-214 74.82 AM-243 74.66 PB-214 74.82 TH-228 74.82 PB-214 74.82 PB-212 74.82 PB-214 351. 93 BI-211 351.06 Page 355of614 CAN 0 01:00:00.43 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : R405245015 Acquisition date 3-0CT-2016 04:47:45 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status NA-22 1274.54 99.94* 1.388E+OO 5.065E-02 6.270E-02 117 .10 OK K-40 1460.82 10.66* l.237E+OO 1.762E+Ol 1. 762E+Ol 10.56 OK BA-137M 661.66 89.90* 2.304E+OO 2.806E-01 2.859E-01 43.76 OK CS-137 661.66 85.10* 2.304E+OO 2. 965E-01 3.020E-01 43.76 OK CE-144 80.12 *1:36 4.852E+OO Line Not Found Absent 133.52 11.09* 6.653E+OO 3.755E-01 7.652E-01 72. 97 OK TL-208 277.37 6.60 4.566E+OO Line Not Found Absent 583.19 85.00* 2.540E+OO 4.191E-01 4.191E-01 25.81 OK 860.56 12.50 l.888E+OO Line Not Found Absent PB-212 74.82 10.28 4.343E+OO 1.412E+OO 1. 412E+OO 62.97 OK 77 .11 17.10 4.580E+OO 1. 962E+OO 1. 962E+OO 24.48 OK 238.63 43.60* 5.102E+OO l.165E+OO 1.165E+OO 13.16 OK 300.09 3.30 4.295E+OO Line Not Found Absent BI-214 609.32 45.49* 2.455E+OO l.036E+00 1.036E+OO 21. 37 OK 1120.29 14.92 l.540E+OO Line Not Found Absent 1764.49 15.30 1.044E+OO 5. 371E-01 5.373E-01 78.31 OK PB-214 74.82 5.80 4.343E+OO Line Not Found <<INT Reject 77 .11 9.70 4.580E+OO 3.459E+OO 3.460E+OO 24.48 OK 87.09 3.41 5.411E+OO 1.223E+OO '1.223E+OO 123.00 OK 242.00 7.25 5.054E+00 Line Not Found <<INT Reject 295.22 18.42 4.347E+OO 1.'472E+00 1.473E+OO 25.34 OK 351.93 35.60* 3.782E+OO 1.074E+OO 1. 075E+OO 21. 94 OK RN-222 609.32 45.49* 2.455E+00 1.036E+OO 1.036E+OO 21. 37 OK 1120.29 14.92 1.540E+OO Line Not Found Absent 1764.49 15.30 l.044E+00 5. 371E-01 5.373E-01 78.31 OK RA-224 240.99 4.10* 5.053E+OO 1.236E-02 l.236E-02******* OK RA-226 609.32 45.49* 2.455E+OO l.036E+00 l.036E+00 21. 37 OK 1120.29 14.92 1.540E+OO Line Not Found Absent 1764.49 15.30 1.044E+OO 5.371E-01 5.373E-01 78.31 OK AC-228 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.906E+OO 1.398E+OO 1.398E+OO 36.32 OK 794.95 4.25 2.004E+OO 2.288E+OO 2.288E+OO 55.90 OK 835.71 1. 61 1.930E+OO Line Not Found Absent 911.20 25.80* 1.806E+OO 1.239E+OO 1.239E+OO 26*. 76 OK 968. 97 15.80 1. 723E+OO 9.876E-01 9.876E-01 55.29 OK RA-228 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.906E+00 1.398E+OO 1.398E+OO 36.32 OK 794.95 4.25 2.004E+OO 2.288E+OO 2.288E+OO 55.90 OK 835.71 1. 61 l.930E+00 Line Not Found Absent 911. 20 25.80* 1.806E+OO 1.239E+OO 1.239E+OO 26.76 OK 968. 97 15.80 1. 723E+OO 9.876E-01 9.876E-01 55.29 OK TH-228 74.82 10.28 4.343E+OO l.412E+OO 1.412E+OO 62.97 OK 77 .11 17.10 4.580E+OO 1. 962E+OO 1. 962E+OO 24.48 OK 238.63 43.60* 5.102E+OO 1.165E+OO 1.165E+OO 13.16 OK 300.09 3.30 4.295E+OO Line Not Found Absent TH-230 609.32 45.49* 2.455E+OO 1.036E+OO l.036E+OO 21. 37 OK 1120.29 14.92 l.540E+OO Line Not Found Absent 1764.49 15.30 1.044E+OO 5.371E-01 5. 371E-01 78.31 OK PA-231 283.69 1. 70 4.487E+OO Line Not Found Absent Page 356 of 614 Nuclide Line Activity Report (continued) Page : 3 Sample ID : R405245015 Acquisition date 3-0CT-2016 04:47:45 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 301.36 5.35* 4.264E+OO 1.454E+OO l.454E+OO 100.66 OK TH-232 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11.27 3.906E+OO 1.398E+OO 1.398E+OO 36.32 OK 835.71 1. 61 1.930E+OO Line Not Found Absent 911.20 25.80* l.806E+OO 1.239E+OO l.239E+OO 26. 76 OK 968. 97 15.80 l.723E+OO 9.876E-01 9.876E-01 55.29 OK U-234 609.32 45.49* 2.455E+OO 1.036E+OO l.036E+OO 21. 37 OK 1120.29 14.92 1.540E+OO Line Not Found Absent 1764.49 15. 30* l.044E+OO 5.371E-01 5.371E-01 78.31 OK U-235 89. 96 3.47 5.608E+OO 1.920E+OO 1. 920E+OO 60.67 OK 93.35 5.60 5.777E+OO 1.829E+OO 1.829E+OO 62.91 OK 143.76 10. 96* 6.593E+OO Line Not Found Absent 163.33 5.08 6.362E+OO 3.560E-01 3.560E-01 206.89 OK 185.72 57.20 5.980E+OO 2.274E-01 2.274E-01 42.93 OK 205.31 5.01 5.647E+OO Line Not Found Absent PU-239 129.30 0.01* 6.656E+OO 5.828E+02 5. 828E+02 140.31 OK 375.05 0.00 3.598E+OO Line Not Found Absent 413.71 0.00 3.335E+OO 3.624E+03 3.624E+03 128.89 OK AM-243 43.53 5.90 4.883E-01 Line Not Found Absent 74.66 67.20* 4.343E+OO 2.161E-01 2.161E-01 62.97 OK ANH-511 . 511. 00 100.00* 2.815E+OO 1. 231E-01 1. 231E-01 91. 25 OK Flag: "*" = Keyline Page 357 of 614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:50:06.51 *******************************************************************************

  • GEL Laboratories LLC
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration . DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245015.CNF;l * *Acquisition date 3-0CT-2016 04:47:45 Sensitivity : 3.000 *
  • Detector ID GAM28 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.43 Haif life ratio : ***** *
  • Sample date 15-DEC-2015 14:02:00 Analyst initials: MXRl *
  • Sample ID R405245015 Sample Quantity 1.2058E+02 GRAM. *
  • Batch Number 1596387 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 . * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date l-AUG-2016 10:02:35 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1. 96-sigma) NA-22 6.270E-02 7.195E-02 K-40 1.762E+Ol 1. 824E+OO BA-137M 2.859E-01 1. 22 6E-01 CS-137 3.020E-01 l.295E-01 CE-144 7.652E-01 5.472E-01 TL-208 4.191E-01 1.060E-01 PB-212 1.165E+OO l.502E-01 BI-214 1.036E+OO 2.169E-01 PB-214 l.075E+oo* 2.310E-01 RN-222 1.036E+OO 2.169E-01 RA-224 l.236E-02 1. 541E+OO RA-226 1.036E+OO 2.169E-01 AC-228 1.239E+OO 3.249E-01 RA-228 l.239E+OO 3.249E-01 TH-228 1.165E+OO 1. 502E-01 TH-230 1.036E+OO 2.169E-01 PA-231 1.454E+OO 1.434E+OO TH-232 1.239E+OO 3.249E-01 U-234 1.036E+OO 2.169E-01 U-235 7.778E-02 2.186E-01 PU-239 5.828E+02 8.014E+02 AM-243 2.161E-01 l.333E-01 ANH-511 l.231E-01 1.lOlE-01 Non-Identified Nuclides Nuclide BE-7 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 358 of 614 Key-Line Activity (pCi/GRAM 8.015E+00 O.OOOE+OO -2.122E-02 -1.906E-01 0.000E+OO O.OOOE+OO -l.348E-02 K.L. Cnt Uncert (1. 96-sigma) l.474E+Ol 1.070E+41 2.737E-02 4.223E-01 1.113E+04 4.024E+02 7.397E-02 MDA (pCi/GRAM l.140E-01 6.323E-01 8.148E-02 8.608E-02 7.482E-01 6.453E-02 l.143E-01 1. 621E-01 l.400E-01 1. 621E-01 1.225E+OO l.621E-01 2.835E-01 2.835E-01 l.143E-01 1. 621E-01 8. 831E-01 2.835E-01 1.621E-01 3.951E-01 6.568E+02 1.073E-01 6.468E-02 MDA (pCi/GRAM 2.883E+Ol O.OOOE+OO '4.586E-02 7.754E-01 O.OOOE+OO 0.000E+OO 1. 412E-01 NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 -7.289E-03 4.776E-01 9.447E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF C0-57 5.433E-02 5.876E-02 l.109E-01 NOT IDENT. C0-58 l.838E-01 6. l 71E-01 l.268E+OO NOT IDENT. FE-59 -3. 296E+OO 6. 968E+00 l.254E+Ol NOT IDENT. C0-60 -l.924E-03 4.835E-02 9.367E-02 NOT IDENT. ZN-65 -l.435E-01 2.600E-01 3.868E-01 NOT IDENT. GE-68 l.055E+OO 2.856E+00 5.950E+OO NOT IDENT. AS-73 6.554E+OO l.lOOE+Ol 2.079E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.620E+03 O.OOOE+OO SHORT HLIF SE-75 9.495E-02 2.262E-01 4.439E-01 NOT IDENT. BR-77 O.OOOE+OO 3.297E+36 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 6.915E+02 O.OOOE+OO SHORT HLIF RB-83 -4.905E-01 7.735E-01 l.315E+OO NOT IDENT. KR-85 l.159E+Ol 9.875E+OO 2.000E+Ol NOT IDENT. SR-85 l.132E+OO 9.669E-01 1. 957E+OO NOT IDENT. RB-86 O.OOOE+OO 2.730E+04 0.000E+OO SHORT HLIF Y-88 -3.103E-02 l.739E-01 3.862E-01 NOT IDENT. Y-91 -l.077E+02 6.558E+02 1. 214E+03 NOT IDENT. NB-94 3.457E-06 4.000E-02 7.288E-02 NOT IDENT. NB-95 -9.379E-02 9.539E-01 l.838E+OO NOT IDENT. NB-95M -l.938E+OO 2.865E+00 4.519E+OO NOT IDENT. ZR-95 l.127E+OO 1. 761E+OO 3.183E+OO FAIL ABUN NB-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.012E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 3.777E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.188E+41 O.OOOE+OO SHORT HLIF RH-101 '6.400E-02 8.800E-02 7. 272E-02 FAIL ABUN RH-102 -4.638E-02 7.164E-02 l.194E-01 NOT IDENT. RU-103 -8.249E-01 6 .139E+00 l.123E+Ol FAIL ABUN RH-106 8.765E-02 5.683E-01 1. 081E+OO NOT IDENT. RU-106 8.765E-02 5.683E-01 1. 081E+OO NOT IDENT. AG-108M 1. 722E-02 3 .196E-02 6.362E-02 NOT IDENT. CD-109 1. 749E+OO 2.109E+OO 2.940E+OO FAIL ABUN AG-llOM -9.495E-02 1. 2 68E-01 2.214E-01 FAIL ABUN SN-113 -2.802E-02 3.018E-01 5.530E-01 NOT IDENT. CD-115 O.OOOE+OO 4.033E+38 0.000E+OO SHORT HLIF SN-ll 7M O.OOOE+OO 9.010E+04 O.OOOE+OO SHORT HLIF TE-123M 4.813E-02 l.648E-01 2. 717E-01 NOT IDENT. SB-124 1. 541E+OO 1. 782E+OO 4.750E+OO NOT IDENT. SB-125 6.109E-02 1. 248E-01 2.452E-01 FAIL ABUN TE-125M 2.086E+Ol 3.046E+02 5. 418E+02 NOT IDENT. I-126 0.000E+OO 9.626E+05 O.OOOE+OO SHORT HLIF SB-126 0.000E+OO 8.258E+05 O.OOOE+OO SHORT HLIF SN-126 l.127E-01 l.359E-01 l.942E-01 E,'AIL ABUN SB-127 O.OOOE+OO 6. 991E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.158E+09 O.OOOE'f-00 SHORT HLIF I-132 0.000E+OO 1. 960E+41 o .*oooE+oo SHORT HLIF TE-132 O.OOOE+OO 8.945E+25 O.OOOE+OO SHORT HLIF BA-133 2.370E-04 4.924E-02 8.337E-02 FAIL ABUN I-133 O.OOOE+OO 1. 743E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 8.153E-02 l.434E-01 FAIL ABUN CS-135 1. 079E-01 1. 58 6E-01 2.939E-01 NOT IDENT. I-135 O.OOOE+OO l.577E+41 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 2.422E+05 O.OOOE+OO SHORT HLIF CE-139 -l.682E-02 l.305E-01 2.232E-01 NOT IDENT. BA-140 O.OOOE+OO l.029E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.028E+05 O.OOOE+OO SHORT HLIF CE-141 -6.045E+OO 2.604E+Ol 4.433E+Ol NOT IDENT. CE-143 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF PM-144 -l.604E-03 6.935E-02 1. 2 61E-01 FAIL ABUN PR-144 -l.388E-01 6.00lE+OO 1. 091E+Ol NOT IDENT. PM-146 -5.862E-03 4.877E-02 9.017E-02 NOT IDENT. ND-147 0.000E+OO 2.320E+07 O.OOOE+OO SHORT HLIF PM-147 --:5 .112E+Ol l.078E+03 L 882E+03 NOT IDENT. . PM-149 O.OOOE+OO 5.488E+39 . 0.000E+bO SHORT HLIF EU-150 -2.183E-02 3.377E-02 5.184E-02 FAIL ABUN EU-152 -6.864E-02 l.087E-01 l.909E-01 NOT IDENT. GD-153 l.374E-01 2.074E-01 3. 680E...:01 NOT IDENT. EU-154 l.543E-01 l.770E-01 2.804E-01 FAIL ABUN EU-155 5.039E-02 l.368E-01 2.486E-01 FAIL ABUN TB-160 -7.208E-01 2.073E+OO 3.868E+OO FAIL ABUN H0-166M -6.233E-02 8.565E-02 L 181E-01 FAIL ABUN TM-171 -l.015E+Ol 2. 811E+Ol 4.930E+Ol NOT I DENT .. HF-172 3. 311E-02 2.846E-01 4.672E-01 FAIL ABUN LU-172 -l.773E-02 8.600E-02 l.627E-01 FAIL ABUN LU-176 -l.814E-02 2.949E-02 4.581E-02 FAIL ABUN HF-181 4.091E+OO 4. 601E+OO 9.469E+OO FAIL ABUN Page 359 of 614 TA-182 -7.514E-01 l .119E+OO 1. 911E+OO FAIL ABUN RE..:.183 -1. 248E+OO 3.469E+OO 6.138E+OO FAIL ABUN RE-184 6.169E+OO 3.170E+Ol 6.357E+Ol NOT IDENT. W-188 -3.359E+Ol 1. 319E+02 2.177E+02 NOT IDENT. IR-192 7.621E-02 4.840E-01 9.282E-01 FAIL ABUN HG-203 4.018E-01 2.576E+OO 4.906E+OO NOT IDENT. BI-207 3.847E-02 5.124E-02 l.129E-01 FAIL ABUN PB-210 2.961E-01 4.785E+OO 8.729E+OO NOT IDENT. BI-211 0.000E+OO 6.364E-01 8.898E-01 FAIL ABUN PB-211 -3.267E-Ol 8.928E-01 l.409E+OO NOT IDENT. BI-212 O.OOOE+OO 9.282E-01 l.444E+OO FAIL ABUN RN-219 l.195E-01 4.688E-01 8.955E-01 FAIL ABUN RA-223 5.606E-Ol 7.084E-01 l.324E+OO FAIL ABUN AC-227 -l.459E-02 2.803E-01 4.751E-01 NOT IDENT. TH-227 -l.459E-02 2.803E-01 4.751E-01 NOT IDENT. TH-229 -2.047E-01 5.282E-01 9.779E-01 FAIL ABUN TH-231 5.606E-01 7.084E-01 l.324E+OO FAIL ABUN PA-233 1. 671E-02. 6.563E-02 1. 272E-01 NOT IDENT. PA-234 -l.253E-01 2.660E-01 4,904E-01 NOT IDENT. PA-234M l.920E+00 4.286E+OO 9.529E+OO FAIL ABUN TH-234 4.254E-01 1. 750E+00 3.205E+OO FAIL ABUN NP-237 1. 671E-02 6.563E-02 l.272E-01 NOT IDENT. NP-238 0.000E+OO 4.889E+40 O.OOOE+OO SHORT HLIF U-238 4.254E-01 1. 750E+OO 3.205E+OO FAIL ABUN NP-239 -1. 32 6E-01 2.887E-01 4.885E-01 NOT IDENT. AM-241 .'..8.516E-02 1. 851E-01 3.235E-01 NOT IDENT. CM-243 -8.433E-02 l.228E-01 2.048E-01 NOT IDENT. BK-247 8.317E-02 l.524E-01 'NOT IDENT.

  • CM-247 2.007E-02 4.232E-02 8.274E-02 NOT IDENT. CF-249 -8.284E-03 4.738E-02 8.658E-02 FAIL ABUN CF-251 1. 311E,-02 l.302E-01 2.506E-01 NOT IDENT. Page 360of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:50:04.15 Nuclide Line Activity Report Nuclide Type: .Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error NA-22 1274.54 11 99 .. 94* 1.388E+OO 5.065E-02 6.270E-02 117.10 K-40 1460.82 373 10.66* 1.237E+OO 1. 762E+Ol 1.762E+Ol 10.56 CD-109 88.03 36 3.70* 5. 411E+OO 1.127E+OO 1.749E+OO 123.00 SN-126 64.28 ------9.60 3.124E+OO ------Line Not Found ------86.94 36 8.90 5. 411E+OO 4.686E-01 4.686E-01 123.00 87.57 36 37.00* 5.411E+00 l.127E-01 l.127E-01 123.00 BA-137M 661. 66 93 89.90* 2.30.4E+OO 2.806E-01 2.859E-01 43.76 CS-137 661. 66 93 85.10* 2.304E+OO 2.965E-01 3.020E-01 43.76 CE-144 80.12 ------1. 36 4.852E+OO ------Line Not Found ------133. 52 44 11.09* 6.653E+OO 3.755E-01 7.652E-01 72.97 TL-208 277.37 ------6.60 4.566E+OO ------Line Not Found ------583.19 145 85.00* 2.540E+OO 4.191E-01 4.191E-01 25.81 860.56 ------12.50 1.888E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 4 .138E+OO ------Line Not Found ------. 351. 06 232 12.92* 3.782E+00 2. 960E+OO 2. 960E+OO 21. 94 PB-212 74.82 160 10.28 4.343E+OO 2.235E+OO 2.235E+OO 38.73 77 .11 247 17.10 4.580E+OO 1. 962E+00 1. 962E+00 24.48 238.63 416 43.60* 5.102E+OO l.165E+00 1.165E+OO 13.16 300.09 ------3.30 4.295E+OO ------* Line Not Found ------BI-214 609.32 186 45.49* 2.455E+OO 1.036E+OO 1.036E+OO 21. 37 1120. 29 ------14.92 L 540E+OO ------Line Not Found ------1764.49 14 15.30 1.044E+OO 5. 371E-01 5.373E-01 78.31 PB-214 74.82 160 5.80 4.343E+OO 3. 961E+OO 3. 963E+OO 38.73 77 .11 247 9.70 4.580E+OO 3.459E+OO 3.460E+OO 24.48 87.09 36 3.41 5.411E+OO 1.223E+OO 1.223E+OO 123.00 242.00 87 7.25 5.053E+OO 1.479E+OO 1.480E+OO 54.58 295.22 189 18.42 4.347E+OO 1.472E+OO 1.473E+OO 25.34 351. 93 232 35.60* 3.782E+OO 1.074E+OO 1. 07 5E+OO 21. 94 RN-222 609.32 186 45.49* 2.455E+OO 1. 036E+OO 1.036E+OO 21. 37 1120.29 ------14.92 1.540E+OO ------Line Not Found ------1764.49 14 15.30 1.044E+OO 5. 371E-01 5.373E-01 78.31 RA-224 240.99 87 4.10* 5.053E+OO 2.616E+OO 2.616E+OO 54.58 RA-226 609.32 186 45.49* 2.455E+OO 1.036E+OO 1.036E+OO 21. 37 1120.29 ------14.92 1.540E+OO ------Line Not Found ------1764.49 14 15.30 1.044E+OO 5.371E-01 5.373E-OJ, 78.31 AC-228 105.21 ------1.10 6.315E+OO ------*Line Not Found ------338.32 99 11.27 3.906E+OO 1.398E+OO 1.398E+OO 36.32 794.95 31 4.25 2.004E+OO 2.288E+OO 2.288E+OO 55.90 835.71 ------1. 61 1.930E+OO ------Line Not Found ------911.20 93 25.80* 1.806E+OO 1.239E+OO 1.239E+OO 26.76 968. 97 43 15.80 l.723E+OO 9.876E-01 9.876E-01 55.29 RA-228 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 99 11. 27 3.906E+OO 1.398E+OO 1.398E+OO 36.32 794.95 31 4.25 2.004E+00 2.288E+OO 2. 28.8E+OO 55.90 835.71 ------1. 61 1.930E+OO ------Line Not Found ------911. 20 93 25.80* 1.806E+OO 1. 239E+00 1.239E+OO 26.76 968. 97 43 15.80 1.723E+OO 9.876E-01 9.876E.:..01 55.29 Page 361of614 Nuclide Line Activity Report (continued) Page : 2 Sample ID : R405245015 date 3-0CT-2016 04:47:45 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-228 74.82 160 10.28 4.343E+OO 2.235E+OO 2.235E+OO 38.73 77 .11 247 17.10 4.580E+OO 1.962E+OO 1. 962E+OO 24.48* 238'.63 416 43.60* 5.102E+OO 1.165E+OO 1.165E+OO 13 .16 300.09 ------3.30 4.295E+OO ------Line Not Found ------TH-230 609.32 186 45.49* 2.455E+OO 1.036E+OO 1.036E+OO 21. ;37 1120. 29 ------14.92 1.540E+OO ------Line Not Found ------1764.49 14 15.30 1. 044E+OO 5.371E-01 5.371E-01 78.31 PA-231 283.69 ------1. 70 4.487E+OO ------Line Not Found ------301.36 53 5.35* 4.264E+OO 1.454E+OO 1.454E+OO 100.66 TH-232 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 99 11.27 3.906E+OO 1.398E+OO 1.398E+OO 36.32 835.71 ------1. 61 1.930E+OO ------Line Not Found ------911.20 93 25.80* 1.806E+OO l.239E+00 1.239E+OO 26. 76 968. 97 43 15.80 1. 723E+OO 9.876E-01 9.876E-01 55.29 U-234 609.32 186 45.49* 2.455E+OO 1.036E+OO 1.036E+OO 21. 37 1120.29 ------14.92 l.540E+00 ------Line Not Found ------1764.49 14 15.30 1.044E+OO 5. 371E-01 5.371E-01 78.31 U-235 89. 96 60 3.47 5.608E+OO 1.920E+OO l.920E+OO 60.67 93.35 95 5.60 5.777E'+OO 1.829E+OO 1.829E+OO 62.91 143.76 ------10. 96* 6.593E+00 ------'Line Not Found ------163.33 18 5.08 6.362E+OO 3.560E-01 3.560E-01 206.89 185. 72 125 57.20 5.980E+OO 2.274E-01 2.274E-01 42.93 205.31 ------5.01 5.647E+00 ------Line Not Found ------PU-239 129.30 39 0.01* 6.656E+OO 5.828E+02 5.828E+02 140.31 375.05 ------0.00 3.598E+OO ------Line Not Found ------413.71 28 0.00 3.335E+OO 3.624E+03 3.624E+03 128.89 AM-243 43.53 ------5.90 4.883E-01 ------Line Not Found ------74.66 160 67.20* 4.343E+OO 3.419E.:...01 3.419E-01 38.73 ANH-511 511. 00 56 100.00* 2.815E+OO 1.231E-01 1. 231E-01 . 91. 25 Flag: "*" Key line Page 362 of 614 Page : 3 Summary of Nuclide Activity Sample ID : R405245015 Acquisition date 3-0CT-2016 04:47:45 Total number of lines in spectrum 45 Number of unidentified lines 8 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide NA-22 K-40 CD-109 SN-126 BA-137M CS-137 CE-144 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 PU-239 AM-243 ANH-511 Hlife 2.60Y 1.25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 284.91D 1. 41E'+10Y 7.04E+08Y l.41E+10Y 1600.00Y 1600.00Y 1600.00Y l.41E+l0Y 1600.00Y 1. 41E+10Y 1. 41E+10Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 2.45E+05Y 7.04E+08Y 24110. DOY 7370.00Y 1.00E+09Y Decay 1. 24 1. 00 1. 55 1. 00 1. 02 1. 02 2.04 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1: 00 . 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 5.065E-02 1. 762E+Ol 1.127E+OO 1.127E-01 2.806E-01 2. 965E-01 3.755E-01 4 .191E-01 2. 960E+OO 1.165E+OO 1.036E+OO 1. 074E+OO. 1.036E+OO 2.616E+OO 1.036E+OO 1.239E+OO l.239E+OO 1.165E+OO 1.036E+OO 1.454E+OO l.239E+OO 1.036E+OO 2.274E-01 5.828E+02 3.419E-01 1. 231E-01 6. 231E+02 6. 231E+02 Decay Corr pCi/GRAM 6.270E-02 1.762E+Ol 1. 749E+OO l.127E-01 2.859E-01 3.020E-01 7.652E-01 4.191E-01 2. 960E+OO 1.165E+OO 1.036E+OO 1.075E+OO 1.036E+OO 2.616E+OO 1.036E+OO l.239E+OO 1.239E+OO 1.165E+OO 1.036E+OO 1.454E+OO 1.239E+OO 1.036E+OO 2.274E-01 5.828E+02 3.419E-01 l.231E-01 6.242E+02 6.242E+02 82.22% Decay Corr 2-Sigma Error 7.342E-02 0.186E+Ol 2.152E+OO 1.386E-01 l.251E-01 1.322E-01 5.583E-01 l.082E-01 0.649E+OO 0.153E+OO 0.221E+OO 0.236E+OO 0.221E+OO 1.428E+00 0.221E+OO 0.332E+OO 0.332E+OO 0.153E+OO 0.221E+OO 1.463E+OO 0.332E+OO 0. 221E+OO 0.976E-01 8.178E+02 l.324E-01 l.124E-01 "M" Manually accepted 2-Sigma %Error 117 .10 10.56 123.00 123.00 43.76 43.76 72.97 25.81 21. 94 13.16 21. 37 21. 94 21. 37 54.58 21. 37 26.76 26. 76 13.16 21. 37 100.66 26.76 21. 37 42.93 140.31 38.73 91. 25 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 363of614 Flags K Unidentified Energy Lines Page : 4 Sample ID : R405245015 Acquisition date : 3-0CT-2016 04:47:45 It Energy Are.a Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 209.42 35 80 0.61 419.12 415 8 9.33E-03 96. 4 5.58E+00 T 0 252.99 35 46 2.30 506.34 503 7 9.24E-03 74.8 4.89E+OO T 0 272 .11 59 145 0.66 544.60 537 16 1. 60E-02 95.7 4.63E+00 T 0 328.79 23 63 0.79 658.05 652 10 6.16E-03 **** 4.00E+OO T 0 463.75 26 32 1. 86 928.17 923 9 7.21E-03 89.2 3.04E+OO T 0 573.84 11 22 0.80 1148.52 1144 7 3.08E-03 **** 2.57E+OO 0 616.91 14 20 0.98 1234.71 1229 9 3.84E-03 **** 2.43E+OO T 0 717. 59 17 16 5.03 1436.23 1428 13 4.76E-03 **** 2.17E+OO b 728.28 39 19 1. 93 1457.63 1451 13 1 llE-02 55.4 2.14E+OO T 0 741.84 13 13 1. 08 1484.76 1480 8 3.80E-03 **** 2. llE+OO 0 757:99 9 12 1. 38 1517.08 1512 8 2.44E-03 **** 2.08E+OO T 0 823.27 4 16 0.99 1647.74 1642 9 1.06E-03 **** l.95E+OO 0 862.19 33 25 0.74 1725.64 1719 14 9.55E-03 73.2 l.89E+OO 0 1002.02 4 5 1.14 2005.51 2002 7 l.25E-03 **** 1. 68E+OO T 0 1121.91 38 18 1. 53 2245.47 2238 16 1. lOE-02 59.9 1.54E+OO T 0 1165.75 7 12 0.62 2333.22 2328 9 2.03E-03 **** 1.49E+OO 0 1377.98 18 0 2.50 2758.00 2750 15 5.28E-03 45.9 1.30E+OO 0 1384.86 16 4 2.45 2771.76 2765 14 4.79E-03 66.9 1.30E+OO T 0 1501.25 5 3 0.64 3004. 72 2995 13 l.57E-03 **** 1. 21E+OO .Flags: "T" = Tentatively associated Page 364 of 614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:50:19.74 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245015.CNF;l *
  • Acquisition date 3-0CT-2016 04:47:45 Sensitivity 3.000 *
  • Detector ID GAM28 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.43 Half life ratio : ***** *
  • Sample date 15-DEC-2015 14:02:00 Nuclide Library : SOLID *
  • Sample ID R405245015 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.2058E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date l-AUG-2016 10:02:35 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
  • Combined Critical Level Report NOTE: Not all "Identif{ed Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide NA-22 K-40 BA-137M CS-137 .CE-144 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 PU-239 AM-243 ANH-511 Le (pCi/GRAM 4.951E-02 2.525E-01 3.659E-02 3.865E-02 3.504E-01 2.834E-02 5.333E-02 7.349E-02 6.369E-02 7.349E-02 5.717E-01 7.349E-02 l.237E-01 l.237E-01 5.333E-02 7.347E-02 4.043E-01 l.237E-01 7.347E-02 1.857E-01 3.079E+02 5.066E-02 2.933E-02 Non-Identified Nuclides Nuclide BE-7 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 365of614 Le (pCi/GRAM 1.318E+Ol 0.000E+OO 1.470E-02 3.361E-01 O.OOOE+OO O.OOOE+OO 6.223E-02 4 .113E-01 NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT.

MN-56 C0-57 C0-58 FE-59 C0-60 zN.:..65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 366 of 614 O.OOOE+OO 5.228E-02 5.586E-01 5.362E+OO 3.986E-02 1.687E-01 2.627E+OO 9.767E+OO O.OOOE+OO 2.053E-01 O.OOOE+OO O.OOOE+OO 5.860E-01 9.264E+OO 9.069E-01 O.OOOE+OO 1.368E-01 5.358E+02 3.260E-02 8.214E-01 2 .101E+OO 1.414E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 6.000E+OO 3. 411E-02 5.236E-02 5.044E+OO 4.798E-01 4.798E-01 2.888E-02 1.404E+OO 9.655E-02 2.546E-01 O.OOOE+OO O.OOOE+OO 1.271E-01 1.904E+OO 1.118E-01 2.539E+02 O.OOOE+OO O.OOOE+OO 9.283E-02 O.OOOE+OO O.OOOE+OO 0. OOOE+OO. O.OOOE+OO 3.783E-02 O.OOOE+OO 6.527E-02 1.355E-01 O.OOOE+OO O.OOOE+OO 1.042E-01 O.OOOE+OO O.OOOE+OO 2.078E+Ol O.OOOE+OO 5.635E-02 4.876E+OO 4.041E-02 0. OOOE+OO* 8.846E+02 O.OOOE+OO 2.364E-02 8.679E-02 1. 725E-01 1.218E-01 1.171E-01 1. 685E+OO 5.187E-02 2.305E+Ol 2.182E-dl 6.990E-02 2.075E-02 4.307E+OO 8.282E-01 SHORT HLIF NOT IDENT. NOT IDENT .. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 367of614 2.869E+OO 2.804E+Ol 1. 000E+02 4. 251E-Ol 2.274E+OO 4.929E-02 4.104E+OO 4.277E-01 6.381E-01 6.630E-01 4.099E-01 6.093E-Ol 2.190E-01 2.190E-01 4.558E-01 6.093E-01 5.828E-02 2.052E-01 4.168E+OO 1. 525E+OO 5.828E-02 O.OOOE+OO 1.525E+OO 2.278E-01 1. 521E-01 9.566E-02 7.020E-02 3.790E-02 3. 960E-02 1.172E-01 FAIL ABUN. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:50:25.74 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245015.CNF;l * *Acquisition date .3-0CT-2016 04:47:45 Sensitivity : 3.000 *
  • Detector ID GAM28 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.43 Half life ratio : ***** *
  • Sample date 15-DEC-2015 14:02:00 Nuclide Library : SOLID *
  • Sample ID R405245015 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity 1.2058E+02 GRAM *
  • Quantity Err ( % ) 1. 6587E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 1-AUG-2016 10:'02:35 Eff. Geometry : CAN *'
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) NA-22 6.270E-02 7.198E-02 K-40 1. 762E+Ol 2.045E+OO BA-137M 2.859E-01 l.232E-01 CS-137 3.020E-01 l.302E-01 CE-144 7.652E-01 5.488E-01 TL-208 4.191E-01 1.075E-01 PB-212 1.165E+OO l.626E-'-01 BI-214 1.036E+OO 2.215E-01 PB-214 1.075E+OO 2.354E-01 RN-222 1.036E+OO 2.215E-01 RA-224 1. 236E-02 1. 551E+OO RA-226 1.036E+OO 2.215E-01 AC-228 1.239E+OO 3.311E-01 RA-228 1.239E+OO 3. 311E-01 TH-228 1.165E+OO l.626E-01 TH-230 1.036E+OO 2.214E-01 PA-231 1.454E+OO 1.467E+OO TH-232 1.239E+OO 3. 311E-01 U-234 1.036E+OO 2.214E-01 U-235 7.778E-02 2.186E-01 PU-239 5.828E+02 8.019E+02 AM-243 2 .161E-01 1.350E-01 ANH-511 1.231E-01 l.102E-01 Non-Identified Nuclides Nuclide BE-7 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 368 of 614 Key-Line Activity (pCi/GRAM 8.015E+OO 1.000E+41 -2.122E-02 -l.906E-01 2.602E+03 -4.900E+02 -1.348E-02 K.L Act error ( 1. 96-sigma) l.474E+Ol l.151E+41 2.740E-02 4.224E-01 l .113E+04 4.030E+02 7.398E-02 TPU (1. 96-sigma) 7.198E-02 2.045E+OO 1.232E-01 l.302E-01 5.488E-01 1. 07 5E-01 1. 626E-01 2.215E-01 2.354E-01 2.215E-01 1. 551E+OO 2.215E-01 3.3f1E-01 3. 311E-01 1. 6'26E-01 2.214E-01 1.467E+OO 3. 311E-01 2.214E-01 2.186E-01 8.019E+02 1.350E-01 1.102E-01 TPU ( 1. 96-sigma) ,1.518E+Ol O.OOOE+OO 2.902E-02 4. 311E-01 l .119E+04 4.595E+02 7.423E-02 NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 -7.289E-03 4.776E-01 4.776E-01 NOT IDENT. MN-56 -1.000E+41 6.552E+42 O.OOOE+OO SHORT HLIF C0-57 5.433E-02 5.881E-02 6.371E-02 NOT IDENT. C0-58 1.838E-Ol 6 .171E-01 6.226E-01 NOT IDENT. FE-59 -3. 296E+OO 6. 972E+OO 7.129E+OO NOT IDENT. C0-60 -l.924E-03 4.835E-02 4.836E-02 NOT IDENT. ZN-65 -1.435E-01 2.601E-01 2.680E-01 NOT IDENT. GE-68 l.055E+OO .2. 857E+OO 2. 896E+OO NOT IDENT. AS-73 6.554E+OO 1.108E+Ol l.147E+Ol NOT IDENT. AS-74 3.747E+03 5.629E+03 5.877E+03 SHORT HLIF SE-75 9.495E-02 2.263E-01 2.303E-Ol NOT IDENT. BR-77 2.557E+37 2.160E+38 O.OOOE+OO SHORT HLIF SR-82 -3.595E+02 6.917E+02 7.104E+02 SHORT HLIF RB-83 -4.905E-01 7.764E-01 8.073E-01 NOT IDENT. KR-85 1.159E+Ol 9.886E+OO 1.118E+Ol NOT IDENT. SR-85 1.132E+OO 9.680E-01 l.094E+OO NOT IDENT. RB-86 3.648E+03 2.730E+04 2.735E+04 SHORT HLIF Y-88 -3.103E-02 1.739E-01 1.745E-01 NOT IDENT. Y-91 -l.077E+02 6.558E+02 6.576E+02 NOT IDENT. NB-94 3.457E-06 4.000E-02 4.000E-02 NOT IDENT. NB-95 -9.379E-02 9.539E-01 9.549E-01 NOT IDENT. NB-95M -1.938E+OO 2.869E+OO 2.999E+00 NOT JDENT. ZR-95 1.127E+OO 1. 761E+OO 1.833E+OO FAIL ABUN NB-97 1.000E+41 3.822E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 l.013E+41 O.OOOE+OO SHORT HLIF M0-99 l.163E+31 3.778E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 l.192E+41 O.OOOE+OO SHORT HLIF RH-101 6.400E-02 8.876E-02 9.333E-02 FAIL ABUN RH-102 -4.638E-02 7.174E-02 7.473E-02 NOT IDENT. RU-103 -8.249E-01 6.139E+OO 6.150E+OO FAIL ABUN RH-106 8.765E-02 5.684E-01 5.697E-01 NOT IDENT. RU-106 8.765E-02 5.684E-01 5.697E-01 NOT IDENT. AG-108M 1.722E-02 3 .196E-02 3.289E-02 NOT IDENT. CD-109 1. 749E+OO 2 .114E+OO 2.256E+OO FAIL ABUN AG-llOM -9.495E-02 l.269E-01 . 1.339E-01 FAIL ABUN SN-113 -2.802E-02 3.018E-01 3.020E-01 NOT IDENT. CD-115 -2.194E+38 4.051E+38 O.OOOE+OO SHORT HLIF SN-ll 7M -l.448E+04 9.012E+04 9.036E+04 SHORT HLIF TE-123M 4.813E-02 l.648E-01 1.662E-01 NOT IDENT. SB-124 1. 541E+OO 1.784E+OO 1.915E+OO NOT IDENT. SB-125 6.109E-02 l.248E-01 1.278E-01 FAIL ABUN TE-125M 2.086E+Ol 3.046E+02 3.048E+02 NOT IDENT. I-126 -1.023E+05 9.627E+05 9.638E+05 SHORT HLIF SB-126 -3.259E+05 8.280E+05 8.409E+05 SHORT HLIF SN-126 l.127E-01 1. 360E-01 1.452E-01 FAIL ABUN SB-127 -1. 671E+21 7.342E+21 0.000E+OO SHORT HLIF I-131 -5.321E+08 3.158E+09 3.167E+09 SHORT HLIF I-132 1. 000E+41 2.028E+42 O.OOOE+OO SHORT HLIF TE-132 -3.656E+25 9.062E+25 O.OOOE+OO SHORT HLIF BA-133 2.370E-04 4.924E-02 4.924E-02 FAIL ABUN I-133 1. 000E+41 2.481E+41 O.OOOE+OO SHORT HLIF CS-134 1. 488E-01 8.178E-02 l.058E-01 FAIL ABUN CS-135 1.079E-01 1.588E-01 l.660E-01 NOT IDENT. I-135 1.000E+41 6.797E+41 O.OOOE+OO SHORT HLIF CS-136 -2.972E+05 2.444E+05 2.787E+05 SHORT HLIF CE-139 -l.682E-02 1.305E-01 l.307E-01 NOT IDENT. BA-140 6.050E+04 1.029E+06 l.030E+06 SHORT HLIF LA-140 -1.182E+05 3.028E+05 3.075E+05 SHORT HLIF CE-141 -6.045E+OO 2.604E+Ol 2.618E+Ol NOT IDENT. CE-143 l.000E+41 2.529E+41 O.OOOE+OO SHORT HLIF PM-144 -1.604E-03 6.935E-02 6.935E-02 FAIL ABUN PR-144 -l.388E-01 6.00lE+OO 6. OOlE+OO NOT IDENT. PM-146 -5.862E-03 4.877E-02 4.884E-02 NOT IDENT. ND-147 l.136E+07 2.321E+07 2.377E+07 SHORT HLIF PM-147 -5 .112E+Ol 1.078E+03 1.078E+03 NOT IDENT. PM-149 *-1. 673E+39 5.500E+39 O.OOOE+OO SHORT HLIF EU-150 -2.°183E-02 3.379E-02 3.519E-02 FAIL ABUN EU-152 -6.864E-02 1.088E-01 1.131E-01 NOT IDENT. GD-153 1.374E-01 2.075E-01 2 .166E-01 . NOT IDENT. EU-154 1.543E-01 1. 771E-01 l.903E-01 FAIL ABUN EU-155 5.039E-02 1.368E-01 l.387E-01 FAIL ABUN TB-160 -7.208E-01 2.073E+OO 2.099E+OO FAIL ABUN H0-166M -6.233E-02 8. 571E-02 9.020E-02 FAIL ABUN TM-171 -l.015E+Ol *2. 812E+Ol 2.849E+Ol NOT IDENT. HF-172 3.311E-02 2.846E-01 2.850E-01 FAIL ABUN LU-172 -l.773E-02 8.602E-02 8.639E-02 FAIL ABUN LU-176 -l.814E-02 2.950E-02 3.061E-02 FAIL ABUN HF-181 4.091E+OO 4.605E+OO 4. 960E+OO FAIL ABUN Page 369of614 TA-182 -7.514E-01 1.119E+OO l.169E+OO FAIL ABUN RE-183 -1.248E+OO 3 .. 474E+OO 3.520E+OO FAIL ABUN RE-184 6.169E+OO 3.174E+Ol 3.186E+01 NOT IDENT. w-188 -3.359E+Ol l.320E+02 1.328E+02 NOT IDENT. IR-192 7.621E-02 4.840E-01 4.852E-01 FAIL ABUN HG.:...203 4.018E-01 2.576E+OO 2.583E+OO NOT IDENT. BI-207 3.847E-02 5.126E-02 5. 411E-02 FAIL ABUN PB-210 2. 961E-01 4.785E+OO 4.787E+OO NOT IDENT. BI-211 2. 960E+OO 6.502E-01 l.484E+OO FAIL ABUN PB-211 -3.267E-01 8.929E-01 9.0SOE-01 NOT IDENT. BI-212 1. 709E+OO 9.323E-01 l.210E+OO FAIL ABUN RN-219 1.195E-01 4.690E-01 4. 721E-01 FAIL ABUN RA-223 5.606E-01 7.092E-01 7.529E-01 FAIL ABUN AC-227 -l.459E-02 2.803E-01 2.804E-01 NOT IDENT. TH-227 -l.459E-02 2.803E-01 2.804E-01 NOT IDENT. TH-229 -2.047E-01 5.283E-01 5.363E-01 FAIL ABUN TH-231 5.606E-01 7.092E-01 7.529E-01 FAIL ABUN PA-233 1. 671E-02 6.564E-02 6.607E-02 NOT IDENT. PA-234 -1.253E-01 3.022E-01 3.074E-01 NOT IDENT. PA-234M 1.920E+OO 4.287E+OO 4.374E+OO FAIL ABUN TH-234 4.254E-01 1. 752E+OO 1. 763E+OO FAIL ABUN NP-237 1. 671E-02 6.564E-02 6.607E-02 NOT IDENT. NP-238 2.456E+40 4.890E+40 O.OOOE+OO SHORT HLIF U-238 4.254E-01 l.752E+OO 1. 763E+OO FAIL ABUN NP-239 -1. 326E-01 2.889E-01 NOT IDENT. AM-241 -8. 516E...:.02 1.852E-01 1. 891E-01 NOT IDENT. CM-243 -8.433E-02 1.231E-01 l.288E-01 NOT IDENT. BK-247 -2.954E-02 8.338E-02 8.444E-02 NOT IDENT. CM-247 2.007E-02 4.246E-02 4.341E-02 NOT IDENT. CF-249 -8.284E-03 4.739E-02 4.753E-02 FAIL ABUN CF-251 1. 311E-02 1.302E-01 1.304E-01 NOT IDENT. Page 370 of 614

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT
  • ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 66.6899 879.38 118.0664 482.18 62.9878 45.60 63.8882 87.57 122. 6371 133.52 72. 7222 46.54 76.6296 87.09 122.6676 264.66 64.8372 49. 72 0.0000 87.57 136.4026 122.06 68 .1184 51. 35 67.9370 88.03 136.5033 140.51 0.0000 51. 87 70.1419 88.34 104.7052 143.76 65.0288 52.39 74.4794 193.51 104. 7269 144.24 66.2929 52.97 71.3792 89.96 100.4113 145.44 81.1374 53.44 62.9216 90.64 91.3812 152.43 76.8293 125.81 58.7367 91.11 0.0000 153.25 0.0000 57.36 0.0000 63.29 91.6608 154.21 80.7065 57.53 64.5531 143.76 91. 7688 156.02 0.0000 57.98 77.5366 94.56 91. 9403 158.56 0.0000 1093.63 84.2235 94.65 91. 9525 159.00 63.2421 57.98 95. 0311 94.67 91.9556 162.33 71.8215 59.54 95.0741 94.87 91.9836 162.66 0.0000 60. 96 84.5148 97.43 53.'8661 163.33 71. 8994 61.17 99.7266 311. 90 82.0764 165.86 69.1587 62. 93 127.2747 946.00 82.0775 176.31 73.7257 63.29 105.5937 . 99. 53 69.4743 1048.07 0.0000 63.58 96.9404 1221. 41 67.2160 177.52 67.8768 64.28 88*.3484 265.00 74.3789 739.50 0.0000 66.73 121.6459 103.18 94.2934 181.52 71. 5577 67.24 98.7280 103.37 85.0044 711. 68 63. 2196 67.68 91.1257 116.74 85.0044 185. 72 63.3009 67.75 91.1371 105.21 77.0570 193.51 71. 5367 69.67 93.6717 105.31 77.0678 /197.03 70.9109 70.83 89.8233 106.12 67.8046 127.23 70.9759 72. 81 107.8841 106.47 79.5350 306.78 74.7041 279.20 112.3293 109.28 72.8048 203.43 64.3751 72.87 112. 3293 111. 00 81.2184 205.31 58.8222 74.66 96.7519 228.16 0.0000 210.85 64.3738 74.82 96.7791 114. 06 73.2858 215.65 65.0895 1063.66 96.8050 116.30 0.0000 222 .11 66.3437 238.63 97 .1714 116.74 74.7370 290.67 58.6329 351.93 97 .1714 119. 76 61. 9353 177.52 5,8.6476 78.74 97.0735 121.12 83.5234 228.16 0.0000 79.69 85.2652 121. 22 83.5341 228.18 57.7981 80.12 86.8248 121.78 68.0706 235.69 75 .1671 80.19 0.0000 122.06' 65.7061 256.23 68.4706 80.57 86.8914 122.92 70.5630 238.63 64.5857 81. 00 83.9561 123.07 74.1657 238.98 0.0000 81. 07 83. 9664 123.68 79.8106 240.99 64.7109 81. 75 96. 0716 125.81 64.0230 242.00 64.7644 323.87 101. 6716 127.23 75.3621 344.28 59.4983 84.00 102.8374 127. 91. 75.4272 252.40 0.0000 85.43 99.6815 129.30 75.5584 252.80 40. 8311 86.55 118. 0204 131.20 29.0061 254.15 0.0000 Page 371 of 614 ENERGY MDA COUNTS ENERGY* MDA COUNTS ENERGY MDA COUNTS 256.23 47.7653 351.93 34.0465 583.19 17.5358 260.90 0.0000 507.63 0.0000 584.27 17.5436 264.66 43.0422 356.01 32.1823 595.83 0.0000 264.80 46.7106 364.49. 0.0000 600.60 26.5000 265.00 52.2141 366.42 0.0000 602.52 0.0000 268.22 34.4353 372.51 25.6128 604. 72 31.5233 269.46 50.5532 129.30 46.3708 607.14 36.5369 270.03 50.5744 377.52 34.5827 609.32 31. 5836 271.23 50.6203 383.85 40.6630 497.08 31.5975 273.65 0.0000 388.16 41. 7 599 433.94 13.3262 356.01 41. 5778 388.63 0.0000 696.49 16.6833 277.37 45.7688 391.69 46.8279 620.36 20.0391 277.60 62.4216 400.66 37.0550 621. 93 18.9382 278.00 47.1775 401.81 35.0748 667.71 0.0000 279.20 50.9224 402.40 32.0794 631.29 25.7206 279.54 56.4925 404.85 37.6450 453.88 21.2644 279.70 57.4249 410.95 34.2490 595.83 0.0000 280.46 50.9706 413. 71 34.8060 635.95 20.1672 283.69 40.8731 414.70 0.0000 636.99 0.0000 364.49 0.0000 423. 72 0.0000 645.85 24.7473 285.41 43. 7144 404.85 32.5228 884.68 22.0391 285.90 0.0000 427.87 28.4694 657.90 0.0000 402.40 40.9859 433.94 24.4824 661. 66 26.0350 29'0. 67 43.4140 333.97 30. 69'27 664.57 0.0000 293.27 0.0000 453.88 26.8040 666.33 0.0000 295.22 39.3408 463.37 23.8278 720. 70 0.0000 295. 96 39.3613 468.07 27.4162 667.71 0.0000 298.58 33.8005 685.70 0.0000 677.62 21.6410 299.98 39.4733 475.06 40.6448 685.70 0.0000 300.09 39.4758 476.78 31. 2921 695.00 0.0000 300.13 39.4767 477.60 29.2179 696.49 24.0916 301.36 39.5109 482.18 20.9176 696. 51 24.0916 302.85 39.5519 1596. 21 0.0000 697.00 0.0000 304.50 39.5980 527.90 0.0000 697.30 18.3613 537.26 0.0000 497.08 28.4469 697.49 17.2150 306.78 42.4933 505.52 14.2817 702.65 24.1479 316.51 48.2151 507.63 0.0000 706.68 24.1838 311. 90 36.0092 511. 00 31. 8204. 711. 68 29.4211 316.51 37.0735 514.00 31.8652 720.70 0.0000 531. 02 0.0000 514.00 31.8652 721. 93 0.0000 320.08 0.0000 520.40 31. 9617 1690.97 9.2682 427.87 44.8141 238.98 0.0000 722. 91 9.2686 323.87 30.0920 522.65 0.0000 1274.44 12.1667 325.23 48.7640 527.90 0.0000 724 .19 12.1705 328.76 0.0000 528.26 29.9414 727. 33 13.9253 388.16 37.4901 520.40 18.1898 733.00 10.4656 333.97 49.0452 529.87 0.0000 735.93 16. 2969 334.37 41.8433 531.02 0.0000 737.46 17.4707 338.28 39.5386 537.26 0.0000 739.50 0.0000 911. 20 39.5394 546.56 0.0000 747.24 16.6557 340.48 36.2144 552.55 18.3814 748.06 16.6604 340.55 0.0000 563.25 13.0376 752.31 17.5641 344.28 44.5307 795.86 17.9744 753.82 0.0000 345.93 38.3754 569.50 19.6099 756.73 19.7025 351.06 34.0280 569.70 19.6121 756.80 19.7032 Page 372of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 763.94 17.6367 984.45 0.0000 1596.21 0.0000 765.81 22.9428 996.26 13.0166 1620.50 3.2944 766.42 25.5954 1001.03 6.0826 1621. 92 5.4922 766.84 22.0680 1002.74 15.2139 1678.03 0.0000 772.60 0.0000 1004.73 15.2227 1690.97 1.1130 776.52 0.0000 1021.30 0.0000 1750.46* 0.0000 777.92 0.0000 1025.87 0.0000 1764.49 2.7076 778.90 15.0695 1028.54 0.0000 1770.23 8.1312 783.70 0.0000 846.77 10.5629 1771.35 .3.6146 727.33 20.4338 1038.76 0.0000 1791.20 0.0000 792.07 15.6723 1046.59 11.5518 1808.65 4.5486 794.95 11. 5876 1048.07 0.0000 846.75 0.0000 795.86 11. 5912 1049.04 20.2284 1836.06 2.7423 801.95 17.3587 621. 93 8.6726 810.06 15.2309 1063.66 8.7039 810.29 15.2319 1077.00 0.0000 810.45 15.2325 1077.34 11. 6484 810.76 15.2345 1085.87 16.5403 815.77 0.0000 1093.63 14.6246 818.51 0.0000 1099.45 16.5995 832.01 11. 7325 1112. 07 12.7366 834.85 20.7764 1112.84 15.6787 835.71 21.6863 1115. 54 23.5342 1260.41 0.0000 609.32 12.7635 846.75 0.0000 889.28 12.7643 846.77 15.4166 1121.30 12.7667 856.80 0.0000 1129. 67 12.3727 860.56 15.4856 1131.51 0.0000 702.65 18.2794 1147.95 0.0000 873.19 18.2916 1173.23 7.9619 529.87 0.0000 1177.95 10.9604 879.38 19.2440 1189.05 17.9846 880.51 12.8340 1204.77 21.0641 883.24 14.6797 1221. 41 22.1571 884.68 24.7835 1231. 02 18.1714 889.28 19.3036 1235.36 0.0000 903.'28 9.2081 1238.28 16.1807 898.04 1260.41 0.0000 900.72 12.9152 1271.87 9.7863 903.28 16.6185 1274.44 14.6883 911. 20 15.7336 1274.54 14.6892 912.08 15.7378 1099.45 13.3134 923. 98, 0.0000 1298.22 0.0000 926.50 21. 3856 1312 .11 0.0000 929 .11 13.9581 1332.49 11. 3719 937.49 13.9938 1362.66 0.0000 944.13 0.0000 1365.19 6.2487 946.00 13.0938 .1368.63 0.0000 949.00 19.6587 1384.29 3.3469 954.55 0.0000 1408.0i 8.4106 962. 31 16 .1112 1457.56 0.0000 964.08 21.0629 1460.82 5.3165 966 .17 21. 0759 696. 51 1. 0696 968. 97 17.8914 1505.03 *3.4340 983.53 0.0000 1584.12 Page 373 of 614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:50:56.68 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road* *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245016.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM36.CNF;52 Background date : Z-OCT-2016 11:02:08. Sample date 15-DEC-2015 14:06:00 Acquisition date : 3-0CT-2016 04:48:08. Sample ID R405245016 Sample quantity : 1.25408E+02 GRAM Detector name : GAM36 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.35 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596387 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 0 2 2 3 2 4 0 5 0 6 4 7 4 8 0 9 0 10 0 11 6 12 6 13 4 14 4 15 2 16 2 17 0 18 0 19 0 20 4 21 4 22 1 23 1 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 .34* 0 Page 374of614 Energy 54.00 74.69* 77.03* 84.27* 87 .11 89.88 92.88* 105.69 129.44 185.91* 209.28 211. 42 238.70* 241.52 295.22* 300.26 312.57 328.29* 338.71 351.99* 354.27 460.15 462.89 487.73 510.87* 583.07* 609.46* 662.00 727.39 757.19 761.30 802.59 861.23 911.21* BACKGROUND SAMPLE PEAK REPORT Area Bkghd FWHM Channel Left Pw Cts/Sec %Err Fit 17 93 156 23 77 52 58 34 28 92 40 14 286 85 115 27 16 22 35 162 16 17 21 9 19 80 104 17 13 12 9 19 15 51 86 101 109 93 81 52 102 89 111 95 48 34 38 39 23 27 15 48 60 33 25 18 14 13 40 22 15 ', 14 15 12 3 3 11 11 1. 22 1. 04 1. 04 0.79 1. 24 0.92 1.31 1.10 1. 08 1.29 1.29 1. 35 1. 04 1. 62 1. 41 1. 37 1.16 0.75 0.86 1. 52 1. 49 1. 46 1. 46 0.57 1. 08 1. 33 1. 23 0.87 1. 30 2.46 0.83 0.61 0.95 1. 33 107.97 149.36 154.02 168.52 174.20 179.73 185.74 211.36 258.86 371.81 418. 55 422.82 477.38 483.03 590.43 600.51 625 .13 656.55 677.40 703.97 708.52 920.26 925.73 975.42 1021.68 1166. 06 1218.85 1323.90 1454.65 1514.24 1522.46 1605.01 1722.25 1822.18 106 144 144 166 172 178 178 208 256 365 414 414 472 472 584 584 623 . 654 672 697 697 912 912 969 1016 1160 1214 1318 1449 1509 1519 1599 1716 1816 7 4. 72E-03 15 2.58E-02 15 4.33E-02 6 6.48E-03 6 2.13E-02 16 1. 43E-02* 16 l.61E-02 9 9.55E-03 9 7. 71E-03 14 2.55E-02 12 1. llE-02 12 3.92E-03 20 7.94E-02 20 2.36E-02 20 3.20E-02 20 7.42E-03 5 4.44E-03 8 6. OlE-03 10 9. 72E-03 17 4.50E-02 17 4.46E-03 23 4.65E-03 23 5.92E-03 9 2.37E-03 13 5.38E-03 11 2.22E-02 10 2.90E-02 11 4.70E-03 10 3.61E-03 10 3.25E-03 6 2.55E-03 11 5.33E-03 12 4.07E-03 11 1.40E-02 93.o 21.1 3.17E+OO 13.6 70.1 21. 9 24. 3 1. 25E+OO 35.3 52.1 70.8 25.5 35.4 l.81E+OO 73.4 6.9 l.53E+OO 23.3 12.4 2.07E+OO 37.0 44.1 61.1 44.7 9.6 6.78E+00 88.7 49 .1 *8. 54E-01 41. 6 84.7 81. 5 16.3 12.5 49.0 62.3 63.5 44.3 28.3 53.7 19.5 Peak Search Report (continued) Page : 2 Sample ID : R405245016 Acquisition date 3-0CT-2016 04:48:08 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 920.49 11 5 1. 08 1840.75 1835 12 2.93E-03 55.2 36 0 934.50 16 2 0.76 1868.76 1864 9 4.39E-03 30.4 37 1 964.76 22 9 1. 84 1929.24 1923 23 6. 38.3 2.29E+00 38 1 969.09 36 16 1. 85 1937.92 1923 23 1. OlE-02 24.4 39 0 1031.82 16 5 1. 86 2063.32 2059 9 4.31E-03 35.4 40 0 1121.17* 18 14 1. 50 2241.95 2237 13 5.07E-03 48.0 41 0 1149.84 10 4 0.80 2299.26 2295 7 2.64E-03 46.0 42 o. 1174.31 16 0 1. 03 2348.19 2345 8 4.44E-03 25.0 43 0 1237.79 23 3 2.55 2475.08 2468 14 6.27E-03 27.4 44 0 1461.11* 196 0 1. 76 2921. 48 2916 12 5.44E-02 7.2 45 0 1764. 96* 14 0 1. 47 3528.78 3523 11 3.82E-03 31.2 Flag: "*" = Peak. area was modified by background subtraction Page 375 of 614 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 05:50:58 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245016.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 15-DEC-2015 14:06:00 R405245016 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 04:48:08 125.41 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA36 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Page 376 of 614 Nuclide PB-214 PB-214 PB-214 PB-214 PB-21'4 PB-214 PB-214 PB-214 PB-214 PB-214 Line 87.09 87.09 87.09 87.09 87.09 242.00 74.82 74.82 74.82 351.93 Detector geometry: Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide EU-155 SN-126 SN-126 CD-109 TH-229 RA-224 AM-243 TH-228 PB-212 BI-211 Line 86.55 86.94 87.57 88-. 03 88.47 240.99 74.66 74.82 74.82 351.06 CAN 0 01:00:00.35 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : R405245016 Acquisition date 3-0CT-2016 04:48:08 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 6.546E-01 1.595E+Ol 1.595E+Ol 14.45 OK AS-73 53.44 10.30* 1.564E+OO 7.267E-01 9.086E+OO 186.02 OK CD-109 88.03 3.70* 4.288E+OO 1.976E+OO 3.067E+OO 73.58 OK SN-126 64.28 9.60 2.567E+OO Line Not Found Absent 86.94 8.90 4.288E+OO 8.215E-01 8.215E-01 73.58 OK 87.57 37.00* 4.288E+OO 1.976E-Ol l.976E-01 73.58 OK BA-137M 661. 66 89.90* 1.334E+OO 8.434E-02 8. 591E-02 97. 96 OK CS-137 661.66 85.10* 1.334E+OO 8.910E-02 9.076E-02 97. 96 OK EU-155 86.55 30.70 4.288E+OO 2.382E-01 2.677E-01 73.58 OK 105.31 21.10* 4.943E+00 2.188E-01 2.460E-01 104.18 OK TL-208 277.37 6.60 3. 041E+OO Line Not Found Absent 583.19 85.00* 1. 496E+00 3.785E-01 3.785E-01 32.56 OK 860.56 12.50 1.057E+OO 6.519E-01 6.519E-01 107.47 OK PB-212 74.82 10.28 3.472E+OO 9.916E-01 9.916E-01 77.64 OK 77 .11 17.10 3.649E+OO 1.689E+OO 1. 689E+OO 27.12 OK 238.63 43.60* 3.499E+OO 1.189E+OO 1.189E+OO 13.77 OK 300.09 3.30 2.818E+OO 1.800E+OO 1.800E+OO 74.08 OK BI-214 609.32 45.49* l.437E+00 9.587E-01 9.590E-01 24.90 OK 1120.29 14.92 8.366E-01 8.456E-01 8.459E-01 95.99 OK 1764.49 15.30 5.417E-01 9.309E-01 9.312E-01 62.50 OK PB-214 74.82 5. 80* 3.482E+OO Line Not Found <<INT Reject 77 .11 9.70 3.649E+OO 2.978E+OO 2.979E+OO 27.12 OK 87.09 3.41 4.287E+OO Line Not Found <<INT Reject 242.00 7.25 3.455E+OO Line Not Found <<INT Reject 295.22 18.42 2.864E+OO 1.368E+OO 1.369E+OO 24.70 OK 351. 93 35.60* 2.414E+OO 1.169E+OO 1.169E+OO 19. 29 OK RN-222 609.32 45.49* 1.437E+OO 9.587E-01 9.590E-01 24.90 OK 1120. 29 14.92 8.366E-01 8.456E-01 8.459E-01 95.99 OK 17 6'4. 49 15.30 5.417E-01 9.309E-01 9.312E-01 62. 50 OK RA-224 240.99 4.10* 3.461E+OO 1.384E+OO 1.384E+OO 135.16 OK RA-226 609.32 45.49* 1.437E+OO 9.587E-01 9.590E-01 24.90 OK 1120.29 14.92 8.366E-01 8.456E-01 8.459E-01 95.99 OK 1764.49 15.30 5.417E-01 9.309E-01 9.312E-01 62.50 OK AC-228 105.21 1.10 4.943E+OO 4.198E+OO 4.198E+OO 104.18 OK 338.32 11.27 2.506E+OO 7.705E-01 7.705E-01 89.44 OK 794.95 4.25 1.134E+OO Line Not Found Absent 835. 71 1. 61 1.085E+OO Line Not Found Absent 911.20 25.80* 1.006E+OO 1.141E+OO 1.141E+OO 39.08 OK 968. 97 15.80 9.525E-01 1.412E+OO 1.412E+OO 48.75 OK RA-228 105.2.1 1.10 4.943E+00 4.198E+00 4.198E+OO 104.18 OK 338.32 11. 27 *2. 506E+OO 7.705E-01 7.705E-01 89.44 OK 794.95 4.25 1.134E+OO Li he Not Found Absent 835.71 1. 61 1.085E+OO Line Not Found Absent 911. 20 25.80* 1.006E+OO 1.141E+OO 1.141E+OO 39.08 OK 968. 97 15.80 9.525E-01 1.412E+OO 1.412E+OO 48. 7.5 OK TH-228 74.82 10.28 3.472E+00 9.916E-01 9.916E-01 77.64 OK 77 .11 17.10 3.649E+OO 1.689E+OO 1.689E+OO 27.12 OK 238.63 43.60* 3.499E+OO 1.189E+OO 1.189E+OO 13.77 OK 300.09 3.30 2.818E+00 1.800E+OO 1.800E+OO 74.08 OK Page 377of614 Nuclide Line Activity Report (continued) Page : 3 Sample ID : R405245016 Acquisition date 3-0CT-2016 04:48:08 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-229 85.43 14.70 4.130E+OO 2.586E-01 2.586E-01 140.29 OK 88.47 24.00 4.288E+OO 3.046E-01 3.047E-01 73.58 OK 193.51 4.41* 4.174E+OO Line Not Found Absent 210.85 2.80 3.889E+OO 8.273E-01 8.274E-01 146.71 OK TH-230 609.32 45.49* 1.437E+OO 9.587E-01 9.587E-01 24.90 OK 1120.29 14.92 8.366E-01 8.456E-01 8.456E-01 95.99 OK 1764.49 15.30 5.417E-01 9.309E-01 9.309E-01 62.50 OK PA-231 283.69 1. 70 2.976E+OO Line Not Found Absent 301.36 5.35* 2.818E+OO l. llOE+OO l. llOE+OO 74.08 OK TH-232 105.21 1.10 4.943E+OO 4.198E+OO 4.198E+OO 104.18 OK 338.32 11. 27 2.506E+OO 7.705E-01 7.705E-01 89.44 OK 835.71 1. 61 l.085E+OO Line Not Found Absent 911.20 25.80* 1.006E+00 l.141E+OO l .141E+OO 39.08 OK 968. 97 15.80 9.525E-01 l.412E+OO l.412E+OO 48.75 OK PA-233 300.13 6.63 2.818E+OO 8.957E-01 8.957E-01 74.08 OK 311. 90 . 38.50* 2.710E+OO 9.579E-02 9.579E-02 88.17 OK 340.48 4.45 2.493E+OO Line Not Found Absent U-234 609.32 45.49* 1.437E+00 9.587E-01 9.587E-01 24.90 OK 1120.29 14.92 8.366E-01 8.456E-01 8.456E-01 95. 99. OK 1764.49 15.30 5.417E-01 9.309E-01 9:309E-01 62.50 OK U-235 89.96 . 3. 47 4.426E+00 2.247E+OO 2.247E+OO 48.65 OK 93.35 5.60 4.559E+OO l.516E+OO l.516E+00 70.56 OK 143.76 10.96* 4.954E+OO Line Not Found Absent 163.33 5.08 4.674E+OO Line Not Found Absent 185.72 57.20 4.300E+OO 2.405E-01 2.405E-01 50.93 OK 205.31 5.01 3.984E+OO Line Not Found Absent AM-243 43.53 5.90 5.957E-01 Line Not Found* Absent 74.66 67.20* 3.472E+OO 1. 517E-01 1. 517E-01 77.64 OK ANH-511 511. 00 100.00* .1.690E+OO 6.949E-02 6.949E-02 162.95 OK Flag: "*" = Keyline Page 378of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:50:59.72 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245016.CNF;l *
  • Acquisition date 3-0CT-2016 04:48:08 Sensitivity : 3.000 *
  • Detector ID GAM36 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.35 Half life ratio : ***** *
  • Sample date 15-DEC-2015 14:06:00 Analyst initials: MXRl *
  • Sample ID R405245016 Sample Quantity 1.2541E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;.6 . * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 1-JUN-2016 09:39:12 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;?
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l.595E+Ol 2.258E+OO AS-73 9.086E+OO 1. 656E+Ol CD-109 3.067E+OO 2.212E+OO SN-126 1. 976E-01 1.425E-01 BA-137M 8.591E-02 8.248E-02 CS-137 9.076E-02 8.713E-02 EU-155 2.460E-01 2. 511E-01 TL-208 3.785E-01 l.208E-01 PB-212 1.189E+OO l.604E-01 BI-214 9.590E-01 2.340E-01 PB-214 1.169E+OO 2.210E-01 RN-222 9.590E-01 2.340E-01 RA-224 1. 384E+OO 1.833E+OO RA-226 9.590E-01 2.340E-01 AC-228 1.141E+OO 4.369E-01 RA-228 1.141E+OO 4.369E-01 TH-228 1.189E+OO 1.604E-01 TH-229 8.490E-02 6.283E-01 TH-230 9.587E-01 2.340E-01 PA-231 1.llOE+OO 8.b59E-01 TH-232 1.141E+OO 4.369E-01 PA-233 9.579E-02 8.277E-02 U-234 9.587E-01 2.340E-01 U-235 9.463E-02 2.339E--;01 AM-243 1.5"17E-01 l.154E-01 ANH-511 6.949E-02 1. llOE-01 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 379 of 614 Key-Line Activity (pCi/GRAM -1.622E+Ol -1.656E-02 O.OOOE+OO -4.814E-02 K.L. Cnt Uncert ( 1. 96_-sigma) 1.437E+Ol 7.382E-02 1.960E+41 5.672E-02 MDA (pCi/GRAM 1. 017E+OO 1.635E+Ol 2. 061E+OO l.334E-01 8.896E-02 9.397E-02 2.159E-01 1.095E-01 1. 072E-01 1.775E-01 1.406E-01 1. 775E-01 1.152E+OO 1. 775E-01 3.619E-01 3.619E-01 l.072E-01 1.177E+OO 1.774E-01 9.973E-01 3.619E-01 1.392E-01 l.774E-01 4.437E-01 1. 076E-01 7.354E-02 MDA (pCi/GRAM 2.364E+Ol l.465E-01 O.OOOE+OO 8.333E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 4.749E-02 5.584E-01 1.121E+OO FAIL ABUN V-48 O.OOOE+OO l.787E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.690E+02 O.OOOE+OO SHORT HLIF MN-54 6.456E-02 9.595E-02 2. llOE-01 NOT IDENT. C0-56 4. 372E-01 6.585E-01 1.467E+OO FAIL ABUN MN--56 O.OOOE+OO 1.479E+41 O.OOOE+OO SHORT HLIF C0-57 3.170E-02 5.435E-02 1.091E-01 NOT IDENT . C0-58 -1.006E-01 6.956E-01 1. 372E+OO . NOT IDENT. FE-59 -9.855E-03 8.435E+OO 1. 788E+Ol NOT IDENT. C0-60 2.155E-02 6.161E-02 1.399E-01 FAIL ABUN ZN-65 1.244E-01 2.582E-01 5.578E-01 NOT IDENT. GE-68 -1.022E+OO 4.002E+OO 7.285E+OO NOT IDENT. AS-74 O.OOOE+OO 7.228E+03 O.OOOE+OO SHORT.HLIF SE-75 -1.1B3E-01 2.554E-01 4.425E-01 NOT IDENT. BR-77 O.OOOE+OO 3.518E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 9.068E+02 O.OOOE+OO SHORT HLIF RB-83 -1.390E-01 7.774E-01 1.548E+OO *NOT IDENT. KR-85 4.339E+OO 1.124E+Ol 2.127E+Ol NOT IDENT. SR-85 4.240E-01 1.101E+OO 2.083E+OO NOT IDENT. RB-86 O.OOOE+OO 3.855E+04 O.OOOE+OO SHORT HLIF Y-88 1. 474E-01 3.804E-01 9.308E-01 NOT IDENT. Y-91 -1. 84 6E+02 7.203E+02 l.422E+03 NOT IDENT. NB-94 3.776E-02 4.164E-02 9.629E-02 NOT IDENT. NB-95 -1.149E+OO 1. 317E+OO 2.154E+OO NOT IDENT. NB-95M -4.748E-01 3.154E+OO 5.226E+OO NOT IDENT. ZR-95 2.560E+OO 3.185E+OO 4.897E+OO FAIL ABUN NB-97 O.OOOE+OO 7.987E+40 O.OOOE+OO SHORT HLIF ZR-97 0. OOOE+OO. 1.610E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 4 .111E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 2.198E-02 4.015E-02 7.544E-02 NOT IDENT. RH-102 -3.285E-02 8.402E-02 1.564E-01 NOT IDENT. RU-103 -8.661E-02 6.145E+OO 1.253E+Ol FAIL ABUN RH-106 -2.049E-01 7.138E-01 l.366E+00 NOT IDENT. RU-106 -2.049E-01 7.138E-01 1.366E+OO NOT IDENT. AG-108M -2.088E-02 3.473E-02 6.429E-02 NOT IDENT. AG-llOM 1.246E-01 1.068E-01 2. 872E-01 NOT IDENT. SN-113 -1.086E-01 2.773E-01 5.330E-01 NOT IDENT. CD-115 O.OOOE+OO 4.890E+38 0.000E+OO SHORT HLIF SN-ll 7M O.OOOE+OO 8.319E+04 O.OOOE+OO SHORT HLIF TE-123M 9.929E-02 1.517E-01 3.027E-01 NOT IDENT. SB-124 -1.026E+OO 3.270E+OO 6.478E+00 NOT IDENT. SB-125 9.450E-03 1. 513E-01 3.035E-01 FAIL ABUN TE-125M 1. 960E+02 2.944E+02 5.652E+02 NOT IDENT. I-126 O.OOOE+OO 9*. 344E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO i.Ol9E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 8. 371E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.588E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1. OOOE+26 0.000E+OO SHORT HLIF BA-133 3.188E-02 5.419E-02 1.035E-01 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 3 .119E-02 7.628E-02 1.602E-01 FAIL ABUN CS-135 -1.682E-01 2.132E-01 3.512E-01 NOT IDENT. I-135 O.OOOE+OO 1.103E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.607E+05 O.OOOE+OO SHORT HLIF CE-139 -6.559E-02 1.284E-01 2.286E-01 NOT IDENT. BA-140 O.OOOE+OO 1.249E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.438E+05 O.OOOE+OO SHORT HLIF CE-141 -1.875E+Ol 2.783E+Ol 4.798E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -2.456E-01 4.908E-01 8.126E-01 NOT IDENT. PM-144 2. 271E-02 8.065E-02 1.665E-01 NOT IDENT. PR-144 2.023E+OO 6.990E+OO 1.444E+Ol NOT IDENT. PM-146 2.104E-02 6.474E-02 1.241E-01 NOT IDENT. ND-147 o. ooo*E+oo 2.758E+07 O.OOOE+OO SHORT HLIF PM-147 6. 761E+02 9.676E+02 1.957E+03 NOT IDENT. PM-149 O.OOOE+OO 6.154E+39 O.OOOE+OO SHORT HLIF EU-150 l.822E-02 3.712E-02 6.793E-02 FAIL ABUN EU-152 -1.004E-01 l.229E-01 l.939E-01 FAIL ABUN GD-153 -3.213E-01 2.345E-01 3.635E-01 NOT IDENT. EU-154 -3.583E-02 l.829E-01 3.649E-01 FAIL ABUN TB-160 2.044E+OO 2.258E+OO 5.484E+OO FAIL ABUN H0-166M -8.298E-02 7.573E-02 1.150E-01 NOT IDENT. TM-171 6.870E-02 2.209E+Ol 4.154E+Ol NOT IDENT. HF-172 3.447E-02 2.651E-01 5.108E-Ol FAIL ABUN LU-172 8.646E-02 l.341E-01 2.900E-01 FAIL ABUN LU-176 6.935E-03 3.106E-02 5.930E-02 FAIL ABUN Page 380 of 614 HF-181 -3.692E+OO 6.169E+OO. 9.781E+OO NOT IDENT. TA-182 4.910E-01 1.487E+OO 3.178E+OO FAIL ABUN RE-183 -6.672E-01 3.291E+OO 5.982E+OO NOT IDENT. RE-184 l.388E+Ol 4.069E+01 8.560E+Ol NOT IDENT. W-188 -7.042E+Ol 1. 511E+02 2.348E+02 NOT IDENT. IR-192 4.802E-02 6.324E-01 l.164E+OO FAIL ABUN HG-203 9.392E-01 3.083E+00 5.832E+OO NOT IDENT. BI-207 5.229E-02 5.937E-02 l.476E-01 FAIL ABUN PB-210 -4.857E-02 2.992E+00 6.008E+OO NOT IDENT. BI-211 O.OOOE+OO . 6.089E-01 1.033E+OO FAIL ABUN PB-211 -5.749E-01 8.548E-01 1. 57 8E+OO NOT IDENT. BI-212 9.436E-01 l.151E+OO 1. 780E+OO FAIL ABUN RN-219 2.147E-01 5.3El9E-01 l.120E+OO NOT IDENT. RA-223 2.641E-01 8.304E-01 1.582E+OO FAIL ABUN AC-227 -7.475E-03 2.845E-01 5.259E-01 FAIL ABUN TH-227 -7.475E-03 2.845E-01 5.259E-01 FAIL ABUN TH-231 2.641E-01 8.304E-01 1.582E+OO FAIL ABUN PA-234 8.287E-03 4.630E-01 9.035E-01 NOT IDENT. PA-234M 4.205E+OO 8. 8'77E+OO 1. 809E+Ol NOT IDENT. TH-234 8.009E-01 1.425E+OO 2.916E+OO FAIL ABUN NP-237 9.579E-02 8.277E-02 1. 676E-01 FAIL ABUN NP-238 O.OOOE+OO 7.738E+40 O.OOOE+OO SHORT HLIF U-238 8.009E-01 1.425E+OO 2.916E+OO FAIL ABUN NP-239 -3.862E-02 2.554E-01 4.855E-01 FAIL ABUN PU-239 5.692E+02 7.902E+02 8.147E+02 FAIL ABUN AM-241 4.282E-02 1.441E-01 2.938E-01 NOT IDENT. CM-243 -3.757E-02 1.130E-01 1.958E-01 NOT IDENT. BK-24'7 -7. 021E-02 9.667E-02 1. 6'06E-01 FAIL ABUN CM-247 l.333E-02 4.534E-02 9.462E-02 NOT IDENT. CF-249 -l.871E-02 4.950E-02 9.496E-02 NOT IDENT. CF-251 -1.602E-02 l.480E-01 2.728E-01 NOT IDENT. Page 381of614 VAX/VMS' Nuclide Identification Report Generated 3-0CT-2016 05:50:57.44 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 186 10.66* 6.546E-01 1.595E+Ol 1.595E+Ol 14.45 AS-73 53.44 20 10.30* 1.564E+OO 7.267E-01 9.086E+OO 186.02 CD-109 88.03 86 3.70* 4.288E+OO 3.237E+OO 5.024E+OO 43.87 SN-126 64.28 ------9.60 2. 567.E+OO ------Line Not Found ------86.94 86 8.90 4.288E+OO 1.346E+OO 1.346E+OO 43.87 87.57 86 37.00* 4.288E+OO 3.237E-01 3.237E-01 43.87 BA-137M 661. 66 17 89.90* 1.334E+OO 8.434E-02 8.591E-02 97. 96 CS-137 661. 66 17 85.10* 1.334E+OO 8.910E-02 9.076E-02 97. 96 EU-155 86.55 86 30.70 4.288E+00 3. 901E-01 4.385E-01 43.87 105.31 38 21.10* 4.943E+OO 2.188E-01 2.460E-01 104.18 TL-208 277 .37. ------6.60 3.041E+OO ------Line Not Found ------583.19 80 85.00* 1. 496E+OO 3.785E-01 3.785E-01 32.56 860.56 14 12.50 1.057E+OO 6.519E-01 6.519E-01 107.47 BI-211 72. 87 ------1. 23 3.327E+OO ------Line Not Found ------351. 06 168 12.92* 2.414E+OO 3.221E+OO 3.221E+OO 19.29 PB-212 74.82 105 10.28 3.472E+OO 1.7'64E+OO 1.764E+OO 42.30 77 .11 176 17.10 3.649E+OO 1.689E+OO 1. 689E+oo* 27.12 238.63 303 43.60* 3.499E+OO l.189E+00 1.189E+OO 13. 77 300.09 28 3.30 2.818E+OO 1.800E+OO 1.800E+OO 74.08 BI-214 609.32 105 45.49* l.437E+OO 9.587E-01 9.590E-01 24.90 1120.29 18 14.92 8.366E-01 8.456E-01 8.459E-01 95.99 1764.49 13 . 15. 30 5.417E-01 9.309E-01 9.312E-01 62.50 PB-214 74.82 105 5.80 3.472E+OO 3.126E+OO 3.127E+00 42.30 77 .11 176 9.70 3.649E+OO 2.978E+OO 2.979E+OO 27.12 87.09 86 3.41 4.288E+OO 3.512E+OO 3.514E+OO 43.87 242.00 90 7.25 3.461E+OO 2 .151E+OO 2.152E+OO 46.60 295.22 121 18.42 2.864E+OO 1.368E+OO 1.369E+OO 24.70 351.93 168 35.60* 2.414E+OO l.169E+OO 1.169E+OO 19.29 RN-222 609.32 105 45.49* 1.437E+OO 9.587E-01 9.590E-01 24.90 1120.29 18 14.92 8.366E-01 8.456E-01 8.459E-01 95.99 1764.49 13 15.30 5.417E-01 9.309E-01 9.312E-01 62.50 RA-224 240.99 90 4.10*. 3.461E+OO 3.803E+OO 3.803E+OO 46.60 RA-226 609.32 105 45.49* 1.437E+OO 9.587E-01 9.590E-01 24.90. 1120.29 18 14.92 8.366E-01 8.456E-01 8.459E-01 95.99 1764.49 13 15.30 5.417E-01 9.309E-01 9.312E-01 62.50 AC-228 105.21 38 1.10 4.943E+OO 4.198E+OO 4.198E+OO 104.18 338.32 3.6 11. 27 2.506E+OO 7.705E-01 7.705E-01 89.44 794.95 ------4.25 1.134E+OO ------Line Not Found ------835.71 ------1. 61 1.085E+OO ------Line Not Found ------911.20 49 25.80* 1.006E+OO l .141E+OO l.141E+00 39.08 968. 97 35 15.80 9.525E-01 1.412E+OO 1.412E+OO 48.75 RA-228 105.21 38 1.10 4.943E+OO 4.198E+OO 4.198E+00 104.18 338.32 36 11.27 2.506E+OO 7.705E-01 7.705E-01 89.44 794.95 ------4.25 1.134E+00 ------Line Not Found ------835. 71 ------1. 61 1.085E+OO ------Line Not Found ------911. 20 49 25.80* 1.006E+OO l.141E+OO 1.141E+OO 39.08 968. 97 35 15.80 9.525E-01 1.412E+OO 1.412E+OO 48.75 Page 382 of 614 Nuclide Line Activity Report (continued) Page : 2 Sample ID : R405245016 Acquisition date 3-0CT-2016 04:48:08 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Ef f pCi/GRAM pCi/GRAM %Error TH-228 74.82 105 10.28 3.472E+OO 1. 764E+OO 1.764E+OO 42.30 77 .11 176 17.10 3.649E+OO 1.689E+00 1. 68 9E+OO 27.12 238.63 303 43.60* 3.499E+OO 1.189E+OO l.189E+OO 13.77 300.09 28 3.30 2.818E+OO 1.800E+OO l.800E+OO 74.08 TH-229 85.43 26 14.70 4.130E+OO 2.586E-01 2.586E-01 140.29 88.47 86 24.00 4.288E+OO 4.990E-01 4.991E-01 43.87 193.51 ------4.41* 4.174E+OO ------Line Not Found ------210.85 15 2.80 3.889E+OO 8.273E-01 8.274E-01 146. 71 TH-230 609.32 105 45.49* l.437E+OO 9.587E-01 9.587E-01 24.90 1120.29 18 14.92 8.366E-01 8.456E-01 8.456E-01 95.99 1764.49 13 15.30 5.417E-01 9.309E-01 9.309E-01 62.50 PA-231 283.69 ------1. 70 2.976E+OO ------Line Not Found ------301.36 28 5.35* 2.818E+OO 1. llOE+OO 1. llOE+OO 74.08 TH-232 105.21 38 1.10 4.943E+OO 4.198E+OO 4.198E+OO 104.18 338.32 36 11. 27 2.506E+OO 7.705E-01 7.705E-01 89.44 835. 71 ------1. 61 1.085E+OO ------Line Not Found ------911.20 49 25.80* 1.006E+OO 1.141E+OO l.141E+00 39.08 968.97 35 15.80 9.525E-01 1.412E+OO 1.412E+OO 48.75 PA-233 300.13 28 6.63 2.818E+OO 8.957E-01 8.957E-01 74.'08 311. 90 17 38.50* 2.710E+OO 9.579E-02 9.579E-02 88.17 340.48 ------4.45 2.493E+OO ------Line Not Found ------U-234 609.32 105 45.49* 1.437E+OO 9.587E-01 9.587E-01 24.90 1120.29 18 14.92 8.366E-01 8.456E-01 8.456E-01 95.99 1764.49 13 15.30 5.417E-01 9.309E-01 9.309E-01 62.50 U-235 89. 96 58 3.47 4.426E+OO 2.247E+OO 2.247E+OO 48.65 93.35 65 5.60 4.559E+OO 1.516E+OO 1.516E+OO 70.56 143.76 ------10. 96* 4.954E+00 ------Line Not Found ------163.33 ------5.08 4.674E+OO ------Line Not Found ------185.72 99 57.20 4.300E+OO 2.405E-01 2.405E-01 50.93 205.31 ------5.01 3.984E+OO ------Line Not Found ------AM-243 43.53 ------5.90 5.957E-01 ------Line Not Found ------74.66 105 67.20* 3.472E+OO 2.698E'-01 2.698E-01 42.30 ANH-511 511. 00 20 100.00* 1.690E+OO 6.949E-02 6.949E-02 162.95 Flag: "*" Key line Page 383 of 614 Page : 3 Summary of Nuclide Activity Sample ID : R405245016 Acquisition date 3-0CT-2016 04:48:08 Total number of lines in spectrum 45 Number of unidentified lines 7 Number of lines tentatively identified by NID 38 Nuclide Type : Nuclide K-40 AS-73 CD-109 SN-126 BA-137M CS-137 EU-155 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-:-228 TH-229 TH-230 PA-231 TH-232 PA-233 U-234 U-235 AM-243 ANH-511 Hlife l.25E+09Y 80.30D 461.40D 2.30E+05Y 30.0BY 30.0BY 4.75Y 1.41E+10Y 7.04E+08Y 1.41E+l0Y 1600. OOY 1600. OOY 1600.00Y l.41E+l0Y 1600. OOY 1. 41E+10Y 1. 41E+10Y 1.41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 2.14E+06Y 2.45E+05Y 7.04E+08Y 7370.00Y 1.00E+09Y Decay 1. 00 12.5 1. 55 1. 00 1. 02 1. 02 1.12 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 06 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.595E+Ol 7.267E-01 3.237E+OO 3.237E-01 8.434E-02 8.910E-02 2.188E-01 3.785E-01 3.221E+OO 1.189E+OO 9.587E-01 l.169E+OO 9.587E-01 3.803E+OO 9.587E-01 1.141E+OO 1.141E+OO 1.189E+00 4.990E-01 9.587E-01 1. llOE+OO 1.141E+OO 9.579E-02 9.587E-01 2.405E-01 2.698E-01 6.949E-02 4.208E+Ol 4.208E+Ol Decay Corr pCi/GRAM 1.595E+Ol 9.086E+OO 5.024E+OO 3.237E-01 8. 591E-02 9.076E-02 2.460E-01 3.785E-01 3.221E+OO 1.189E+00 9.590E-01 1.169E+OO 9.590E-01 3.803E+OO 9.590E-01 l.141E+OO 1.141E+OO 1.189E+OO 4.991E-01 9.587E-01 1. llOE+OO 1.141E+OO 9.579E-02 9.587E-01 2.405E-01 2.698E-01 6.949E-02 5.225E+Ol 5.225E+Ol 84.44% Decay Corr 2-Sigma Error 0.230E+Ol 16.90E+OO 2.204E.+00 1.420E-01 8.416E-02 8. 8 91E-02 2.562E-01 1.233E-01 0.621E+OO 0.164E+OO 2.388E-01 0.226E+00 2.388E-01 1.772E+OO 2.388E-01 0.446E+OO 0.446E+OO 0.164E+OO 2.190E-01 2.387E-01 0.822E+00 0.446E+OO 8.446E-02 2.387E-01 l.225E-01 1.141E-01 11. 32E-02 "M" Manually accepted 2-Sigma %Error 14.45 186. 02 43.87 43.87 97. 96 97. 96 104.18 32.56 19.29 13.77 24.90 19.29 24.90 46.60 24.90 39.08 39.08 13.77 43.87 24.90 74 .*OB 39.08 88.17 24.90 50.93 42.30 162.95 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 384 of 614 Flags K K Unidentified Energy Lines Page : 4 Sample ID : R405245016 Acquisition date : 3-0CT-2016 04:48:08 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 129.44 30 122 . 1. 08 258.86 256 9 7.71E-03 **** 5.08E+OO T 6 209.28 43 52 1. 29 418.55 414 12 l.llE-02 70.7 3.92E+OO 0 328.29 23 50 0.75 656.55 654 8 6. OlE-03 **** 2.58E+OO T 4 354.27 17 26 1. 49 708.52 697 17 4.46E-03 **** 2.40E+OO T 1 460.15 17 18 1. 46 920.26 912 23 4.65E-03 98.2 l.86E+OO 1 462.89 22 14 1. 46 925.73 912 23 5.92E-03 83.1 l.85E+OO T 0 487.73 *9 14 0.57 975.42 969 9 2.37E-03 **** l.77E+OO T 0 727.39 13 15 1. 30 1454.65 1449 10 3. 61E-03 **** 1.23E+OO T 0 757.19 12 . 12 2.46 1514.24 1509 10 3.25E-03 **** 1.18E+OO T 0 7 61. 30 9 3 0.83 1522.46 1519 6 2.55E-03 88.6 1.18E+OO 0 802.59 19 3 0.61 1605.01 1599 11 5.33E-03 56.7 1.12E+OO .T 0 920.49 10 5 1. 08 1840.75 1835 12 2.93E-03 **** 9.97E-01 0 934.50 15* 2 0.76 1868.76 1864 9 4.39E-03 60.8 9.83E-01 1 964. 76 21* 9 1. 84 1929.24 1923 23 6.0lE-03 76.6 9.56E-01 T 0 1031.82 15 4 1. 86 2063.32 2059 9 4. 31E-03 70.8 9.0lE-01 0 1149.84 9 3 0.80 2299.26 2295 7 2.64E-03 92.1 8.18E-01 0 1174.31 15 0 1. 03 2348.19 2345 8 4.44E-03 50.0 8.02E-01 T 0 1237.79 22 3 2.55 2475.08 2468 14 6.27E-03 54.8 7.65E-01 T Flags: "T" = Tentatively associated Page 385of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:51:12.12 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245016.CNF;l *
  • Acquisition date 3-0CT-2016 04:48:08 Sensitivity 3.000 *
  • Detector ID GAM36 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.35 Half life ratio : ***** *
  • Sample date 15-DEC-2015 14:06:00 Nuclide Library : SOLID *
  • Sample ID R405245016 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.2541E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 AS-73 CD-109 SN-126 BA-137M CS-137 EU-155 TL-208 PB-212 .BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 PA-233 U-234 U-235 AM-243 ANH-511 Le (pCi/GRAM *3. 925E-01 7.499E+OO 9.493E-01 6.147E-02 3.754E-02 3. 966E-02 9.893E-02 4.830E-02 4.820E-02 7.622E-02 6.071E-02 7.622E-02 5.177E-01 7.622E-02 1. 496E-01 1.496E-01 4.820E-02 5.433E-01 7.620E-02 4.437E-01 1. 496E-01 6.169E-02 7.620E-02 2.065E-01 5.020E-02 3.192E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 386of614 Le (pCi/GRAM 9.845E+OO 5.978E-02 O.OOOE+OO 2.634E-02 4. 713E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG--llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 387 of 614 0.000E+OO O.OOOE+OO 9 .114E-02 6. 287E.-Ol O.OOOE+OO 5.050E-02 5.570E-Ol 7.333E+OO 5.736E-02 2.351E-01 3.028E+OO O.OOOE+OO l.973E-01 0.000E+OO O.OOOE+OO 6.587E-01 9.453E+OO 9.256E-01 0.000E+OO 3.606E-01 5.836E+02 4.168E-02 9 .114E-01 2.389E+OO 2.148E+OO 0. OOOE+O.O O.OOOE+OO O.OOOE+OO 0.000E+OO 3.487E-02 6.603E-02 5.351E+OO 5. 821E-01 5.821E-01 2.753E-02 1.192E-01 2.326E-01 O.OOOE+OO O.OOOE+OO 1.399E-01 2.368E+00 l.349E-01 2.614E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.587E-02 O.OOOE+OO 6.912E-02 1.591E-01 O.OOOE+OO O.OOOE+OO l.045E-01 O.OOOE+OO O.OOOE+OO 2.220E+Ol O.OOOE+OO 3.760E-01 7.200E-02 6.249E+OO 5.468E-02 O.OOOE+OO 9.077E+02 O.OOOE+OO 3.054E-02 8.385E-02 1. 676E-01 l.493E-01 2. 311E+OO 4.540E-02 1.906E+01 2.359E-01 1. 24 7E-01 2.646E-02 4.207E+OO SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 . RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 388of614 1.361E+OO 2.763E+OO 3. 631E+Ol 1.045E+02 5.239E-01 2.656E+OO 6.120E-02 2.766E+OO 4.903E-01 6.859E-01 7.904E-01 5.012E-01 7.122E-01 2.364E-01 2.364E-01 7.122E-01 3.821E-01 8.00lE+OO l.366E+OO 7.590E-02 O.OOOE+OO 1;366E+OO 2. 221E-01 3.814E+02 l.358E-01 8.955E-02 7.164E-02 4.193E-02 4.179E-02 1.256E-01 FAIL ABUN

  • NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:51:18.98 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R405245016.CNF;l *
  • Acquisition date 3-0CT-2016 04:48:08 Sensitivity : 3.000 *
  • Detector ID GAM36 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.35 Half life ratio : ***** *
  • Sample date 15-DEC-2015 14:06:00 Nuclide Library : SOLID *
  • Sample ID R405245016 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.2541E+02 GRAM *
  • Quantity Err(%) : 1.5948E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
  • Eff. File . : DKA100: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1 . 96-sigma ) K-40 1.595E+Ol 2.407E+OO 2.407E+OO AS-73 9.086E+OO l.667E+Ol 1.667E+Ol CD-109 3 .. 067E+OO 2.239E+OO 2.239E+OO SN-126 l.976E-01 1.439E-01 l.439E-01 BA-137M 8.591E-02 8.256E-02 8.256E-02 CS-137 9.076E-02 8.722E-02 8.722E-02 EU-155 2.460E-01 2. 517E-Ol* 2.517E--:01 TL-208 3.785E-01 l.219E-01 1.219E-01 PB-212 1.189E+OO 1.723E-01 1.723E-01 BI-214 9.590E-01 *2.376E-01 2.376E-01 PB-214 1.169E+OO 2.263E-01 2.263E-01 RN-222 9.590E-01 2.376E-01 2.376E-01 RA-224 1.384E+OO 1. 841E+OO 1.841E+OO RA-226 9.590E-01 2.376E-01 2.376E-01 AC-228 1.141E+OO 4.408E-01 4.408E-01 RA-228 1.141E+OO 4.408E-01 4.408E-01 TH-228 1.189E+OO l.723E-01 1. 723E-01 TH-229 8.490E-02 .6.284E-01 6.284E-01 TH-230 9.587E-01 2.376E-01 2.376E-01 PA-231 1. llOE+OO 8.400E-01 8.400E-01 TH-232 l .141E+OO 4.408E-01 4.408E-01 PA-233 9.579E-02 8.290E-02 8.290E-02 U-234 9.587E-01 2.376E-01 2.376E-01 U-235 9.463E-02 2.339E-01 2.339E-01 AM-243 1. 517E-'01 l.168E-01 1.168E-01 ANH-511 6.949E-02 1. llOE-01 l. llOE-01 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1 . 96-s i gma ) ( 1. 96-sigma) BE-7 -1.622E+Ol l.438E+Ol l.613E+Ol NOT IDENT. NA-22 -l.656E-02 7.382E-02 7.420E-02 NOT IDENT. NA-24 -l .'OOOE+41 3.694E+41 O.OOOE+OO SHORT HLIF AL-26 -4.814E-02 5.680E-02 6.081E-02 NOT IDENT. Page 389 of 614 SC-46 4.749E-02 5.584E-01 5.588E-01 FAIL ABUN V-48 -5.155E+03 l.787E+04 l.802E+04 SHORT HLIF CR-51 -6.238E+Ol 4.690E+02 4.698E+02 SHORT HLIF MN-54 6.456E-02 9 .. 599E-02 l.003E-01 NOT IDENT. C0-56 4. 372E-01 6.587E-01 6.876E-01 FAIL ABUN MN-56 1.000E+41 l.480E+41 O.OOOE+OO SHORT HLIF C0-57 3.170E-02 5.437E-02 5.621E-02 NOT IDENT. C0-58 -1.006E-01 6.956E-01 6.971E-01 NOT IDENT. FE-59 -9.855E-03 8.435E+OO 8.435E+OO NOT IDENT. C0-60 2.155E-02 6.161E-02 6.237E-02 FAIL ABUN ZN-65 1.244E-01 2.582E-01 2.642E-01 NOT IDENT. GE-68 -l.022E+00 4.002E+OO 4.029E+OO NOT IDENT. AS-74 -2.880E+03 7.232E+03 7.348E+03 SHORT HLIF SE-75 -1.183E-01 2.554E-01 2.609E-01 NOT IDENT. BR-77 2.606E+37 2.201E+38 O.OOOE+OO SHORT HLIF SR-82 -5 .119E+02 9.072E+02 9.360E+02 SHORT HLIF RB-83 -l.390E-01 7.777E-01 7.802E-01 NOT IDENT. KR-85 4.339E+OO 1.124E+Ol l .141E+Ol NOT IDENT. SR-85 4.240E-01 1.101E+OO l.117E+OO NOT IDENT. RB-86 -l.547E+04 3.855E+04 3.918E+04 SHORT HLIF Y-88 1.474E-01 3.805E-01 3.862E-01 NOT IDENT. Y-91 -1.846E+02 7.203E+02 7.251E+02 NOT IDENT. NB-94 3.776E-02 4.167E-02 4. 501E-02 NOT IDENT. NB-95 -1.149E+OO 1.318E+OO 1.416E+OO NOT IDENT. NB-95M -4.748E-Oi 3.154E+OO 3.161E+OO NOT IDENT. ZR-95 2.560E+OO 3.187E+OO .3. 389E+OO FAIL ABUN NB-97 1.000E+41 7.998E+40 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 l.610E+41 o. *oooE+oo SHORT HLIF M0-99 -1. 391E+31 4 .113E+31 O.OOOE+OO SHORT HLIF TC-99M 1. OOOE+41 4.238E+41 O.OOOE+OO SHORT HLIF RH-101 2.198E-02 4.035E-02 4.155E-02 NOT IDENT. RH-102 -3.285E-02 8.407E-02 8.536E-02 NOT IDENT. RU-103 -8.661E-02 6.145E+OO 6.145E+OO FAIL ABUN RH-106 -2.049E-01 7 .139E-01 7.199E-01 NOT IDENT. RU-106 -2.049E-01 7.139E-01 7.199E-01 NOT IDENT. AG-108M -2.088E-02 3.474E-02 3.599E-02 NOT IDENT. AG-110M l.246E-01 1. 070E-01 l.209E-01 NOT IDENT. SN-113 -l.086E-01 2.773E-01 2.816E-01 NOT IDENT. CD-115 -7.602E+37 4.892E+38 O.OOOE+OO SHORT HLIF SN-117M 8.094E+03 8.320E+04 8.328E+04 SHORT HLIF TE-123M 9.929E-02 l.518E-01 1.582E-01 NOT IDENT. SB-124 -l.026E+00 3.270E+OO 3.303E+OO NOT IDENT. SB....:125 9.450E-03 l.513E-01 l.514E-01 FAIL ABUN TE-125M 1. 960E+02
  • 2.946E+02 3.076E+02 NOT IDENT. I-126 -8.095E+04 9.344E+05 9. 351E+05 SHORT HLIF SB-126 -2.854E+05 l.020E+06 1.028E+06 SHORT HLIF SB-127 -3.826E+21 9.820E+21 O.OOOE+OO SHORT HLIF I-131 -2.452E+09 3.590E+09 3.756E+09 SHORT HLIF I-132 l.000E+41 1. 848E+42 O.OOOE+OO SHORT HLIF TE-132 6.699E+25 l.035E+26 O.OOOE+OO SHORT HLIF BA-133 3.188E-02 5. 421E-02 5.608E-02 NOT IDENT. I-133 1.000E+41 2.849E+41 O.OOOE+OO SHORT HLIF CS-134 3 .119E-02 7.629E-02 7.757E-02 FAIL ABUN CS-135 -1.682E-01 2 .135E-01 2.266E-01 NOT I DENT*. I-135 -1.000E+41 6.703E+41 O.OOOE+OO SHORT HLIF CS-136 3.223E+05 2.630E+05 3.005E+05 SHORT HLIF CE-139 -6.559E-02 1.290E-01 1.324E-01 NOT IDENT. BA-140 -4.474E+05 1.249E+06 l.265E+06 SHORT HLIF LA-140 -5.938E+05 6.445E+05 6.978E+05 SHORT HLIF CE-141 -1. 875E+Ol 2.784E+Ol 2.910E+Ol NOT IDENT. CE-143 1.000E+41 6.062E+41 O.OOOE+OO SHORT HLIF CE-144 -2.456E-01 4.910E-01 5.034E-01 NOT IDENT. PM-144 2.271E-02 8.066E-02 8.131E-02 NOT IDENT. PR-144 2.023E+OO 6.991E+OO 7.050E+00 NOT IDENT. PM-146 2.104E-02 6.475E-02 6.545E-02 NOT IDENT. ND-147 9.460E-t:06 2.758E+07 2.791E+07 SHORT HLI'F PM-147 6.761E+02 9. 681E+02 l.015E+03 NOT IDENT. PM-149 6.804E+39 6.327E+39 O.OOOE+OO SHORT HLIF EU-150 1.822E-02 3.713E-02 3.803E-02 FAIL ABUN EU-152 -l.004E-01 1.230E-01 1. 311E-01 FAIL ABUN GD-153 -3.213E-01 2.352E-01 2.763E-01 NOT IDENT. EU-154 -3.583E-02 1.829E-01 l.836E-01 FAIL ABUN TB-160 2.044E+OO 2.261E+OO 2.442E+OO FAIL ABUN H0-166M -8.298E-02 7.587E-02 8.459E-02 NOT IDENT. TM-171 6.870E-02 2.209E+Ol 2.209E+Ol NOT IDENT. HF-172 3.447E-02 2.651E-01 2.656E-01 FAIL ABUN LU-172 8.646E-02 l.343E-01. l.399E-01 FAIL ABUN LU-176 6.935E-03 3.106E-02 3.122E-02 FAIL ABUN Page 390of614 HF-181 -3.692E+OO 6 .171E+OO 6. 391E+OO NOT IDENT. TA-182 4.910E-01 1.487E+OO l.504E+OO FAIL ABUN RE-183 -6.672E-01 3.293E+00 3.306E+OO NOT IDENT. RE-184 1. 388E+Ol 4.082E+Ol 4.130E+Ol NOT IDENT. W-188 -7.042E+Ol 1.513E+02 1. 54 6E+02 NOT IDENT. IR-192 4.802E-02 6.324E-01 6.328E-01 FAIL ABUN HG-203 9.392E-Ol 3.083E+OO 3.112E+OO NOT IDENT. BI-207 5.229E-02 5.941E-02 6.392E-02 FAIL ABUN PB-210 -4.857E-02 2.992E+OO 2.992E+OO NOT IDENT. BI-211 3.221E+OO 6.255E-01 1.581E+OO FAIL ABUN PB-211 -5.749E-Ol 8.553E-01 8.937E-01 NOT IDENT. BI-212 9.436E-01 1.152E+OO 1. 228E+OO FAIL ABUN RN-219 2.147E-Ol 5.376E-01 5.462E-01 NOT IDENT. RA-223 2.641E-Ol 8.306E-01 8.391E-01 FAIL ABUN AC-227 -7.475E-03 2.845E-01 2.846E-01 FAIL ABUN TH-227 -7.475E-03 2.845E-01 2.846E-01 FAIL ABUN TH-231 2. 641E-01 8.306E-01 8.391E-01 FAIL ABUN PA-234 8.287E-03 4.631E-01 -4. 631E-01 NOT IDENT. PA-234M 4.205E+OO 8.879E+OO 9.079E+OO NOT IDENT. TH-234 8.009E-01 1.436E+OO 1.481E+OO FAIL ABUN NP-237 9.579E-02 8.290E-02 9.347E-02 FAIL ABUN NP-238 -2.158E+40 7.739E+40 O.OOOE+OO SHORT HLIF U-238 8.009E-01 l.436E+00 1. 481E+OO FAIL ABUN NP-239 -3.862E-02 2.554E-01 2.560E-01 FAIL ABUN PU-239 5.692E+02 7.906E+02 8.312E+02 FAIL ABUN AM-241 4.282E-02 1.442E-01 1.455E-01 NOT IDENT. CM-243 -3.757E-02 1.131E-01 1.143E-01 NOT IDENT. BK-247 -7. 021E-02 9.770E-02 1. 027E'-.01 FAIL ABUN CM-247 1.333E-02 4.540E-02 4.580E-02 NOT IDENT. CF-249 -1. 871E-02 4.952E-02 *5. 023E-02 NOT IDENT. CF-251 -l.602E-02 1.480E-01 l.482E-01 NOT IDENT*. Page 391of614
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 23.4484 87.09 45.8392 136. *47 55.1405 45.60 40.9384 87.57 45.8880 140.51 0.0000 46.54 38.7005 88.03 45.9344 143.76 50.8884 49.72 0.0000 88.34 45. 9658 144.24 47.9884 51. 35 39.5837 88.47 45.9789 145.44 64.7583 51. 87 48.2217 89.96 52.0428 152.43 61.4816 52.39 41.8604 1093.63 52 .1195 153.25 0.0000 52.97 33.3340 91.*ll 0.0000 323.87 51.7017 53.44 40.9208 92.59 52.3377 156.02 0.0000 54.07 46.1253 93.35 52.4223 158.56 0.0000 57.36 0.0000 94.56 52.5562 159.00 38.0481 50.1513 94.65 52.5660 162.33 50.3029 57.98 53.4923 94.67 52.5682 162.66 0.0000 59.27 43.5574 94.87 52.5902 163.33 31.2323 59.32 43.5637 97.43 69.6922 165.86 47.5214 59.54 44.4139 98.43 48.1620 176.31 48.2077 60. 96 64.4140 98.44 48.1632 17 6. 60 0.0000 61.17 61.9735 99.53 51. 5884 177.52 47.2585 62.93 54.8061 100 .11 44.3999 181.07 0.0000 63.29 52.3669 102.03 38.8099 181.52 34.4269 63.58 47.4175 103.18 44.9763 184.41 42.5052 64.28 63.3450 103.37 44.9933 143.76 42.5772 66.73 45.3071 105.21 40.2738 193.51 46.1478 67.24 56.2905 105.31 40.2819 197.03 44.2430 125.81 63.0850 106.12 40.3450 198.01 55.8984 67.75 63. 0964 106.47 40.3725 201.83 40.2654 69.67 59.1869 109.28 38 .1300 203.43 33.9736 70.83 55.4056 111. 00 60.1569 205.31 29.7940 72.81 64.7762 111.76 0.0000 210.85 37.4882 72.87 64.7860 114. 06 55.8458 215.65 39.8522 74.66 65.0753 116. 30 0.0000 222 .11 30.3819 74.82 65.1009 116.74 41.1540 227.09 39.2811 74.97 65.1252 119.76 43.2580 227.38 30.5618 77 .11 65.4656 121.12 50.9035 228.16 0.0000 78.74 64.5688 121. 22 41.4843 228.18 31. 6816 79.69 64.7147 121.78 43.4124 116.74 31.6816 80.12 62.4666 122.06 41.5454 235.69 41.1216 80.19 0.0000 122.92 50 .1185 235. 96 42.6026 80.57 55.5845 123.07 50.1315 . 238. 63 26.5192 81. 00 71.2896 265.00 54.9193 238.98 0.0000 81. 07 71. 3008 125.81 46.5680 240.99 26.5858 81. 75 56.8990 127.23 39.3768 242.00 26.6144 83.79 58.3333 127.91 52.1394 244.70 19.2762 84.00 58.3613 129.30 46.8444 252.40 0.0000 85.43 50.9389 131.20 46;9940 252.80 30.2798 86. 55 51.0668 133. 02 52.5863 254.15 0.0000 86.79 45.8083 133.52 62.8989 256.23 27.0095 86.94 45.8237 136.00 45.4323 260.90 0.0000 Page 392of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 29.5087 355.39 0.0000 584.27 21. 3556 264.80 29.5126 356.01 13 .1191 595.83 0.0000 265.00 34.0594 364.49 0.0000 427.87 14.3597 268.22 45.5566 366.42 0.0000 602.52 0.0000 269.46 34. 2096 372.51 24.9146 604. 72 7.1951 270.03 41. 0735 375.05 18.7221 607.14 12. 9672 271.23 25 .1300 377.52 16.6728 609.32 12.5012 273.65 0.0000 356.01 18.4269 610.33 12.5075 276.40 36.7354 388.16 22.6868 614,. 28 9.2551 277.37 35.6205 388.63 0.0000 618.01 10.6249 277.60 32.1802 391.69 20.2183 620.36 6.7693 278.00 32.1930 264.66 23.7418 621. 93 12.5816 279.20 29.9276 401.81 19.5186 630.19 0.0000 279.54 31.0886 402.40 16.9796 631. 29 13.6132 279.70 32.2451 404.85 20.4111 633.25 8.7598 280.46 27.6584 410.95 20.4995 634.78 0.0000 283.69 26.5867 413.71 25.6738 635.95 13.6445 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 20.8405 423. 72 0.0000 645.85 13. 7112 285.90 0.0000 427.09 19.0025 657.76 2.9552 287.50 31.3217 427.87 20.7412 657.90 0.0000 290.67 29.4749 433.94 18.2233 661.66 9.8690 293.27 0.0000 439.40 20.0319 664.57 0.0000 351.93 26.8717 453.88' 14.5083 666.33 0.0000 295.96 26.8893 463.37 13.2703 666.50 0.0000 879.38 26.9531 468.07 17.3033 667.71 0.0000 299.98 26.9875 473.00 0.0000 677.62 9.9443 300.09 26.9903 475.06 12.4779 685.70 0.0000 300.13 26.9910 476.78 16.0602 695.00 0.0000 301.36 21.9297 477.60 19.6390 696.49 11. 0354 302.85 25.0964 482.18 20.1425 696. 51 11. 0354 256.23 24.7401 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 13.0465 306.78 20.0687 497.08 11.7445 697.49 13.0476 308.46 26.0095 505.52 10.8962 702.65 6.0361 311. 90 20.5542 507.63 0.0000 706.68 14 .1105 316.51 26.1921 511. 00 1-4.5757 711. 68 14.1424 319.41 0.0000 514.00 16.4268 720.70 0.0000 320.08 0.0000 514.00 16.4268 721. 93 0.0000 321.04 26.2942 520.40 10.9922 722.78 4.5685 323.87 22.7637 520.69 0.0000 722. 91 12.1831 325.23 30.3864 522.65 0.0000 723.31 12.1855 328.76 0.0000 527.90 0.0000 724 .19 10.6666 333.37 24.1528 528.26 12.8829 727.33 lL 1902 333 .. 97 19.3320 529.59 10.1299 733.00 15.2972 334.37 19.3384 529.87 0.0000 735.93 7.1481 338.28 25.4637 531.02 0.0000 333.97 12.2622 338.32 25.4643 537.26 0.0000 739.50 0.0000 311. 90 37.2515 546.56 0.0000 747.24 13. 3407 340.48 37.2515 552.55 14. 9271 748.06 10.2657 340.55 0.0000 563.25 15.0150 752.31 9.2560 344.28 24.3695 569.33 14.1235 753.82 0.0000 345.93 15.8612 946.00 16.9497 756.73 9.2739 351.06 13.4764 569.70 16.0094 756.80 9.2739 351. 93 13.4858 583.19 18. 9722 884.68 9.3025 Page 393of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 19.6541 1274.44. 6.7751 1620.50 1.0057 766.42 16.5553 1001.03 12.4412 1621. 92 2.0120 766.84 10.3487 1002.74 10.1851 1678.03 *O. 0000 772.60 0.0000 1004.73 .14.7218 1690.97 4.0859 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 0.0000 778.90 7.2811 1028.54 0.0000 1063.66 2.0778 783.70 0.0000 1037.84 5. 7255 1771.35 2.3751 785.37 3.1289 1038.76 0.0000 1791.20 0.0000 792.07 11. 5049 631.:29 9.1868 1808.65 5.2359 794.95 10.4712 1048.07 0.0000 1810.72 0.0000 795.86 9.4277 1049.04 5.7463 1836.06 2.1061 810.06 3.1609 1050.41 3.4495 810.29 5.2686 1063.66 2. 3096 344.28 6.3228 1077.00 0.0000 810.76 7.3774 1077.34 10.4385 815.77 0.0000 1085.87 9.3040 1048.07 0.0000 1093.63 6.9951 832.01 14.8813 1099.45 7.0083 834.85 7.4492 1112. 07 11. 432 9 835.71 9.5808 1112.84 12.3158 836.80 0.0000 1115.54 5.8695 846.75 0.0000 1120.29 8.8171 846.77 6.4150 1120. 55 8.8177 856.80 0.0000 1221. 41 8.8202 8 60. 56 7.5244 1129. 67 8.8428 871.09 6.4756 1131. 51 0.0000 873.19 7.5608 1147.95 0.0000 875.33 0.0000 1173.23 5.7344 879.38 3.2480 1177.95 5.7426 880.51 7.5819 1189.05 10.8025 883.24 8.6742 1204.77 9.0436 884.68 1.0848 1221.41 9.0875 889.28 8.6940 1231. 02 3.6450 894.76 8. 7119 1235.36 0.0000 898.04 9. 812 6 1238.28 6.3920 900. 72 8.7311 1260.41 0.0000 903.28 7. 6471 1271.87 4.6088 911. 20 7.6694 1274.44 8.3018 912.08 3.2880 1274.54 8.3024 923.98 0.0000 1291.59 3.7073 926.50 5.2885 1298.22 0.0000 929 .11 3.9702 1312 .11 0.0000 937.49 6.6370 1332.49 4.6857 944.13 0.0000 1362.66 0.0000 946.00 9.9858 1365.19 3.7810 949.00 5.5536 1368.63 0.0000 667.71 0.0000 1384.29 4.7498 962. 31 11.7177 1408.01 6.6902* 964.08 8.9333 1457.56 0.0000 966 .17 8.9398 1460.82 3.8740 911. 20 8.9486 1489.16 2.9257 968.97 8.9486 1505.03 3.9160 983.53 0.0000 1584.12 0.9974 984.45 0.0000 1596. 21 0.0000 Page 394of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:51:49.57 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R1203621685.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM44.CNF;lll Background date : Z-OCT-2016 11:02:28. Sample date 12-SEP-2016 00:00:00 Acquisition date : 3-0CT-2016 04:48:39. Sample ID R1203621685 Sample quantity : l.55344E+02 GRAM Detector name : GAM44 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.56 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596387 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 59.87 10 23 1. 08 120.19 116 6 2.79E-03 81. 3 2 0 63.86* 5 36 0.69 12 8. 17 124 7 l.29E-03233.9 3 0 93.21* 17 60 1. 80 186.90 180 14 4.78E-03104.0 4 0 110. 65 6 29 0.48 221. 7 9 219 6 l.65E-03146.2 5 0 158.74 13 15 1. 30 318.00 316 5 3. 61E-03 52.6 6 0 185.79* 10 29 1. 26 372.13 369 9 2.70E-03117.5 7 0 273.12 12 33 4.31 546.87 539 13 3.19E-03106.4 8 0 343.09 12 5 1. 41 686.87 683 7 3.29E-03 43.2 9 0 345.93 15 1 1. 48 692.56 690 6 4; llE-03 28.9 10 0 469.07 15 -3 2.80 938. 96 933 11 4.24E-03 33.1 11 0 511.78* 13 22 1. 97 1024.42 1017 18 3. 57E-03114. 4 12 0 698.41 12 6-3.37 1397.90 1391 11 3.43E-03 46.7 13 0 818.88 12 3 1. 51 1639.00 1633 11 3 .A3E-03 38.5 Flag: "*" = Peak area was modified by background subtraction Page 395of614 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 05:51:51 Configuration Analyses by Sample title Sample date Sample ID Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Rl203621685.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4 MXRl 12-SEP-20l6 00:00:00 R1203621685 SOLID GAMMA44 0 01:00:00.00 1. 50 keV No Linear 75.00 Acquisition date : Sample quantity Sample geometry Detector geometry: Elapsed real time: Half life ratio : Systematic Error Efficiencies at 3-0CT-2016 04:48:39 155.34 GRAM CAN 0 01:00:00.56 10.00 0.00 % Peak Energy 0.0% No interference performed Page 396 of 614 Nuclide Line Activity Report Sample ID : R1203621685 Nuclide Type: Nuclide Energy Area SN-117M 156.02 ------158.56 16 TE-123M 159.00 16 TE-125M 109.28 8 TH-234 63.29 6 92.59 22 U-238 63.29 6 92.59 22 AM-241 59.54 13 ANH-511 511. 00 14 Flag: "*" Key line Page 39?°of 614 %Abn 2 .11 86.40* 84.00* 0.27* 3.70* 4.23 3.70* 4.23 35.90* 100.00* Acquisition date Page : 2 3-0CT-2016 04:48:39 Uncorrected Decay Corr 2-Sigma %Eff pCi/GRAM pCi/GRAM %Error 5.817E+OO ------Line Not Found ------5.787E+OO 1.535E-02 4.528E-02 105.19 5.787E+OO 1.579E-02 1.787E-02 105.19 5.638E+OO 2.383E+OO 3.079E+OO 292.42 2. lllE+OO 3.805E-01 3.805E-01 467.75 4.869E+OO 5.175E-01 5.175E-01 207. 92 2. lllE+OO 3.805E-01 3.805E-01 467.75 4.869E+OO 5.175E-01 5.175E-01 207.92 1.642E+OO 1.098E-01 1.098E-01 162.66 2.428E+OO 2.782E-02 2.782E-02 228.88 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:51:53.02 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration D.KAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R1203621685.CNF;l *
  • Acquisition date 3-0CT-2016 04:48:39 Sensitivity : 3.000 *
  • Detector ID GAM44 Energy toler?nce: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl *
  • Sample ID Rl203621685 Sample Quantity 1.5534E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF'GAM44 CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide SN-117M TE-123M TE-125M TH-234 U-238 . AM-241 ANH-511 Activity (pCi/GRAM 4.528E-02 l.787E-02 3.079E+OO 3.805E-01 3.805E-01 l.098E-01' 2.782E-02 Non-Identified Nuclides Key-Line Activity K.L. Nuclide (pCi/GRAM BE-7 -1.073E-01 NA-22 -1. 072E-02 NA-24 O.OOOE+OO AL-26 -7.083E-03 K-40 7.906E-02 SC-46 5.955E-03 V-48 l.004E-02 CR-51 -1. 811E-01 MN-54 7.585E-04 C0-56 O.OOOE+OO MN-56 O.OOOE+OO C0-57 4.404E-03 C0-58 8.887E-03 'FE-59 -l.120E-02 C0--60 -8.835E-03 ZN-65 -1.326E-02 GE-68 -1.927E-01 AS-73 1. 714E-01 AS-74 -1. 5.8 8E-02 SE-75 2.122E-02 BR-77 -1.578E+Ol SR-82 -6.920E-02 RB-83 -8.lOlE-03 Page 398of614 Cnt uncert ( 1. 96-sigma) 4.668E-02 1.842E-02 8.824E+OO 1.744E+OO 1. 744E+OO 1. 751E-01 6.239E-02 Cnt Uncert ( 1. 96-sigma) 1.659E-01 1.925E-02 3.623E+08 2.099E-02 2.638E-01 2.287E-02 3.587E-02 2.003E-01 2.161E-02 2.747E-02 1.960E+41 1.274E-02 2.688E-02 4.404E-02 2.105E-02 4. 222K-02 7.108E-01 7.999E-01 6.178E-02 2.539E-02 2.519E+Ol 2.270E-01 4.469E-02 MDA (pCi/GRAM 6.980E-02 3.028E-02 1.122E+Ol 1.728E+OO l.728E+00 2.305E-01 3.580E-02 MDA (pCi/GRAM 3.027E-01 3.556E-02 O.OOOE+OO 4.219E-02 6.887E-01 5.356E-02 9.315E-02 3.604E-01 4.484E-02 5.552E-02 O.OOOE+OO 2.693E-02 5.877E-02 9.366E-02 4.102E-02 8.636E-02 1.456E+OO 1.708E+OO 1.227E-01 5.550E-02 4.850E+Ol 4.331E-01 8.953E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT 'IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

KR-85 8.016E+OO 5.519E+OO 1.295E+Ol NOT IDENT. SR-85 4.519E-02 3 .117E-02 7.310E-02 NOT IDENT. RB-86 2.267E-Ol 5.096E-01 l.259E+00 NOT. IDENT. Y-88 -6.030E-03 l.182E-02 1.819E-02 NOT IDENT. Y-91 6.078E+OO 1.148E+Ol 2.817E+Ol NOT IDENT. NB-94 2.616E-02 2.193E-02 5.248E-02 NOT IDENT. NB-95 1.254E-02 2.471E-02 5.699E-02 NOT IDENT. NB-95M l .116E-02 5.839E-02 1.177E-01 NOT IDENT. ZR-95 l.684E-02 3.874E-02 9.179E-02 NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 4.669E+08 O.OOOE+OO SHORT HLIF M0-99 1.683E+Ol 3.301E+Ol 7.647E+Ol NOT IDENT. TC-99M O.OOOE+OO 3.536E+23 O.OOOE+OO SHORT HLIF RH-101 -6.940E-03 l.467E-02 2.748E-02 NOT IDENT. RH-102 -2.700E-03 3.421E-02 6.922E-02 FAIL ABUN RU-103 -1. 7 90E-02 2.824E-02 5. ll 7E-02 NOT IDENT. RH-106 1.509E-02 2.200E-01 4.514E-01 NOT IDENT. RU-106 l.509E-02 2.200E-01 4.514E-01 NOT IDENT. AG-108M 9.582E-03 1.503E-02 3.574E-02 NOT IDENT. CD-109 2.184E-01 3.295E-01 7.244E-01 NOT IDENT. AG-llOM -4.466E-04 3.002E-02 6.550E-02 NOT IDENT. SN-113 -1. 211E-02 2.457E-02 4.728E-02 NOT IDENT. CD-115 1.193E+Ol 3.072E+Ol 7.553E+Ol NOT IDENT. SB-124 7 .118E-02 1.733E-01 NOT IDENT. SB-125 6.832E-03 4.799E-02 l.043E-01 NOT IDENT. I-126 -8.678E-02 1. 976E-01 3. 631E-01 NOT IDENT. SB-126 -5.294E-03 1.056E-01 2.199E-01 FAIL ABUN SN-126 1.481E-02 , 3. 255E-02 6.908E-02 FAIL ABUN SB-127 6.589E-02 2.082E+OO 4.437E+00 NOT IDENT. I-131 8.310E-04 l.213E-01 2.512E-01 NOT IDENT. I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 4.347E-01 2.826E+OO FAIL ABUN BA-133 -5.548E-03 2.467E-02 4.956E-02 NOT IDENT. I-133 O.OOOE+OO 4.063E+05 O.OOOE+OO SHORT HLIF CS-134 l.271E-02 1.952E-02 4.921E-02 NOT IDENT. CS-135 -l.314E-02 7.997E-02 l.493E-01 NOT IDENT. I-135 O.OOOE+OO 1. 220E+22 0.000E+OO SHORT HLIF CS-136 -2.324E-02 6.214E-02 1. 285E-01 FAIL ABUN BA-137M -6.667E-03 2.097E-02 4.013E-02 NOT IDENT. CS-137 -7.043E-03 2.216E-02 4.239E-02 NOT IDENT. CE-139 -l.OOOE-02 1.609E-02 2.855E-02 NOT IDENT. BA-140 5.864E-02 2.259E-01 4.908E-01 NOT IDENT. LA-140 -2.045E-02 7.712E-02 .1. 576E-01 NOT IDENT. CE-141

  • 5.884E-03 3.336E-02 6.816E-02 NOT IDENT. CE-143 O.OOOE+OO l.184E+03 O.OOOE+OO SHORT HLIF CE-144 -l.813E-02 l.006E-01 l.955E-01 NOT IDENT. PM-144 3.247E-03 2 .172E-02 4.560E-02 NOT IDENT. PR-144 2.518E-01 1.633E+OO 3.430E+OO NOT IDENT. PM-146 2.208E-02 2.147E-02 5.415E-02 NOT IDENT. ND-147 -2.337E-04 4.697E-01 9.846E-01 NOT IDENT. PM-147 -7.348E+Ol 3.763E+02 7.368E+02 NOT IDENT. PM-149 -1.152E+02 3.029E+02 6.082E+02 NOT IDENT. EU-150 -9.176E-03 l.324E-02 2.484E-02 NOT IDENT. EU-152 7.182E-02 6.077E-02 1.107E-01 FAIL ABUN GD-153 6.598E-04 4. 513E-02 8.618E-02 NOT IDENT. EU-154 -2.788E-02 5.538E-02 l.050E-01 NOT IDENT. EU-155 -2.940E-02 4. 851E-02 9. 031E-02 NOT IDENT. TB-160 l.043E-01 8. 965E-02 2.326E-01 NOT IDENT. H0-166M -l.974E-02 3.562E-02 6.317E-02 FAIL ABUN TM-171 -2.201E+OO 1. 725E+Ol 3.534E+Ol NOT IDENT. HF-172 -5.140E-02 8.765E-02 1. 611E-01 FAIL ABUN LU-172 -9.886E-03 2.287E-02* 4.691E-02 FAIL ABUN LU-176 -4.735E-03 l.320E-02 2.651E-02 NOT IDENT. HF-181 2.688E-02 3.288E-02 7.542E-02 FAIL ABUN TA-182 -1.201E-01 9.614E-02 1.150E-01 NOT IDENT. RE-183 -8.348E-02 1.454E-01 2.591E-01 FAIL ABUN RE-184 3.681E-03 9.074E-02 1. 966E-01 NOT IDENT. W-188 -8.627E-01 3.429E+OO 7.087E+OO FAIL ABUN IR-192 4.760E-03 l.794E-02 3.982E-02 FAIL ABUN HG-203 4.643E-03 2.270E-02 4.877E-02 NOT IDENT. BI-207 l.613E-02 3.325E-02 7.794E-02 NOT IDENT. TL-208 4.725E-03 2. 421E-02 5.144E-02 NOT IDENT. PB-210 3.062E-02 3.459E+OO 7.637E+OO NOT IDENT. BI-211 -7.327E-02 l.262E-01 2.429E-01 NOT IDENT. PB-211 -2.005E-Ol 3.285E-01 6.174E-01 NOT IDENT. .BI-212 -l.591E-01 2.450E-01 4.178E-01 NOT IDENT. PB-212 -1.185E-02 2.714E-02 5.414E-02 NOT IDENT. BI-214 3.962E-02 5.239E-02 1.172E-01 NOT IDENT. Page 399of614 PB-214 -5.405E-02 4:824E-02 8.476E-02 NOT IDENT. RN-219 7.242E-02 2. lOlE-01 4.707E-01 NOT IDENT. RN-222 3. 962E-02 5.239E-02 l. l 72E-01 NOT IDENT. RA-223 6.435E-02 3.080E-01 6.782E-01 FAIL ABUN RA-224 -2. 968E-01 2.982E-01 4.622E-01 NOT IDENT. RA-226 3. 962E-02 5.239E-02 1.172E-01 NOT IDENT. AC-227 -8.820E-03 l.252E-01 2.400E-01 NOT IDENT. TH-227 -8.820E-03 1.252E-01 2.400E-01 NOT IDENT. AC-228 -5. 481E-02 9. 021E.:._02 1. 728E-01 NOT IDENT. RA-228 -5.481E-02 9.021E-02 1. 728E-01 NOT IDENT. TH-228 -l.185E-02 2.714E-02 5.414E-02 NOT IDENT. TH-229 1.072E-01 2.576E-01 5.346E-01 NOT IDENT. TH-230 3. 962E-02 5.238E-02 1.172E-01 NOT IDENT. PA-231 -2.374E-02 1.983E-01 4.222E-01 NOT IDENT. TH-231 6.435E-02 3.0BOE-01 6.782E-01 NOT IDENT. TH-232 -5. 481E-02 9. 021E-02 1. 728E-01 NOT IDENT. PA-233 ...:.1. 410E-02 2.734E-02 5. 396E-02 NOT IDENT. PA-234 2.167E-02 1. 774E-01 3.974E-01 FAIL ABUN PA-234M -l.408E-01 2.061E+OO 4.643E+OO NOT IDENT. U-234 3.962E-02 5.238E-02 l.172E-01 NOT IDENT. U-235 -7.152E-02 9.518E-02 1.673E-01 FAIL ABUN NP-237 -1.410E-02 2.734E-02 . 5. 396E-02 FAIL ABUN NP-238 O.OOOE+OO 6.348E+Ol 0.000E+OO SHORT HLIF NP-239 -6.829E-02 1. 409E-01 2.640E-01 NOT IDENT. PU-239 2.426E+Ol 1. 584E+02 3. 261E+02 NOT IDENT. AM-243 1.078E-02 2.767E-02 6.030E-02 NOT IDENT. CM-243 3.064E-03 5.024E-02 1.043E-01 NOT IDENT. BK-247 2.294E-02 4.359E_:02 9.138E-02 NOT IDENT. CM-247 l.252E-02 1. 879E-02 4.440E-02 NOT IDENT. CF-249 6.673E-03 2.288E-02 4.989E-02 NOT IDENT. CF-251 -1.693E-02 5.894E-02 1. llOE-01 NOT IDENT. Page 400of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:51:50.38 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Krror SN-117M 156.02 ------2 .11 5.817E+OO ------Line Not Found ------158.56 16 86.40* 5.787E+OO l.535E-02 4.528E-02 105.19 TE-123M 159.00 16 84.00* 5.787E+OO 1.579E-02 1. 787E-02 105.19 TE-125M 109.28 8 0.27* 5.638E+OO 2.383E+OO 3.079E+OO 292.42 TH-234 63.29 6 3.70* 2. lllE+OO 3.805E-01 3.805E-01 467.75 92.59 22 4.23 4.869E+OO 5.175E-01 5.175E-01 207.92 U-238 63.29 6 3.70* 2. lllE+OO 3.805E-01 3.805E-01 467.75 92.59 22 4.23 4.869E+OO 5.175E-01 5.175E-01 207.92 AM.:.241 59.54 13 35.90* l.642E+OO 1.098E-01 l.098E-01 162.66 ANH-511 511. 00 14 100.00* 2.428E+OO 2.782E-02 2.782E-02 228:88 Flag: "*" Key line Page401 of614 Summary of Nuclide Activity Sample ID : Rl203621685 Acquisition date Page : 2 3-0CT-2016 04:48:39 Total number of lines in spectrum 13 Number of unidentified lines O Number of lines tentatively identified by NID 13 100.00% Nuclide Type : Uncorrected Decay Corr Decay Corr 2-Sigma Nuclide Hlife Decay pCi/GRAM pCi/GRAM 2-Sigma Error %Error Flags SN-117M 13.60D 2.95 l.535E-02 4.528E-02 4.763E_.:02 105.19 TE-123M 119. 20D 1.13 l.579E-02 l.787E-02 l.879E-02* 105.19 TE-125M 57.40D 1. 29 2.383E+OO 3.079E+OO 9.004E+OO 292.42 'TH-234 4.47E+09Y 1. 00 3.805E-01 3.805E-01 17.80E-01 467.75 U-238 4.47E+09Y 1. 00 3.805E-01 3.805E-01 17.80E-01 467.75 AM-241 432.60Y 1. 00 1.098E-01 1.098E-01 1. 786E-01 162.66 ANH-511 l.OOE+09Y 1. 00 2.782E-02 2.782E-02 6.366E-02 228.88 ------------------Total Activity 3. 313E+OO 4.041E+OO Grand Total Activity 3.313E+OO 4.041E+OO Flags: "K" Key line not found "M" Manually accepted "E" = Manually. edited "A" = Nuclide specific abn. limit Page 402of614 Unidentified Energy Lines Page : 3 Sample ID : R1203621685 Acguisition date : 3-0CT-2016 04:48:39 It Energy Area. Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 185.79 12 35 1. 26 372 .13 369 9 2.70E-03 **** 5. 41E+OO T 0 273.12 13 38 4.31 546.87 539 13 3.19E-03 **** 4.13E+OO T 0 343.09 13 6 1. 41 686.87 683 7 3.29E-03 86.3 3.41E+OO T 0 345.93 17 1 1. 48 692.56 690 6 4. llE-03 57.8 3.39E+00 T 0 469.07 17 3 2.80 938. 96 933 11 4.24E-03 66.2 2.61E+OO T 0 698.41 13 6 3.37 1397.90 1391 11 3.43E-03 93.3 1.88E+OO T 0 818.88 13 3 1. 51 1639.00 1633 11 3.43E-03 77 ."0 1. 66E+OO T Flags: "T" = Tentatively associated Page 403 of 614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:52:07.30 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE.DATA * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R120362lq85.CNF;l *
  • Acquisition date 3-0CT-2016 04:48:39 Sensitivity : 3.000 *
  • Detector ID GAM44 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID * **Sample ID R1203621685 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.5534E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF' GAM44 CAN.CNF;3
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide SN-117M TE-123M TE-125M TH-234 U-238 AM-241 ANH-511 Le (pCi/GRAM 3.079E-02 1.352E-02 5.009E+OO 7.698E-01 7.698E-01 1. 02 9E-01 1. 511E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 *co-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 Page 404 of 614 Le (pCi/GRAM 1.180E-01 1.197E-02 O.OOOE+OO 1.334E-02 2.844E-01 2.165E-02 3.487E-02 1.476E-01 1.812E-02 2.274E-02 O.OOOE+OO 1.199E-02 2.442E-02 3. 431E-02 1.453E-02
  • 3.239E-02 5.641E-01 7.640E-01 4.911E-02 2.463E-02 2.107E+Ol 1.706E-01 3.731E-02 5.827E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RH-106 RU-106 AG-108M CD-109 AG-110M SN-113 CD-115 SB-124

  • SB-125 I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150
  • EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 TL-208 PB-210 BI-211 PB-211 BI-212 PB-212 BI-214 PB-214 Page 405of614 3.290E-02 5 .. 024E-01 0.000E+OO 1.138E+Ol 2.265E-02 2.366E-02 5.130E-02 3.710E-02 O.OOOE+OO O.OOOE+OO 3.173E+Ol O.OOOE+OO 1.197E-02 2.865E-02 2.122E-02 l.915E-01 1.915E-01 l.517E-02 3.185E-01 2.649E-02 l.972E-02 3.008E+Ol 6.715E-02 4:394E-02 1. 489E-01 8.756E-02 3.027E-02 1. 782E+OO 1.094E-01 0. OOOE+OO. 1. 249E+OO 2.143E-02 O.OOOE+OO 1.989E-02 6.436E-02 O.OOOE+OO 4. 551E-02 1.625E-02 1. 716E-02 1. 2-57E-02 2.077E-01 5.584E-02 3.023E-02 O.OOOE+OO 8.658E-02 1. 907E-02 l.435E+OO 2.316E-02 4.085E-01 3.257E+02 2.609E+02 1.037E-02 4.774E-02 3.803E-02 3.609E-02 3.899E-02 9.891E-02 2.488E-02 1.577E+Ol 6.978E-02 1.524E-02 l.130E-02 3.304E-02 3.420E-02 1.115E-01 8.097E-02 3.005E+OO l.714E-02 2. 153E-02 ' 3.233E-02 2.207E-02 3.297E+OO l.056E-01 2 .. 477E-01 1.536E-01 2.361E-02 5.154E-02 3.662E-02 NOT IDENT. .NOT IDENT. NOT "IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT .IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT'IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN . NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

RN-219 RN-222 RA-223 RA-224 RA-226 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-231 TH-232 PA-233 PA-234 PA-234M U-234 U-235 NP-237 NP-238 NP-239 PU-239 AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 Page 406 of 614 2.007E-01 5.154E-02 2.911E-01 1.941E-01 5.154E-02 1.033E-01 l.033E-01 6.941E-02 6.941E-02 2.361E-02 2.375E-01 5.154E-02 1. 774E-01 2. 911E-01 6.941E-02 2.215E-02 1.610E-01 1. 759E+OO 5.154E-02 7.288E-02 2.215E-02 O.OOOE+OO 1.167E-01 1.443E+02 2.697E-02 4.586E-02 4.026E-02 l.902E-02 2.158E-02 4.825E-02 NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT. I DENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:52:13.14 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road * *
  • Charleston, SC 29407 . * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Rl203621685.CNF;l *
  • Acquisition date 3-0CT-2016 04:48:39 Sensitivity : 3.000 *
  • Detector ID GAM44 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID R1203621685 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.5534E+02 GRAM *
  • Quantity Err(%) : 1.2875E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry' : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3 .
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1 . 96-sigma ) SN-ll 7M 4.528E-02 4. 672E-02 4. 672E-02 TE-123M 1. 787E-02 1.843E-02 l.843E-02 TE-125M 3.079E+OO 8.826E+OO 8.826E+OO TH-234 3.805E-01 1. 746E+OO 1. 746E+OO U-238 3.805E-01 1. 746E+OO 1. 746E+OO AM-241 l.098E-01 1. 753E-01 1. 753E-01 ANH-511 2.782E-02 6.240E-02 6.240E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7. -1. 073E-01 l.660E-01 1.729E-01 NOT IDENT. NA-22 -1. 072E-02 l.925E-02 l.985E-02 NOT IDENT. NA-24 1. 023E+07 3.623E+08 3:623E+08 SHORT HLIF AL-26 -7.083E-03 2.099E-02 2.123E-02 NOT IDENT. K-40 7.906E-02 2.638E-01 2.662E-01 NOT IDENT. SC-46 5.955E-03 2.287E-02 2.303E-02 NOT IDENT. V-48 1.004E-02 3.587E-02 3.616E-02 NOT IDENT. CR-51 -1. 811E-01 2.005E-01 2.165E-01 NOT IDENT. MN-54 7.585E-04 2.161E-02 2 .161E-02 NOT IDENT. C0-56 O.OOOE+OO 2.747E-02 O.OOOE+OO NOT IDENT. MN-56 O.OOOE+OO 7.571E+41 0. OOO'E+OO SHORT HLIF C0-57 4.404E-03 1.274E-02 1. 2 90E-02 NOT IDENT. C0-58 8.887E-03 2.688E-02 2.718E-02 NOT IDENT. FE-59 -1.120E-02 4.405E-02 4.434E-02 NOT IDENT. C0-60 -8.835E-03 2.106E-02 2.143E-02 NOT IDENT. ZN-65 -1. 326E-02 4.223E-02 4.265E-02 NOT IDENT. GE-68 -1.927E-01 7.109E-01 7.162E-01 NOT IDENT. AS-73 1.714E-01 8.007E-01 8.044E-01 NOT IDENT. AS-74 -1.588E-02 6.179E-02 6.220E-02 NOT IDENT. SE-75 2.122E-02 2.541E-02 2. 715E-02 NOT IDENT. BR-77 -1.578E+Ol 2.699E+Ol 2. 7 91E+Ol NOT IDENT. SR-82 -6.920E-02 2.270E-01 2.292E-01 NOT IDENT. RB-83 -8.lOlE-03 4.470E-02 4.485E-02 NOT IDENT. Page 407 of 614 KR-85 8.016E+00 5.528E+OO 6.605E+OO NOT IDENT. SR-85 4.519E-02 3.122E-02 3.728E-02 NOT IDENT. RB-86 2.267E-01 5.097E-01 5.199E-01 NOT IDENT. Y-88 -6.030E-03 l.182E-02 l.213E-02 NOT IDENT. Y-91 6.078E+00 l.148E+Ol l.180E+Ol NOT IDENT. NB-94 2.616E-02 2 .196E-02 2.493E-02 NOT IDENT. NB-95 l.254E-02 2.471E-02 2.535E-02 NOT IDENT. NB-95M 1.116E-02 5.839E-02 5.861E-02 NOT IDENT. ZR-95 l.684E-02 3.875E-02 3.948E-02 NOT IDENT. NB-97 1.000E+41 2.493E+41 O.OOOE+OO SHORT HLIF ZR-97 -1.719E+08 4.669E+08 4.733E+08 SHORT HLIF M0-99 1.683E+Ol 3.302E+Ol 3.388E+Ol NOT IDENT. TC-99M 1.248E+23 3.538E+23 O.OOOE+OO SHORT HLIF RH-101 -6.940E-03 l.473E-02 1.506E-02 NOT IDENT. RH-102 -2.700E-03 3.421E-02 3.424E-02 FAIL ABUN RU-103 -1. 7 90E-02 2.825E-02 2.938E-02 NOT IDENT. RH-106 l.509E-02 2.200E-01 2.201E-01 NOT IDENT. RU-106 1.509E-02 2.200E-Ol* 2.201E-01 NOT IDENT. AG-108M 9.582E-03 1.504E-02 l.565E-02 NOT IDENT. CD-109 2.184E-01 3.299E-01 3.443E-01 NOT IDENT. AG-llOM -4.466E-04 3.002E-02 3.002E-02 NOT I-DENT. SN-113 -1. 211E-02 2.458E-02 2.518E-02 NOT IDENT. CD-115 1.193E+Ol 3.073E+Ol 3 .119E+Ol NOT IDENT. SB-124 2.607E-02 7.120E-02 7.216E-02 NOT IDENT. SB-125 6.832E-03 4.799E-02 4.809E-02 NOT IDENT. I-126 -8.678E-02 1.977E-01 2.015E-01 NOT IDENT. SB-126 -5.294E-03 1.056E-01 l.056E-01 FAIL ABUN SN-126 l.481E-02 3.256E-02 3.324E-02 FAIL ABUN SB-127 6.589E-02 2.082E+OO 2.082E+OO NOT IDENT. I-131 8.310E-04 1.213E-01 l.213E-01 NOT IDENT. I-132 l.000E+41 3.675E+41 O.OOOE+OO SHORT HLIF TE-132 4.347E-01 1.393E+OO 1.407E+OO FAIL ABUN BA-133 -5.548E-03 2.467E-02 2.479E-02 NOT IDENT. I-133 l.107E+05 4.066E+05 4. 096E+05 SHORT HLIF CS-134 1.271E-02 1.952E-02 2.035E-02 NOT IDENT. CS-135 -l.314E-02 7.997E-02 8.019E-02 NOT IDENT. I-135 7.823E+21 1.278E+22 O.OOOE+OO SHORT HLIF CS-136 -2.324E-02 6.217E-02 6.304E-02 FAIL ABUN BA-137M -6.667E-03 2.098E-02 2 .119E-02 NOT IDENT. CS-137 -7.043E-03 2.216E-02 2.239E-02 NOT IDENT. CE-139 -l.OOOE-02 1.622E-02 1.683E-02 NOT IDENT. BA-140 5.864E-02 2.259E-01 2.275E-01 NOT IDENT. LA-140 -2.045E-02 7. 713E-02 7.767E-02 NOT IDENT. CE-141 5.884E-03 3.336E-02 3.346E-02 NOT IDENT. CE-143 -5.253E+02 l.185E+03 l.208E+03 SHORT HLIF CE-144 -l.813E-02 1. 006E-01 1.009E-01 NOT IDENT. PM-144 3.247E-03 2 .172E-02 2.177E-02 NOT IDENT. PR-144 2.518E-01 1.633E+OO l.637E+OO NOT IDENT. PM-146 2.208E-02 2.152E-02 2.371E-02 NOT IDENT. ND-147 4.697E-01 4.697E-01 NOT IDENT. PM-147 -7.348E+Ol 3.764E+02 3.778E+02 NOT IDENT. PM-149 -,-l .152E+02 3.033E+02 3.077E+02 NOT IDENT. EU-150 -9.176E-03 l.324E-02 1.388E-02 NOT IDENT. EU-152 7.182E-02 6.090E-02 6.897E-02 FAIL ABUN GD-153 6.598E-04 4.513E-02 4.514E-02 NOT IDENT. EU-154 -2.788E-02 5.539E-02 5.680E-02 NOT IDENT. EU-155 -2.940E-02 4.856E-02 5.033E-02 NOT IDENT. TB-160 1.04JE-01 8.985E-02 1.014E-01 NOT IDENT. H0-166M -1.974E-02 3.564E-02 3.673E-02 FAIL ABUN TM-171 -2. 201E+OO 1. 726E+Ol 1. 728E+Ol NOT IDENT. HF-172 -5.140E-02 8.805E-02 9.104E-02 FAIL ABUN LU-172 -9.886E-03 2.289E-02 2.332E-02 FAIL ABUN LU-17 6 -4.735E-03 1.320E-02 l.337E-02 NOT IDENT. HF-181 2.688E-02. 3.290E-02 3.506E-02 FAIL ABUN TA-182 -1.201E-01 9.625E-02 l.104E-01 NOT IDENT. RE-183 -8.348E-02 1.457E-01 1. 504E--01 FAIL ABUN RE-184 3.681E-03
  • 9.074E-02 9.076E-02 NOT IDENT. W-188 -8.627E-01 3.430E+OO 3.452E+OO FAIL ABUN IR-192 4.760E-03 l.794E-02 1.807E..'...02 FAIL ABUN HG-203 4.643E-03 2.270E-02 2.280E-02 NOT IDENT. BI-207 1.613E-02 3.326E-02 3.405E-02 NOT IDENT. TL-208 4. 725E-03 2.421E-02 2.430E-02 NOT IDENT. PB-210 3.062E-02 3.459E+OO 3.459E+OO NOT *IDENT. BI-211 -7.327E-02 1. 263E-01 1.305E-01 NOT IDENT. PB-211 -2.005E-01 3.286E-01 3.408E-01 NOT IDENT. BI-212 -l.591E-01 2.452E-01 2.554E-01 NOT IDENT. PB-212 -1.185E-02 2. 715E-02 2.767E-02 NOT IDENT. BI-214 3.962E-02 5.241E-02 5.537E-02 NOT IDENT. Page 408 of 614 PB-214 -5.405E-02 4.829E-02 5.409E-02 NOT IDENT. RN-219 7.242E-02 2.103E-01 2.128E-01 NOT IDENT. RN-222 3. 962E-02 5.241E-02 5.537E-02 NOT IDENT. RA-223 6.435E-02 3.081E-01 3.094E-01 FAIL ABUN RA-224 -2.968E-01 2.987E-01 3.272E-01 NOT IDENT. RA-226 3.962E-02 5.241E-02 5.537E-02 NOT IDENT. AC-227 -8.820E-03 1.252E-01 1.252E-01 NOT IDENT. TH-227 -8.820E-03 1.252E:-01 l.252E-01 NOT IDENT. AC-228 -5.481E-02 9.025E-02 9.357E-02 NOT IDENT. RA-228 -5.481E-02 9.025E-02 9.357E-02 NOT IDENT. TH-228 -1.185E-02 2.715E-02 2.767E-02 NOT IDENT. TH-229 1.072E-01 2.577E-01 2.622E-01 NOT IDENT. TH-230 3. 962E-02 5.241E-02 5.537E-02 NOT IDENT. PA-231 -2.374E-02 l.984E-01 1.987E-01 NOT IDENT. TH-231 6.435E-02 3.081E-01 3.094E-01 NOT IDENT. TH-232 -5.481E-02 9.025E-02 9.357E-02 NOT IDENT. PA-233 -1.410E-02 2.735E-02 2.808E-02 NOT IDENT. PA-234 2.167E-02 1. 791E-01 1.794E-01 FAIL ABUN PA-234M -1.408E-01 2.061E+OO 2.062E+OO NOT IDENT. U-234 3. 962E-02 5.241E-02 5.537E-02 NOT IDENT. U-235 -7.152E-02 9.524E-02 1.006E-01 FAIL ABUN NP-237 -1.410E-02 2.735E-02 2.808E-02 FAIL ABUN NP-238 3.788E+OO 6.348E+01 6.350E+Ol SHORT HLIF NP-239 -6.829E-02 1.410E-01 1.443E-01 NOT IDENT. PU-239 2.426E+Ol 1.584E+02 1.588E+02 NOT IDENT. AM-243 1.078E-02 2.768E-02 2.SlOE-02 NOT IDENT. CM-243 3.064E-03 5.024E-02 5.026E-02 NOT IDENT. BK-247 2.294E-02 4.383E-02 4.504E-02 NOT IDENT. CM-247 1.252E-02 1.890E-02 1.973E-02 NOT IDENT. CF-249 6.673E-03 2.289E-02 2.308E-02 NOT IDENT. CF-251 -1.693E-02 5.897E-02 5.946E-02 NOT IDENT. Page 409 of 614
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 14.9948 87.09 .15.7644 136.47 17.1838 45.60 16.8701 87.57 11. 8350 140.51 19.4485 46.54 13.3577 88.03 10.5299 143.76 24.9692 49. 72 17.9833 88.34 10.5365 144.24 20.6412 51. 35 18.0699 88.47 10.5393 145.44 18.5004 51. 87 16.2875 89. 96 18.4993 152.43 23.0806 52.39 21.7493 90.64 16. 8706, 153.25 19.8059 52.97 22.6933 91.11 16.8864 154.21 22.0355 53.44 18.1789 92.59 16.9359 156.02 20.6178 54.07 17.30.08 93.35 16. 9612 158.56 18.8420 57.36 0.0000 . 94. 56 17.0013 159.00 23.2892 57.53 14.7090 94.65 17.0043 162.33 16.7095 57.98 19.6358 94.67 17.0049 162.66 23.4036 59. 27 23.0903 94.87 17.0115 163.33 23.4244 59.32 23.0933 97.43 18.7713 165.86 26.8601 59.54 23.1068 98.43 20.1503 176.31 11. 3425 60. 96 27.8317 98.44 '20 .1507 176.60 11.3466 61.17 27.8469 99.53 20.1921 177.52 18.1755 62.93 22.3788 100.11 24.2567 181.07 14.8327 63.29 22.3993 102.03 13.1860 181.52 12.5576 63.58 22.4158 103.18 17.2795 184.41 21. 3851 64.28 19.9604 103.37 17. 2856 185. 72 11.4746 66.73 12.5515 105.21 20.4041 193.51 16.2138 67.24 14.1380 105.31 20.4077 197.03 23.2578 67.68 *18.8710 106.12 17.3718 198.01 15.1346 67.75 18.8741 106.47 17.3827 201.83 23.3862 69.67 19.9097 109.28 23.2927 203.43 12.8858 70.83 13.3097 111. 00 24.7372 205.31 21.1303 72.81 21. 0122 111.76 20.6415 210.85 20.0796 72.87 21.0152 114. 06 27.9762 215.65 16.6231 74.66 19.1833 116. 30 29.1228 222 .11 8.3692 74.82 19.1904 116.74 26.0218 227.09 19.2300 74.97 19 .1969 119.76 26.1528 227.38 13.2246 77.11 18.3251 121. 12 22.0174 228.16 15.6418 78.74 21. 2952 121. 22 22.0211 228.18 14.4390 79.69 16. 4896 121.78 14.6941 235.69 13.3381 80.12 23.3013 122.06 17.8510 235. 96 14.5545 80.19 23.3047 122.92 22.0819 238.63 9.7292 80.57 20.4085 123.07 18.9321* 238.98 10.9492 81. 00 18.4821 123.68 18.9507 240.99 20.7234 81. 07 15.5662 125.81 21.1284 242.00 9.7621 81. 75 25.3319 127.23 21.1758 244.70 15.9058 83.79 21.5278 127.91 16.9590 252.40 14.7929 84.00 18.6005 129.30 18.0581 252.80 11. 098 9 85.43 18.6562 131. 20 21. 3080 254.15 0.0000 86.55 13.7786 133.02 18.1624 256.23 13.6100 86.79 13.7853 133.52 22.4532 260.90 9.9421 86.94 13.7897 136.00 22.5378 264.66 11. 2242 Page 410 of 614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.80 12.4731 364.49 15.3423 600.60 8.3102 265.00 12.4753 366.42 16.2675 602.52 0.0000 268.22 15.0150 372. 51 8 .1696 604. 72 11. 4498 269.46 11. 2742 375.05 8.1846* 607.14 13.5475 270.03 13.7866 377.52 7.2879 609.32 6.2595 271.23 14.2203 383.85 12.8111 610. 3'.3 8.3499 273.65 14.2514 388.16 11. 0142 614.28 5.2289 276.40 12.6062 388.63 11.0176 618.01 7.3335 277.37 20.1875 391.69 12.8812 620.36 4.1953 277.60 20.1914 400.66 13.8864 621.93 8.3971 278.00 20.1987 401.81 8.3383 630.19 0.0000 279.20 16.8506 402.40 6.4880 631.29 8.4349 279.54 16.8555 404.85 10.2122 633.25 8.4427 279.70 16.0150 410.95 14.9150 634.78 10.5611 280.46 14.3389 413.71 11.2068 635.95 11. 6235 283.69 15.2260 414.70 12.1486 636.99 6.3433 284.31 13.5417 423.72 6.5804 645.85 7.4312 285.41 15.2490 427.09 8.4791 657.76 3.2024 285.90 16.1031 427.87 8.4833 657.90 0.0000 287.50 15.2772 433 _*94 5.6776 661.66 8.5550 290.67 12.7661 439.40 8.5459 664.57 0.0000 293.27 0.0000 453.88 3.8327 666.33 10.7166 295.22 12.8162 463.37 10.4084 666.50 8.5739 295. 96 9.4046 468.07 3.8660 667.71 0.0000 298.58 11.9962 473.00 7.2702 677.62 7.5400 299.98 12.8683 475.06 1. 9411 685.70 5.4053 300.09 12.8696 476.78 9.7154 695.00 9.7694 300 .13 12.8699 477.60 8.7480 696.49 7.6033 301.36 10.3066 482.18 8.7719 696.51 7.6036 302.85 12.8995 487.02 11.7290 697.00 7. 6050' 304.50 11. 1952 492.35 13.7261 697.30 7.6061 304.85 8.6141 497.08 13.7636 697.49 7.6067 306.78 14.6678, 505.52 16.2996 702.65 3.2673 308.46 10.3682 507.63 0.0000 706.68 7. 6372 311. 90 11.2642 511. 00 9.9093 711. 68 8.7471 316.51 10.4370 514.00 9.9259 720.70 5.4883 319 .. 41 12.2050 514.00 9.9259 721. 93 0.0000 320.08 14.8283 520.40 9. 9613 722.78 1.0986 321. 04 12.2209 520.69 9. 9630 722.91 3.2960 323.87 10.4990 522.65 0.0000 723.31 3.2966 325.23 11.3864 527.90 3.0.007 724.19 5. 4964 328.76 10.5398 528.26 3. 0013 727.33 6.6045 333.37 16:7487 529.59 6. 0071 733.00 5.5170 333.97 14.9926 529.87 0.0000 735.93 9.9426 334.37 15.8796 531. 02 8.0156 737.46 4.4219 -338.28 15.9280 537.26 8.0430 739.50 4.4256 338.32 15.9283 546.56 0.0000 747.24 4.4399 340.48 10.6367 552*. 55 8.1087 748.06 1.1104 340.55 10. 6372 563.25 12.2314 752.31 5.5615 344.28 2.6669 569.33 5 .1125 753.82 1.1130 345.93 6.6757 569.50 5 .1129 756.73 3.3430 . 351. 06 14.2969 569.70 5 .1135 756.80 3.3431 351.93 19.6707 583.19 5.1489 763.94 7.8234 355.39 0.0000 584.27 11.3339 765.81 4.4740 356.01 16.1433 595.83 7.2544 766.42 4 .. 4749 Page 411of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 766.84 4.4757 1002.74 1.8284 1678.03 0.0000 772. 60 0.0000 1004.73 3.6593 1690.97 2.1854 776.52 6.7400 1021.30 0.0000 1750.46 0.0000 777.92 5.6197 1025.87 0.0000 1764.49 2.2188 778.90 7.8707 1028.54 0.0000 1770.23 3.3322 783.70 9.0124 1037.84 3.6985 1771. 35 0.0000 785.37 5.6366 1038.76 0.0000 '1791.20 0.0000 792.07 5.6517 1046.59 3.7085 1808.65 2.2385 794.95 2.2632 1048.07 3.7104 1810.72 0.0000 795.86 2. 26i'.10 1049.04 3.7114 1836.06 0.9002 801. 95 6.8083 1050.41 3.7131 810.06 3.4149 1063.66 4.6606 810.29 3.4153 1077.00 2.8079 810.45 5.6923 1077.34 5.6162 810.76 5.6932 1085.87 1.8770 815.77 5.1337 1093.63 2.8222 818.51 5. 7102 1099.45 3.7695 832.01 8.0356 1112. 07 1. 8920 834.85 5.7458 1112.84 4.7308 835. 71 5.7479 1115.54 4.7348 836.80 0.0000 1120.29 4.7415 846.75 0.0000 1120.55 5.6902 846.77 6.9263 1121.30 2.8456 856.80 5.7935 1129.67 1.9019 860.56 5.8016 1131.51 0.0000 871.09 4.6592 1147.95 0.0000 873.19 2.3314 1173.23 5.7784 875.33 0.0000 1177.95 10.6079 879.38 2.6288 1189.05 1.9348 880.51 6.1363 1204.77 2.9150 883.24 9.6522 1221.41 7.8096 884.68 6.1455 1231. 02 0.9788 889.28 4.3970 1235.36 3.9197 894.76 5.2868 1238.28 0.0000 898.04 9.7036 1260.41 0.0000 900. 72 7.9470 1271.87 1. 97 94 903.28 7.0703 1274.44 3. 9614 911. 20 7.0903 1274.54 3. 9614 912.08 7.0925 1291.59 1. 98 97 923.98 0.0000 1298.22 0.0000 926.50 3.5642 1312 .11 5.0012 929 .11 4.4592 1332.49 4.0222 937.49 3.5778 1362.66 0.0000 944.13 3.5859 1365.19 3.0417 946.00 5.3824 1368.63 0.0000 949.00 5.3879 1384.29 2.0376 954.55 0.0000 1408.01 2. 0496 962. 31 5.4122 1457.56 0.0000 964. 08 3.6104. 1460.82 0.0000 966.17 3.6129 1489.16 2.0898 968. 97 4.5204 1505.03 1. 0488 983.53 1.8170 1584.12 4. 2712 984.45 0.0000 1596.21 3.2119 996.26 3.6492 1620.50 3.2291 1001. *03 3.6549 1621. 92 4.3069 Page 412of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:35:13.71 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R1203621686.CNF;l BacKground file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM05.CNF;477 Background date : Z-OCT-2016 11:00:07. Sample date 15-DEC-2015 10:14:00 Acquisition date : 3-0CT-2016 05:34:41. Sample ID R1203621686 Sample quantity : 1.55344E+02 GRAM Detector name GAM05 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.56 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596387 Detector SN# Matrix Spike ID : LCS ID : 1556 Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 0 2 2 4 4 0 0 0 0 0 0 3 3 0 0 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 413of614 Energy 39.41 46.10* 52.64* 62. 67* 74.46* 76.74* 83.94* 86.80* 89.66 92.75* 98.79* 128.42 185.70* 209.00 238.36* 241.54 294.85* 300.50 320.44 338.07* 341.31 351.70* 463.29 510.89* 583.01* 609.20* 661.10 672.89 728. 30 755.76 769.47 786.00 790.90 857.31 BACKGROUND CORRECTED SAMPLE PEA*K REPORT Area 39 122 23 18 165 325 59 106 60 122 38 26 94 57 370 110 168 10 39 48 20 249 12 49 89 173 37 12 31 17 40 20 4 10 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 104 153 124 264 152 117 131 110 118 149 102 82 85 88 68 62 36 32 70 57 53 56 24 41 33 27 21 16 18 5 12 6 9 6 1. 66 0.83 1. 36 0.97 0.83 0.74 1.15 1. 06 0.98 1.18 0.97 1. 79 1. 42 1. 30 0.98 1. 50 1. 28 0.81 6.79 1. 63 1. 66 1. 02 1. 08 1. 85 1.16 1.26 1.10 0.97 1. 36 1. 05 3.41 2 .13 0.50 1. 45 80.65 94.01 107.09 127.13 150. 71 155.26 169.66 175.37 181.08 187.26 199.34 258.54 373.02 419 .. 59 478.27 484.64 591.18 602.46 642.32 677.56 684.03 704.80 927.83 1022.97 1167 .10 1219:46 1323.19 1346.74 1457.50 1512.38 1539.79 1572. 82 1582.61 1715.35 78 89 104 124 147 147 166 166 178 184 195 256 367 415 473 473 585 598 633 672 672 700 923 1015 1161 1213 1317 1342 1452 1507 1533 1568 1579 1711 8 1. 08E-02 47. 9 9 3.39E-02 21.5 8 6.50E-03 86.9 10 4.90E-03177.5 12 4.58E-02 13.5 2.99E+OO 12 9.02E-02 7.3 13 1.65E-02 33.8 4.23E+OO 13 2.94E-02 18.0 6 1.67E-02 31.3 10 3.38E-02 22.5 9 1. 07E-02 50. 6 7 7.35E-03 59.7 11 2.60E-02 22.8 10 1.59E-02 33.3 17 1.03E-01 6.3 3.57E+OO 17 3.04E-02 18.6 12 4.66E-02 10.7 6 2.89E-03 90.9 16 1. lOE-02 50. 5 23 l.33E-02 33.6 6.llE-01 23 5.50E-03 75.3 9 6.92E-02 8.5 7 3.23E-03 76.5 17 1.37E-02 38.6 12 2.46E-02 17.1 12 4.80E-02 9.9 12 1.03E-02 29.8 8 3."32E-03 66.9 12 8.61E-03 32.7 10 4.72E-03 34.6 17 1.12E-02 25. 7 9 5.49E-03 32.5 8 1.09E-03137.3 7 2.71E-03 54.5 Peak Search Report (continued) Page : 2 Sample ID : Rl203621686 Acquisition date 3-0CT-2016 05:34:41 Pk It Energy / Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 861.68* 7 15 3.38 1724.08 1717 10 2.00E-03109.9 36 0 880.47 7 24 4.25 1761. 64 1752 11 1.84E-03150.5 37 0 911.91* 100 17 1. 97 1824.49 1818 17 2.78E-02 13.8 38 0 956.16 21 6 . 4. 85 1912.92 1907 12 5.768-03 32.3 39 0 969. 04 53 4 1. 97 1938.66 1934 9 l.46E-02 15.6 40 0 1120.22* 52 9 1. 94 2240. 85 2235 13 1.46E-02 18.8 41 0 1239.18 10 13 0.77 2478.61 2473 8 2.66E-03 74.5 42 0 1252.83 17 2 1. 48 2505.90 2501 9 4.64E-03 29.4 43 0 1346.09 10 5 1. 08 2692.32 2686 9 2.64E-03 51. 7 44 0 1378.33 16 5 3.53 2756.75 2752 10 4.44E-03 36.2 45 0 1461. 01* 365 *o 2.37 2922.00 2914 15 1.0lE-01 5.3 46 0 1510.47 10 6 1. 91 3020.87 3015 10 2.65E-03 61. 8 47 0 1764.84 42 3 1. 77 3529.33 3523 12 l.17E-02 17.4 Flag: "* ... = Peak area was modified by background subtraction Page 414of614 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 06:35:15 DKAlOO: PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 15-DEC-2015 10:14:00 R1203621686 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 05:34:41 155.34 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMAS 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 HF-172 52i97 HF-172 52.97 HF-172 52.97 HF-172 52.97 PB-214 351. 93 Page 415of614 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 TH-229 85.43 SN-126 86.94 SN-126 87.57 'CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 TM-171 51. 35 TM-171 52.39 AS-73 53.44 HF-172 54.07 BI-211 351.06 CAN 0 01:00:00.56 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : Rl203621686 Acquisition date 3-0CT-2016 05:34:41 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.244E+OO 1.289E+Ol 1.289E+Ol 10.55 OK CD-109 88.03 3.70* 8.913E+OO 1.003E+OO l.557E+OO 74.94 OK SN-126 64.28 9.60 9.093E+OO Line Not Found Absent 86.94 8.90 8. 913E+OO 4.170E-01 4.170E-01 74.94 OK 87.57 37.00* 8.913E+OO l.003E-01 1.003E-01 74.94 OK BA-137M 661.66 89.90* 2.418E+OO 8."692E-02 8.855E-02 59.56 OK CS-137 661.66 85.10* 2.418E+OO 9.183E-02 9.354E-02 59.56 OK TL-208 277.37 6.60 4.923E+OO Line Not Found Absent 583.19 85.00* 2.674E+00 2.020E-01 2.020E-01 34.12 OK 860.56 12.50 1.957E+OO 1. 466E-01 1.466E-01 219.85 OK PB-210 46.54 4.25* 9.664E+OO 1.956E+OO 2.005E+OO ,43. 04 OK BI-212 727. 33 6.67* 2.239E+OO l.051E+00 1. 051E+OO 65.48 OK *785.37 1.10 2.106E+OO 4.283E+OO 4.283E+OO 64.93 OK 1620.50 1. 47 1.126E+OO Line Not Found Absent PB-212 74.82 10.28 8.980E+OO 5.173E-01 5.173E-01 64.02 OK 77 .11 17.10 8.967E+OO 1. 335E+OO 1.335E+OO 14.70 OK 238.63 43.60* 5.564E+OO 8.658E-01 8.658E-01 12.52 OK 300.09 3.30 4.608E+OO 3.794E-01 3.794E-01 181. 80 *OK BI-214 609.32 45.49* 2.581E+OO 7.590E-01 7.593E-01 19.78 OK 1120.29 14.92 1.576E+OO 1.075E+OO 1.076E+OO 37.59 OK 1764.49 15.30 1.032E+OO 1.221E+OO 1. 221E+OO 34.85 OK PB-214 74.82 5.80 8.977E+OO Line Not Found <<INT Reject 77.11 9.70 8. 967E+OO 2.353E+OO 2.354E+OO 14.70 OK 87.09 3.41 8.912E+OO Line Not Found <<INT Reject 242.00 7.25 5.497E+OO Line Not Found <<INT Reject 295.22 18.42 4.681E+OO 1.083E+OO 1.084E+OO 21. 31 OK 351. 93 35.60* 4.043E+OO 9.454E-01 9.457E-01 16.95 OK RN-222 609.32 45.49* 2.581E-f-OO 7.590E-01 7.593E-01 19.78 OK 1120.29 14.92 1. 576E-i-OO 1.075E+OO 1.076E+OO 37.59 OK 1764.49 15.30 1.032E+OO 1.221E+OO 1.221E+OO 34.85 OK RA-224 240.99 4.10* 5.505E+OO 8.375E-01 8.375E-01 131. 42 OK RA-226 609.32 45.49* 2.581E+OO 7.590E-01 7.593E-01 19.78 OK 1120.29 14.92 1.576E+OO 1. 075E+OO 1.076E+OO 37.59 OK 1764.49 15.30 1.032E+OO 1.221E+OO 1.221E+OO 34.85 OK AC-228 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27 4.178E+OO 5.569E-01 5.569E-01 67.24 OK 794.95 4.25 2.087E+OO Line Not Found Absent 835.71 1. 61 2.005E+OO Line Not Found Absent 911.20 25.80* 1.869E+OO 1.026E+OO 1. 026E+OO 27.65 OK 968. 97 15.80 1. 779E+OO 9.170E-01 9.170E-01 31.19 OK RA-228 105.21 1.10 8.704E+OO Line Not Found Abs*ent 338.32 11.27 4.178E+OO 5.569E-01 5.569E-01 67 .24 OK 794.95 4.25 2.087E+OO Line Not -Found Absent 835. 71 1. 61 2.005E+OO Line Not Found Absent . 911.20 25.80* 1.869E+00 1.026E+OO 1. 026E+OO 27.65 OK 968.97 15.80 1. 779E+OO 9.170E-01 9.170E-01 31.19 OK TH-228 74.82 10.28 8.980E+OO 5.173E-01 5.173E-01 64.02 OK 77 .11 17.10 8. 967E+OO 1.335E+OO 1.335E+OO 14.70 OK 238.63 43.60* 5.564E+00 8.658E-01 8.658E-01 12.52 OK Page 416 of 614 Nuclide Line Activity Report (continued) Page : 3 Sample ID : Rl203621686 Acquisition date 3-0CT-2016 05:34:41 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 4.608E+OO 3.794E-01 3.794E-01 181.80 OK TH-229 85.43 14.70 8.913E+OO 2.524E-01 2.525E-01 74.94 OK 88.47 24.00 8.893E+OO 1. 749E-01 l.749E-01 62.68 OK 193.51 4.41* 6. 511E+OO Line Not Found Absent 210.85 2.80 6 .116E+OO Line Not Found Absent TH-230 609.32 45.49* 2.581E+OO 7.590E-01 7.590E-01 19.78 OK 1120.29 14.92 1.576E+OO 1. 07 5E+OO l.075E+OO 37.59 dK 1764.49 15.30 1.032E+OO 1.221E+OO 1.221E+OO 34.85 OK PA-231 283.69 1. 70 4.833E+OO Line Not Found Absent 301.36 5.35* 4.608E+OO 2.340E-01 2.340E-01 181. 80 OK TH-232 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27 4.178E+OO 5.569E-01 5.569E-01 67.24 OK 835.71 1. 61 2.005E+OO Line Not Found Absent 911.20 25.80* 1.869E+OO 1.026E+OO 1. 026E+OO 27.65 OK 968. 97 15.80 1. 779E+OO 9.170E-01 9.170E-01 31.19 OK TH-234 63.29 3.70* 9.128E+OO 3.352E-01 3.352E-01 355.04 OK 92.59 4.23 8.866E+OO 2. OllE+OO 2. OllE+OO 44.95 OK U-234 609.32 45.49* 2. 581E+OO 7.590E-01 7.590E-01 19.78 OK 1120.29 14.92 1.576E+OO 1.075E+OO 1.075E+OO '37. 59 OK 1764.49 15.30 1.032E+OO 1.221E+OO 1. 221E+OO 34.85 OK U-235 89.96 3.47 8.893E+OO 1.209E+OO 1.209E+OO 62.68 OK 93.35 5.60 8.866E+OO l.519E+OO 1.519E+OO 44.95 OK 143.76 10.96* 7.808E+OO Line Not Found Absent 163.33 5.08 7.279E+OO Line Not Found Absent 185. 72 57.20 6. 701E+OO 1.420E-01 l.420E-01 45.51 OK 205.31 5.01 6.238E+OO Line Not Found Absent U-238 63.29 3.70* 9.128E+OO 3.352E-01 3.352E-01 355.04 OK 92.59 4.23 8.866E+OO 2. OllE+OO 2. OllE+OO 44.95 OK AM-243 43.53 5.90 9.491E+OO Line Not Found Absent 74.66 67.20* 8.980E+OO 7.913E-02 7.914E-02 64.02 015 ANH-511 511. 00 100.00* 2.974E+OO 8.709E-02 8.709E-02 77.30 OK Flag: "*" = Keyline Page 417 of 614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:35:17.10 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R1203621686.CNF;l *
  • Acquisition date 3-0CT-2016 05:34:41 Sensitivity : 3.000 *
  • Detector ID GAM05 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 15-DEC-2015 10:14:00 Analyst initials: MXRl *
  • Sample ID Rl203621686 Sample Quantity 1.5534E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF';20
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.289E+Ol l.332E+OO CD-109 1.557E+OO 1.144E+OO SN-126 1.003E-01 7.366E-02 BA-137M 8.855E-02 5.168E-02 CS-137 9.354E-02 5.459E-02 TL-208 2.020E-01 6.754E-02 PB-210 2.005E+OO 8.459E-01 BI-212 1. 051E+OO 6.744E-01 PB-212 8.658E-01 1.062E-01 BI-214 7.593E-01 1.472E-01 PB-214 9.457E-01 1.571E-01 RN-222 7.593E-01 1. 472E-01 RA-224. 8.375E-01 1.079E+OO RA-226 7.593E-01 l.472E-01 AC-228 1.026E+OO 2. 781E-01 RA-228 1.026E+OO 2.781E-01 TH-228 8.658E-01 1.062E-01 TH-229 1.358E-01 3.445E-01 TH-230 7.590E-01 1.471E-01 PA-231 2.340E-01 4.170E-01 TH-232 1.026E+OO 2.781E-01 TH-234 3.352E-01 1.166E+OO U-234 7.590E-01 l.471E-01 U-235 -2.770E-02 1.276E-01 U-238 . 3. 352E-01 1.166E+OO AM-243 7.914E-02 4. 965E-02 ANH-511 8.709E-02 6.597E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 418 of 614 Key-Line Activity (pCi/GRAM 3.988E-01 -3.609E-03 O.OOOE+OO K.L. Cnt Uncert ( i. 96-sigma) 8.952E+OO 3.566E-02 l.462E+41 MDA (pCi/GRAM 4.454E-01 5.953E-01 3.832E-02 4.447E-02 4.698E-02 5.359E-02 4.884E-01 7.068E-01 6.822E-02 9.773E-02 l.045E-01 9.773E-02 7.319E-01 9.773E-02 2.185E-01 6.822E-02 6.776E-01 9.770E-02 5.432E-01 2.185E-01 7.202E-01 9.770E-02 2.400E-01 7.202E-01 4.354E-02 4.343E-02 MDA (pCi/GRAM 1. 790E+Ol 7.125E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 9.098E-03 1.942E-02 5 .196E-02 NOT IDENT. SC-46 l.127E-01 2.071E-01 4. 7 51E-01 FAIL ABUN V-48 0.000E+OO 7.578E+03 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 7.571E+02 O.OOOE+OO SHORT HLIF MN-54 8.188E-03 5.329E-02 l.044E-01 NOT IDENT. C0-56 -9.034E-02 3.795E-01 7.217E-01 FAIL ABUN MN-56 O.OOOE+OO l.960E+41 0.000E+OO SHORT HLIF C0-57 -3.925E-03 2.749E-02 5.380E-02 NOT I DENT .. C0-58 8.916E-02 3.898E-01 8.020E-01 NOT IDENT. FE-59 2.019E-01 4.847E+OO 9.907E+OO NOT IDENT. C0-60 -2.293E-02 3. 401E-02 5.901E-02 NOT IDENT. ZN-65 6.988E-02 1.508E-01 2.955E-01 NOT IDENT. GE-68 -2.853E-01 1.834E+OO 3.641E+OO NOT* IDENT. AS-73 1.953E+OO 3.326E+OO 2.838E+OO FAIL ABUN AS-74 O.OOOE+OO 3.933E+03 0.000E+OO SHORT HLIF SE-75 -9.053E-02 1.643E-01 2.863E-01 NOT IDENT. BR-77 O.OOOE+OO 2.464E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.740E+02 O.OOOE+OO SHORT HLIF RB-83 6.640E-02 5.816E-01 1.148E+OO NOT IDENT. KR-85 -3.191E+OO 6.047E+OO 9. 741E+OO NOT IDENT. SR-85 -3.146E-01 5.933E-01 9.553E-01 NOT IDENT. RB-86 O.OOOE+OO 1. 710E+04 O.OOOE+OO SHORT HLIF Y-88 2.529E-02 1. 517E-01 3.560E-01 NOT IDENT. Y-91 9.192E+Ol 4.600E+02 9.276E+02 NOT IDENT. NB-94 4.434E-02 3.008E-02 6. 691E-02 NOT IDENT. NB-95 -1.377E-01 6. 271E-01 1.036E+OO NOT IDENT. NB-95M -1. 221E-02 l.850E+OO 3.178E+OO NOT IDENT . . ZR-95 1. 726E+OO 1.169E+OO 2.174E+OO FAIL ABUN NB-97 O.OOOE+OO 1.394E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 0. OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.472E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 3.376E-02 3.947E-02 3.991E-02 FAIL ABUN RH-102 5.036E-02 4.610E-02 l.045E-01 NOT IDENT. RU-103 -8.974E-01 3.566E+OO 6.932E+OO FAIL ABUN RH-106 -4.685E-03 3.439E-01 6.859E-01 NOT IDENT. RU-106 -4.685E-03 3.439E-01 6.859E-01 NOT IDENT. AG-108M 1.603E-02 2.164E-02 4.677E-02 NOT .I DENT. AG-llOM l.894E-02 5.339E-02 1.199E-01 NOT IDENT. SN-113 -3.205E-03 l.573E-01 3.180E-01 NOT IDENT. CD-115 O.OOOE+OO 2.498E+38 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 4.745E+04 O.OOOE+OO SHORT HLIF TE-123M 1.978E-02 B.872E-02 l.744E-01 NOT IDENT. SB-124 -1.210E+OO l.408E+OO 2.028E+OO NOT IDENT. SB-125 5.869E-02 7.914E-02 1.713E-01 FAIL ABUN TE-125M l.514E+02 l.510E+02 3.223E+02 NOT IDENT. I-126 O.OOOE+OO 4.503E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 6.329E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 5.125E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 1.842E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 6.512E+25 O.OOOE+OO SHORT HLIF BA-133 -l.909E-02 2.775E-02 4.941E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 5.236E-02 4.345E-02 9.489E-02 NOT IDENT. CS-135 -1.086E-01 1. 200E-.Ol 1. 996E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 1. 525E+05 O.OOOE+OO SHORT HLIF CE-139 -l.524E-02 6.992E-02 l.325E-01 NOT IDENT. BA-140 O.OOOE+OO 6.109E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 1.508E+05 O.OOOE+OO SHORT HLIF CE-141 -9.598E+OO 1. 384E+Ol 2.527E+Ol NOT IDENT. CE-143 0.000E+OO 7.488E+40 O.OOOE+OO SHORT HLIF CE-144 7.153E-02 2.331E-01 4.669E-01 NOT IDENT. PM-144 -l.607E-02 4.059E-02 7.436E-02 NOT IDENT. PR-144 -1.366E+OO 3.517E+OO 6.452E+OO NOT IDENT. PM-146 2.813E-02 3.576E-02 7.692E-02 NOT IDENT. ND-147 O.OOOE+OO l.508E+07 O.OOOE+OO SHORT HLIF PM-147 -3.021E+02 5 .12 6E+0'2 9.615E+02 NOT IDENT. PM-149 O.OOOE+OO 3.715E+39 O.OOOE+OO SHORT HLIF EU-150 5.497E-03 2.051E-02 3.634E-02 FAIL ABUN EU-152 -5.663E-03 6.425E-02 1.299E-01 NOT IDENT. GD-153 O.OOOE+OO 2.144E-01 1.703E-01 FAIL ABUN EU-154 -6.787E-03 8. 821E-02 1.769E-01 FAIL ABUN EU-155 2.229E-02 6.301E-02 1.288E-01 FAIL ABUN TB-160 9.383E-01 2.768E+OO 3.352E+OO FAIL ABUN H0-166M -l.979E-02 4.696E-02 8.583E-02 FAIL ABUN TM-171 4.564E+OO 7.774E+OO 6.665E+OO FAIL ABUN Page 419 of 614 HF-172 9.668E-02 1. 481E-01 2.893E-01 FAIL ABUN LU-172 5.628E-02 7.085E-02 l.558E-01 FAIL ABUN LU-176 -2.232E-02 1.850E-02 2.839E-02 FAIL ABUN HF-181 -l.465E+OO 2.529E+OO 4.700E+OO NOT IDENT. TA-182 2.280E-01 6.891E-01 l.456E+OO FAIL ABUN RE-183 3.058E-01 6.300E-01 1.340E+OO NOT IDENT. RE-184 -1.459E+Ol 2.036E+Ol 3.351E+Ol FAIL ABUN W-188 -6.536E+OO 7.543E+Ol 1.286E+02 FAIL ABUN IR-192 . -9.560E-02 4.014E-01 6.524E-01 FAIL ABUN HG-203 3.994E-01 1.840E+OO 3.468E+OO NOT IDENT. BI-207 2.863E-02 3.885E-02 8.737E-02 FAIL ABUN BI-211 O.OOOE+OO 4.328E-01 7.758E-01 FAIL ABUN PB-211 4.632E-01 5.047E-01 l.108E+OO NOT IDENT. RN-219 -2.499E-01 2.510E-01 4.457E-01 NOT IDENT. RA-223 -l.449E-01 4. 531E-01 7.302E-01 FAIL ABUN AC-227 1.403E-01 1.602E-01 3.322E-01 FAIL ABUN TH-227 l.403E-01 l.602E-01 3.322E-01 FAIL ABUN TH-231 -1.449E,-01 4.531E-01 7.302E-01 FAIL ABUN PA-233 -2.934E-02 4.617E-02 7.807E-02 FAIL ABUN PA-234 -2.000E-02 2.029E-01 3.874E-01 FAIL ABUN PA-234M -3.902E+OO 3.365E+OO 5.674E+OO NOT IDENT. NP-237 -2.934E-02 4.617E-02 7.807E-02 FAIL ABUN NP-238 O.OOOE+OO 3.692E+40 O.OOOE+OO SHORT HLIF NP-239 2. 2.32E-02 1. 402E-01 2.824E-01 FAIL ABUN PU-239 3.074E+02 3.595E+02 4.023E+02 FAIL ABUN AM-241 -l.419E-03 3.646E-02 6.979E-02 NOT IDENT. CM_.:243 3. 451E-03 5.620E-02 1.127E-01 FAIL ABUN BK-247 -3.985E-02 6.181E-02 *1. 064E-01 FAIL ABUN CM-247 -2.297E-02 2.529E-02 4.558E-02 NOT IDENT. CF-249 -5.124E-03 2.832E-02 5.594E-02 NOT IDENT. CF-251 7.974E-03 8.483E-02 l.634E-01 NOT IDENT, Page 420of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:35:14.46 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 354 10.66* l.244E+OO l.289E+Ol l.289E+Ol 10.55 AS-73 53.44 32 10.30* 9.492E+OO l.559E-01 1.953E+OO 173.78 CD-109 88.03 137 3.70* 8.913E+OO 2.00lE+OO 3.107E+OO 36.02 SN-126 64.28 ------9.60 9.093E+OO ------Line Not Found ------86.94 137 8.90 8.913E+OO 8.320E-01 8.320E-01 36.02 87.57 137 37.00* 8.913E+OO 2.00lE-01 2.00lE-01 36.02 BA-137M 661.66 39 89.90* 2.418E+OO 8.692E-02 8.855E-02 59.56 CS-137 661.66 39 85.10* 2.418E+OO 9.183E-02 9.354E-02 59.56 TM-171 51. 35 32 0.27 9.492E+OO 5.949E+00 7.946E+00 173.78 52.39 32 0.47* 9.492E+OO 3.417E+00 4.564E+OO 173.78 66.73 ------0.14 9.052E+OO ------Line Not Found ------HF-172 52. 97 32 36.00 9.492E+OO 4.462E-02 6.005E-02 173.78 54.07 32 63.00 9.492E+OO 2.549E-02 3.432E-02 173.78 61.17 23 20.30 9.128E+OO 6.llOE-02 8.224E-02 355.04 62.93 23 4.50 9.128E+OO 2.756E-01 3.710E-01 355.04 67.68 ------5.99 9.039E+OO ------Line Not Found' ------81. 75 ------4.50 8.942E+OO ------Line Not Found ------114.06 ------2.60 8.540E+OO ------Line Not Found ------122.92 ------1.14 8.344E+OO ------Line Not Found ------125.81 ------11. 30* 8.274E+OO ------Line Not Found ------127.91 33 1. 46 8.210E+OO 1. 329E+00 1. 788E+OO 119. 31 TL-208 277.37 ------6.60 4.923E+OO ------Line Not Found ------583,19 95 85.00* 2.674E+OO 2.020E-01 2.020E-01 34.12 860.56 7 12.50 1.957E+OO 1.466E-01 1. 466E-01 219.85 PB-210 46.54 166 4.25* 9.664E+OO 1.956E+OO 2.005E+00 43.04 BI-211 72.87 ------1. 23 8.990E+OO ------Line Not Found ------351.06 282 12.92* 4.043E+OO 2.605E+OO 2.605E+OO 16.95 BI-212 727.33 32 6.67* 2.239E+OO 1.051E+OO 1.051E+OO 65.48 785.37 21 1.10 2.106E+OO 4.283E+OO 4.283E+OO 64.93 1620.50 ------1. 47 1.126E+OO ------Line Not Found ------PB-212 74.82 216 10.28 8.980E+OO 1.128E+OO 1.128E+OO 26.98 77 .11 424 17.10 8. 967E+OO l.335E+00 1.335E+OO 14.70 238.63 435 43.60* 5.564E+OO 8.658E-01 8.658E-01 12.52 300.09 12 3.30 4.608E+OO 3.794E-01 3.794E-01 181.80 BI-214 609.32 184 45.49* 2.581E+OO 7.590E-01 7.593E-01 19.78 1120.29 52 14.92 1. 576E+OO 1.075E+OO 1.076E+OO 37.59 1764.49 40 15.30 l.032E+00 1. 221E+OO l.221E+OO 34.85 PB-214 74.82 216 5.80 8.980E+OO 2.000E+OO 2. OOlE+OO 26. 98 77 .11 424 9.70 8. 967E+OO 2.353E+00 2.354E+00 14.70 87.09 137 3.41 8.913E+OO 2.171E+OO 2. l 72E+OO 36.02 242.00 129 7.25 . 5. 505E+OO 1.557E+OO 1.557E+OO 37.13 295.22 193 18.42 4. 681E+OO 1.083E+OO l.084E+00 21. 31 351. 93 f 2 82 35.60* 4.043E+OO 9.454E-01 9.457E-01 16.95 RN-222 609.32 18 4 45.49* 2.581E+OO 7.590E-01 7.593E-01 19.78 1120.29 52 14.92 1.576E+OO 1.075E+OO 1. 076E+OO 37.59 1764.49 40 15.30 l.032E+OO 1. 221E+OO 1.221E+OO 34.85 RA-224 240.99 129 4.10* 5.505E+OO 2.753E+OO 2.753E+OO 37.13 Page 421of614 Nuclide Line Activity Report (cont_inued) Page*: 2 Sample ID : Rl203621686 Acquisition date 3-0CT-2016 05:34:41 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error RA-226 609.32 184 45.49* 2.581E+OO 7.590E-01 7.593E-01 19.78 1120.29 52 14.92 l.576E+OO 1.075E+OO 1. 076E+OO 37.59 1764.49 40 15.30 1.032E+OO 1. 221E+OO 1.221E+OO 34.85 AC-228 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 54 11. 27 4.178E+OO 5.569E-01 5.569E-01 67.24 794.95 ------4.25 2.087E+OO ------Line Not Found ------835.71 ------1. 61 2.005E+OO ------Line Not Found ------911. 20 102 25.80* 1.869E+OO l.026E+OO 1.026E+OO 27.65 968. 97 53 15.80 1. 779E+OO 9.170E-01 9.170E-01 31.19 RA-228 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 54 11. 27 4.178E+OO 5.569E-01 5.569E-01 67.24 794.95 ------4.25 2.087E+OO ------Line Not Found ------835. 71 ------1. 61 2.005E+OO ------Line Not Found ------911. 20 102 25.80* l.869E+00 1. 026E+00 l.026E+OO 27.65 968.97 53 15.80 1. 779E+00 9.170E-01 9.170E-01 31.19 TH-228 74.82 216 10.28 8.980E+OO l.128E+OO l.128E+OO 26.98 77 .11 424 17.10 8. 967E+OO l.335E+OO 1.335E+OO 14.70 238.'63 435 43.60* 5.564E+OO 8.658E-01 8.658E-01 12.52 300.09 12 '3. 30 4.608E+OO 3.794E-01 3.794E-01 181.80 TH-229 85.43 137 14.70 8.913E+OO 5.037E-01 5.038E-01 36.02 88.47 77 24.00 8.893E+OO 1. 749E-01 1. 749E-01 62. 68 193.51 ------4.41* 6. 511E+OO ------Line Not Found ------210.85 ------2.80 6 .116E+OO ------Line Not Found ------TH-230 609.32 184 45.49* 2.581E+00 7.590E-01 7.590E-01 19.78 1120.29 52 14.92 1.576E+OO l.075E+OO 1. 075E+OO 37.59 1764.49 40 15.30 l.032E+OO 1. 221E+OO 1.221E+OO 34.85 PA-231 283.69 ------1. 70 4.833E+OO ------Line Not Found ------301. 36 12 5.35* 4.608E+OO 2.340E-01 2.340E-01 181.80 TH-232 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 54 11.27 4.178E+OO 5.569E-01 5.569E-01 67.24 835. 71 ------1. 61 2.005E+OO ------Line Not Found ------911.20 102 25.80* l.869E+00 1. 026E+OO
  • 1. 026E+00 27.65 968. 97 53 15.80 1. 779E+00 9.170E-01 9.170E-01 31.19 TH-234 63.29 23 3.70* 9.128E+OO 3.352E-01 3.352E-01 355.04 92.59 156 4.23 8.866E+OO 2. OllE+OO 2. OllE+OO 44.95 U-234 609.32 184 45.49* 2.581E+00 7.590E-01 7.590E-01 19.78 1120.29 52 14.92 l.576E+00 l.075E+OO 1.075E+OO 37.59 1764.49 40 15.30 l.032E+OO 1. 221E+OO 1. 221E+OO 34.85 U-235 89. 96 77 3.47 8.893E+OO l.209E+OO l.209E+OO 62. 68 93.35 156 5.60" 8.866E+OO l.519E+OO 1.519E+OO 44.95 143.76 ------10. 96* 7.808E+OO ------Line Not Found ------163.33 ------5.08 7.279E+OO ------Line Not Found ------185.72 113 57.20 6.701E+OO 1. 420E-01 l.420E-01 45.51 205.31 ------5.01 6.238E+OO ------Line Not Found ------U-238 63.29 23 3.70* 9.128E+OO 3.352E-01 3.352E-01 355.04 92.59 156 4.23 8.866E+OO 2. OllE+OO 2. OllE+OO 44.95 AM-243 43.53 ------5.90 9. 491E+OO ------Line Not Found ------74.66 216 67.20* 8.980E+OO l.726E-01 l.726E-01 26.98 ANH-511 511. 00 54 100.00* 2.974E+OO 8.709E-02 8.709E-02 77.30 Page 422 of 614 Nuclide Line Activity Report (continued) Sample ID R1203621686 Acquisition date Flag: "*" Key line Page423 of614 Page : 3 3-0CT-2016 05:34:41 Page : 4 Surrunary of Nuclide Activity Sample ID : R1203621686 Acquisition date 3-0CT-2016 05:34:41 Total number of lines in spectrum 47 Number of unidentified lines 9 Number of lines tentatively identified by NID 38 Nuclide Type : Nuclide K-40 AS-73 CD-109 SN-126 BA-137M CS-137 TM-171 HF-172 TL-208 PB-210 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 80.30D 461. 40D 2.30E+05Y 30.08Y 30.08Y l.92Y 1.87Y 1. 41E+10Y 22.20Y 7.04E+08Y 1.41E+l0Y 1. 41E+10Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+l0Y 1600. OOY l.41E+l0Y l.41E+l0Y l.41E+l0Y 7340.00Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 12.5 1. 55 1. 00 1. 02 1. 02 1. 34 1. 35 1. 00 1. 03 1. 00 1.00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.289E+Ol 1.559E-01 2.00lE+OO 2.00lE-01 8.692E-02 9.183E-02 3.417E+00 2.549E-02 2.020E-01 l.956E+OO 2.605E+OO 1.051E+OO 8.658E-01 7.590E-01 9.454E-01 7.590E-01 2.753E+OO 7*. 590E-01 l.026E+OO 1.026E+OO 8.658E-01 1. 749E-01 7.590E-01 2.340E-01 1.026E+OO 3.352E-01 7.590E-01 l.420E-01 3.352E-01 1. 726E-01 8.709E-02 3.847E+Ol 3.847E+Ol Decay Corr pCi/GRAM 1. 28 9E+Ol 1.953E+OO 3.107E+OO 2.00lE-01 8.855E-02 9. 3'54E-02 4.564E+OO 3.432E-02 2.020E-01 2.005E+OO 2.605E+00 1. 051E+OO 8.658E-01 7.593E-01 9.457E-01 7.593E-01 2.753E+OO 7.593E-01 1.026E+OO 1.026E+OO '8. 658E-01 1. 749E-01 *7.590E-01 2.340E-01 1.026E+OO 3.352E-01 7.590E-01 1.420E-01 3.352E-01 1.726E-01 8.709E-02 4.258E+Ol 4.258E+Ol 80.85% Decay Corr 2-Sigma Error 0.136E+Ol 3.394E+OO 1.119E+OO 0. 721E-01 5.273E-02 5. 571E-02 7.932E+OO 5. 964E-02 0.689E-01 0.863E+OO 0.442E+OO 0.688E+OO 1. 084E-01 1.502E-01 1.603E-01 l.5'02E-01 1.022E+OO 1.502E-01 0.284E+OO 0.284E+OO .1. 084E-01 l.096E-01 1.501E-01 4.255E-01 0.284E+OO 11. 90E-01 1. 501E-01 0.646E-01 11. 90E-01 0.466E-01 6.732E-02 "M" Manually accepted 2-Sigma %Error 10.55 173.78 36. 02 36.02 59.56 59.56 173.78 173.78 34.12 43.04 16.95 65.48 12.52 19.78 16.95 19.78 37 *.13 19.78 27.65 27.65 12.52 62. 68 19.78 181.80 27.65 355.04 19.78 45.51 355.04 26.98 77 .*30 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 424of614 Flags K K K Unidentified Energy Lines Page : 5 Sample ID : Rl203621686 Acquisition date : 3-0CT-2016 05:34:41 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 39.41 54 144 1. 66 80.65 78 8 1.08E-02 95.7 8.32E+OO 4 83.94 77 170 1.15 169.66 166 13 1.65E-02 67.7 8.93E+OO T 0 98.79 49 130 0.97 199.34 195 9 1. 07E-02 **** 8.80E+OO T 0 209.00 68 104 1. 30 419.59 415 10 l.59E-02 66.6 6.16E+OO 0 320.44 45 79 6.79 642.32 633 16 1. lOE-02 **** 4.37E+00 T 3 341.31 22 60 1. 66 684.03 672 23 5.50E-03 **** 4.15E+00 T 0 463.29 13 27 1. 08 927.83 923 7 3.23E-03 **** 3.22E+OO T 0 672.89 13 17 0.97 1346.74 1342 8 3.32E-03 **** 2.38E+00 0 755.76 18 5 1. 05 1512.38 1507 10 4.72E-03 69.1 2.17E+OO T 0 769.47 42 12 3.41 1539.79 1533 17 1.12E-02 51. 3 2.14E+00 0 790.90 4 9 0.50 1582.61 1579 8 1.09E-03 **** 2.lOE+OO T 0 857.31 10 6 1. 45 1715.35 1711 7 2.71E-03 **** 1. 96E+OO T 0 880.47 7 25 4.25 1761.64 1752 11 1.84E-03 **** l.92E+OO T 0 956.16 21 6 4.85 1912.92 1907 12 5.76E-03 64.7 1.80E+OO 0 1239.18 9 13 0.77 2478.61 2473 8 2.66E-03 **** 1. 44E+00 T 0 1252.83 16 2 1. 48 2505.90 2501 9 4.64E-03 58.7 1. 43E+00 0 1346.09 9 4 1. 08 2692.32 2686 9 2.64E-03 **** l.34E+00 0 1378.33 16 5 3.53 2756.75 2752 10 4.44E-03 72 .3 l.31E+OO 0 1510.47 9 6 1. 91 3020.87 3015 10 2.65E-03 **** 1.21E+OO Flags: "T" '= Tentatively associated Page 425 of 614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:35:30.07 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R1203621686.CNF;l *
  • Acquisition date 3-0CT-2016 05:34:41 Sensitivity 3.000 *
  • Detector ID GAM05 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 15-DEC-2015 10:14:00 Nuclide Library : SOLID *
  • Sample ID R1203621686 Analyst initials: MXRl * *Batch Number 1596387 Sample*Quantity : 1.5534E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * **
  • Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1.730E-01 2.643E-01 1. 701E-02 1.908E-02 2.016E-02 2.383E-02 2.263E-01 3.085E-01 3.127E-02 4.313E-02 4.750E-02 4.313E-02 3.355E-01 4.313E-02 9.545E-02 9.545E-02 3.127E-02 3.147E-01 4. 311E-02 2.437E-01 9.545E-02 3.391E-01 4. 311E-02 l .119E-01 3.391E-01 2.060E-02 1.944E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 ( Page 426of614 Le (pCi/GRAM 8.014E+OO 2.981E-02 O.OOOE+OO l.945E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 ' TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 .CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 427 of 614 1. 981E-01 O.OOOE+OO O.OOOE+OO 4.582E-02 3.142E-01 O.OOOE+OO 2.483E-02 3.436E-01 4.252E+OO 2.408E-02 1. 287E-01 l.553E+OO 1.327E+OO O.OOOE+OO l.307E-01 O.OOOE+OO O.OOOE+OO 5. 201E-01 4.315E+OO 4*. 232E-01 O.OOOE+OO 1.333E-01 4.087E+02 3.054E-02 4.437E-01 1.471E+OO 9.519E-01 0. OOOE'+OO o*. OOOE+OO O.OOOE+OO O.OOOE+OO 1.848E-02 4.671E-02 3.035E+OO 2. 968E-01 2.968E-01 2 .118E-02 4.912E-02 l.424E-01 O.OOOE+OO 0.000E+OO 8.108E-02 6.410E-01 7.754E-02 l.508E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.180E-02 O.OOOE+OO 4.254E-02 9.133E-02 O.OOOE+OO O.OOOE+OO 6. 096E-02 O.OOOE+OO O.OOOE+OO 1.168E+Ol O.OOOE+OO 2.176E-01 3.209E-02 2.786E+OO 3.'494E-02 O.OOOE+OO 4.445E+02 O.OOOE+OO 1.646E-02 5.846E-02 7.873E-02 7.417E-02 6.008E-02 l.485E+OO 3.747E-02 3 .119E+OO 1.346E-01 FAIL ABUN SHORT HLIF SHORT HLIF . NOT I DENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF* NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. . NOT I DENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF .SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT-HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 .NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 428of614 6.912E-02 l.258E-02 2. 026E+OO* 6.291E-01 6.296E-01 1. 388E+Ol 5.768E+Ol 2. 969E-01 1.600E+OO 3.819E-02 3.750E-01 5.040E-01 l.943E-01 3.255E-01 l.523E-01 l.523E-01 3.255E-01 3.505E-02 1. 631E-01 2.379E+OO 3.505E_.:02 O.OOOE+OO l.308E-01 l.876E+02 3.274E-02 5. 243E-0,2 4.871E-02 2. 01 7E-0'2 2.519E-02 7.588E-02 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL' ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN

  • NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:35:35.78 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Rl2036,21686.CNF;l '*
  • Acquisition date 3-0CT-2016 05:34:41 Sensitivity : 3.000 *
  • Detector ID GAM05 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000, *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 15-DEC-2015 10:14:00 Nuclide Library : SOLID *
  • Sample ID Rl203621686 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity 1.5534E+02 GRAM *
  • Quantity Err(%) l.2875E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry : 0. 00000 * * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 4-SEP-2016 08: 00: 28 Eff. 'Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 l.289E+Ol 1.492E+OO l.492E+OO CD-109 1.557E+OO 1.167E+OO 1.167E+OO SN-126 l.003E-01 7.496E-02 7.496E-02 BA-137M 8.855E-02 5.182E-02 5.182E-02 CS-137 9.354E-02 5.474E-02 5.474E-02 TL-208 2.020E-01 6.808E-02 6.808E-02 PB-210 2.005E+OO 8.659E-01 8.659E-01 BI-212 l.051E+OO 6.765E-01 6.765E-01 PB-212 8.658E-01 1.157E-01 1.157E-01 BI-214 7.593E-01 1.507E-01 l.507E-01 PB-214 9.457E-01 1.620E-01 1.620E-01 RN-222 7.593E-01 l.507E-01 1.507E-01 RA-224 8.375E-01 1.087E+OO 1.087E+OO RA-226 7.593E-01 1.507E-01 1.507E-01 AC-228 1.026E+OO 2.830E-01 2.830E-01 RA-228 1.026E+00 2.830E-01 2.830E-01 TH-228 8.658E-01 l.157E-01 1.157E-01 TH-229 1.358E-01 3.445E-01 3.445E-01 TH-230 7.590E-01 1.507E-01 1.507E-01 PA-231 2.340E-01 4.200E-01 4.200E-01 TH-232 1.026E+OO 2.830E-01 2.830E-01 TH-234 3.352E-01 1.169E+OO 1.169E+OO U-234 7.590E-01 1.507E-01 l.507E-01 U-235 -2.770E-02 l.277E-01 l.277E-01 U-238 3.352E-01 l.169E+OO 1.169E+OO AM-243 7.914E-02 5.127E-02 5.127E-02 ANH-511 8.709E-02 6.607E-02 6.607E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi'/GRAM ( 1. 96-sigma) ( 1 . 96-sigma) BE-7 3.988E-01 8.952E+OO 8.953E+OO NOT IDENT. NA-22 -3.609E-03 3.566E-02 3.569E-02 NOT IDENT. NA-24 -1. OOOE+41 1.523E+41 O.OOOE+OO SHORT HLIF Page429 of614 AL-26 9.098E-03 1.943E-02 1. 986E-02 NOT IDENT. SC-46 1.127E-01 2.071E-01 2 .133E-01 FAIL ABUN V-48 -4.832E+03 7.580E+03 7.887E+03 SHORT HLIF CR-51 7.654E+02 7.579E+02 8.327E+02 SHORT HLIF MN-54 8.188E-03 5.329E-02 5.342E-02 NOT IDENT. C0-56 -9.034E-02 3.795E-01 3.817E-01 FAIL ABUN MN-56 -1.000E+41 4.267E+41 O.OOOE+OO SHORT HLIF C0-57 -3.925E-03 2.749E-02 2.755E-02 NOT IDENT. C0-58 8.916E-02 3.898E-01 3.919E-01 NOT IDENT. FE-59 2.019E-01 4.847E+OO 4.848E+OO NOT IDENT. C0-60 -2.293E-02 3.402E-02 3.555E-02 NOT IDENT. ZN-65 6.988E-02 1.508E-01 1.541E-01 NOT IDENT. GE-68 -2.853E-01 l.834E+OO 1.838E+OO NOT IDENT. AS-73 1.953E+OO 3.350E+OO 3.464E+OO FAIL ABUN AS-74 6.422E+02 3.934E+03 3.944E+03 SHORT HLIF SE-75 -9.053E-02 1.644E-01 l.694E-01 NOT IDENT. BR-77 2.009E+37 l.698E+38 O.OOOE+OO SHORT HLIF SR-82 -4.247E+02 5.744E+02 6.054E+02 SHORT HLIF RB-83 6.640E-02 5.817E-01 5.825E-01 NOT IDENT. KR-85 -3 .191E+OO 6.049E+OO 6.217E+OO NOT IDENT. SR-85 -3.146E-01 5.934E-01 6.102E-01 NOT IDENT. RB-86 -4.740E+02 l.710E+04 1. 71.0E+04 SHORT HLIF Y-88 2.529E-02 1.517E-01 l.521E-01 NOT IDENT. Y-91 9.192E+..01 4.600E+02 4.618E+02 NOT IDENT. NB-94 4.434E-02 3.014E-02 3.617E-02 NOT IDENT. NB-95 -1.377E-01 6.271E-01 6.302E-01 NOT IDENT. NB-95M -1. 221E-02 1.850E+OO 1.850E+OO NOT IDENT. ZR-95 1. 726E+OO 1.171E+OO
  • 1. 406E+00 FAIL ABUN NB-97 -l.000E+41 1.394E+41 0.000E+OO SHORT HLIF ZR-97 1.000E+41 3.326E+41 O.OOOE+OO SHORT HLIF M0-99 -9.070E+30 2.473E+31 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 9.462E+42* O.OOOE+OO SHORT HLIF RH-101 3.376E-02 3.994E-02 4.274E-02 FAIL ABUN RH-102 5.036E-02 4.629E-02 5.156E-02 NOT IDENT. RU-103 -8.974E-01 3.567E+OO 3.589E+OO FAIL ABUN RH-106 -4.685E-03 3.439E-01 3.439E-01 NOT IDENT. RU-1-06 -4.685E-03 3.439E-01 3.439E-01 NOT IDENT. AG-108M l.603E-02 2.165E-02 2.283E-02 NOT IDENT. AG-llOM 1.894E-02 5.340E-02 5.408E-02 NOT IDENT . SN-113 . -3.205E-03 1.573E-01 l .. 573E-01 NOT IDENT. CD-115 2. 072E+38 2.525E+38 O.OOOE+OO SHORT HLIF SN-ll 7M -4.133E+03 4.746E+04 4.749E+04 SHORT HLIF TE-123M 1. 97 8E-02 8. 872E-02 8.917E-02 NOT IDENT. SB-124 -1. 210E+00 l.409E+OO 1. 511E+OO NOT IDENT. SB-125 5.869E-02 7.918E-02 8.348E-02 FAIL ABUN TE-125M 1.514E+02 1.513E+02 1.660E+02 NOT IDENT. I-126 -1 .. 687E+04 4.503E+05 4.503E+05 SHORT HLIF SB-126 6. 313E+03 6.329E+05 6.329E+05 SHORT HLIF SB-127 -3.334E+20 5.145E+21 O.OOOE+OO SHORT HLIF I-131 -1. 499E+09 l.843E+09 1. 963E+09 SHORT HLIF I-132 -1. OOOE+41 2.421E+42 O.OOOE+OO SHORT HLIF TE-132 -2.609E+24 6.513E+25 O.OOOE+OO SHORT HLIF BA-133 -1.909E-02 2.776E-02 2.907E-02 NOT IDENT. I-133 O.OOOE+OO l.136E+42 O.OOOE+OO SHORT HLIF CS-134 5.236E-02 4. 351E-02 4.950E-02 NOT IDENT. CS-135 -1.086E-01 1.202E-01 1.298E-01 NOT IDENT. I-135 1.000E+41 9.526E+42 O.OOOE+OO SHORT HLIF CS-136 -8.466E+03 l.525E+05 1.526E+05 SHORT HLIF CE-139 -1.524E-02 6.998E-02 7.032E-02 NOT IDENT. BA-140 -3.223E+05 6. 111E+05 6.281E+05 SHORT HLIF LA-140 -1.539E+05 1.510E+05 1.662E+05 SHORT HLIF CE-141 -9.598E+OO 1.385E+Ol 1. 451E+Ol NOT IDENT. CE-143 1.000E+41 7.554E+40 O.OOOE+OO SHORT HLIF CE-144 7.153E-02 2.332E-01 2.354E-01 NOT IDENT. PM-144 -l.607E-02 4.060E-02 4.124E-02 NOT IDENT. PR-144 -l.366E+OO 3.518E+OO 3. 571E+OO NOT IDENT. PM-146 2.813E-02 3.581E-02 3.799E-02 NOT IDENT. ND-147 -2.558E+06 l.508E+07 l.513E+07 SHORT HLIF PM-147 -3. 021E+02 5.128E+02 5.305E+02 NOT IDENT. PM-149 -2. 727E+39 3.762E+39 O.OOOE+OO SHORT HLIF EU-150 5.497E-03 2. 051E-02 2.066E-02 FAIL ABUN EU-152 -5.663E-03 6.425E-02 6.430E-02 NOT IDENT. GD-153 2.160E-01 2.147E-01 2.358E-01 FAIL ABUN EU-154 -6. 78.7E-03 8.821E-02 8.826E-02 FAIL. ABUN EU-155 2.229E-02 6.303E-02 6.382E-02 FAIL ABUN TB-160 9.383E-01 2.768E+OO 2. 8 OlE+OO. FAIL ABUN H0-166M -1.979E-02 4.697E-02 4.781E-02 FAIL ABUN TM-171 4.564E+OO 7.784E+OO 8.051E+OO FAIL ABUN *Page 430of614 HF-172 9.668E-02 1.490E-01 1.552E-01 FAIL ABUN LU-172 5.628E-02 7.108E-02 7.547E-02 FAIL ABUN LU-176 -2.232E-02 1.853E-02 2.108E-02 FAIL ABUN HF-181 -1. 465E+00 2.530E+00 2.614E+00 NOT IDENT. TA-182 2.280E-01 6.891E-01 6.967E-01 FAIL ABUN RE-183 3.058E-01 6.318E-01 6'. 466E-01 NOT IDENT. RE-184 -1. 459E+Ol 2.064E+Ol 2.166E+Ol FAIL ABUN W-188 -6.536E+00 7.543E+Ol 7.549E+Ol FAIL ABUN IR-192 -9.560E-02 4.014E-01. 4.037E-01 FAIL ABUN HG-203 3.994E-01 1.841E+OO 1.849E+OO NOT IDENT. BI-207 2.863E-02 3.887E-02 4. 096E-02 FAIL ABUN BI-211 2.605E+OO 4.482E-01 1.257E+OO FAIL ABUN PB-211 4.632E-01 5.053E-01 5.467E-01 NOT IDENT. RN-219 -2.499E-01 2.530E-01 2.769E-01 NOT IDENT. RA-223 -1. 449E-01 4.532E-01 4.578E-01 FAIL ABUN AC-227 l.403E-01 1.613E-01 1. 733E-01 FAIL ABUN TH-227 1.403E-01 l.613E-01 l.733E-01 FAIL ABUN TH-231 -l.449E-01 4.532E-01 4.578E-01 FAIL ABUN PA-233 .-2.934E-02 4.619E-02 4.805E-02 FAIL ABUN PA-234 -2.000E-02 2.042E-01 2.044E-01 FAIL ABUN PA-234M -3.902E+OO 3.370E+OO 3.801E+OO NOT IDENT. NP-237 -2.934E-02 4.619E-02 4.805E-02 FAIL ABUN NP-238 -1.163E+40 3.693E+40 O.OOOE+OO SHORT HLIF NP-239 2.232E-02 l.402E-01 1. 406E-01 FAIL ABUN PU-239 3.074E+02 3.597E+02 3.855E+02 FAIL ABUN AM-241 -l.419E-03 3.646E-02 3.646E-02 NOT IDENT. CM-243 3. 451E-03 5.620E-02 5.622E-02 FAIL ABUN BK-247 -3.985E-02 6.233E-02 6.487E-02 FAIL ABUN CM-247 -2.297E-02 2.558E-02 2.760E-02 NOT IDENT. CF-249 -5.124E-03 2.833E-02 2.842E-02 NOT IDENT. CF-251 7.974E-03 8.483E-02 8.491E-02 NOT IDENT. Page431 of614
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 53.7281 87.09 76.1071 136.47 58.3932 45.60 53.3932 87.57 21.1009 140.51 0.0000 46.54 53.5864 88.03 21.1247 143.76 64.0697 49. 72 0.0000 88.34 21.1406 144.24 56.2303 51. 35 57.9720 88.47 21.1474 145.44 64.2532 51. 87 57.0234 89. 96 93.7391 152.43 71.0065 52.39 57.1284 1093.63 77.9487 153.25 0.0000 52.97 57.2445 91.11 0.0000 323.87 62.1854 53.44 57.3385 92.59 55.1738 156.02 0.0000 54.07 59.5920 93.35 55.2727 158.56 0.0000 57.36 0. oo.oo 94.56 55.4292 159.00 53.5693 57.53 63.7909 94.65 55. 4411 162.33 54.8668 57.98 68.7373 94.67 55.4434 162.66 0. 00.00 59.27 83.3736 94.87 55.4690 163.33 54.9525 59.32 83.3873 97.43 53. 9969 165.86 49.0386 59.54 78.0278 98.43 54 .1193 176.31 50.8520 60. 96 72.9398 98'. 44 54.1205 176.60 0.0000 61.17 83.8819 99.53 54.2537 177.52 55.1002 62.93 86.2630 100 .11 55.5314 181.07 0.0000 63. 29 86.3593 102.03 53.3435 181.52 50.1921 63.58 86.4366 103.18 59.2514 184.41 48.2994 64.28 86.6223 103.37 58.3638 143.76 48.3893 66.73 95.2995 105.21 58.5972 193.51 48.9157 67.24 91. 0046 105.31 57.6941 197.03 41.6708 125.81 93.3456 106.12 58.7119 198.01 51. 3545 67.75 89.1963 106.47 58.7559 201.83 54.8427 69.67 82.9927 109.28 49.8707 203.43 57.1139 70.83 99.8108 111. 00 70.4406 205.31 48.9732 72.81 87. 9658 111.76 0.0000 210.85 42.0716 72. 87 87.9809 114. 06 61.5568 215.65 58.0197 74.66 102. 8720 116.30 0.0000 222 .11 39.7271 74.82 102.9172 116.74 49.6996 227.09 54.4027 74.97 102.9597 119. 76 49.0539 227.38 53.3108 77 .11 103.5606 121.12 62.4264 228.16 0.0000 78.74 90.5457 121. 22 62.4385 228.18 46.6924 79.69 75.8358 121. 7 8 54.9295 116.74 46.6924 80.12 93.1759 122.06 51.1692 235.69 52.3455 80.19 0.0000 122.92 55.0507 235. 96 52.3626 80.57 100.1955 123.07 59.8138 238.63 40.5198 81. 00 88.7782 265.00 53.2297 238.98 0.0000 81. 07 88.7947 125.81 45.8108 240.99 40.6307 81.75 70.4673 127.23 61.2439 242.00 40.6785 83.79 75.4816 127.91 50.7825 244.70 36.2705 84.00 75.5219 129.30' 50. 9135 252.40 0.0000 85.43 75.7943 131.20 60.4109 252.80 25.1646 86.55 76.0059 133. 02 58.0325 254.15 0.0000 86.79 76.0509 133.52 56.1486 256.23 26.4084 86.94 76.0793 136.00 52.5103 260.90 0.0000 Page 432of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 2 64. 66 47.5089 355.39 0.0000 584.27 22.1768 264.80 47.5164 356.01 28.3117 595.83 0.0000 265.00 52.1631 364.49 0.0000 427.87 17.9048 268.22 56.9957 366.42 0.0000 602.52 0.0000 269.46 37.2705 372. 51 26.4823 604. 72 16. 4496 270.03 31.4659 375.05 23.1136 607.14 13.4769 271.23 46.6748 377.52 25.7330 609.32 18.9900 273.65 0.0000 356.01 23.2778 610.33 19.5008 276.40 38.7152 388.16 30.2782 614.28 16.8369 277.37 46.9751 388.63 0.0000 618.01 16.0671 277.60 46.9861 391.69 25.1579 620. 36 15.0824 278.00 31. 7288 264.66 21. 8399 621. 93 14.0889 279.20 43.5344 401.81 27.9798 630.19 0.0000 279.54 40.0181 402.40 32.3660 631. 29 9.1022 279.70 40.0243 404.85 21. 0337 633.25 15.1862 280.46 38.8778 410.95 27.2947 634.78 0.0000 283.69 26.0042 413.71 13.2346 635.95 20.2775 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 29.6021 423. 72 0.0000 645.85 21. 4016 285.90 0.0000 427.09 22.2778 657.76 21.5341 287.50 23.7311 427.87 20.5073 657.90 0.0000 290.67 26.9810 433.94 20.5981 661. 66 12. 3296 293.27 0.0000 439.40 22.4772 664.57 0.0000 351. 93 27.1027 453.88 21. 7998 '666. 33 0.0000 295.96 27.1228 463.37 17.8290 666.50 0.0000 879.38 23.9929 468.07 18.3447 667. 71 0.0000 299.98 36.8397 473.00 0 .. oooo 677. 62 30.0384 300.09 36.8434 475.06 31.3334 685.70 0.0000 300.13 36.8453 476.78 18.4530 695.00 0.0000 301.36 25.6621 477.60 24.0015 696. 49 17.7734 302.85 41. 7612 482.18 19.4453 696. 51 17.7740 256.23 36.1963 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 16.7350 306.78 39.9035 497.08 19.6358 697.49 16.7363 308.46 31. 4891 505.52 23.9732 702.65 15.7300 311. 90 36.4526 507.63 0.0000 706.68 22.0647 316.51 39.0508 511. 00 24.5284 711. 68 18.9580 319.41 0.0000 514.00 28.3557 720.70 0.0000 320.08 0.0000 514.00 28.3557 721.93 0.0000 321.04 26. 9602 520.40 29.4182 722.78 12.7056 323.87 27.8498 520.69 0.0000 722. 91 11.1182 325.23 21.3234 522.65 0.0000 723.31 12.7090 328.76 0.0000 527.90 0.0000 724.19 15.8929 333.37 34.6992 528.26 12.3970 727.33 15.9161 333.97 26.4518 529.59 20.0421 733.00 12.7671 334.37 29.7686 529.87 0.0000 735.93 15.9808 338.28 29.8726 531.02 0.0060 333.97 17.0579 338.32 29.8733 537.26 0.0000 739.50 0.0000 311. 90 29.9304 546.56 0.0000 747.24 13.9225 340.48 29.9304 552.55 14.5154 748.06 17.1419 340.55 0.0000 563.25 24.3449 752.31 4.8307 344.28 28.3617 569.33 17.5906 753 .. 82 0.0000 345.93 36.3385 946.00 17.5928 756.73 16 .1346 351.06 33.5628 569.70 20.5266 756.80 16 .1353 351.93 33.5881 583.19 21. 6715 884.68 14.5690 Page433 of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 14.5811 1274.44 9.7764 1620.50 2.1292 766.42 12. 9644 1001.03 17.8058 1621. 92 3.1948 766.84 12.9668 1002.74 19.5984 1678.03 0.0000 772. 60 0.0000 1004.73 8.9145 1690.97 5.4105 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 4.3999 778.90 11. 9507 1028.54 0.0000 1063.66 4.4053 783.70 0.0000 1037.84 16.2345 1771.35 2.2032 785.37 6.5374 1038.76 0.0000 1791.20 0.0000 792.07 31.1440 631. 29 9.9513 1808.65 1.1105 794.95 16.4124 1048.07 0.0000 1810.72 0.0000 795.86 10.5082 1049.04 9.0546 1836.06 2.2340 810.06 11.0136 1050.41 11. 7765 810.29 8. 8115 1063.66 9.0997 344.28 8.8122 1077.00 0.0000 810.76 9.9152 1077.34 12.7994 815.77 0.0000 1085.87 16.5037 1048.07 0.0000 1093.63 11. 9503 832.01 11.1165 1099.45 11. 9733 834.85 15.5819 1112. 07 18.4973 835.71 14.4742 14.8008 836.80 0.0000 1115. 54 10.3701 846.75 0.0000 1120.29 9.2731 846.77 '13.'4224 1120.55 9.2743 856.80 0.0000 1221. 41 9.2761 860.56 8.4369 1129. 67 11.1621 871.09 14.6864 1131. 51 0.0000 873.19 13.5684 1147.95 0.0000 875.33 0.0000 1173.23 13.2036 879.38 11. 9018 1177.95 11. 3342 880.51 11. 9073 1189.05 18.0085 883.24 10.2173 1204.77 16.1907 884.68 4.5436 1221.41 10.5294 889.28 4.5521 1231. 02 13.4403 894.76 5.7023 1235.36 0.0000 898.04 15.9875 1238.28 19.2419 900.72 6.8589 1260.41 0.0000 903.28 14.8757 1271. 87 12.6318 911.20 16.0701 1274.44 9.7241 912.08 16.0753 1274.54 9. 7241 923.98 0.0000 1291.59 9.7723 926.50 9.2373 1298.22* 0.0000 929 .11 5.7790 1312 .11 0.0000 937.49 17.3926 1332.49 11.8638 944 .13 0.0000 1362.66 0.0000 946.00 10.4692 . 1365.19 5.9861 949.00 10.4810 1368.63 0.0000 667.71 0.0000 1384.29 9.1691 962. 31 18.0571 1408.01 4. 0371 964.08 8.4322 1457.56 0.0000 966 .17 23. 9096 1460.82 4.0935 911.20 13 .1992 1489.16 6.1853 968. 97 13.1992 1505.03 3.3121 983.53 0.0000 1584.12 8.4429 984.45 0.0000 1596.21 0.0000 Page 434of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:09:36.84 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R1203621687.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM11.CNF;517 Background date : Z-OCT-2016 11:00:34. Sample date 12-SEP-2016 00:00:00 Acquisition date : 3-0CT-2016 04:53:57. Sample ID Rl203621687 Sample quantity : 1.15000E+02 GRAM Detector name : GAMll Detector geometry: CAN Elapsed live time: 0 00:15:00.00 Elapsed real time: 0 00:15:06.51 0.7% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID
  • 1596387 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 0 2 0 3 0 4 0 5 0 6 0 7 0 8 0 9 0 10 0 11 0 12 0 13 0 14 0 15 0 16 0 17 0 18 0 19 0 20 .o 21 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 8 32 0 33 0 34 0 Page435 of614 Energy 46.42* 59.46 88.00 121. 78 129.70 157.09 160.06 214.22 259.51 325.09 332.46 338.69* 363.40 416.58 431.82 625.68 636.02 661.65* 744.80 756.15 858.21 909.43 948.19 1098.69 1115. 98 1164. 48 1173.28 1244.74 1267.54 1332.58* 1403.68 1539.25* 1681.35 1701. 94 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 11776 24098 3273 205 99 40 52 67 116 57 106 37 92 77 42 45 48 14981 53 55 40 35 37 36 90 45 9309 22 21 8566 15 8 15 22 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6823 4611 1523 1070 827 466 588 518 641 400 611 360 596 512 604 492 182 525 182 318 426 293 443 323 414 255 293 29 86 102 24 15 10 4 0.83 0.82 0.82 1.13 1. 30 1.19 1. 34 1. 03 2.32 1. 35 1. 62 0. 86 1. 29 1. 99 1. 34 0.49 1. 80 .1.40 0.76 3.32 0.66 1. 44 1. 65 1. 32 3.14 4.18 1. 78 0.71 4.77 1. 78 1. 44 1. 02 3.83 4.57 92.71 118. 83 175.93 243.55 259.40 314.21 320.16 428.56 519.19 650.43 665.18 677.64 727. 08 833.51 861.01 1251.90 1272. 60 1323.88 1490.23 1512.95 1717.13 1819.60 1897.13 2198.19 2232. 7'8 2329.81 2347.40 2490.34 2535.94 2666.03 2808.22 3079.35 3363.52 3404.69 88 114 171 240 256 312 318 427 515 648 661 676 722 831 860 1246 1270 1317 1487 1508 1714 1818 1895 2191 2227 2322 2339 2486 2523 2657 2802 3075 3357 3396 10 1. 31E+Ol 1. 6 10 2.68E+Ol 0.8 9 3.64E+00 2.8 9 2.28E-01 29.6 8 1. lOE-01 51. 0 5 4.45E-02 82.5 6 5.79E-02 74.6 5 7.43E-02 52.6 8 1.28E-01 39.1 6 6.36E-02 56.8 9 1.18E-01 42.9 5 4.12E-02 78.5 9 1. 02E-01 49. 2 7 8.55E-02 49.9 8 4. 72E-02101. 4 14 5.03E-02104.8 6 5.36E-02 46.3 15 1.66E+Ol 0.9 7 5.89E-02 44.5 11 6 .15E-02 63. 7 11 4.45E-02101.0 7 3.85E-02 83.3 9 4.09E-02104.0 10 3.99E-02 95.7 13 1. OlE-01 47. 7 14 4.96E-02 77.4 17 1.03E+Ol 1.1 8 2.46E-02 47.6 17 2.35E-02104.l 19 9. 52E+OO 1.1 13 1. 62E-02 72. 9 8 8.64E-03 95.5 11 l.68E-02 49.3 15 2.45E-02 28.7 Fit Peak Search Report (continued) Page : 2 Sample ID : R1203621687 Acquisition date 3-0CT-2016 04:53:57 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1743.31 16 19 4.05 3487.42 3479 15 1.79E-02 63.6 36 0 1748.34 6 7 0.60 3497.47 3493 8 6.75E-03 88.6 37 0 1759.92 16 9 2.89 3520.63 3514 .12 1.78E-02 45.0 38 0 1799.64 29 22 5.73 3600.07 3586 22 3.22E-02 45.2 39 0 1878.07 10 8 2.75 3756.87 3749* 11 1.08E-02 65.6 40 0 1932.51 17 6 1. 33 3865.74 3861 12 1.84E-02 38.7 41 0 1961.35 18 11 1. 35 3923.40 3916 15 2.02E-02 46.3 Flag: "*" = Peak area was modified by background subtraction Page 436 of 614 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 05:09:38 Configuration Analyses by Sample title Sample date Sample ID Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Rl203621687.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4 MXRl 12-SEP-2016 00:00:00 Rl203621687 SOLID GAMMAll 0 00:15:00.00 1.50 keV No Linear 75.00 Acquisition date : Sample quantity Sample geometry Detector geometry: Elapsed real time: Half life ratio : Systematic Error Efficiencies at 3-0CT-2016 04:53:57 115. 00 GRAM CAN 0 00:15:06.51 10.00 0.00 % Peak Energy 0.7% No interference correct{on performed Page 437of614 Nuclide Line Activity Report Page : 2 Sample ID : Rl203621687 Acquisition date 3-0CT-2016 04:53:57 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error C0-57 122.06 -.215 85.60* 7.218E+OO 9.084E-01 9.589E-01 59.24 136.47 ------10.68 7.146E+OO ------Line Not Found ------C0-60 1173.23 8867 99.85 l.491E+OO 1.556E+02 1. 567E+02 2.24 1332.49 8112 99.98* 1.340E+OO 1.581E+02 l.593E+02 2.24 ZN-65 1115. 54 86 50.60* l.553E+OO 2. 871E+OO 3.049E+00 95.50 CD-109 88.03 3475 3.70* 6.300E+OO 3.893E+02 4.019E+02 5.54 SN-117M 156.02 42 2 .11 6.846E+OO 7.508E+OO 2.213E+Ol 165.09 158.56 42 86.40* 6.846E+OO 1.834E-01 5.404E-01 165.09 TE-123M 159.00 54 84.00* 6.792E+OO 2.472E-01 2.796E-01 149.20 SN-126 64.28 ------9.60 4.012E+00 ------Line Not Found ------86.94 3475 8.90 6.300E+OO l.619E+02 1. 619E+02 5.54 87.57 3475 37.00* 6.300E+OO 3.893E+Ol 3.893E+Ol 5.54 I-131 80.19 ------2. 62 5.729E+OO ------Line Not Found ------284.31 ------6.12 4.622E+OO ------Line Not Found ------364.49 92 81.50* 3.783E+OO 7.811E-01 4.873E+00 98.39 636.99 47 7.16 2.412E+OO 7.129E+OO 4.448E+Ol 92.58 BA-137M 661.66 14632 89.90* 2.339E+OO 1. 817E+02 1.819E+02 1. 77 CS-137 661. 66 14632 85.10* 2.339E+00 1.920E+02 1.922E+02 1. 77 PM-147 121. 22 215 0.00* 7.218E+OO 2.728E+04 2. 771E+04 59.24 PB-210 46.54 12822 4.25* l.357E+OO 5.805E+03 5.816E+03 3.22 AM-241 59.54 25987' 35.90* 3.351E+OO 5.641E+02 5.642E+02 1. 68 Flag: "*" Key line Page 438of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:09:40.08 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Rl203621687.CNF;l *
  • Acquisition date 3-0CT-2016 04:53:57 Sensitivity : 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:15:06.51 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl *
  • Sample ID R1203621687 Sample Quantity 1.1500E+02 GRAM *
  • Batch Number 1596387 Wet Weight 0.00000 * *Wet wt corr : 1.00000 Dry Weight : 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide C0-57 C0-60 ZN-65 CD-109 SN-117M TE-123M SN-126 I-131 BA-137M CS-137 PM-147 PB-210 AM-241 Activity (pCi/GRAM 9.589E-01 1.593E+02 3.049E+OO 4.019E+02 5.404E-01 2.796E-01 3.893E+Ol 4.873E+OO l.819E+02 l.922E+02 2. 771E+04 5.816E+03 5.642E+02 Cnt uncert ( 1. 96-sigma) 5.567E-01 3.489E+OO 2.854E+OO 2.182E+Ol 8.744E-01 4.089E-01 2 .114E+OO 4.698E+OO 3.150E+00 3.327E+OO 1.609E+04 l.837E+02 9.291E+OO Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-4D SC-46 V-48 CR....:51 MN-54 C0-56 MN-56 C0-58 FE-59 GE-68 AS-73 AS-74 SE-75 Page 439 of 614 Key-Line Activity (pCi/GRAM -5.060E+OO -2.058E-01 O.OOOE+OO 4.050E-02 -1. 797E+OO -5.656E-01 3.691E-01 1. 301E+OO 9.503E-04 1.054E-01 O.OOOE+OO 9. 301E-02 l.401E'+OO -l.009E+Ol -l.329E+Ol 6.248E-01 -2.325E-01 K.L. Cnt Uncert (1.96-sigma) 6.214E+OO 3.140E-01 4.441E+09 2.467E-01 2.120E+OO 7.801E-Ol 1.884E+OO 5.494E+OO 6.214E-01 7.580E-01 1. 960E+41 7.061E-01 2.628E+OO 2.235E+Ol l.584E+Ol 1.687E+OO 6.338E-01 MDA (pCi/GRAM 4.869E-01 6.590E-01 2.578E+OO 1.456E+Ol 1.288E+OO 5.094E-01 1.416E+OO 5.174E+OO 9.321E-01 9.847E-01 l.406E+04 l.060E+02 4.241E+OO MDA (pCi/GRAM 1.071E+Ol 5.436E-01 0.000E+OO 4.875E-01 3'.570E+OO 1 .. 273E+OO 3.171E+OO 1.009E+Ol 1.057E+OO 1.293E+OO O.OOOE+OO 1.212E+OO 3.203E+OO 3.918E+Ol 2.829E+Ol 3.005E+OO 1.042E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL' ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN BR-77 6.028E+02 6. 541E+02 l .134E+03 NOT IDENT. SR-82 -l.445E+OO 6.366E+OO 1.079E+Ol NOT IDENT. RB-83 -1.327E-01 1. lllE+OO 1.955E+OO NOT IDENT. KR-85 3.573E+Ol 1.007E+02 l.802E+02 NOT IDENT. SR-85 2. OllE-01 5.688E-01 1.018E+OO NOT IDENT. RB-86 -1.303E+Ol 1.760E+Ol 3.049E+Ol NOT IDENT. Y-88 -1.769E-01 3.122E-01 5.301E-01 NOT IDENT. Y-91 -4.902E+Ol 2.326E+02 4.144E+02 NOT IDENT. NB-94 4.528E-01 4.425E-01 8.076E-01 NOT IDENT. NB-95 2. 396E-02 6.744E-01 l.159E+OO NOT IDENT. NB-95M 5.353E-01 1.535E+OO 2. 611E+OO NOT IDENT. ZR-95 l.539E+OO 1.922E+OO 2.123E+OO FAIL ABUN NB-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF ZR-97 0.000E+OO 9.884E+09 O.OOOE+OO SHORT HLIF M0-99 -6.687E+Ol 8. 716E+02 l.497E+03 NOT IDENT. TC-99M O.OOOE+OO 7 .112E+24 O.OOOE+OO SHORT HLIF RH-101 -1.531E-01 3.378E-01 5.379E-01 FAIL ABUN RH-102 3.108E-01 8.541E-01 1.367E+OO NOT IDENT .* RU-103 -2.661E-01 7.080E-01 1.236E+OO NOT IDENT. RH-106 -9.529E-01 5.383E+OO 8.317E+OO NOT IDENT. RU-106 -9.529E-01 5.383E+OO 8.317E+OO NOT IDENT. AG-108M -3.621E-01 5.630E-01 8.772E-01 NOT IDENT. AG-llOM -3 .115E-01 9.865E-01 1.641E+OO NOT IDENT. SN-113 2.708E-01 6.982E-01 1.268E+OO NOT IDENT. CD-115 -4.282E+02 1.169E+03 2.034E+03 FAIL ABUN SB-124 2.388E-01 6.625E-01 1.342E+OO NOT IDENT. SB-125 9. 771E-02 1.622E+OO 2.609E+00 FAIL ABUN TE-125M 5.411E+Ol 1.086E+02 1.945E+02 NOT IDENT. I-126 -2.633E+OO 4.783E+OO 7. l 72E+OO NOT IDENT. SB-126 2 .130E+OO 2.859E+OO 5.126E+OO FAIL ABUN SB-127 7.945E+OO 5.652E+Ol 9.883E+Ol NOT IDENT. I-132 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF TE-132 4.795E+OO 3.469E+Ol 5.864E+Ol NOT IDENT. BA-133 5.436E-01 5.928E-01 1.101E+OO NOT IDENT. I-133 O.OOOE+OO l.145E+07 0.000E+OO SHORT HLIF CS-134 -3.328E-01 6.847E-01 1.143E+OO NOT IDENT. CS-135 6.401E-01 2.049E+OO 3.452E+00 NOT IDENT. I-135 O.OOOE+OO 2.694E+23 O.OOOE+OO SHORT HLIF CS-136 8.548E-01 2.616E+OO 4.736E+OO NOT IDENT. CE-139 -9.636E-02 3. 096E-01 5.284E-01 NOT IDENT. BA-140 2. 714E-01 5.676E+OO 1.002E+Ol NOT IDENT. LA-140 -l.005E-02 7. 714E-01 1. 481E+OO NOT IDENT. "' CE-141 -2.030E-02 7.092E-01 1. 232E+OO NOT IDENT. CE-143 O.OOOE+OO 3.383E+04 O.OOOE+OO SHORT HLIF CE-144 1.440E-01 2.230E+OO 3.613E+OO NOT IDENT. PM-144 3.376E-01 4.488E-01 8.108E-01 NOT IDENT. PR-144 2.513E+Ol 3.369E+Ol 6.083E+Ol NOT IDENT. PM-146 8. 271E-01 7.488E-01 1.370E+OO NOT IDENT. ND-147 5.758E+00 1.221E+Ol 2 .196E+Ol NOT IDENT. PM-149 -3.194E+03 8.287E+03 l.354E+04 NOT IDENT. EU-150 1.059E-01 3.888E-01 6.447E-01 NOT IDENT. EU-152 -3.504E-02 1.314E+OO 2.381E+OO FAIL ABUN GD-153 -4.893E-01 8.762E-01 1.531E+OO NOT IDENT. EU-154 -5.814E-01 8.869E-01 1.535E+OO FAIL ABUN EU-155 -l.551E-01 1.078E+OO 1.900E+OO FAIL ABUN TB-160 -1. 404E+OO 2.773E+OO 4.576E+OO FAIL ABUN H0-166M -1.601E-01 8.652E-01 1.485E+OO NOT IDENT. TM-171 -l.324E+02 3.105E+02 5.584E+02 NOT IDENT. HF-172 -4.376E-01 2.372E+OO 3.361E+OO FAIL ABUN LU-172 2.689E-01 1. 313E+OO 2.086E+OO FAIL ABUN LU-176 6.929E-02 3.709E-01 6.169E-01 FAIL ABUN HF-181 -1. 505E-01 8.378E-01 l.473E+OO NOT IDENT. TA-182 -l.445E+00 1.653E+OO 2.806E+00 NOT IDENT. RE-183 0.000E+OO 1.200E+Ol 9.456E+OO FAIL ABUN RE-184 -4.334E-01 2.785E+OO 4.654E+OO NOT IDENT. W-188 -4.589E+Ol l.033E+02 1.6B2E+02 NOT IDENT. IR-192 -l.076E-01 5.159E-01 8.427E-01 NOT IDENT. HG-203 -5.270E-01 5.535E-01 8.862E-01 NOT IDENT. BI-207 -1.280E-01 9.466E-01 l.681E+OO NOT IDENT. TL-208 -2.539E-01 4.915E-01 8.452E-01 NOT IDENT. BI-211 1. 651E+OO 2.732E+OO 5.042E+OO NOT IDENT. PB-211 9.303E+OO 1. llOE+Ol 2.037E+Ol NOT IDENT. BI-212 9.898E-01 7.401E+OO l.286E+Ol NOT IDENT. PB-212 7.264E-0°1 7.069E-01 1.231E+OO NOT IDENT. BI-214 -4.295E-01 9.568E-01 1.644E+OO NOT IDENT. PB-214 1.499E-01 1.008E+OO 1.834E+OO FAIL ABUN RN-219 -5.933E+OO 6.185E+OO 1.076E+Ol NOT IDENT. RN-222 -4.295E-01 9.568E-01 1.644E+OO NOT IDENT. Page 440of614 RA-223 9.104E+OO 1.013E+Ol 1.435E+Ol FAIL ABUN RA-224 -5.099E+OO 7.653E+OO l.254E+Ol NOT IDENT. RA-226 -4.295E-01 9.568E-01 1. 644E+OO NOT IDENT. AC-227 -9.465E-Ol 3.677E+OO 5.590E+00 NOT IDENT. TH-227 -9.465E-Ol 3.677E+00 5.590E+OO NOT IDENT. AC-228 -1.062E+OO 3.319E+00 4.868E+OO FAIL ABUN RA-228 -1.062E+OO 3.319E+OO 4.868E+OO FAIL ABUN TH-228 7.264E-01 7.069E-01 1. 231E+OO NOT IDENT. TH-229 3.690E+OO 5.909E+OO 1.028E+Ol FAIL ABUN TH-230 -4.295E-01 9.568E-01 l.644E+OO NOT IDENT. PA-231 9.666E-01 6.527E+OO 1.085E+Ol NOT IDENT. TH-231 9.104E+OO 1. 013E+Ol l.435E+Ol FAIL ABUN TH-232 -1.062E+OO 3.319E+OO 4.868E+OO FAIL ABUN PA-233 4.638E-01 9.382E-01 1.575E+OO NOT. IDENT. PA-234 -4.542E-01 7.143E+OO 1.058E+Ol FAIL ABUN PA-234M -2.103E+Ol 8.169E+Ol 1. 451E+02 NOT IDENT. TH-234 2.362E+OO l.280E+Ol 2.174E+Ol NOT IDENT. U-234 -4.295E-01 9.568E-01 1.644E+OO NOT IDENT. U-235 3.699E-01 2.009E+OO 3.517E+OO NOT IDENT. NP-237 4.638E-01 9.382E-01 l.575E+OO NOT IDENT. NP-238 0.000E+OO 3.048E+03 O.OOOE+OO SHORT HLIF U-238 2.362E+OO 1.280E+Ol 2.174E+Ol NOT IDENT. NP-239 l.050E+OO 2. 717E+OO 4.841E+OO NOT IDENT. PU-239 5. 971E+03 5. 966E+03 6.240E+03 FAIL ABUN AM-243 l.404E-01 5.286E-01 9.553E-01 NOT IDENT. CM-243 2.186E-01 1.103E+OO 1. 964E+OO NOT IDENT. BK-247 -8.523E-01 1. lllE+OO 1.800E+OO NOT IDENT. CM-247 -2. %4E-02 5.545E-01 9.926E-01 NOT IDENT. CF-249 3.736E-02 5.843E-01 1.053E+OO FAIL ABUN CF-251 5.917E-01 1.385E+OO 2. 411E+OO NOT IDENT. ANH-511 -1.307E-01 4.433E-01 7.862E-01 NOT IDENT. Page 441of614 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:09:37.61 Nuclide Line Activity Report Nuclide Type: Nuclide C0-57 C0-60 ZN-65 CD-109 SN-ll 7M TE-123M SN-126 I-131 BA-137M CS-137 PM-147 PB-210 AM-241 Flag: "*" Page 442of614 Energy 122.06 136.47 1173.23 1332.49 1115. 54 88.03 156.02 158.56 159.00 64.28 86.94 87.57 80.19 284.31 364.49 636.99* 661. 66 661.66 121.22 46.54 59.54 Key line Area 2i5 88 67 8112 86 3475 42 42 54 3475 3475 92 47 14632 14632 215 12822 25987 %Abn 85.60* 10.68 99.85 99.98* 50.60* 3.70* 2 .11 86.40* 84.00* 9.60 8.90 37.00* 2.62 6.12 81.50* 7.16 89.90* 85.10* 0.00* 4.25* 35.90* %Eff 7.218E+OO 7.146E+OO 1.491E+OO 1.340E+OO 1.553E+OO 6.300E+OO 6.846E+OO 6.846E+OO 6.792E+00 4.012E+OO 6.300E+OO 6.300E+OO 5.729E+OO 4.622E+OO 3.783E+OO 2.412E+OO 2.339E+OO 2.339E'.t-OO 7.218E+OO 1.357E+OO 3.351E+00 Uncorrected Decay Corr pCi/GRAM pCi7GRAM 9.084E-01 9.589E-01 ------Line Not Found l.556E+02 l.567E+02 l.581E+02 l.593E+02 2.871E+OO 3.893E+02 4.019E+02 7.508E+OO 2.213E+Ol l.834E-01 5.404E-01 2.472E-01 2.796E-01 ------Line Not Found l.619E+02 l.619E+02 3.893E+Ol 3.893E+Ol ------Line Not Found ------Line Not Found 7.811E-01 4.873E+OO 7.129E+00 4.448E+Ol l.817E+02 l.819E+02 l.920E+02 1.922E+02 2.728E+04 2.771E+04 5.805E+03 .5.816E+03 5.641E+02 5.642E+02. 2-Sigma %Error 59.24 2.24 2.24 95.50 5.54 165.09 165.09 149.20 5.54 5.54 98.39 92.58 1. 77 1. 77 59.24 3.22 1. 68 Summary of Nuclide Activity Sample ID : Rl203621687 Acquisition date Page : 2 3-0CT-2016 04:53:57 Total number of lines in spectrum 41 Number of unidentified lines 19 Number of lines tentatively identified by NID 22 53.66% Nuclide Type : Uncorrected Decay Corr Decay Corr 2-Sigma Nuclide Hlife Decay pCi/GRAM pCi/GRAM 2-Sigma Error %Error Flags C0-57 271. 74D 1. 06 9.084E-01 9.589E-01 5.681E-01 59.24 C0-60 5.27Y 1. 01 1.581E+02 1.593E+02 0.036E+02 2.24 ZN-65 244.06D 1. 06 2.871E+OO 3.049E+oo* 2.912E+OO 95.50 CD-109 461.40D 1. 03 3.893E+02 4.019E+02 0.223E+02 5.54 SN-117M 13.60D 2.95 l.834E-01 5.404E-01 8.922E-01 165.09 TE-123M 119.20D 1.13 2.472E-01 2.796E-01 4. l 72E-01 149.20 SN-126 2.30E+05Y 1. 00 3.893E+Ol 3.893E+Ol 0.216E+Ol 5.54 I-131 8.03D 6.24 7. 811E-01 4.873E+OO 4.794E+OO 98.39 BA-137M 30.08Y 1. 00 1. 817E+02 1.819E+02 0.032E+02 1. 77 CS-137 30.08Y 1. 00 l.920E+02 1.922E+02 0.034E+02 1. 77 PM-147 2.62Y 1. 02 2.728E+04 2.771E+04 1. 641E+04 59.24 PB-210 22.20Y 1. 00 5.805E+03 5.816E+03 0.187E+03 3.22 AM-241 432.60Y 1. 00 5. 641E+02 5.642E+02 0.095E+02 1. 68 ------------------Total 3. 462E+04 3.507E+04 Grand Total Activity 3: 462E+o4* 3.507E+04 Flags: "K" Keyline not found "M" Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit Page 443of614 Unidentified Energy Lines Page : 3 Sample ID : Rl203621687 Acquisition date : 3-0CT-2016 04:53:57 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 129.70 104 8 64 1. 30 259.40 256 8 1.lOE-01 **** 7.20E+OO T 0 214.22 69 531 1. 03 428.56 427 5 7.43E-02 **** 5.73E+OO T 0 259.51 118 652 .2.32 519.19 515 8 1.28E-01 78.2 4.97E+OO T 0 325.09 58 402 1. 35 650.43 648 6 6.36E-02 **** 4.14E+OO T 0 332.46 107 614 1. 62 665.18 661 9 1.18E-01 85. 9 4.07E+OO T 0 338.69 37 362 0. 8 6 677. 64 676 5 4.12E-02 **** 4.0lE+OO T 0 416. 58 *,_ 77 5'10 1. 99 833.51 831 7 8.55E-02 99.8 3.38E+OO 0 431.82 42 600 1. 34 864.01 860 8 4.72E-02 **** 3.28E+OO 0 625.68 44 481 0.49. 1251.90 1246 14 5.03E-02 **** 2.44E+OO 0 744.80 52 177 0.76 1490.23 1487 7 5.89E-02 88.9 2.13E+00 0 756.15 54 308 3.32 1512.95 1508 11 6.15E-02 **** 2. llE+OO T 0 858.21 39 411 0.66 1717.13 1714 11 4.45E-02 **** 1. 91E+OO T 0 909.43 33 283 1. 44 1819.60 1818 7 3.85E-02 **** 1.83E+OO 0 948.19 35 426 1. 65 1897.13 1895 9 4.09E-02 **** 1.77E+OO T 0 1098.69 34 309 1. 32 2198.19 2191 10 3.99E-02 **** 1.57E+OO T 0 1164. 48 43 243 4.18 2329.81 2322 14 4.96E-02 **** 1. 50E+OO 0 1244.74 21 27 0.71 2490.34 2486 8 2.46E-02 95.2 1. 42E+OO 0 1267.54 20 81 4.77 2535.94 2523 17 2.35E-02 **** 1.40E+OO 0 1403.68 14 23 1. 44 2808.22 2802 13 1.62E-02 **** 1. 28E+00 0 1539.25 7 14 1. 02 3.079.35 3075 8 8.64E-03 **** 1.18E+OO 0 1681. 35 14 9 3.83 3363.52 3357 11 1.68E-02 98.6 1. 09E+00 0 1701.94 21 4 4.57 3404.69 3396 15 2.45E-D2 57.4 1. 08E+OO 0 1743.31 15 18 4.05 3487.42 3479 15 l.79E-02 **** 1. 05E+OO 0 1748.34 6 6 0.60 3497.47 3493 8 6.75E-03 **** 1. 05E+*oo 0 1759.92 15 8 2.89 3520.63 3514 12 1.78E-02 89.9 1.04E+OO 0 1799.64 27 21 5.73 3600.07 3586 22 3.22E-02 90.4 l.02E+00 0 1878.07 9 8 2.75 3756.87 3749 11 1.08E-02 **** 9.78E-01 0 1932.51 15 6 1. 33 3865.74 3861 12 1.84E-02 77.3 9.50E-01 0 1961. 35 17 10 1. 35 3923.40 3916 15 2.02E-02 92.7 9.36E-01 Flags: "T" = Tetitatively associated Page 444of614 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:09:54.59 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Rqad *
  • Charleston, SC 29407. * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]R1203621687.CNF;l *
  • Acquisition date 3-0CT-2016 04:53:57 Sensitivity : 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:15:06.51 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID Rl203621687 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : 1.1500E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN * *'Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;14
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide C0-57 C0-60 ZN-65 CD-109 SN-117M TE-123M SN-126 I-131 BA-137M CS-137 PM-147 PB-210 AM-241 Le (pCi/GRAM 2.374E-01 3.032E-01 1.242E+OO 7.125E+OO 6.266E-01 2.477E-01 6.930E-01 2.516E+OO 4.494E-01 4.748E-01 6.856E+03 5.241E+Ol 2.092E+OO ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-58 FE-59 GE-68 AS-73 AS-74 SE-75 BR-77 Page 445 of 614 Le (pCi/GRAM 5.207E+OO 2.462E-01 O.OOOE+oo 2.092E-01 1.519E+OO 6.142E-01 1. 535E+OO 4.902E+OO 5. 096E-01 6.248E-01 O.OOOE+OO 5.843E-01 *1. 547E+00 '1. 888E+Ol 1.398E+01 1.449E+00 5.074E-01 5.532E+02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SH.ORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT.

SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SB-124 SB-125 TE-125M. I-126 SB-126 SB-127 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 TL-208 BI-211 PB-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-223 Page 446 of 614 5.197E+OO 9.447E-01 8.726E+Ol 4.929E-01 1:469E+Ol 2.245E-01 l.954E+02 3.881E-01 5.584E-01 1. 272E+OO 1.023E+OO O.OOOE+OO O.OOOE+OO 7.200E+02 ' 0. OOOE+OO 2.617E-01 6.573E-01 5.988E-01 4.009E+OO 4.009E+OO 4.268E-01 7.933E-01 6.169E-01 9.837E+02 5.840E-01 1.268E+OO 9.487E+Ol 3.443E+OO 2.466E+OO 4.751E+Ol O.OOOE+OO 2.860E+Ol 5.356E-01 O.OOOE+OO 5.510E-01 1. 681E+OO O.OOOE+OO 2.287E+OO 2.569E-01 4.846E+OO 6.385E-01 5.995E-01 O.OOOE+OO 1.760E+OO 3.891E-01 2.919E+Ol 6.678E-01 1.061E+Ol 6.582E+03 3 .133E-01 1.157E+OO 7.465E-01 6.953E-01 9.258E-01 2.212E+OO 7 .131E-01 2.759E+02 1.636E+OO 1.007E+OO 2.999E-01 7.159E-01 1.301E+OO 4.689E+OO 2.252E+OO 8.172E+Ol 4.092E-01 4.305E-01 8 .115E-01 4.066E-01 2.451E+OO 9.918E+OO 6.189E+00 6. OOlE-01 7.'909E-01 8.919E-01 5.226E+00 7.909E-01 6. 965E+OO NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN RA-224 RA-226 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-231 TH-232 PA-233 PA-234 PA-234M TH-234 U-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 ANH--511 Page 447 of 614 6.106E+OO 7.909E-01 2.721E+OO 2. 721E+OO 2.360E+OO 2.360E+OO 6. OOlE-01 5.012E+OO 7.909E-01 5.275E+OO 6. 965E+OO 2.360E+OO 7.665E-01 5.124E+OO 7.008E+Ol 1.062E+Ol 7.909E-01 1. 713E+OO 7.665E-01 O.OOOE+OO 1.062E+Ol 2.359E+OO 3.042E+03 4.676E-01 9.579E-01 8.761E-01 4.823E-01 5 .115E-01 1.174E+OO 3.809E-01 NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:10:00.57 **********.*********************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.*GAMMA]Rl203621687.CNF;l *
  • Acquisition date 3-0CT-2016 04:53:57 Sensitivity : 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:15:06.51 Half life ratio : *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID R1203621687 Analyst initials: MXRl *
  • Batch Number 1596387 Sample Quantity : l.1500E+02 GRAM *
  • Quantity Err(%): 1.7391E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION. * * *
  • Eff. Cal. date 2-AUG-20'16 10:31:39 Eff. Geometry . : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) C0-57 9.589E-01 5.585E-01 5.585E-01 C0-60 1.593E+02 6.820E+OO 6.820E+OO ZN-65 3.049E+OO 2.856E+00 2.856E+OO CD-109 4.019E+02 3.939E+Ol 3.939E+Ol SN-ll 7M 5.404E"-01 8.747E-01. 8.747E-01 TE-123M 2.796E-01 4. 091E-01 4.091E-01 SN-126 3.893E+Ol 3.210E+OO 3.210E+OO I-131 4.873E+OO 4.704E+OO 4.704E+00 BA-137M
  • 1.819E+02 8.432E+OO 8.432E+OO CS-137 1.922E+02 8.888E+OO 8.888E+00 PM-147 2. 771E+04 1.614E+04 1.614E+04 PB-210 5.816E+03 5.389E+02 5.389E+02 AM-241 5.642E+02 4.257E+Ol 4.257E+Ol Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1 .. 96-sigma) ( 1 . 96-sigma ) BE-7 -5.060E+00 6.218E+OO 6.623E+OO NOT IDENT. NA-22 -2.058E-01 3.141E-01 3.275E-01 NOT IDENT. NA-24 2.494E+09 4.443E+09 4.583E+09 SHORT HLIF AL-26 4.050E-02 2.467E-01 2.474E-01 NOT IDENT. K-40 -l.797E+OO 2.122E+OO 2.271E+OO NOT IDENT. SC-46 -5.656E-01 7.804E-01 8.210E-01 NOT IDENT. V-48 3.691E-01 1.884E+OO 1.892E+OO NOT IDENT. CR-51 1. 301E+OO 5.494E+OO 5.525E+OO NOT IDENT. MN-54 9.503E-04 6.214E-01 6.214E-01 NOT IDENT. C0-56 l.054E-01 7.580E-01 7.595E-01 NOT IDENT. MN-56 l.OOOE+41 6.892E+41 O.OOOE+OO SHORT HLIF C0-58 9.301E-02 7.061E-01 7.074E-01 NOT IDENT. FE-59 1.401E+00 2.630E+OO 2.705E+OO FAIL ABUN GE-68 -1.009E+Ol 2.235E+Ol 2. 281E+Ol NOT IDENT. AS-73 -1. 32 9E+Ol 1.607E+Ol l.715E+Ol NOT IDENT. AS-74 6.248E-01 1.688E+OO 1. 711E+OO FAIL ABUN SE-75 -2.325E-01 6.339E-01 6.425E-01 FAIL ABUN Page 448of614 BR-77 6.028E+02 7.516E+02 7.992E+d2 NOT IDENT. SR-82 -1.445E+OO 6.366E+OO 6.399E+OO NOT IDENT. RB-83 -l.327E-01 1. lllE+OO 1.113E+OO NOT IDENT. KR-85 3.573E+Ol 1. 007E+02 l.020E+02 NOT IDENT. SR-85 2. OllE-01 5.688E-01 5.760E-01 NOT IDENT. RB-86 -l.303E+Ol 1. 761E+Ol 1.856E+Ol NOT IDENT. Y-88 -l.769E-01 3.124E-01 3.225E-01 NOT IDENT. Y-91 -4.902E+Ol 2.326E+02 2.336E+02 NOT IDENT. NB-94 4.528E-01 4.429E-01 4.877E-01 NOT IDENT. NB-95 2. 396E-02 6.744E-01 6.745E-01 NOT IDENT. NB-95M 5.353E-01 1.535E+OO l.554E+OO NOT IDENT. ZR-95 l.539E+00 1. 924E+OO 2.045E+OO FAIL ABUN NB-97 l.000E+41 3.743E+41 0.000E+OO SHORT HLIF ZR-97 5.192E+09 9.886E+09 1. 016E+10 SHORT HLIF M0-99 -6.687E+Ol 8.716E+02 8.721E+02 NOT IDENT. TC-99M -3.672E+24 7 .121E+24 O.OOOE+OO SHORT HLIF RH-101 -1.531E-01 3.389E-01 3.458E-01 FAIL ABUN RH-102 3.108E-01 8.545E-01 8.659E-01 NOT IDENT. RU-103 -2.661E-01 7.081E-01 7.182E-01 NOT IDENT. RH-106 -9.529E-01 5.384E+OO 5.401E+OO NOT IDENT. RU-106 -9.529E-01 5.384E+OO 5.401E+OO NOT IDENT. AG-108M -3.621E-01 5.632E-01 5.863E-01 NOT IDENT. AG-llOM -3.115E-01 9.867E-01 9. 966E-01 NOT IDENT. SN-113 2.708E-01 6.982E-01 7.088E-01 NOT IDENT. CD-115 -4.282E+02 1.170E+03 l.185E+03 FAIL ABUN SB-124 2.388E-01 6.627E-01 6.713E-01 NOT IDENT. SB-125, 9. 771E-02 1.622E+OO 1.623E+OO FAIL ABUN TE-125M 5. 411E+Ol 1. 086E+02 l .113E+02 NOT IDENT. I-126 -2.633E+OO 4.785E+OO 4.930E+OO NOT IDENT. SB-126 2.130E+OO 2.867E+OO 3.023E+OO FAIL ABUN SB-127 7.945E+OO 5.653E+Ol 5.664E+Ol NOT IDENT. I-132 1.000E+41 1.836E+42 O.OOOE+OO SHORT HLIF TE-132 4.795E+OO 3.469E+Ol 3.476E+Ol NOT IDENT. BA-133 5.436E-01 5.932E-01 6.418E-01 NOT IDENT. I-133 3.855E+06 1.146E+07 l.160E+07 SHORT HLIF CS-134 -3.328E-01 '6.848E-01 7. OllE-01 NOT IDENT. CS-135 6.401E-01 2.050E+OO 2.070E+OO NOT IDENT. I-135 -l.181E+23 2.754E+23 O.OOOE+OO SHORT HLIF CS-136 8.548E-01 2.617E+OO 2.645E+OO NOT IDENT. CE-139 -9.636E-02 3.102E-01 3 .132E-01 NOT IDENT. BA-140 2.714E-01 5.676E+OO 5.677E+OO NOT IDENT. LA-140 -1.005E-02 7.714E-01 7.714E-01 NOT IDENT. CE-141 -2.030E-02 7.092E-01 7.092E-01 NOT IDENT, CE-143 2.243E+04 3.385E+04 3.533E+04 SHORT HLIF CE-144 l.440E-01 2.230E+OO 2.231E+OO NOT IDENT. PM-144 3.376E-01 4.491E-01 4. 741E-01 NOT IDENT. PR-144 2.513E+01 3.370E+Ol 3.556E+Ol NOT IDENT. PM-146 8.271E-01 7.512E-01 8.386E-01 NOT IDENT. ND-147 5.758E+OO 1.221E+Ol 1.248E+Ol NOT IDENT. PM-149 -3.194E+03 8.298E+03 8.422E+03 NOT IDENT . EU-150 l.059E-01 . 3 .. 889E-01 3.918E-01 NOT IDENT. EU-152 -3.504E-02 1.314E+OO 1.314E+OO FAIL AB{JN GD-153 -4.893E-01 8.766E-01 9.039E-01 NOT IDENT. EU-154 -5.814E-01 8.872E-01 9. 251E-01 FAIL ABUN EU-155 -l.551E-01 l.078E+OO 1.080E+OO FAIL ABUN TB-160 -1.404E+OO 2.774E+OO 2. 846E+OO FAIL ABUN H0-166M -1. 601E-01 8.652E-01 8.682E-01 NOT IDENT. TM-171 -1.324E+02 3.107E+02 3.164E+02 NOT IDENT. HF-172 -4.376E-01 2.373E+OO 2.381E+OO FAIL ABUN LU-172 2.689E-01 l.313E+OO 1.319E+OO FAIL ABUN LU-176 6.929E-02 3.709E-01 3.722E-01 FAIL ABUN HF-181 -l.505E-01 8.378E-01 8.406E-01 NOT IDENT. TA-182 -l.445E+OO 1.654E+OO 1.777E+OO NOT IDENT. RE-183 7.284E+02 7.570E+Ol 3.370E+02 FAIL ABUN RE-184 -4.334E-01 2.785E+OO 2.792E+OO NOT IDENT. W-188 -4.589E+Ol l.034E+02 l.055E+02 NOT IDENT. IR-192 -1. 076E-01 5.159E-01 5.182E-01 NOT IDENT .. HG-203 -5.270E-01 5.541E-Ol 6.029E-01 NOT IDENT. BI-207. -1.280E-01 9.466E-01 9.484E-01 NOT IDENT. TL-208 -2.539E-01 4.916E-01 5.048E-01 NOT IDENT. BI-211 l.651E+OO 2.733E+OO 2.833E+OO NOT IDENT. PB-211 9.303E+OO l. lllE+Ol 1.188E+Ol NOT IDENT. BI-212 9.898E-01 7.401E+OO 7.415E+OO NOT IDENT. PB-212 7.264E-01 7.079E-01 7.800E-01 NOT I DENT., BI-214 -4.295E-01 9.570E-01 9.764E-01 NOT IDENT. PB-214 1.499E-01 1.008E+OO l.OlOE+OO FAIL ABUN RN-219 -5.933E+OO 6.230E+OO 6.779E+OO NOT IDENT. RN-222 -4.295E-01 9.570E-01 9.764E-01 NOT IDENT. Page 449of614 RA-223 9.104E+OO 1.015E+Ol l.095E+Ol FAIL ABUN RA-224 -5.099E+OO 7.658E+OO 7.995E+OO NOT IDENT. RA-226 -4.295E-01 9.570E-01 9.764E-01 NOT IDENT. AC-227 -9.465E-01 3.679E+OO 3.704E+00 NOT IDENT. TH-227 -9.465E-01 3.679E+OO 3.704E+OO NOT IDENT. AC-228 -1.062E+OO 3.319E+OO 3.354E+OO FAIL ABUN RA-228 -1.062E+OO 3.319E+OO 3.354E+OO FAIL ABUN TH-228 7.264E-01 7.079E-01 7.800E-01 NOT IDENT. TH-22'9 3.690E+OO 5.912E+OO 6.141E+OO FAIL ABUN TH-230 -4.295E-01 9.570E-01 9.763E-01 NOT IDENT. PA-231 9.666E-Ol .6. 530E+OO 6.544E+OO NOT IDENT. TH-231 9.104E+OO 1.015E+Ol l.095E+Ol FAIL ABUN TH-232 -l.062E+OO 3.319E+OO 3.354E+OO FAIL ABUN PA-233 4.638E-01 9.385E-01 9.615E-01 NOT IDENT. PA-234 -4.542E-01 7.162E+OO 7.165E+OO FAIL ABUN PA-234M -2.103E+Ol 8.169E+Ol 8.224E+Ol NOT IDENT. TH-234 2.362E+OO 1. 281E+Ol l.285E.+Ol NOT IDENT. U-234 -4.295E-01 9.570E-01 9.763E-01 NOT IDENT. U-235 3.699E-01 2.009E+OO 2.016E+OO NOT IDENT. NP-237 4.638E-01 9.385E-01 9.615E-01 NOT IDENT. NP-238 2.726E+03 3.050E+03 3.289E+03 SHORT HLIF U-238 2.362E+OO 1.281E+Ol l.285E+Ol NOT IDENT. NP-239 1.050E+OO 2.718E+OO 2.759E+OO NOT IDENT. PU-239 5. 971E+03 5.972E+03 6.550E+03 FAIL ABUN AM-243 1. 404E-01 5.286E-01 5.324E-01 NOT IDENT. CM-243 2.186E-01 1.103E+OO l.107E+OO NOT IDENT. BK-247 -8.523E-01 l.124E+OO l.188E+00 NOT IDENT. CM-247 .:..2. 964E-02 5.545E-01 5.546E-01 'NOT IDENT. CF-249 3.736E-02 5.843E-01 5.845E-01 FAIL ABUN CF-251 5.917E-01 1. 38 6E+OO 1.412E+OO NOT IDENT. ANH-511 -1.307E-01 4.434E-01 4.473E-01 NOT IDENT. Page 450 of 614
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT
  • ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 2702.3931 87.09 669.3035 136.47 460.4278 45.60 2389.0461 87.57 669. 9716 140.51 484.8883 46.54 2396 .1536 88.03 670. 6072 143.76 445.7536 49.72 2060.5361 88.34 671.0309 144.24 450.2180 51. 35 2137.7312 88.47 671.2101 145.44 440.6143 51. 87 2185.8535 89. 96 548.4362 152.43 471.2664 52.39 2218.5422 90.64 528.9883 153.25 412.9630 52.97 2299.2927 91.11 510.5358 154.21 436.3124 53.44 2323.2012 572.2518 156.02 458.5038 54.07 2364.7126 93.35 533.1262 158.56 410.7107 57.36 0.0000 94.56 488.5938 159.00 410.9534 57.53 2643.6135 94.65 488.6797 162.33 445.4338 57.98 1631.4543 94.67 488.6992 162.66 445.6319 59.27 1637.1488 94.87 472.6579 163.33 420.4595 59 .*32 1637.3687 97.43 528.7451 165.86 416.8863 59.54 1638.3331 98.43 461.4917 176.31 433.3862 60. 96 567.3392 98.44 461. 5027 176.60 433.5449 61.17 567.6523 99.53 505.8140 177.52 425.3645 62.93 598.7089 100 .11 498.6507 181.07 426.1647 63.29 581. 4637 102.03 473.3419 181.52 427.4939 63.58 605.6458 103.18 503.4504 184.41 454.1849 64.28 599.5908 103.37 492.9544 185. 72 522.8760 66.73 631.1188 105.21 495.5908 193.51 444.7971 67.24 659.7780 105.31 489.8371 197.03 439.9711 67.68 636.1986 106.12 476.9048 198.01 452.7080 67.75 662.4067 106.47 499.6523 201. 83 470.3424 69.67 621.2048 109.28 485.4944 203.43 499.1844 70.83 647 .4111 111. 00 510.5818 205.31 468.8468 72.81 665.9266 111. 76 471. 8555 210.85 496. 5912 72. 87 666.0214 114. 06 488.5765 215.65 518.8894 74.66 674.2770 116. 30 449.7444 222 .11 489.0038 74.82 644.3218 116.74 450.0796 227.09 461.7271 74.97 643.6318 119.76 442.0486 227.38 508.9741 77 .11 703.8044 121.12 502.4290 228.16 503.6372 78.74 646.3539 121.22 502.5094 228.18 503.6505 79.69 695.8260 121. 7 8 502.9728 235.69 453 .*1080 80.12 657.5864 122.06 503.2065 235. 96 452.0741 80.19 657.6893 122.92 503.9150 238.63 439.3581 80.57 692.5389 123.07 504.0375 238.98 449.9755 81. 00 740.5147 123.68 483.7681 240.99 499.8214 81. 07 740.6243 125.81 457.8690 242.00 474.6677 81. 75 664.5739 127.23 447.4523 244.70 463.0897 83.79 697.0492 127.91 415.5575 252.40 458.3524 84.00 652.5267 129.30 450.2736 252.80 449.1005 85.43 710.7059 131. 20 465.1840 254.15 0.0000 86.55 668.5538 133. 02 443.3817 256.23 462.0210 86.79 668.8852 133. 52 457. 3311 260.90 419.7343 86.94 669.0970 136. 00 450.8765 264.66 464.9341 Page451 of614 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.80 464.9936 364.49 409.1471 600.60 231.6917 265.00 484.1694 366.42 378.6073 602.52 0.0000 268.22 429.4020 372.51 375.0820 604. 72 232.1657 269.46 447.8572 375.05 394.0341 607.14 245.4194 270.03 467.2668 1093.63 392.9917 609.32 233.6953 271.23 432.9951 383.85 395.6379 610.33 232.8104 273.65 459.2090 388.16 386.3070 614.28 222.2529 276.40 431. 4289 388.63 401.3626 618.01 242.7090 277.37 398.0383 391. 69 397.8174 620.36 231. 9493 277.60 404.1510 400.66 383.4559 621.93 245.6839 278.00 415.1663 401.81 436.9417 630.19 0.0000 279.20 437.3541 402.40 391.8937 631. 2 9 193.8047 279.54 454.4175 404.85 402.3195 633.25 192.4689 279.70 454.4749 410.95 429.8402 634.78 192.6084 280.46 397.9366 413. 71 415.4462 635.95 218.5137 283.69 419.7130 414.70 418.4026 636. 99' 232.2828 284.31 432.0824 423. 72 428.0920 645.85 241. 8 931 285.41 . 416.7123 427.09 415.3313 657.76 286.6747 285.90 415.6749 427.87 401. 7494 657.90 0.0000 287.50 419.9107 433.94 467.1526 661.66 239.5796 290.67 412.5358 439.40 481.4986 664.57 0.0000 293.27 0.0000 453.88 429.0571 666.33 217.0078 295.22 419.0669 463.37 441. 7146 666.50 223.1818 295. 96 399.7201 468.07 '454.0791 667.71 0.0000 298.58 422.7458 473.00 522. 2114 677.62 170.1697 299.98 403.5637 475.06 453.2109 685.70 199.7695 300.09 403.5938 476.78 463.9.039 695.00 195.4050 300.13 403.6138 477.60 463.1971 696.49 160.1660 301.36 401.5706 482.18 410.3695 696.51 160.1723 302.85 399.6112 487.02 361.0269 697.00 179.9690 304.50 401.4099 492.35 328.3813 697.30 169.5927 304.85 401.5190 497.08 341. 5163 697.49 169.6060 306.78 383.6118 505.52 329.9354 702.65 162.6904 308.46 405.2173 507.63 0.0000 706.68 183.8705 311. 90 395.2000 511. 00 312.9434 711. 68 203.1174 316.51 377.9825 514.00 293.5223 720.70 180.7834 319.41 385.1316 514.00 293.5223 721.93 0.0000 320.08 369.4911 520.40 280.2786 722.78 228.2844 321. 04 352.5930 520.69 279.3729 722.91 216.7292 323.87 381. 5029 522.65 0.0000 723.31 211. 5015 325.23 365.1695 527.90 299.6400 724.19 198.9514 328.76 335 .1301 528.26 291.0736 727.33 210.8154 333.37 393.2487 529.59 269.2574 733.00 213.4332 333.97 378.2576 529.87 0.0000 735.93 215.8120 334.37 373.3144 531. 02 254.1201 737.46 210.6602 338.28 402.3834 537.26 280.9621 739.50 216.1357 338.32 402.3930 546.56 0 .. 0000 747.24 213.6525 340.48 353. 4811 552.55 282.3088 748.06 218.5110 340.55 353.4981 563.25 228.2966 752.31 214.1023 344.28 392.7733 569.33-234.8926 753.82 228.6219 345.93 356.6683. 569.50 233.9430 756.73 207.0249 351.06 370.0303 569.70 236.8992 .7 56. 80 207.0328 351. 93 394.2210 583.19 233.6151 763.94 212.9922 355.39 0.0000 584.27 230.7913 765.81 229.2210 356.01 381. 7066 595.83 226.1816 766.42 230.3534 Page 452 of 614 ENERGY MDA COUNTS ENERGY MDA COUNTS. ENERGY MDA COUNTS 766.84 220.7442 1002.74 275.9134 1678.03 0.0000 772.60 0.0000 1004.73 266.4453 1690.97 11. 5250 776.52 231.2982 1021.30 0.0000 1750.46 0.0000 777.92 196.9841 1025.87 0.0000 1764.49 8.5107 778.90 225.0560 1028.54 0.0000 1770.23 10.6506 783.70 234.1209 1037.84 250. 6996 1771. 35 10.6531 785.37 214.8465 1038.76 0.0000 1791.20 0.0000 792.07 216.5039 1046.59 245.1892 1808.65 10.7330 794.95 231. 9291 1048.07 245.3071 1810. 72 0.0000 795.86 258.0270 1049.04 240.0403 1836.06 16.1874 801. 95 241.2588 1050.41 262.3743 810.06 242.0266 1063.66 264.3657 810.29 238.7827 1077.00 261.8804 810.45 238.7916 1077.34 248.4445 810.76 234.4651 1085.87 255.3989 815.77 242.5686 1093.63 250.9576 818.51 254.8627 1099.45 228.2822 832.01 257.2800 1112. 07 268.3223 834.85 243.2565 1112. 84 261.1230 835.71 229.0235 1115. 54 229.5746 836.80 0.0000 1120.29 170.1070 846.75 0.0000 1120. 55 168.6645 846.77 262.0443 1121.30 155.6202 856.80 278.0157 1129. 67 168.5822 860.56 281.7423 1131.51 0.0000 871.09 304.5923 1147.95 0. 0000. 873.19 261. 2791 1173.23 133. 9542 875.33 0.0000 1177.95 113. 8532 879.38 305.5254 1189.05 89.9310 880.51 267.5816 1204.77 95.9150 883.24 283.5338 1221.41 72.9727 884.68 293.7799 1231. 02 38.4600 889.28 281. 9154 1235.36 52.5957 894.76 286.9684 1238.28 40.4175 898.04 322.2388 1260.41 0.0000 900.72 303.3802 1271.87 34.9065 903.28 300.2674 1274.44 4*1. 7 656 911.20 351. 4856 1274.54 41.7656 912.08 331.2167 1291.59 41.0027 923.98 0.0000 1298.22 0.0000 926.50 336.8903 1312 .11 41. 2258 929 .11 331.4956 1332.49 44.3351 937.49 367.8840 1362.66 0.0000 944.13 353.1491 1365.19 24.2981 946.00 324.8438 1368. 63 0.0000 949.00 367.0443 1384.29 22.4609 954.55 0.0000 1408.01 20.4331 962. 31 368. 7239 1457.56 0.0000 964.08 334.3567 1460.82 18.9061 966 .17 288.4420 1489.16 16.0273 968.97 309.4933 1505.03 16.0869 983.53 288.9600 1584.12 8.1899 984.45 0.0000 1596.21 13.3444 996.26 268.0432 1620.50 19.6077 1001.03 281. 0121 1621.92 15.4852 Page 453 of 614 Continuing Calibration . Data Page 454of614

_ C> cJ ouq--Review of Gamma Spectrometer QA results (Daily calibration & background checks) 3-0CT-2016 09:29:18.00 Run Date Detector Parameter Flag 3-0CT-2016 GAMOl Cal Check NLACTVTY-662 Investigate 0 K 3-0CT-2016 GAM02 Cal Check PSFWHM-59 Investigate. 6(l 5-JUL-2016 GAM03 Cal Check may not have run since 3-0CT-20161v-18-SEP-2016 GAM03 Bkg Check may not have run since 3-0CT-2016 3-0CT-2016 GAM05 Cal Check NLACTVTY-662 3-0CT-2016 GAM05 Cal Check PSFWHM-59 3-0CT-2016 GAM06 Cal Check NLACTVTY-662 3-0CT-2016 GAM06 Cal Check NLACTVTY-1332 3-0CT-2016 GAM07 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 GAMOB Cal Check NLACTVTY-662 3-0CT-2016 GAM09 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 GAMlO . Cal Check NLACTVTY-662 3-0CT-2016 GAMll All Parameters Passed Weekly Background check completed on*3-0CT-2016 No daily Bkg Check necessary. 3-0CT-2016 GAM12 Cal Check PSFWHM-59 -----------GAM13 Cal Check may not have run 3 -lJUL -2 016 GAM13

  • Bkg Check may not have run 3-0CT-2016 GAM14 Cal Check PSFWHM-59 3-0CT-2016 GAM16 Cal Check NLACTVTY-1332 10-AUG-2016 GAM17 Cal Check may not have run 3-0CT-2016 GAM18 Cal Check PSFWHM-1332 3-0CT-2016 GAM18 Cal Check PSFWHM-59 3-0CT-2016 GAM19 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 GAM20 All Parameters Passed Page 455of614 Weekly Background check completed on 3-QCT-2016 . No daily. Bkg Check necessary. Investigate o/('._ Action () c..l 6' VV' l CJ \2 InvestigateOl( Investigate Investigate Investigate 01(_ Investigate ClfL since since 3-0CT-2016 Action ....._<::! f'Q. 'cl( InvestigateOlL since Investigate cl(, Investigate* CJ/(

GAM21 Cal Check may hot have run 25-SEP-2016 GAM21 Bkg Check may not have run 8-JUL-2016 GAM22 Cal Check may not have run 7-AUG-2016 GAM22 Bkg Check may not have run 3-0CT-2016 GAM24 . All Parameters Passed Weekly Background check completed on 3-0CT-2016 No daily Bkg Check necessary. 3-0CT-2016 GAM25 Cal Check PSFWHM-662 3-0CT-2016 GAM26 All Parameters Passed 3-0CT-2016 GAM27 Cal Check PSFWHM-662 3-0CT-2016 GAM28 All Parameters Passed Weekly Background check completed on 3-0CT-2016 No ¢aily Bkg Check necessary. 3-0CT-2016 GAM29 Cal Check NLACTVTY-1332 3-0CT-2016 Cal Check *NLACTVTY-59 3-0CT-2016 GAM31 Cal Check PSFWHM-662 3-0CT-2016 GAM32 All Parameters Passed Weekly Background check_ completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 GAM33 Cal Check PSFWHM-662 3-0CT-2016 GAM36 Cal Check PSFWHM-662 3-0CT-2016 GAM39 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. since 3-0CT-2016 since 3-0CT-2016 since 3 -OCT-2 0 i6;1J-since 3-0CT-2016 . ? 6 l C>(( Action P Investigate ol( Investigate Investigate bl( Investigate e.tt( Investigate Cl( Investigate 6'f( 26-JUN-2016 GAM40 GAM40 Cal Check may not have run since Bkg Check may not have run since 3-0CT-2016 GAM41 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. ' 3-0CT-2016 GAM43 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 GAM44 All Parameters Passed Weekly Background check completed on 3-0CT-2016 *No daily Bkg Check necessary. 3-0CT-2016 WELL Cal Check PSFWHM-1332 3-0CT-2016 XRAYl All Parameters Passed Page 456of614 Weekly Background check completed on 3-0CT-2016 . *No daily Bkg Check necessary. Investigate cµc.

3-0CT-2016 XRAY2 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 XRAY3 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 XRAY4 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg*check necessary. 3-0CT-2016 XRAY5 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 XRAY6 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. APPROVAL DATE:. LD l '1 \ \..6 APPROVAL TIME : l z ' \ l APPROVED BY: f2_ PROCEDURE # GL-RAD-I-001 Report completed at 3-0CT-2016 09:33:35.49 Page 457of614 Page 458of614 Background and Efficiency Data QA filenafYle ParafYleter NafYle 5tart/End Dates Lower/Upper LMts: DKA100: [CANBERRA.GAMMA.SCU5R.QA]QCC_GAM01_500MLMB.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 4-APR-2016 06:13:18 through 1-0CT-2016 12:00:00 57.5400 through 61.5400 61 *, .......... " ............. * ............ " .... *.* ...... * ............. * ............ . :::.::: a: w 0.. . . . . 60 ............................................................................ . . . . . 59 58 ........... *' ............ *' ........... * .............. *'* ........... *' ............ . 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA:scU5R.QA]QCC_GAM01_500MLMB*,QAF;1 P5FWHM-59 (PEAK FWHM AM-241) . 4-APR-2016 06:13:18 through 1-0CT-2016 12: 00:00 1.02147 +-5.951646E-02 (5.83 %) ., .. ..-.::t N I :E <J: :E I 3 LL <J: UJ CL 1.1 1 . x . . . x . . : x : x: xx : x : -* ........................................ *X ................................ . . . . x xx . . X *X X *. X X *.x x x x xx x x . x x x x x -x x >x x x . xX x . x xx: xx x

  • x x ;_ x:::X x x x x x>'X x x . : x -x . xx 0 ',( ',( . ',( v x . ' , x x x: *X I ** 9 -* * * * * * * * * * * *, * * * * * * * * * * * * *, * * * * * * * * * * * * *' * * * * * * * * * * * *, * * * * * * * * * * *
  • 01 0 *
  • 0
  • 0
  • 0 * *
  • 0
  • x '8 -_. ........... ; ............. ; ............ ; ............. ; ............. ; ............ . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe ACT INV MEAN INV ACT QA filenarrre Pararrreter Narrre. Start/End Dates Mean +-Std Dev DKA100: NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06:13:18 through 1-0CT-2016 12:00:00 63306.3 +-2800. 78 (4.42 %) H f-(j a: 0 llJ f-(j llJ 0:: 0:: 0 (j >-<r: (j llJ 0 70000 65000 60000 0 o ' I ' . . . x . . ..... . . . . . . . . . . . . . . . . . . . . . . . . . *. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . *. .. . . . . . . . . . . . . v x x x x x x x x x x X xx x . x. x x x x . x: *x x Xx >(..' X .;(-X % X X X x x >C: xx . xx x 0 x : 0 * * * * * -* *X ... ,),(, ... *>!-..... -"'. x* .. *X* ..... * .......... x* .*. *X* ........ : ............ . ,
  • A *A ' '
  • X X XX X . X v x 2< : x x x: x ><>< : xx v X XX *X X X x .xx .: *x x xx X. x xx *x . : x : . : . x x x -f : x . . . * . x . ........ ' ....... *'*.* ......................................... x* ....... 'x' ........... . x x x x x x x x. . . . . . . 5 5 0 0 0 * * * * * * * * * * * . I * * * * * * * * * * * * .I * * * * * * * * * * *
  • I. * * * * * * * * * ; *
  • I * * * * * * * * * * * * .I * * * * * * * * * * * *
  • 4-16 5..:.16 6-16 7-16 .8-16 9-16 Measurerrrent Date/Tirrre ACT INV MEAN INV ACT QA filenarrie Pararrieter Narrie 5tart/End Dates Mean +-5td Dev DKA100: [CANBERRA.GAMMA.5CU5R.QA]LBC_GAM01.QAF;1 BACKRATE (5pectrurri Background Rate) 3-APR-201612:17:38 through 1-0CT-2016 12: 00:00 1.44447 +-2.145394E-02 (1.49 3) 1.5 -* O I o O O I o o o
  • o0 o o o o o o o o O I o o 11 o o o o o o ' o o O O I 1o o o o o o I o o O I I o0o o o o o o o I I 0 o o ',' o o o I o o o o
  • I I I 1J c :J 0 D.O .Y. 0 itj co E :J .J.Jo 0 Q) 0.. (f) x x x x: x x x* 1. 45 ..... * * * * * * * * * * *: * * * *
  • x * * * * * * *: * * *
  • x: * * * * * * * :* * * * * * * * * * * * *:* * * * * * * *x * * * *: * * * * * * *x * * * .-* 0 x x x x x x x :x x x *x x x x 1. 4 I'-* ............................................................................... . I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Oate/Tirrie ACT INV MEAN INV ACT QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM05_CAN.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 4-APR-2016 06:24:06 through 1-0CT-2016 12: 00:00 57.5400 through 61.5400 61 o ' e o o ' o o o o ' ,' o o o ' o o o o ' 0 I o o' o o 0 ' o o 0 o o o o o ', o o o o I o o o o o o ,', o I o o o o o o o o o ,' o o o o o I o o o o o o 0 .-I ""'" N I E a: C!:r 0:: LlJ z LlJ :::.::: a: LlJ 0.. I o o o I 60 ........... * ............. * .............. * ........... *.* ........... * ............. . 59 ........... '* ................................................................... . 58 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM05_CAN.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:24:06 through 1-0CT-2016 12:00: 00 0. 931135 +-5. 131084E-02 (5.51 %) ...... """ N I E <:r: E LL <:r: UJ CL 1.1 1 . 9 . . . . . -* o o o o o o o o o 0 0 0 o 0 0 o o o o o o o o o o o o o o o o 0 o o o ' o o o o o o o o o o o o 0 o o o o o o o o o o o o I I o o o o ' o o o o o I o . . . . . x x -* ........... * ............. * ............ * .............. *-........... : ............ . x x. x . . . . . x 'A A *x ><S<><x x x x -* ..... *x ... -:* ... * .. *x.* ... *: ....... x" .. *:-.. "x' .... 'x -:* ........... -: ............ . XX X . X . . . X . x x x x x x x x x x x< x x x x ; xx x ::<<x XY:' x . x-x . xx x x x x " )!K . " v X A Yi( " . :X. X X )t x _ x x *x xx x :x . . . . . x x . 8 -* .......... *: ............ *: ............ :* ... x* *0x* )( *:* x' ..... ...... *.z.* : : : ><xx : v x XX: S& 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie ACT INV MEAN INV ACT QA filenafY'le ParafY'leter NafY'le Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM05_CAN.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06:24:06 through 1-0CT-2016 12: 00:00 63104.2 +-525.196 (0.83"%) *X x x x x
  • x :x x x x x x >x :% x x x x x . x x x xx x v x x* x x x x x ,/ x x x --H 64000 f-u a: D LLJ f-u LLJ x. x ;x. ;<.. " x . -* ........ *%** ......... *XX .. * ........... x** ............ * ... *X ...... X. : ............ . x . . . . . . Xx . XX X X. X . X . X . X XX xx x . . . . x .x x xx x xx X -f'X X XX X .. X X X -1 X >5< . X X X :% X X ....,, x """' et:: et:: x 0 u )-<C u LLJ D x x. x x x x x x x x x x xx x 62000 ,_. * * * * * * * * * * *** * * * * * * * * * * * *. * *' .* *' * * * * , .* * * * * * *** * * *' *** *. '* * * * * * * * *. . x . . x ' ' x ' ' ' ' ' :% x x x x x x r r r r r .. 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le ACT INV MEAN INV ACT QA filenarrie Pararrieter Narrie 5tart/End Dates Mean +-5td Dev DKA100: BACKRATE (5pectrurri Background Rate) 3-APR-201612:18:01 through 1-0CT-2016 12:00:00 1.53310 2.296009E-02 (1.50 %) 1. 6 -* ................. r... .......................... * ....*.. *,* ........... '* ............ . LJ c :J o I-'OJ) .Y. u nj co E :J I-..:0 u ID n. (,f) 1.55 1.5 x x . X* . . . ............... *'* ........... *'* ...................................... *' ........ x ... . x x x x x x x x* x *X x x x x x x x x . . . . : x f-.* *****************************************************************.********* . . x . . . x x I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe ACT INV MEAN INV ACT QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA10 0: [CANS ERRA. GAMM.A. 5CUSR. QA] QCC_GAM06_500MLMB. QAF; 1 PSENERGY-59 (PEAK ENERGY AM-241) 4-APR-201606:13:24 through 1-0CT-2016 12:00:00 57.5000 through 61.5000 61 ........................................ * ........... *.* ........... * ............. . .,..j ¢ N I a: et:: LLJ z LLJ :::.:: a: LLJ o.: 59 . . . . . ............................................................................ . . . . . . 58 ............................................................................ . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenafYle ParafYle ter NafYle Start/End Dates Mean +-Std Dev x x. DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM06_500MLMB.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:13:24 through *1-0CT-2016 12:00: 00 0.936438 +-4. 666342E-02 (4.88 %) x x x x *x x ' x x . . x . x* x x . x 1 """' 'Of" N I E a: E I 3 LL* :::..:: a: LLl . 9 O...* ......... <* .......... }/:-.. ...... *> ........... -:* .:>< .... -: ..... )( *:* .. . x x *x x x xxx x x x *x x x 0 x x xx x x. X* x xx x x x x x x x x :x x X X X v: X xX X. X X X X X xX x x x '}<. A )<.. . x x x . . xx *xx x x. x .xx: x. x x. x x* x x x< Xx:* x x x-x x x x x ... ><x ..... x*: .. *x. . *:x ...... x .... :* ........... *:* ............ *: ............ . x . x . . x . x . x MeasureMent Date/ TifY'le ACT INV MEAN INV ACT QA filenairre Pararrre ter Narrre Start/End Dates Mean +-Std Dev x DKA100: NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-201606:13:24 through 1-0CT-2016 12:00:00 62995.7 +-1389.67 (2.21 %) ACT 6 6 0 0 0 .... . . . . . . . . . . . . : . . . . . . . . . . . . *: x. . . . . . . . . . . : . . . . . . . . . . . . . : . . . . .. . . . . . . . . *: . . . . . . . . . . . . . x x INV H Ll a:. 0 I.LI Ll I.LI 0 Ll a: Ll I.LI 0 x xx x 64000 62000 x x x x x xx *x x x x x . xx . . . . x 'X x -* * * * * * * * * * * * * * * *x * * * * * *: * * >:: * * * * * * * * * > * *X * ,><; * * * * * < * *
  • l:<* * * * *
  • x* *: * * * * * * * * * * *xX* : x . x x . x x x xx x \c: x x . f x x x x x x x xxx x MEAN ;<.. A . X X ,X," x* x x
  • x x * * :x x x x ><x x x x xx xx xx x
  • x** *Xx x *xx x * ..... x ....... : *x ....... x .. ..... :::< ... ;:.<.>< : .... ;:.:l! ....... : ............. : .. *x. : ...... . xx . x. x x :x x x. x xx x x x x x: x Xx x X* x x INV 60000 -* I o o o o o o o o o o' o o o ' o o o o o o o o o' o o o o o o ' o o o o o ', o o o o o o 0 o o o o o'o o o o o o o o o o o o ,' 0 o o ' ' I o ' ' 0 ' I o x : x ACT 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre QA filenarrie Pararrieter Narrie Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]*LBC_GAM06.QAF;1 BACKRATE (Spectrurri Background Rate) 3-APR-2016 12:.18:07 through 1-0CT-2016 12:00: 00 1.24317 +-1.196i23E-02 (0.96*3) 1.26 -* ........... * ............. * ............ * .............. * ............. * ............ . . . . . . x 1J !: :J x x 0 l-. "0.0 X* .Y. (J i1j co x x x E 1.24 :J l-(J (I) f..X ........... : .........*... : .... ::>< *.****. : *****.****.** : **.***** * ****. : .****.******* . x. . . . x x x x x x: 0.. 01 *x x x *x *x . . . x . . . . INV MEAN 1. 22 -* .......... *: ............. *: ............ :* ........... *:* ........... *:. . . . . . . . . . . . . INV x x r r I I 4-16 5-16 9-16 6-16 7-16 8-16 ACT Measurerrient Date/Tirrie 0 ......., 0\ ...... QA filenal'te Paral'teter Narrie Start/End Oates Lower/Upper Lrrits: DKAiOO: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM07_JAR.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 1-SEP-2016 13:47:02 through 1-0CT-2016 12:00: 00 5715000 through 61.5000 61 ................ " ............ * ....................... * ................... * ..... . :::.::: a: w 0... 60 x x x :x x x x x x :x x x x *x x X X X *X X 59 . . -. . ............................................................................ 0 I o o . . . . 58 ............................................................................ . . . . 9-01 9-08 9-15 9-22 9-29 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrie ter Narrie Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM07_JAR.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 1-SEP-2016 13: 47:02 through 1-0CT-2016 12:00:00 1.03858 +-2.533066E-02 (2.44 %) x x 1.1 1--* **************** * ***************** * ****************** * ***************** * ******* "<-I -=:!" N I 2: <I: 2: I 3 LL <I: UJ 0.. x x x x x x x x . 1.05 . . x . . 1--* *************** * ..................................... * ******************* * ****** xx x. x x :x -x *x :x x *x x 1 .................................. , ..... * ..................................... . x x I I I I 9-01 9-08 9-15 9-22 9-29 Measurerrient Date/Tirrie ACT INV MEAN INV ACT QA filenar.-.e Parar.-.eter Nar.-.e st*art/ End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM07_JAR.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 1-SEP-2016 13:47:02 through 1-0CT-2016 12: 00*: 00 57291.8 +-1611.56 (2.81 3) H 1-u([ D LL.I I-. u LL.I i:::t:: i:::t:: o. u ([ u LL.I D 62000 ,... ................................... ' ........... ; .............................. . x 60000 -* ................ : ................. : .................. : ............... x.: ...... . *x x x x x x . . . x . . 58000 -£ * * * * * * * * * * * * * * *. *
  • x * * * * * * * * * * * * * .. * * * * ** * * * * * * * * * *x* *. * * * * * * * * * * * * * * * * * *x* * * * *
  • xx x x x *x 56000 ,... .. : ............. *, ............. x ..................... * ................... * ..... . x x . . x . . 'X x 54000 -* ...... :)( ....... *: ................. :* ................ *: ................. :* ..... . I I I I 9-01 9-08 9-15 9-22 9-29 MeasureMent Date/Tir.-.e ACT INV MEAN INV ACT QA filenaMe ParaMeter NaMe Start/End Dates Mean +-Std Dev : DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM07,QAF;1 : BACKRATE (SpectruM Background Rate) 3-SEP-2016 10:23:03 through 1-0CT-2016 12:00: 00 : 1.33664 +-2.151268E-02 (1.61 %) 1. 4 -* * * * * * * * * * * * * * * * * * .* * * * * * * * * * * .... * * * " ....... * * ......... : ................. .,. . ACT Ll c ::J 0 '0.0 .::L u i'(i co E ::J .µ u Q) 0. 01 INV 1. 35 r--* ***************** * ******************* * ****************** * ******************* * ** x MEAN x x X* 1. 3 -* .................. * .................. * .. * ................ * ..................... *.* . INV I I I I 10-01 ACT 9-03. 9-24 9-10 9-17 MeasureMent Date/TiMe QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [CANBERRA.GAMMA.SCU5R.QA]QCC_GAM08_JAR.QAF;1 P5ENERGY-59 (PEAK ENERGY AM-241) 4-APR-2016 06:13: 29 through 1-0CT-2016 12:00: 00 57.5000 through 61.5000 T"f tj' N I :E a: (!) 0::: LlJ z LlJ ::...: a: LlJ CL 61 ........... " ............ * .... * .......... * ........... *.* ........... " ............ . 60 . . . . .. x x >.< %>J'S<:xx xx * '%.x't }1Cv * :X, x .X% x x x . 0 x *A/!'.:-xx .x " ;<.)<'..)(
  • x . x . X . x
  • x . . . . . x xx . x . . . x . x 59 ............ -: ............ *: ............ :-........... -:* ........... -: ....... *x. *x . . . . . 58 ............................................................................ . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Mean .+-std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM08_JAR.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:13:29 through 1-0CT-2016 12:00:00 f, 07206 +-3.912322E-02 (3.65 %) x. x x x , x Xx x .,... """ 1.1 N I ::E a: ::E x xx x . x *x x: x: :::i x x x* xx x X. x . x x x X X: >1< X : X X : _ : X . X : X X _ X X. X
  • X * * * . Xx -* . . . . *. x* . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ">< ... xx . x . x x x : x x ' . x x X X Xx x x . x x x x xx x x ..., x ..., v ' I 3 LL Xx* A x x x x x x:X x x a: UJ 0.. x x xx X* X>Z x x x x Xx x'.\ x x x x x . *X x xx x x xx :x -x ><< x x x x x x x x x x 1 -* * * * * * * * * * * *:* * * * * * * * * * * * *: * * * * * *: * * * * *:* ********xx**:*.************:************* x x ,* I I I I ,, 4-16 5-16 6-16 7-16 8-16. 9-16. Measurerrient Date/Tirrie J ACT INV MEAN INV. ACT QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Mean +-Std Dev H (j a: D LLJ u LLJ Ct'. Ct'. 0 u a: u LLJ D 65000 60000 x 55000 4-16 x x x >)< x x x x DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM08_JAR,QAF:1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) . 4-APR-2016 06:13:29 through 1-0CT-2016 12l00:00 -5 919 9. 1 +-2 0 9 2' 11 ( 3. 5 3 % ) x x x x x xx x x x x " x x *x :x :i<. x. xx* )§( x x x >>< x x. x x x '** x x x x xx *x x x X>< x x *X x x x :x . x *X x x x x x 0 x V* v x I I I I I 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e x v x x x x x* x x x x x ACT INV MEAN INV ACT QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM08:QAF;1 BACKRATE (SpectruM Background Rate) 3-APR-2016 12: 18: 12 through 1_-0CT-2016 12: 00 :. 00 1.43104 +-1.778290E-02 %) . . . . . 1J c 1.45 -* ........... * ........ x .... * ............ * ............. * ............. * ..... *: ...... . . :::; 0 1-"0.0 ::i. 0 l1j cc E :::; I-"""' 0 I]) a. 01 x x: x x x x x x x .x *x x x. x x x x x x x *X x x x 1. 4 -* ' o o o ' ' 0 o 0 I ,o o o o 0 o* o o o 0 I I 0 *'.* I I o 0 o I I 0 o o I '1 o o 0 o I 0 o o o I o o'O *, 0 I 0 o o o I o o 0 ,o I o o o 0 I 0 0 0 o ' I o I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Oate/Tir.-.e ACT INV MEAN INV ACT QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM09_500MLMB.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 4-APR-2016 06:24:11 through 1-0CT-2016 12:00:00 57.5000 through 61.5000 61 ......................... * .............. * ........... *.* ........... * ............. . .,-l tj" N I a: (.!) 0::: I.LI z I.LI ::..! a: I.LI CL 60 59 . . . ... . . ............................................................................ . . . . . . . . . . 58 ............................................................................ . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe ParaMe ter NaMe 5tart/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCU5R.QA]QCC_GAM09_500MLMB.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06: 24:11 through 1-0CT-2016 12:00:*00 0. 843482 +-5. 677858E-02 (6. 73 %) .., -=:!" N I 2: a: 2: I 3 LL a: LLJ Q. x 1 ,.... * * * * * * * * * * *:* * * * * * * * * * * * *: * * * * * * * * * * * *:* * * * * * * * * * * * *:* * * * *
  • x* * * * * *: * * * * * * * * * * * * * .9 .8 x x x x x v x x x x . . x ............... *:* ........... *: ........... *:** .......... x*:* ........... *: ..... '/ ..... . . *
  • X x* x
  • x x x .X x x x x . x x . x x x x x x x . x . ' x x: " . . )( X :x X 0 X : )Ip< X X--./ >§< X X X X Xx X : X X X *
  • x0 J<*x x *x x x -.... 0. x : \* ... ; . x *>j,* .x#7 .. x . x .. "\ >1<: :-:;. _x .... x,'\*x p xx" .x ... x x x x x x xx:xxx X* * . X . M .XX xx. x* x x x x x x xx x x I *7 '"""' '*
  • o o 1 ' o o o ' 11 o o o 1 ' o o o o 1 ' o "1 1 1 o o o 1 1 o ' o 1 11 o o o ' o o o o o 1 ' ooo o ' 1 o o o ' ' o o o "' o o o o 1 o o o o ' ' o ' ' ' '. ' 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe ACT INV MEAN INV ACT QA filenarrie
  • Pararrie ter Na.rrie Start/End Date8 Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM09_500MLMB.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06:24:11 through 1-0CT-2016 12:00:00 62249.4 +-1409.24 (2. 26 %) . x 70000 *********** .. *x***********.********.**** .. ************.************ .. ************* H u a: D w u w O:'. O:'. D u a: u w D 65000 60000 55000 x x x x xx x xx . x . . . . x x x x* :x x *x X. .......... x x x< x x. *x x x x x 2::x x x ::K x x %. x x x x: x x X< x. x x . x . x *X X X *X x . xx
  • x x M xx X-*xx
  • x xi< x x * * *Xx ::x X X X . X X *
  • X X
  • X X.' X . X XX . . . x . . x x xx x . x x ...................................... x ......................................... . 4-16 .5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie ACT INV MEAN INV ACT QA filenarrre Pararrreter NaMe Start/End Dates DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM09.QAF;1 BACKRRTE (Spectrurrr Background Rate) 3-APR-2016 12:18:18 through 1-0CT-2016 12:00:00 1 .. 26523 +-1.466291E-02 (1.16 %) -Mean +-Std Dev 1. 3 -* .......... * ............. * .............. * ........... *.* ........... * ........... * .. . x x x x x: . : x : x : : : . x 1. 28 ,__. * * * * * * * * * * *.* * * * * * * * * * * * *. * * * * * * * * * * * *.* * * * * * * * * * * * *.*
  • x* * * * * * * * * *. * * * * * * *x * * * *
  • x x x x . ?< *X x x. . x x v .. : x. 1.26 . x . x -* ................................................................... , ............ . x x 1. 24 ..... o o 0 o o 0 0 0 o I 'o ,' o o o o o o o 0 0 0 0 o, 0 0 I 0 o o o o o o o o ,o"o ,: 0 0 I o o o o I I o,o 0 0 I 0 o o I I o o o o, 0 0 0 0 0 I 0 o o o I o o I I I r I 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrren t Date IT irrre ACT INV MEAN INV ACT QA filenafYle ParafYle ter. NafYle 5tart/End Dates Lower/Upper LMts: DKA100: [CANBERRA.GAMMA.5CU5R;QA]QCC_GAM11_JAR.QAF;1 P5ENERGY-59 (PEAK ENERGY AM-241) 4-APR-2016 06:24:16 through 1-0CT-2016 12:00:00 57.5000 through 61. 5000 61 ........... * ............. * ............... * ........... *.* ........... * ............. . .., ""'" N I ::E a: 0::: LLJ z LLJ ::...::: a:* LLJ 0.. 60 59 . . . . . ............................................................................ . ' . . . . . . . 58 ........................................................................... -. . . . ' .* 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle UP LOW QA filenafYle ParafYleter NafYle Start/End Dates Mean +-Std Dev x x DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM11_JAR.QAF;1 PSFWHM-69 (PEAK FWHM AM-241) 4-APR-2016 06:24:16 through 1-0CT-2016 12:00:00 0.811280 +-2.896668E-02 (3.67 %) x x x x . 86 : x : x : : x x : -* .. x-. *x .................... *x* ............. *x. % .. *><:* ..... * .......... *X* ..... . x x >!'. . .-1 v N I. ::E a: :E I .3 LL. :::..::: a: UJ 0.. . 8 X_X x x x x )1( . x* x x x x Wx : x* : x'"' x x: ' x v x x . x x x . x . "X x x . x ............... *: ....... ... *: .... x ... *x* .... "x ..... *x* .. .. xx* ... x* . ......... * .. . xX . X. X . X X-XX X x x x . x *x . f-XX X X* X X X x* X X X XX . X x . x x x xx: x x 0 .x x xxx x xx.x xX x x x *XX . 76 -* .......... -: .......... -: ............ :-........... *:* ........... -: .... * ........ . x I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle ACT INV MEAN INV ACT QA filenarrie P.ararrie ter Narrie Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM11_JAR.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) : 4-APR-2016 06:24:16 _through 1-0CT-2016 12:00:0D 60054.4 +-1312.98 (2.19 %) 64000 x x x . x 62000 H 1--. (j a: D LL.I I-(j LL.I -* *g* ....... ........... :-.......... _-: ............ ?<* ...... >< .. .......... .. . x . . x . . x . . x . x . . x . x x x x x :x x *.x x . x x x x xx. x x . >><x x x x x x x x x
  • x x M "" x x ><x v x '.,,>}
  • v x* X et:: 60000 et:: 0 (j )-a: (j LL.I D 58000 ... r.: ..... X ........ *x ................................... *x .......... *x* x* ...... . : X XX : X X : X X Xx : X X X X .X X* XX X *
  • X X* X :x X x *
  • x* x x x x x x >><-><;: x :x x x x 0x x* x x . xx . x* x . x x .** . x . x ** . x -* * -* * ::< * * * *> X* X * *
  • X. * * * * *> * .. )< * * *. * * <* :X: ......... X.: ............ -: : .......... 'f(: x . x v *x x x 56000 -* ................................................................................. . I I I I u I 4-16 5-16 6-16 . 7-16 8-16 9-16 Measurerrient Oqte/Tirrie ACT INV MEAN INV ACT QA filenal'le Paral'Jeter Nal'le Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCU5R.QA]LBC_GAM11.QAF;1 BACKRATE (5pectrul'l Background Rate) 3-APR-2016 12:18:24 through 1-0CT-2016 12:00: 00 1.54973 +-1. 740346E-02 (1.12 3) 1.6 lo-o ' o 0 o 0 I o 0 o I o' o o o I o o 0 o ' o I o o' o I o o o ' o o o o o o 'o o ' o o I o I o o I o ,o, o o I o o o I 0 ' o o o' o o I o o o ' o o o o I o 1J c ::::;_ 0 '0.0 .Y. u llj co E ::::; u ID u en x x x x x x :x : x x x x x x x x: *X . . .......... * ............. * ............ * ......... V, .. * ............. * ....... * .... . 1.55 . . x . . . x x x .x x x 1. 5 1--o I o 1 o 1 1 o o o 1 *; 0 0 o o o o o o o o ' o *; o O o o o o ' 1 o o o O ;* o o o o o o o 0 0 1 1 *;* o 1 1 O o o o o o o o *;' o o o o 1 o o 0 0 o O o 4-16 5-16 6-16 7-16 8-16 9-16 Measurel'lent Date/Til'le ACT INV MEAN INV ACT QA filenarrie Pararrieter Narrie 5tart/ End oa*tes Lower/Upper Lrrits: ,* DKA100: [CANBERRA.GAMMA.5CU5R.QA]QCC_GAM18_CAN.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 4-APR-201606:13:40 through 1-0CT-2016 12:00:00 57.5000 through 61.5000 61 ........... * ............. * .............. * ........... *.* ........... * ............. . .-I tj" N I a: (!) et:: LLJ z LLJ ::..:: a: LLJ 0... 60 59 ........................... * ....................................... : ............ . . . . . . . . . 58 ............................................................................ . . . . . 4-16 5-16 6-16 .8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Mean +-Std oe*v DKA100: PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:13: 40 1-0CT-2016 12: 00:00 0. 960465 +-3. 090899E-02 (3. 22 %) x 1. 1 ........... * ............. * .............. * ........... *.* ........... * ...... ' ...... . o:-1 -.::!" N I E cJ: E I 3 LL :,.,,:: cJ: UJ CL x *x . . . . . 1 . *:X: ......... : ............. : ............ : .......... g, . : ............. : ............ . . ?< . x x x x . x XX K : )(. X X . X X 1x xX X : X x x.
  • NX . .9 x x . 8 ............ * ............. * ......................... * ............. * ............ . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe ACT INV MEAN INV ACT QA filenafY'le ParafY'Jeter NafY'le Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM18_CAN.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06:13:40 through 1-0CT-2016 12:00: 00 63719.3 +-1431.59 (2.25 %) H 1-u(( D LiJ 1-u LiJ 0:::. 0::: 0 u (( u LiJ D 66000 64000 62000 60000 x x x . . -. . x . x . -* ' o o o ' ' o o o ' o o ' ' o o o ' ' 0 o oO o o I ' o o o o o o o o oo o o o o o o o 0 o I 0 ooo o o o o o o o o o 0 o "0 o o o o o o o o o o o o x x x x x x . x x . X X 1< *. xX x x *X X X .x .x ....... x: ...... _x _x ... x. x_ ....... ... X".xxx x ... X .. ?<. ><* x_ .*.... x. *x .. .
  • X *
  • X *, X
  • vX '>:' A x* x x Xx x* x x x -; . x xx "x xx xxxx x xx :x x x:><xx xX x X XX X 0( X X .X
  • _ ...... .. xx ... x ..... : .. *>x* .... ........... x.:x.: ... *xX* ....... 0. x . x . . . . x
  • 9 x x x :x x x x xx x x x *v xx x* -* o o o o o o o o o o ,' o o o o o o o o o o o o *.' o o o o o o o o o o o o ', o o o o o o o o ', o o ,', o o 0 0 o o I 0 o o o ,' o o o o o o o o o o 0 0 o . . . . . x x I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe ACT INV MEAN INV ACT QA filenar....e ParaMeter Name Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM18.QAF;1 BACKRATE (Spectrum Background Rate) 3-APR-2016 12:18:51 through 12:00: oo 2. 12760 +-2.980382E-02 (1.40 %) x 2.2 I--* ************************ *' *************************************** *' ************* lJ c :J o 1-'QI) .::L. (.) l1j ID E. :J .µ (.) Q) 0.. ([) x x. x x 2.15 1-o* ************************************************************ ' ............ * .****** x x x x x x x x* x x x 2. 1 .x x . . . . . x x . . x . x . . ,_ .................................................................... x* .......... . x x 2. 05 -* .......... * ............. * .............. * ........... *,* ........... * ............. . I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Time ACT INV MEAN INV ACT QA filenaMe DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM19_CAN.QAF;1 ParaMeter NaMe PSENERGY-59 (PEAK ENERGY AM-241) Start/End Dates 4-APR-2016 06:54:25 through 1-0CT-2016 12: OO:OO Lower/Upper LMts: 57.5000 through 61.5000 ..-4 v N I E a: (!:I 0::: I.LI z I.LI )o.::; a: I.LI CL . 61 ........... * ............. * .............. * ........... *.* ........... " ............ . 60 . . '. . . 59 . . . . . ............................................................................ . . . . . . . . . . 58 ..................... "* ..................................................... . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM19_CAN.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:54:25 through 1-0CT-2016 12:00:00 1. 02481 +-2.522724E-02 (2.46 %) .,..j """" N I E a: :E I 3 LL a: UJ 0.. 1.1 1.05 x X* x x x *x x x x x x x % x . . x . . . 0 . . .. >Q< .vv . -* .................... x ............................ ..................... . : *X X : X X * : : X : x xx x ::w: x 9 x xx Xx x* x x x x xx x x ..,... ..,.... x xX , ... A X A xx: X X A X x* x* x x x. x x >-:: x x Q >x x x* x x x xx: x % xx x . x x x x x x x x * *x xx 1 ... ... .... x .. : ..... x ........ : .. x. . .. x .. x ..... R* .. .... x. -r-. .. ?< .... *x ... . x. xx* Xx ::i< x x x x
  • x x *x :x x: x x x "X xx . x . . . . . x x . 95 -* .......................................................................... . r r r r r 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie ACT INV MEAN INV ACT QA filenaMe ParaMeter NaMe Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM19_CAN.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06:54:25 through 1-0CT-2016 12:00: 00 70341.0 +-1743.47 (2.48 %) 75000 -* ............................................................................... . H u a: D Li.I u Li.I 0::: 0::: 0 u a: u Li.I D. 70000 xX Xx x x :xx x x x x x x x x x x x: x x x x: x x *x x x x x x x x x x x x x Xx x x: x x x x x x x x x X X X X xX Xx v x x x* x x x ..,,. x
  • x " : : .X. }( : X : X X A :x X -* * * * * * * * * * * "* ********xx* -.x * * * * * * * * * *x** * * * * * *x * *.** * * *x * * * * * "* * *x * * * *x * * *
  • x :>< . x ><x . x. x x: x x : xx : xx xx X x x x. x x x X X X xX . x x x x x x x x x x x x x I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe ACT INV MEAN INV ACT QA filenaMe ParaMe ter NaMe Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM19.QAF; 1 BACKRATE (SpectruM Background Rate) 3-APR-2016 12:18:56 through 1-0CT-2016 12: 00:00 1.95658 +-1. 990679E-02 (1.02 %) x 2 r-. . . . . . . . . . . . :-. . . . . . . . . . . -: . . . . . . . . . . . . :-. . . . . . . . . . . . :-. . . . . . . . . . . *:-. . . . . . . . . . . . lJ !: :J 0 1-'0.0 .::L. u l1j (Q E :J u Q) CL ({) x x: ' x x x x x x x x x x. x )( x x x . . :x . . 1.95 -* .......... ',',' .......... " ... * .... x* .. *.* ........... *.* .... x* .................... . x . . . . . x . . x x x . . . . -* ........... , ............. , .. '* ......... , ........................... , ............ . I I I I I 1.9 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe ACT INV MEAN INV ACT QA filenaMe DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM20_500MLMB.QAF;1 ParaMeter NaMe PSENERGY-59 (PEAK ENERGY AM-241) Start/End Dates 4-APR-2016 06:24:37 through 1-0CT-2016 12:00:00 Lower/Upper LMts: 57.500IT through 61.5000 ::..::: a: LL.I 0.. 5*1 . * .......... " ........ : ... " ............ " ........... *.* ........... " ............ . 60 . . . ' . 59 . . . . . ............................................................................ . . . . . . . 5.8 ............................................................................ . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaJTJe Pararrreter Narrre Start/End Dates Mean +-Std Dev :. DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM20_500MLMB.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:24:37 through 1-0CT-2016 12:00:00 1.06508 +-5.344863E-02 (5.02 %) 1.2 -* ; O o O I O O O O O o1 o O o I o o o o o I I o o0 o o o o o o I I o o o 0 ', 0 0 0 0°0 o 0 o 0 I I o0o o I o o o o o 0 o 0 o 11 I 0 0 '.' I 0 o 0 o I 0 o I I o 0 I x ...... 'I:!" 1.1 N I ::E. a: x x . x . . xx . 'X . . x x . :J-x. x . . . x x x< x xx xx 1< x. x.x .... :.::?:<. ?<x .. *x*. ::< ......... x .. ':< ..... >.¢!::: *.***.*** x* .x ..... .. :X: 0 . x x . x x. x x . x x x . x . x x . x -. x . x x x. .x ::E I 3 *. LL x ::..::: a: UJ CL 1 x . . x . . . x . . xx . xx . .... . . . . . . . . . . . :K .. .. .. ... W< .. ?<;>. .. x .... x-... *x* ... x .. :.: .. .. .. x-x* x< x . -;<. xx M x .x x x x -;(. . x S< >¢< . x x . x x x. x x 0 x fx* x x x x x ACT INV MEAN INV I I I I I 4-,_1_6 _____ 5 __ _._1_6 _____ 6 __ ...... 1_6 _____ 7 __ ..... 1_6 _____ 8 __ ...... 1_6 _____ 9 __ ..... 1-6 ______
  • ACT MeasureJTJent Date/Tirrre QA f i lenafY'le _ ParafY'le ter NafY'le Start/End Dates Mean +-Std Dev x x DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM20_500MLMB.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06:24:37 through 1-0CT-2016 12;00:00 62671. 1 +-1539. 86 (2. 46 3) x: x >>:: x x x xx : x x x .7X * * * *
  • x . 0x . xx. . . . H I-u a: D l.J.J I-u w O:'. O:'. 0 u )-a: u l.J.J D 65000 60000 -. >)\ . . . . . . >: . . . . . . . . . . . . . .: . . . . . . . . . ?<. . : . . . . . . . . . . . . . : . . . . . . . . . . . . .: . . . : . . . . . . . . . x x x x x x *x x x -x:. xx x x xx x xx xx xx x x x x:x A x x x x x x x x x x M x x: .;(-x x x x x x x . x x xx x nx x x x x x :xx x xx: x x x x x x :x x x x x x x 0-x x x x x x x x . . ::< . x . . -* ... -. -----.. ---.. ----* .. --. ------.. ---;x:----_-. ----. --. --. x ---.. ---... ---.. -----. -x ,, x x: I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le ACT INV MEAN INV ACT QA filenafYle ParafYleter NafYle Start/End Oates Mean +-Std Dev : DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM20.QAF;1 : BACKRATE (SpectrufYl Background Rate) 3-APR-2016 12:19:02 through 1-0CT-2016 12:00:00 1.40579 +-1. 881187E-02 (1.34 %) 1.45 1--* **********************.********************************************************** LI c :J 0 '0.0 .Y. u l1j ca E :J u I]) 0.. (!) x x x* x x x x x x x x x* :x x x . . . . . x -* ........... * ............. * ... : ...... 0. * ............ x ............ : ............ . 1. 4 . . . . . :x x x x x x I I o o ' 1, 35 -* ........... I ............. I .. * . *. * * .... I ..... * * ...... I ........ * ..... I ..... * * * * ... . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TifYle ACT INV MEAN INV ACT QA filenarrie Pararrie ter Narrie 5tart/End Dates Lower/Upper Lrrits: DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM24_JAR.QAF;1 P5ENERGY-59 (PEAK ENERGY AM-241) 4-APR-2016 06:13:51 through 1-0CT-2016 12:bO:OO 57.5400 through 61.5400 . . . . . 61 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .,...i '=.!" N I ::i:: a: (!) et:: LLJ z LLJ 60 . . . . . ;:,..::: a: LLJ 59 ................................................................................ . 0.. 58 4-16-5-16 6-16 7-16 8-16 9-16 Measurerrient Oate/Tirrie UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM24_JAR.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:13:51 through 1-0CT-2016 12:00:00 1.04071 +-3. 445093E-02 (3.31 3) , ' 1.1 -* o o ' o ' o ' ' ' ' , o o ' ' o o o ' ' ' o : o ' ' o o o o o o o ' o ', 0 o o o o o o o o o o 0 o o ' I o o o o o o o o o : ' ' o 0 0 I o ' o 0 o o o ..-1 -=:!" N I E a: E I 3 LL ::..::: a: LU 0. x x x Xx x . . . . . x<.* xX x :xx x. x. x .x
  • x x x x x x xX >OX x x x x xx x x . x x . ?::: x x xx x x x x x x xx Xx XX X x x xx x x x x* xx: x x. x x xx V'
  • x x . . . . . x x x x* x x x x x x x x xx x x 1 .............................. x .. x* ................................................. . . . . . x . x x x x x x . . x x x x A x x 4-16 x ..,,..x x ., 5-16 x x x X.: x *V x x n X x x ' ' ' 6-16 7-16 8-16 Measurer.-.ent Date/Tir.-.e x x x ' 9-16 ACT INV MEAN INV ACT QA filenal'le Paral'Jeter Nal'le Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM24_JAR.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06:13:51 through 1-0CT-2016 12:.00:00 61710.4 +-1354. 76 (2.20 %) H I-u a: D UJ I-u UJ 0::: 0::: 0 u >-<C u UJ D 64000 62000 60000 x x x. x x . . . . . -* * * * *
  • X* * * * *.* * * * * * * * * * * * *. * * * * * * * * * * * *.* * * * * * * *.* * * * *.* * * * * * * * * * * * *. * * *X * * * * * * * *
  • X . X .
  • XX*
  • X x x: x x x X* X x Xx X: X x x x x X X X X
  • X X* X xx . x . . . x . x X xX . X >)< . . X X X . X X* X -* ........ x .: ... .... 0 ... : .... .;<-.... x* .: ............. : ..... .. *x*X* ......... >::x. . )( . v . x . v. . . )( x N' x "f( x . A x 'A' x x . A x x x: x x x ><x x . x . X* xx x x X Xx xx x x x x x x x . x x . x x xx x x x x x ... * * * * * * * * * * ... * * * * * * * * * * * .. * * * * * * * * * * * ... * *: * * * * * * * * *** * * * * * *x * * *
  • x * * * * * * *:x* * * * . x : x : x x x :xx . ->!-: x x x x )( A :x A x :x x x x 58000 -* ............................................... *.* .............................. . I I I I I 4-16 5-16 6-16 7-16 . 8-16 9-16 Measurel'lent Date/Til'le ACT INV MEAN INV ACT QA f i lenarrie -Pararrieter Narrie 5tart/End Dates Mean +-5td Dev DKA100: [CANBERRA.GAMMA.5CUSR.QA]LBC_GAM24.QAF;1 BACKRATE (Spectrurri Background Rate) 3-APR-201612:19:22 through 1-0CT-2016 12: 00:00 1.65570 +-2. 053930E-02 (1.24 %) x 1 7 -***********<**********.-*<************>************>**********>!'.:.: ............ . . x x x x x x x x x 1.65 -* ................................................................................ * ... . x : x x :x x x x x x . . . . 1. 6 1--* ********** * **** ' ******** * ************** * *********** *** *********** *, ************* I I I I I 47"'16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie ACT INV MEAN INV ACT QA filenarrre Pararrreter Narrre Start/End Dates Lower/Upper Lrrrts: DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM28_JAR.QAF;1 PSENERGY-59 ENERGY AM-241) 4-APR-2016 06:40:16 through 1-0CT-2016 12:00: 00 57.5400 through 61.5400 61 ............ * ............. * ............ * ............. * ............. * ............ . ;:,,,::: a: w 0.. . . . . . 60 ............................................................................. . . . . . 59 58 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW QA filenarrre Pararrreter Narrre Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM28_JAR.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06: 40:16 through 1-0CT-2016 12:00:00 1.13880 +-7. 316274E-02 (6.42 %) .,...i """ N I E a: E I 3 LL. a: UJ CL 1.3 1.2 1.1 -* ........... * ............. * ............ * .......................... : ............ . . . . . . . x *X : x X* :x . x. . x x: -* .** ><; ..***.. * ...... ................ " ........... " .... x ...................... . : * : . x : : : x x x x >>:< X X XX X* xX v x v x x )!!< ><y xx x v x x-.x v x " ">{ -? x x : xv >x x x x x '"': x x x : v, x : x x xx xx :xx x x . . 'X . X X 'X )IX X . X . X . .;(-. X . X . X X>,>c ... x * * "x* *x .x:/ * * * * * * * * * * *
  • x. x* * *x * * * :-* * * * .x * * * * *:0 * *x * * * * *:-* * * * * * * * * *x * '.(S'. x x x 0 x x: xx: x x >>x x X ")( *X X >(< X x :x x x. xx xx x x x x 0 x x* 1 . . . . . . . . . . -: . . . . . . . . . . . . -: . . . . . . . . . . . . :-. . . . . . . . . . . -: . . . . . . . . . . . . *:-. . . . . . . . . . . . 4-16'* 5-16 6-16 7-16 8-16 9-16
  • Measurerrrent Date/Tirrre ACT °INV MEAN INV ACT QA fiienar.-.e Parar.-.eter Nar.-.e Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM28_JAR.QAF;1
  • NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06: 40:16 through 1-0CT-2016 12:00: 00 63769.8 +-1297.66 (2.03 %) H u a: D LLJ u LLJ Ct:: Cl:'. 0 u a: u LLJ D x x x* 6 8 0 0 0 -. . . . . 0 . . . . . : . . . . . . x . . . . . .: . . . . . . . . . . . . : . . . . . . . . . . . . . : . . . . . . . . . . . . .: . . . . . . . . . . . . . x . x x :xx x :x xX x x x x x x x .v 66000 64000 ................ : . ?< 'x .. x* ... x* ........... : ........... * ... : ..... x .... ..... x ..... x X *x X X *X X . X X . X X x.. *X X x. X *x
  • x x xx x xx* x
  • x x* x x . x . x x . ,)( . x x . x . . x x x x x . . x x-xx x . . x. 'X x. x xx ........ Xx ...... .-...... *x . .. : .... *x .. x ... * .. x* .x ....... :x; ... x ....... : ............ . . . *v . . . . 62000 ..'II'.. x
  • A x:: x xxx x " . .)<. X 0 X Xx-?: % x x x x ; x x . X
  • Xxi x xx x x . x .
  • x
  • x
  • x *x
  • x x ................................................. *><:: .....*....... x* .................. . . x. . x x x x x -x x x x x 6 0 0 0 0 -. . . . . . . . . . . . : . . . . . . . . . . . . .: . . . . . . . . . . . . : . . x . . . . . . . . . . : . . . . . . . . . . . . .: . . . . . . . . . . . . . x I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tir.-.e ACT INV MEAN INV ACT QA filenarrie Pararrie ter Narrie Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM28.QAF;1 BACKRATE (Spectrurri Background Rate) 3-APR-2016 12:19:38 through 1-0CT-2016 12: 00:00 1. 50994 +-1.525503E-02 (1.01 %) x ACT 1. 54 -* . . . . . . . . . . .. . . . . . . . . . . . . .. . . . . . . . . . . . . .. . . . . . . . . . . . ... . . . . . . . . . . . .. . . . . . . . . . . . . . INV "O c ::::; 0 "OJ) .::t. (..) (lj Ill E ::::; (..) Q) Q. en x x x 1.52 -* ........................... 0 ................................................... . x x x x x* x x v x x x x x 1; 5 I-""' o *
  • o o ' o o o ' o' o o o I 0 o o 0 o o o o o' o o o o 0 0 o 0 0 o 0 I 0o o o o o I o o o o I I o0o o I I o I o o o 0 o 0 ,* o o o o o I o o o o I 0 o . . x . . x x x x 1.48 1--' ' *** ' ******.************ : **************************** -*********** : ************* r 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tirrie MEAN INV ACT QA filenaMe DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM29_CAN.QAF;1 ParaMeter NaMe PSENERGY-59 (PEAK ENERGY AM-241) Start/End Dates 4-APR-2016 06:13:57 through 1-0CT-2016 12: 00:00 Lower/Upper LMts: 57.5400 through 61.5400 "<"'i ""'" N I :E a: (!:! O:'. L1.J z L1.J 61 60 ............ * ............. * ............ * ............. * ............. * ............ r. . . . . . ............................................................................ . . . . . . . . . ::..::: a: L1.J 59 ........... " ................................................................... . 0... 58 ................... * ...... *' ............ '* ......................... " ............ . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe ParaMeter NaMe 5tart/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM29_CAN.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:13:57 through 1-0CT-2016 12:00:00 0. 992983 +-3.213267E-02 (3.24 %) ""' 'Cj" N I E a: E I 3 LL. a: UJ 0.. 1. o 5 -* ........... : .. * . * * * * * * * * .: * * * * * * * *
  • x * * :. * * * * * * * * * *xx:* * * * * * * * * * * * .: * * * *. * * * * * * * *
  • x 1 . 96 x x xXX *m x x x .X. X x>y x x x x ; x x x xx x x x x . . x . . . x x : x x 0x>O< x x x x xx: x XX f-* .><: ... x ..... : ....... 2. .. : ... ... *X. X ....... *>s .... xx0. . )( v ){ x v Q 0.-x x "' ..,,. A ,..._ 7',' x : . x x p;.. ;x_ x :x xx x ')<!. x x x x x X* :x x x x xx x x x x . x x x x x . x .x . . . x ........ >.< .. * ... *x*x ..... : .... *x* ..... * .... *x ....... * ...... ... : ...... ><;x .... . . . xx . . x x x x .x x )!!( x x )( . x I 9 r-* * * *
  • 0 * * * * * *; * *
  • 0 '
  • 0 0 0
  • 0 0 *; 0
  • 0 0 0 0 *
  • 0 0 0 0 ;* 0 0 0 0
  • 0 0 0 0 ' 0 0; 0 0 *
  • 0 0 0 0
  • 0 0 0, *; 0 0 0 0 0
  • 0 0 0 0 0
  • 0 4-16 6-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe ACT INV MEAN INV ACT QA filenafY'le ParafY'le ter NafY'le Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA,5CU5R.QA]QCC_GAM29_CAN.QAF;1 ** NLACTVTY-69 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06:13:67 through 1-0CT-2016 12:00:00 62841.9 +-1422.21 (2.26 %) 70000 -* I o o I o I I I I o 1
  • o I O I I o o I o o 1 o : o I I ,* o o 1 1 o 1 o O *I o o o o 1 I o o o 1 o o
  • o O ' o o o o o 1 o o o : o o o o o o O O o o o 1 o H ..... u a: D LI.I* ..... u LI.I et:: et:: 0 u <I u LI.I D 66000 60000 . . . . . x v x x v* A . . . x. x . x ,... ........... *:* .. ....... *:* .......... *:* ......... *x *:*x*x*. x* )<'X>.*;":* ...... *X* .. . x x x. 0 x< x X X . X X *X X X X x: X . x. x x x x x x x x x x x: X*X X XX x xx,, .x *X I "' x xx y x x :x :x I )(< x x x X Xx )(< x x xx , x x x x x )( x x )( x 0 >.;: X Xx: X X . x x x .x x
  • x I x x x x x x x x x I I xx x x x ,;:.xx x A x 4-16 6-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le ACT INV MEAN INV ACT QA filenarrre
  • Pararrre ter Narrre Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM29.QAF;1 BACKRATE (Spectrurrr Background Rate) 3-APR-2016 12:19:43 through 1-0CT-2016 12: 00:00 1. 93820 +-2. 105615E-02 (1.09 %) 2 -* * * ........ * ............................ * . . . . . . . . . . . ... . . . . . . . . . . . .. . . . . . . . . . . . . . ACT LI c :J 0 'OJ) .Y. u. tlj co E :J u I]) u (f) x x x x x* x x x *X 1.95 -* ........... :: . x ...... * ... : ............ : ............. : ............. : ............ . x X* x X* x x x x *X x x x x . . . . . 1. 9 -* .......... * ............. * .............. * ........... *.* ........... * ............. . x I I ; I I 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre INV MEAN INV ACT QA filenal'le Paral'te te-r *Name Start/End Dates Lower/Upper Ll'lts: DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM30_CAN.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 4-APR-201606:14:02 through 1-0CT-2016 12:00:00 57.5400 through 61.5400 61 ............ * ............. * ............ * ............. * ............. * ............ . . . . . . 60 ............................................................................ . . . . . . . . . . :::.!: a: LlJ 59 ......................... '* ............ *' ....................................... . 0. 58 4-16 5-16 6-.16 7-16 8-16 9-16 Measurel'lent Date/Til'le UP LOW QA filenaMe ParaMeter Narrie Start/ End Da-tes Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM3D_CAN.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-201606:14:02 through 1-0CT-2016 12:00:00 0.965876 +-1.796214E-02 (1.86 3) ..-! ..,. N I lE a: E: I 3 LL a: LU a.. x A, x x x x x* x x x x x x x v ' . 1 ,.. ........... * ............. * .. *X ....... '.' ... * ........... *.* ........... ............ . x x x x x x x x Xx x x x :x x . x *X x x *X x x x--. x x x x x x -X X . X X XX x-x x xx x x x x x Xx x x xx x X *X xX X XX X *0L x x v x " . x ..; x v x .x. ..... , x x: . ......_ x.x. x v .x. -,....x r...xx r... x* '} x . x x . x x x: x x>< x x x x . xxx xx x . x >.::: x "X . 9-5 x X* *xx x*::>< * -* ,... *-......... .: .......... x . .: ............. :. ... ?< ......... : ... x x* .... : .... x ....... . x x x x " . I I '>( I I 4..:.16 5-16 6-16 7-16 8-16 9-16 MeasureMent_Date/TiMe ACT INV MEAN INV ACT QA filenarrie Pararrieter Narrie 5tart/End Dates Mean +..:.. 5td Dev DKA100: [CANBERRA.GAMMA.5CUSR.QA]QCC_GAM30_CAN.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06:14:02 through 1-0CT-2016 12:00:00 61266.4 +-1042. 70 (1.70 %) H 1-u([ 0 UJ 1-u w Ct: Ct: 0 u )-. ([ u UJ 0 64000 62000 60000 -* ........... * ............ : ............ * ................ ' ......... : ............ . . . . . . x x x x x x x x x ?:: x x x x x x X *
  • X.
  • X
  • XX X
  • x . x . . xx *. . ...... *x* ......... x .. x' .... ; .. **x ........... " .... 'x .... *;* .. *x ....... * ....... *x. *'.:-' .. x . x . x .xx x x x : x x x . X X X X X " . X 0 XX *" , . x x )<. n '7".. )<."
  • A -'¥
  • x
  • x x Xx ., ... X X. *.XX x . x. )( x . x x x .x x . x X X x*
  • X* X . x x . x . x . x x . x . x x x . . .:.i::-x . x x . x x X' . )>:." * >& ....... :ic*. *x* .. * ...... *:* .% ....... *X:* x.. X' ...... *:* ....... *.*. *0*. x-..
  • 1 * .. . . . . . x . x x xx. x x xx x x x x x v )( v x* x x 58000 -************:**********X*<************:*************:************<************* I I I I I , , 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie ACT INV MEAN INV ACT QA filenal'le Paral'Jeter Nal'le Start/End Dates Mean +-Std Dev x DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM30.QAF;1 BACKRATE (Spectrul'I Background Rate) 3-APR-2016 12:19:48 through 1-0CT-2016 12:00:00 1. 38100 +-1.713672E-02 (1.24 %) 1. 4 I"-* ******************************************************************************** "'1J c :J 0 . "0.0 ::L. u l1j CCI E :J .1-) u ID. 0. 01 x x x x x. x x x x x x* x x x x *x x X. x *X x 1.35 ................ : ............. : ............ : ............. : .... ...... : ............ . x I I I I I 4-16 . 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Til'le ACT INV MEAN INV ACT QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper LMts: DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM32_CAN.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 4-APR-2016 06:14l08 through 1-0CT-2016 12:00:00 57.5400 through 61. 5400 . . . . . 61 ** ................................................... ' ...................... . ..,-4. N I ::§:: <J: O:'. LLJ z LLJ U : : : : xx,/:' x :* 59 58 4-16 5-16 6-16 7-16 8-16 9-16 Mea:sureMent Date/Tirrie UP LOW QA filenafYle ParafY"Jeter NafYle Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM32_CAN.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:14:08 through 1-0CT-2016 12:00:00 1.09494 +-3.883722E-02 (3.55 %) ..-!. ""'" N I :E <I E I 3 LL ::..::: <,xx xx >xx x: x
  • x x -;<-x x . :x '5o< xx . : x x
  • x x x* x . x . x . x . :X . x x -;(-.*
  • X. . . X xX X * )):: X X
  • X *
  • R X Xx -* .......... " ............ " ... x ........ " .:,,..* ...................... ,*,. x ............ . x:i< x A x x:A x x: x x x xx.x x x x: x . >>'. x x x x xx x )¢( x ::i< x xX x x x x x x x *x 0 x x xx x x '}( u ,...., xx "'"x x -'.'-"' x x v x x x 1 -* * *
  • X *XK * * *:* * * ">< * * * * * * * *: * * * * * * * *
  • X. *:* X * * * * * * * * * *:* * * * * * * * * * * * *: * * * * * * * * * * * *
  • x x }( I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle ACT INV MEAN INV ACT QA filenal'le Paral'Jeter Nal'Je Start/End Dates Mean +-Std Dev DKA100: NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06:14:08 through 1-0CT-2016 12:00: 00 63906. 6 +-2634. 05 (4. i2 "%) . 70000 -* ........... * ............. * ............ * .............. * ............. * ............ . H I-u a: D LLJ I-u LLJ 0::: 0::: 0 u >-a: u w D 65000 60000 x x x . . x :x % x xx . x . ?< x x x 0 .................. *:X: ...*.. x* .................... ............................ :x; ..... . . Xx X . . ,Y X X . X x x: x -....-7-,: x x :x -....-X X A X X : xX xx x x x :>W< x ""' *. xx x *X xx *x AA . x x. x ::£ X Xx X X* ;'<:: ?: x :x x ;.(<: x *0<:x x x A x x xX x x v x x x x xX .X x : x x Xx x : x . x . x -* ... x. *x ......... *X* .... : ...... * ..................... : .......... x* . x** ........ x ... . . x :x x x . . . x x x x y x x x x I A I I x x *X I I x 4-16 5-16 6-16 7-16 8-16 9-16 Measurel'Jent Date/Til'Je ACT INV MEAN INV ACT QA filenaMe ParaMeter NaMe Start/End Date8 Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM32.QAF;1 BACKRATE (Spectrum Background Rate) 3-APR-2016 12:19:59 through 1-0CT-2016 12:00:00 1.40960 +-1. 667514E-02 (1.18 %) 1. 45 -* ........... * ............. * ............ * ............. * ............. * ............ . LJ c :J 0 '0.0 .::L. (.) itj Ill x x x x X* x x x x x x x :x x x x x x* X* x x . . x . . . x x E :J ...,;. (.) I]) u 01 1. 4 '-* * * * * *x * * * * *.* *. * * * * * * * * * * *. * * * * * * * * * * * *.* * * * * * * * * * * * *.*.* * *
  • X* * * * * * "* * * * * * * * * * * * * : ) : : : : x x I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 MeaBureMent Date/TiMe ACT INV MEAN INV ACT QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM36_CAN.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 9-JUN-2016 07:47:51 through 1-0CT-2016 12:00:00 57.5400 through 61.5400 61 . . . . . . . . ,* . . . . . . . . . -. . . . . . . . . *. . . . . . . . . .-. . . . . . ... * . . . . . . .. . . *. . . . . . . . . : . . . . . . . . .* . . . . . . . 60 ............................................................................. . . . . . . . . ::..:: a: w 59 ............................. , ........ ' ............................. ' ........... . CL 58 6-09 6-23 7-07 7-21 8-04 8-18 9-01 9-15 9-29 MeasureMent Date/TiMe UP LOW QA filenarrie Pararrieter NaMe Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM36_CAN.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 9-JUN-2016 07:47:51 through 1-0CT-2016 12:00: 00 0.844768 +-2.631886E-02 (3.12 %) """' v N I 2: Cl: 2: *I 3. LL x x I 9 -* * * * *
  • 0 * *' * * * *
  • 0 0 0 *"* *
  • 0
  • 0 0 0 0 .. 0 0 0 *
  • 0 0 0 ./' 0 0 0 0 0 ' 0 0 *' 0 *
  • 0 0 0 *
  • 0 '* 0
  • 0 0 0 0 * ' 1 0 0 0
  • 0 0 0 0 ,*' 0 . 85 < )( x: x K 0. x xx x >x x x x *X X*X X* x x x >< x. x x :x; x x K x x x . xx x . vx. )¢( . x. K *x . x x . . . . x . .... >:'. ......... : ...... ........ : ......... :. ..... : ......... : ......... : .. . . x . . . v . , . x . K X X x xx :x; xx ?O< x x X* 0 x :x X* X* x x x x .x x x )< x x* x x X* *x x x. :x; *x x :x x x x x .x I 8 _, 1 o o 0 1 1 ' 00' o ' o o o ' ' ',' o o ' ' o o o '.' o o o ' ' o ' o ',' o o o ' ' o o 0 ' 1 o o o ' ' o ,' o ' ' o o o o 1 : o o o ' o o ' o ',' ' I I I I I I I I 6-'09 6-23. 7-07 7-21 8-04 8-18 9-01 9-15 9-29 Measurerrient Date/Tirrie ACT INV MEAN INV ACT QA filenaMe ParaMeter NaMe Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM36_CAN.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 9-JUN-2016 07:47:51 through 1-0CT-2016 12: 00:00 60493.6 +-1102.76 (1.82 3) H' u a: D LLJ u w O:'. O:'. 0 u (J: u w D . . . . . . . . . 64000 -* ....... * ......... *.* ........ : ........ * ......... * ........... * ........ : ........ * .. . v x* x *x
  • x . . x . . . . . 6 2 o o o ,.... * * * * * * * *: * * * * * * * * -: * * * * * * * * * :* * * * * * *
  • x *: * * * :x* * * * -: * * * * * *
  • x * :-* * * * * * * * : * * * * * * * * *: *
  • 60000 58000 x x x x . xx x x < x x X X'X )Q( ( I". * ' ". x ?< x x x x x *x x '>(. :x X . X . Xx
  • X X *X -* .. Q .... ....... .... )(. : ........ ; ' . x ...... : .. ' .. ' ' ' . : .. ' ... ' ' : ... ' ..... : ' . X X X * *
  • X
  • X
  • X* X* x x x x < X* x: x :x N x x x ?< x .x xx x x x x x < x x x: x X-X x . . .x . xx . . . ,... ......... *.* ....... *.* .................. * ......... *.* ..... , .. *.* ....... *x ........ *.*. . . . . . x' . . x J I I I I I I I 6-09 6-'23 7-07 7-21 8-04 8-18 9-01 9-15 9-29 MeasureMent Date/TiMe ACT INV MEAN INV ACT QA filenaMe ParaMeter NaMe Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM36.QAF; 1 BACKRATE (SpectruM Background Rate) --12-MAY-2016 13: 49:58 through 1-0CT-2016 12:00:00 1. 01797 +-7.627347E-03 (0.75 %) 1J c J 0 "O.I) .:L (..) l1j co E J (..) Q) 0. ([) 1. 04 -* .......... ' ' ................. ,, ............................................... . x 1. 03 -* ............. * ............... * ............... *.* ............... * .............. . x x x x >> ,_ .............. x.* ..... ......................... * .. -............. * ............... . 1. 02 . . . x . x x x *X X x x x 1.01 lo-* o o o o I o 0 0 o o I o o oo o o o o o o I o I I o I o 0
  • o o o o o o o 0 o o o o o o ooo o I o o o o o o o o o I I o 00 o I I o o o o 0 0 0 o o ' I o *X x x . . . . 1 I-* ************* * *************** * .******************************* : ********.****** I I I I 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe ACT INV MEAN INV ACT QA filenat'Ie Parat'Ieter NaMe Start/End Dates Lower/Upper LMts: DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM39_CAN.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 28-JUL-2016 07:23:30 through 1-0CT-2016 12: 00: 00 57.5400 through 61.5400 61 ................. * ........ * ........ *. ,* ...... * ........ * ........ * ........ * ........ : .. . .,-! tj" N I ::E a: (!) et:: LL.I z LL.I . . . . . . . . 5*0 . * ...... * ........ * ........ * ........ * ......... *.* ........ * ........ * ....... : ....... : .. . xxxxxx x xxxx . xx ;<X X* ::..::: a: LL.I 59 ....... , .............................................................. , ....... , .. . 0.. 58 7-28 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 9-29 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM39_CAN.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 28-JUL-2016 07:23:30 through 1-0CT-2016 12: 00:00 1.15408 +-2. 882958E-02 (2.50 3) x 1 2 -. . x: . . . . . . . . . . . .: . . . . . . . . :. . . . . . . .: . . . . . . . . :. . . . . . . .: . . . . . . . . :. . . . ' . . . :. . . . . . : . . . . . -M ""'" N I ::E -0: ::E I 3 LL ::.::: 0: LU CL *X x x x: x* x .x x x x x x* x x x x x 1.15 f ...... ....... *:-.... ><' * ...... *:* .. * .... ....... ... ...... .. .. . . . . . . . x . . x . . x x x x x. xx x: x x x x x* x x x x x 1.1 . x . . . . -* ................ * ........ * ..... x .. * ........ * ........ * ........ * ..... * ... * ........ : .. . . . . . ' . *X x I I I I ; I I I I 7-28 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 9-29 Measurer.-.ent Date/Tir.-.e ACT INV MEAN INV ACT QA filenarrie Pararrie ter Narrie Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM39_CAN.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 28-JUL-2016 07:23:30 through 1-0CT-2016 12:00:00 63705.5 +-872.341 (1.37 %) H . I-(.j a: D LLJ I-(.j LLJ 0::: 0::: 0 (.j )-a: (.j LLJ D 6 6 0 0 0 -* ...... , ..................................................... * ........ ' ....... ' .. . 64000 62000 *x x X* x: K x K * * *
  • x * * * * *
  • X. X * * * * . X . . . x x . x . x . . . . . . ..... -x*: .x ... )<" *: .... :i< .. *: y ..... *: *x ..... *;x: .. )( .. X: .... *x .. xx* ..... :* ...... x: .. . . . x x . x . x . v . . x . . x x: x x: x x x x x. X* x x x X* x. x* x x x x x x . . . . . . . . . . -* .......................................................................... . I " I I I I I I I I 7-28 8-11 8-18 8-25 9-01 9-08 9-15 9-22 9-29 Measurerrient Date/Tirrie ACT INV MEAN INV ACT QA filenarrie Pararrieter NaMe *start/End Dates Mean +-Std Dev x DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM39.QAF;1 BACKRATE (SpectruM Rate) 26-JUL-2016 14:23:41 through 1-0CT-2016 12:00:00 1. 83408 +-1.817269E-02 (0.99 %) n c ::::; 0 1-"0il .::t. (J l1j a::i 1.85 -* ' * * * ' '.t' * * -' ' * * * *' * * * * * ' '*' * * ' ' * * '*' ' * * * * ' '* * * * * * ' ' '*' ' * * * ' ' ._ * * ' *' * *
  • I ' ' * * ' ' *I' * * ' '
  • E ::::; (J Q) 0.. Cf) X* x )(' . x. x X* x x x x X* 1. 8 -* I o o 0 I I 'o o ,' 0 I o o o ', o o o o o o I 'o o o I I o 0 0'1 I 0 o o 0 0 o' o o o o o o o o' I I o 0 0 0 0 o' 0 o I o o o 0 : I o e o 0 o o 'o 0 0 I I o ' I I r I ,, r I r 7-26 8-02 8-09 8-16 8-23 8-30 9-06 9-13 9-20 9-27 MeasureMent Date/Tirrie ACT INV MEAN INV ACT QA f i lenal'le
  • Para!'le ter Na!'le Start/End Dates Lower/Upper LMts: DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM44_CAN.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 4-APR-2016 through 1-0CT-2016 12:00:00 57.5400 through 61.5400 ..-4 tj" N I E a: CJ CJ::: LLJ z LLJ ::..< a: LLJ CL 61 ............ * ............. * .......... * .. * ............. * ............. * ............ . . . . . 60 ........... * ............. * .............. * ........... *.* ............ * ............. . . . x . . . 1xK x x . x . x x . ., xr---x' x x x . x-x. . . X *. X . iX"' . . . . x . . . . . . . x . 59 ................................................................................. . 58 o o o o 0 I o o 0 o I o' o 0 o o I o ; o o I o 0 ,o 0 I 0 o o o o o o o o I 'o o o o o I o o o o I o o*o o I o o o o I I o o o o' o o o o o I o o o o 0 ' o 4-16 5-16 6-16 7-16 8-16 9-16 Measure!'lent Date/Ti!'le UP LOW QA filenarrie Pararrieter NaMe Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM44_CAN.QAF; 1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:24:53 through 1-0CT-2016.12: 00:00 1. 01810 +-5.609688E-02 (5.51 %) . . . 1.1 "<"I """ N I E . . .. * . . . x x -* .. )( .... *x *.* ........... * ........ *x ... * .* *x* .. *x .x ... *.* ..... * ..... * ... x* .... x* .. . xx x : , -X:. x Xi< x : x>s(So< x x x Xx : x ** x
  • xx ..Z. x . x x y. xx x
  • x . >).:(-x x x *xx x* x x ")!. x x: 0 x x x : x xx*: x x . xx x x x x x x x* x x x x x* a: E x )( x I 3 LL. 1 :::..::: a: UJ CL x. .-"-x . x* . . A -* ........................ : ..... * .. x* .. *x ..... x ................... : ..... x .. ... . Xx . ' X . XX X . . X x :x x x x x x x . x x XX X X. Xx *X X
  • X" X X X ).It;: Xx X . .X X X x x x x x x: x x I 9 I--* f *
  • 0 ' ' ' ' ' ' *: * ' ' ' '., 0 ' ' ' ' ' *:' ' ' ' ' ' ' ' 0 ' 0 ':* ' ' ' ' ' o ' ' ' o ' *:* ' ' ' ' 0 ' ' ' o '0 *:' o ' o' ' o 0 0 o ' 1 ' I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tirrie ACT INV MEAN INV ACT QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM44_CAN.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06:24:53 through 1-0CT-2016 12:00: 00 70239.6 +-2304.17 (3.28 %) H u a: D LLl u LLl (t'. (t'. 0 u.* a: u LLl D 75000 70000 x . * . . . s -* ......................... * ................................................. . x x x x x x x x x x x x x x x x x x x x X* x x x x x x x x x x v v v x x x x " i\ ' A
  • A :0,.::' * * .IOI. ...... * * * * * * * * * *x.* * *x* * * * *x* * *.* * * * * * * * * * * * * * * * * * * * * *.* * * * * * * * * * * * ... * * * * * ***-x* * *
  • X . X . . X °X-X X* x x .x
  • x x x* x
  • x x x X X. Xx
  • X X *
  • X xX ::ic x xx x x 0 }( x 0 x x x x 0 :x: X X X. X:x x x x x x x . xx x x x x -x. x xxx x *x *;o:., x 1< x x x . x x x x x :x x Xx>5°< .X x x* x x x x x .x x x X :x AX , X . X . . x x x x x x 65000 ...... * * * * * * * * * * "* * * * * * * * * * * * "* *X * * * * * * * * *" * * * * * * * * * * * **.* * * * * * * * * * * * ** * ... * * * ' ..... x x I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e ACT INV MEAN INV ACT QA filenal'le Paral'Je ter Nari'te Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.5CUSR.QA]LBC_GAM44.QAF;1 BACKRATE (Spectrul'I Background Rate) 3-APR-2016 12:20: 21 through 1-0CT-2016 12:00:00 1.39471 +-2.580503E-Ot (1.85 3) x 1. 45 i--* ********** * ************* * ************.* * *********** *** ********** : *, ************* 1J c :J 0 $.... '0.0 :L u r(i -CQ E :J $.... .µ u ID 0. en x x x x 1. 4 -* ....... * ............................... * ......................................... . x x: x x x x *x x .X x x x x x x: *X x x x 1 ' 3 5 -. : . . -. . . . . . . : . . . . . -. . . . . . *: . . . . . . . . . . . . : . . . . . . 'X -. . . . : . -. . . --. . " . . *: . . . . -. . . . . . . . I I I I r 4-1.6 5-16 6-16 7-16 8-16 9-16 Measurel'lent Date/Til'le ACT INV MEAN INV ACT Page 531of614 RAD Standards
  • Traceability

-. Eckert & Ziegler Analytics 1380. Seaboard Industrial Blvd. Atlanta, Georgia 30318 Tel 404*352*8677 Fax 404*352*2837 www.analyticsinc.com CERTIFICATE OF CALIBRATION Standard Radionuclide Source 84680-278

  • 100 mL Solid in Aluminum Can Customer: GEL Labs P.O. No.: 489884RD, Item 3 Reference Date: Ol-Apr-2011 12:00 PM EST Grams of Master Source: 0.0066498 This standard radionuclide source was prepared using aliquots measured gravimetrically from master radionuclide solutions. Calibration and purity were checked using a germanium gamma spectrometer system. At the time of calibration no interfering ganuna-ray emitting impurities were The gamma ray emission rates for the most intense gamma-ray lines are given. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of Standards and Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15, Revision 1, February, 1979, and compliance with ANSI N42.22-1995, "Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for the production of NIST-traceable sources, and this source was produced iJl accordance with the HPS accreditation requirements. Customers may report any concerns with the accreditation program to the HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA 22101. Density of solid matrix 1.16 glee. Gamma-Ray Nuclide Energy (keV) Pb-210 46.5 Am-241 59.5 Cd-109 88.0 Co-57 122.l Ce-139 165.9 Hg-203 279.2 Sn-113 391.7 Cs-137 661.7 Y-88 898.0 Zn-65 1115.6 Co-60 1173.2 Co-60 1332.5 Y-88 1836.l Half-Life, Days 8.120E+03 l.SBOE+OS 4.626E+02 2.718E+02 l.376E+02 4.661E+Ol l.151E+02 l.098E+04 l.066E+o2 2.441E+02 l.925E+03 l.925E+03 l.066E+02 Master Source* yps/gram l.659E+05 8.949E+04 l.247E+05 2.899E+05 l.739E+05 l.107E+OS 4.246E+05 2.118E+05 2.118E+05 4.49SE+OS This Source 'YPS l.l29E+03 7.638E+02 l.103E+03 5.951E+02 8.292E+02 l.928E+03 l.1S6E+Q3 7.361E+02 2.824E+03 l.445E+03 l.408E+03 l.408E+03 2.989E+03 *Master So).11'C_f-fefera,.19:Analytics' 8-isotope mixture which is calibrated quarterly
  • Uncertainty , o/o Type Calibration UA Ua u Method 0.1 2.1 4.1 4nLS 0.1 1.7 3.5 4rrLs 0.6 2.3 4.8 HP Ge 0.6 2.0 4.2 HP Ge 0.6 1.9 4.0 HP Ge 0.6 1.9 4.0 HP Ge 0.6 1.9 4.0 HP Ge 0.8 1.9 4.1 HP Ge 0.6 1.9 4.0 HP Ge 0.1 1.7 3.S IC 0.7 1.9 4.0 HP Ge 0.7 1.9 4.0 HP Ge 0.1 1.9 4.0 HP Ge . * ..... * .. *. . Methods: 4rf4s. 4 pi Liquid Scintillation Counting, HPGe -High Purity Germanium Gamma-Ray Spectrometer, IC -IonizattOn Ch<U"llbez:. Unceztainty: U -Relative ezj,anded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines for the Uncertainty of NIST Measurement Results." *
  • _.. ... .** ' --::--(Certificate continued on reverse side) , ..... ...* .. -......... -* -,., . MGS Certificate, Rev 2 09*28*2009 Corporate Office 24937 Avenue Tibbitts Valencia, California 91355 Page 532of614 O(pO-lol. Pa e1 of2 Laboratory 1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318 This standard will expire one year after the reference date. Source Prepared by: M:WillifOrdlOChemist QA Approved: MGS Certificate, Rev 2 09-28-2009 Page 533 of 614 '* Date: { i.1 [. u .. , .* J.' Page2 of2 Serial ID: 1556 Name: Mixed Gamma LCS CAN Type: Source Material Employee: Maggie Stamps Supplier: Eckert & Zeigler Analytics

Description:

84680-278 Comments: None A*nalyte Americium-241 Cobalt-60 Report run on: 09-APR-15 Page 534of614 Standard Logbook Open/Reference [?ate: 01-APR-11 Received: 01-APR-11 Expires: 01-APR-37 Verified: 14-JUL-11 Concentration Analyte 125983.3 dpm/mL Cesium-137 84496.9 dpm/mL Aliquot: 1 ml Density: Lot Number: Hand Calculated 84680-278 Concentration 51898.9 dpm/mL GEL Laboratories LLC Page:---------

for Mixed Gamma Standard Michael Hilton 7/1412011 Mean Value (Counting) = stdev= Certificate Value = Lower Limit = Upper Limit = Rule 1 Pass/Fall. Twoslgma= 10%ofMean= Rule 2 (Pass/Fall) Verification Rules Isotope Pb-210 Mixed Gamma N1 Mixed Gamma N2 Mixed Gamma N3 722433.33 30102.713 717965.0 662227.9072 782638.7594 Pass 60205.42611 72243.33333 Pass Result pCUL 722900 752300 692100 pCVL 100.622 pCVL pCVL pCi/L pCIJI... 1556 Isotopic Abundance: Certificate Value (dps): Pass Rule 3 (Pass/Fall) Rule 1 = Tiie certHlcate value (NOT Including any uncertainty) shall lie within the 95% confidence Interval detennlned from the mean and two sigma standard deviation of the three measurements Rule 2 = Tiie two sigma value used for the 95% confidence Interval shall not exceed 1 O"k of the mean value of the three verification measurements.

  • Rule 3 = Tiie determined mean value shall be within 5% of the certificate value. CAN 0.0425 1129 Verification for Mixed Gamma Standard Michael Hilton 7/1412011 Isotope Am-241 Result pCl/L 1556 CAN Mixed Gamma N1 58390 Isotopic Abundance: 0.359 Mean Value (Counting) = Stdev= CertHlcate Value = -LowerLlmH= Upper Limit = Rule 1 Pass/Fall Two sigma= 10%ofMean= Rule 2 (Pass/Fall) VerHlcatlon Rules Mixed Gamma N2 Mixed Gamma N3 58966.67 1566.727 56749.2 s5833.212n 62100.12057 Pass 3133.453898 5896.666667 Pass 60740 Certificate Value (dps): 753.8 57770 pCi/L 103.9074 Pass pCi.JL Rule 3 (Pass/Fall) pCi/L pCi/L pCi/L Rule 1 =The ceitHlcate value (NOT Including any uncertainty) shall lie within the 95% c0nfldence Interval determined from the mean and two sigma standard deviation of the three measurements Rule 2 =The two sigma value 'used for the 95% confidence Interval shall not exceed 10"A. of the mean value of the three verification measurements. Rule 3 = The determined mean value shall be within 5% of the certificate value. -1\-i..o\ 1rl

Verification for Mixed Gamma Standard Michael Hilton '7/14/2011 Isotope Cd-109 Result pCl/L 1556 CAN Mixed Gamma N1 818400 Isotopic Abundance: 0.037 Mean Value (Counting) = Stdev= CertHlcate Value = Lower Limit = Upper Limit= Rule 1 Pass/Fall Twoslgma= 10 %'of Mean= Rule 2 (Pass/Fall) VerHlcatlon Rules Mixed Gamma N2 Mixed Gamma N3 793700.00 27107.010 805697.6 739485.9797 847914.0203 Pass 54214.02033 79370 Pass 798000 Certificate Value (dps): 1103 764700 pCi/L 98.51091 Pass pCi/L Rule 3 (Pass/Fall) pCi/L . pCi/L pCi/L Rule 1 *=The certHlcate value (NOT lncludlng any uncertainty) shall lie within the 95% confidence Interval detennlned from the mean and two sigma standard deviation of the three measurement$ Rule 2 =The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value of the three verification measurements. Rule 3 =The determined-mean value shall be within 5% of the certHlcate value.

Verification for Mixed Gamma Standard Michael Hilton 7/14/2011 Isotope Co-57 Result pCl/L 1556 CAN Mixed Gamma N1 19.090 Isotopic Abundance: 0.856 Mean Value (Counting) = Stdev= Certificate Value = Lower Limit= Upper Limit = Rule 1 Pass/Fail Two sigma= 10%of Mean= Rule 2 (Pass/FalQ Verification Rule$ Mixed Gamma N2 Mixed Gamma N3 18913.33 153.080 18789.5 18607.17433 19219.49233 Pass 306.1590001 1891.333333 Pass 18820 Certificate Value (dps): 595.1 18830 pCl/L 100.6592 Pass pCl/L Rule 3 (Pass/Fall) pCl/L pCi/L pCl/L Rule 1 =The certHlcate value (NOT Including any uncertainty) shall lie within-the 95% confidence Interval determined from the mean and two sigma standard deviation of the three measurements Rule 2 =The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value of the three verification measurements. Rule 3 =The determined mean value shall be within 5% of the certificate value.

. Verification for Mixed Gamma Standard Michael Hilton 7/1412011 Mean Value (Counting) = Stdev= Certificate Value = Lower Limit = Upper Limit = Rule .1 Pass/Fall Two sigma= 10%ofMean= Rule 2 (Pass/Fa!Q Verification Rules Isotope Ce-139 Mixed Gamma N1 Mixed Gamma N2 Mixed Gamma N3 28570.00 936.643 28013;5 26696.71412 30443.28588 .Pass 1873.285883 2857 Pass Result pCl/L 28740 29410 27560 pCilL pCi/L pCVL pCVL pCl/L 101.9865 1556 Isotopic Abundance: Certificate Value (dps): Pass Rule 3 (Pass/Fall) Rule 1 =The certificate value (NOT Including any uncertainty} shall He within the 95% confidence Interval determined from the mean and two sigma standard deviation of the three measurements Rule 2 =The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value of the three verification measurements. Rule.3 =The detennlned mean value shall be within 5% of the certificate value. CAN 0.8 829.2 Verification for Mixed Gamma Standard 1556 Michael Hilton Isotope Result -7/1412011 Hg-203 pCl/L Mixed Gamma N1 Isotopic Abundance: Mixed Gamma N2 68180 Certificate Value (dps): Mixed Gamma N3 64480 Mean Value (Counting)= 66320.00 pCi/L 103.8046 Pass Stdev= 1850.081 pCi/L Rule 3 (Pass/Fall) Certificate Value = 63889.3 pCi/L Lower Limit= 62619.83784 pCi/L Upper Limit = 70020.16216 pCi/L Rule 1 Pass/Fall Pass Two sigma= 3700.162159 10%of Mean= 6632 Rule 2 (Pass/Fall) _ Pass Verification Rules Rule 1 =The certHlcate value (NOT Including any uncertainty) shall lie within the 95% confidence Interval determined from the mean and two sigma standard deviation of the three measurements CAN 0.8156 1928 Rule 2 =The two sigma value used for the 95% con(ldence Interval shall not exceed 10% of-the mean value of the three verHlcatlon measurements. Rule 3 = The determined mean value shall be within 5% of the certHlcate value.

Verification for Mixed Gamma Standard Michael Hilton Isotope Result 7/14/2011 Sn-113 pCl/L Mixed Gamma N1 49560 Mixed Gamma N2 49620 Mixed Gamma N3 48300 Mean Value (Counting) = 49160.00 pCVL 102.2277 Stdev= 745.386 pCVL CertHlcate Value = 48088.7 pCVL Lower Limit = 47669.22839 pCVL Upper Limit = 50650.77161 pCVL Rule 1 Pass/Fall Pass Two sigma= 1490.771612

  • 10 %of Mean= 4916 Rule 2 (Pass/Fall) Pass VerHlcatlon Rules 1556 Isotopic Abundance: Certificate Value (dps): Pass Rule 3 (Pass/Fall) CAN. 0.6497 1156 Rule 1 =The certificate value (NOT Including any uncertainty) shall lie within the 95% confidence Interval determined from the mean and two sigma standard deviation of the three measurements Rule 2 =The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value of the three verification measurements. Rule 3 =The determined mean value shall be within 5% of the certHicate value. 1\1Pl\)

Verification for Mixed Gamma Standard Michael Hilton . 7/1412011 Mean Value (Counting) = stdeV: CertHlcate Value= Lower Limit = Isotope Cs-137 Mixed Gamma N1 Mixed Gamma N2 Mixed Gamma N3 23900,00 170.587 Result pCl/L 23710 23950 24040 pCilL 102.2333 pCi/L pCill. pCllL pCill. 1556 Isotopic Abundance: Certificate Value (dps): Pass Rule 3 (Pass/Fall)

  • Upper Limit= Rule 1 Pass/Fall Twoslgma= 10%ofMean= 23377.9 23558.82556 24241.17444 Fall
  • 341.1744422 2390 Pass *exception taken due to full recovery of standard . Rule 2 (Pass/Fall) VerHlcatlon Rules Rule 1 = The certificate value (NOT Including any uncertainty) shall He within the 95% confidence Interval determined from the mean and two sigma standard deviation of the three measurements -Rule 2 =The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value of the three verHlcatlon measurements. Rule 3 =The determined mean value shall be within 5% of the certHlcate value. CAN 0.851 736.1 Verification for Mixed Gamma Standard 1556 CAN Michael Hilton Isotope Result 7/14/2011 . Y-88 (898) pCl/L Mixed Gamma N1 82690 Isotopic Abundance: o.937 Mixed Gamma N2 81320 Certificate Value (dps): 2824 Mixed Gamma N3 80940 Mean Value (Counting)= 81650.00 pCi/L 100.2381 Pass . Stdev= 920.489 pCVL Rule 3 (Pass/Fall) Certificate Value = 81456.1 pCi/L Lower Limit = 79809.022 pCi/L Upper Limit = 83490.978 pCi/L Rule 1 Pass/Fall Pass Two sigma= 1840.978001 10%ofMean= 8165 Rule 2 (Pass/Fall) Pass VerHlcatlon Rules Rule 1 =The certlflcete*vaiue (NOT Including any uncertainty) shall lie within the 95% confidence Interval determined from the mean and two sigma standard deviation of the three measurements Rule 2 =The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value of the threeverHlcatlon measurements. Rule 3 =The detennlned mean value shall be within 5% of the certificate value.

Verification for Mixed Gamma Standard Michael Hilton 7/14/2011 Mean Value (Counting) = Stdev=

  • Isotope Co-60 (1173) Mixed Gamma N1 Mixed Gamma N2 Mixed Gamma N3 39166.67 506.392 Result pCl/L 38910 39750 38840 pCi/L 102.7694 pCi/L pCi/L pCi/L pCi/L 1556 Isotopic Abundance: Certificate Value (dps): Pass Rule 3 (Pass/Fall) CertHicate Value = Lower Limit = Upper Limit = Rule 1 Pass/Fall Two sigma= 10%ofMean= Rule 2 (Pass/Fall) 38111.2 38153.88173 40179.45161 Fall 1012.784939 3916.666667 Pass taken due to full recovery of standard Verification Rules Rule 1 = The certificate value (NOT Including any uncertainty) shall lie within the 95% confidence Interval detennlned from the mean and two sigma standard deviation of the three measurements Rule 2 =The two sigma \talue used for the 95% confidence Interval shall not exceed 10% of the mean value
  • of the three verification measurements. Rule 3 =The determined mean value shall be within 5% of the certificate value. CAN 0.9985 1408 Verification for Mixed Gamma Standard Michael Hilton 7/14/2011 Mean Value (Counting) = Stdev'= Isotope Co-60 (1332.50) Mixed Gamma N1 Mixed Gamma N2 Mixed Gamma N3 39430.00 675.056 Result pCl/L 38940 40200 39150 pCl/L 103.595 pCi/L pCi/L pCi/L pCi/L 1556 Isotopic Abundance: Certificate Value (dps): Pass Rule 3 (Pass/Fall) Certificate Value = Lower Limit = Upper Limit = Rule 1 Pass/Fall Two sigma= 10%of Mean= Rule 2 (Pass/Fall) 38061.7 38079.88889 40780.11111 Fall 1350.111107 3943 Pass *exception taken due to full recovery of standard VerHlcatlon Rules Rule 1 = The certmcate value (NOT Including any uncertainty) shall He within the 95% confidence Interval determined from the mean and two sigma standard deviation of the three measurements Rule 2 .. The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value of the three measurements. Rule 3 =The determined mean value shall be within 5% of the certificate value. CAN 0,9998 1408 (

Verification for Mixed Gamma Standard Michael Hilton 7/14/2011 Mean Value (Counting)= Stdev= Isotope V-88 (1836.1) Mixed Gamma N1 Mixed Gamma N2 Mixed Gamma N3 83530.00 967.006 Result pCl/L 82870 83080 84640 pCi/L 102.5723 pCi/L pCi/L pCi/L pCi/L 1556 Isotopic Abundance: Certificate Value (dps): Pass Rule 3 (Pass/Fall) CertHlcate Vaiue = Lower Limit = Upper Limit*= _ Rule 1 Pass/Fall Two sigma= 10%ofMean= Rule 2 (Pass/Fall) 81435.3 81595.98862 85464.01138 Fall 1934.011375 8353 Pass taken due to full recovery of standard VerUlcatlon Rules Rule 1 =The certificate value (NOT Including any uncertainty) shall lie within the 95% confidence Interval detennlned from the mean and two sigma standard deviation of-the three measurements Ru1e*2 =The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value of the three verHlcaUon measurements. Rule 3 =The determined mean value shall be within 5% of the certHlcate value. CAN 0.992 2989 Runlogs Page 547of614 Instrument Run Log Instrument Type: GAMMA SPECTROMETER

  • Batch ID: 1596387 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405245001 SAMPLE MXR1 GAM01 OCT-03-16 04:32:47 DONE CAN 20-JUL-16 00:00 405245002 SAMPLE MXR1 GAM05 OCT-03-16 04:33:24 DONE CAN 04-SEP-16 00:00 405245003 SAMPLE MXR1 GAM06 OCT-03-16 04:33:45 DONE CAN 08-MAR-16 00:00 405245004 SAMPLE MXR1 GAM07 OCT-03-16 04:34:09 DONE CAN 19-AUG-16 00:00 405245005 SAMPLE MXR1 GAM18 OCT-03-16 04:34:32 DONE CAN 25-JUN-16 00:00 405245006 SAMPLE MXR1 GAM24 OCT-03-16 04:34:54 DONE CAN 17-JUN-16 00:00 405245007 SAMPLE MXR1 GAM29 OCT-03-16 04:35:17 DONE CAN 25-JUN-16 00:00 405245008 SAMPLE MXR1 GAM30 OCT-03-16 04:35:39 DONE CAN 11-MAR-16 00:00 405245009" SAMPLE MXR1 GA.M32 OCT-03-16 04:36:09 DONE CAN 23-AUG-16 00:00 405245010 SAMPLE MXR1 GAM39 OCT-03-16 04:36:41 DONE CAN 27-JUL-16 00:00 405245011 SAMPLE MXR1 GAM08 OCT-03-16 04:45:57 DONE CAN 21-JUL-16 00:00 405245012 SAMPLE MXR1 GAM09 OCT-03-16 04:46:21 DONE CAN 03-JUN-16 00:00 405245013 SAMPLE MXR1 GAM19 OCT-03-16 04:46:48 DONE CAN 15-JUN-16 00:00 405245014 SAMPLE MXR1 GAM20 OCT-03-16 04:47:25 DONE CAN 30-JUN-16 00:00 405245015 SAMPLE MXR1 GA[y128 OCT-03-16 04:47:45 DONE CAN 01-AUG-16 00:00 405245016 SAMPLE MXR1 GAM36 OCT-03-16 04:48:08 DONE CAN 01-JUN-16 00:00 1203621685 MB MXR1 GAM44 OCT-03-16 04:48:39 DONE CAN 06-SEP-16 00:00 1203621687 LCS MXR1 GAM11 OCT-03-16 04:53:57 DONE CAN 02-AUG-16 00:00 1203621686 DUP MXR1 GAM05 OCT-03-16 05:34:41 DONE CAN 04-SEP-16 00:00 Page 548of614 Gas Flow Raw Data Page 549of614 Effective 3/25/2010 Radiochemistry Batch Checklist Revision 1 Effective March 201 O 27-Sep-2016 Batch# J 5 Cj / Product: __ _,G="'-'*'"-/l&"""'----Date: q f *n } IC* Criteria: Yes No Comments Sa mole Sollds are less than or eciual to 100 mn for GAB. / Samples have been blank corrected (if required). Blank correction renorted Included (if reaulred). IA1!l. . If activity less than lOx MDA/M DC, error is less than or equal to 1SO% of sample activity. ./ Cf greater than 10* MDA/ MDC, error Is 40% or less. [f hnlnU/ the MDA/ MOC. nrrnr Is Cnstrument source check Is within limits. ./ Cnstrument bkn checl< is Ulltli°in limits. Method RDL/ LLD has been met. ,/ Cf duolicate activities are: Less than*S* MDA/ MDC, then RPO ls 100% or less, If greater S* MDA/ MDC, then RPO 20% or less, / [f below the MDA/ MDC, the RPO is 0%, Or meets the client's reouired RER accentance criteria. Tracer yield Is lS-125%
  • Carrier yield 2S-12S%. (Or meets the client's contract acceptance criteria). .NA Method blank Is less than the RDL/ LLD. .,.,.... lfTf < 50/n of ln ... ne* lltotlvltvl* Samole was run within hotd time. v Derz-Sa mole was correctlv oreserved If reauired. /l/A Smears Taken for Radioactive batches. fl/I/ Method Spike and LCS are within 7S-12S% ..,,,,,. fnr mnets the cli .. nt's accentance criterlal. No blank spaces on data forms. / All line outs initialed and dated. Mn nrrnro -*A Aux data is correct. 11/,<j I ....,/ Client Saeclal reouirements oaoe has been checked. Raw Data and/ or saectrum are included and aronerlv statused. / MS, LCS, and Duplicate RPD/RER values uploaded to UMS and / v<>rlfied r .... -n-nln*n {If ., lllA nntnrn..! ln*n / Batch Data Exceotion Reoorts (DER) comoletcd if aoolicable. / 0 l:.:rl I Batch Data Exception Reports (DER) second reviewed. / l Oc-rL !Cf>01775 Dlsnosition verified to be comoleted. :ruI.g.uot If required. /VA' Review sample historical results if available ./v (If REM P, results above MDC have been verified bv historical results recount or re-analvsls. l Primary Review Performed By: __ ___ ..,-_____ _ secondary Review Performed __ -..... ____ _ f'IJ'1;1 c to f<r Page 550of614 GL-CHL-RAD-013Rev1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DAT A EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 27-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: GFPC EPA 900.0/SW846 931 O/SM 711 OB Solid *-Batch ID: Sample Numbers: 1597819 See Below Potentially affected work order(s)(SDG): 405245 Application Issues: Sample Analyzed out of Holding Specification an!'.! Requirements DER Disposition: Exception

Description:

1. Samples 405245001, 405245002, 405245003, 405245004, 1. Reporting results 405245005,405245006,405245007,405245008,405245009, 405245010,405245011,405245012,405245013,405245014, 405245015,405245016, 1203625472, 1203625473,and 1203625474 were received within holding but analyzed out of holding. -Originator's Name: Data Validator/Group Leader: Kenshalla Oston 27-SEP-16 Nat Long 29-SEP-16 Page 551of614 DER Report No.: 1561775 Revision No.: 1 Type: Process Client Code: MJWC Logbook The Determination of Gross Alpha And Gross Non* Volatile Beta in Soil, Filters, Solid Matrices And Direct_ Count Air Filters Batch ID: 1597819 Analyst: Jasmine Conley Instrument: BAL-16107662 Sample ID 405245002 405245003 40524500-l 405245005 405245006 405245007 405245008 405245009 4052450!0 405245011 405245012 405245013 405245014 405245015 405245016 1203625471 1203625472 DUP (405245003) 1203625473 MS (405245003) 1203625474 MSD (405245003) 1203625475 LCS Type Name Run Date RGl\'T RGF-Hydrochloric A<;id RGNT RGF-Hydrofluoric Acid RGNT RGF-1 M Nitric Acid Due Dates for Lab: 30-SEP-2016 Hold: 12-JUN-2016 Package: 02-0CT-2016 SDG: 04-0CT-2016 Serial Number Spike Amount Spike Units :----_-mL -j ' 2438701 j 5 i mL ;_ _______ . _______________ -. Lab SOP: GL-RAD-A-OOlB REV# 17 Method: EPA 900.0/SW846 9310/SM 7110B 1\foditied Detector Spike Pipet ID: RAD-GFC-4497063 Planchets Flamed: Yes Analytical Logbook \'Crsion 1 11-04-2004 GEL Laboratories LLC Logbook The Determination of Gross Alpha And Gross Non-Volatile Beta in Soil, Filters, Soliq An_d :Oirect Count Air Filters Batch ID: 1597819 Analyst: Jasmine Conley Instrument: BAL-16107662 Sample ID Run Date Lab SOP: GL-RAD-A-OOIB REV# 17 Method: EPA 900.0/SW846 9310/SM 7110B Modified # Dry or Wet lntermedkue Um1djustt!d Aliquot lniti31 \Veight Final \\'eight Detector Aliquot Aliquot (g) (g) (gl Weight ----------------------------------------1£L _______________________ _J!!!JlL ________________ *--***--------RGNT RGF-Nitric Acid --T--mL J . SPIKE Strontium-90 SPIKE i 1243-0 I . .1 i mL i Spike Pipet ID: RAD-GFC-4497063 SPIKE Thorium-230 SPIKE :-----149)-3----1-------:1---, --mL--t Planchets Flamed: Yes Analytical version 1 11-04-2004 GEL Laboratories LLC Filename : GAB.XLS File type : Excel Version # : 1.3.1 O Batch: 1597819 Analyst: JAS02031 Prep Date : 9/22/2016 Alpha Method Uncertainty : 0.0928 Beta Method Uncertainty : 0.0628 Geometry: 2 inch Planchett Sample Characteristics Sample Sample Sample Aliquot Residue Wt. Pos. ID G (mg) 1 405245001.1 0.1050 22.1 2 405245002.1 0.1070 22.9 3 405245003.1 0.1090 22.3 4 405245004.1 0.1020 23.B 5 405245005.1 0.1090 26.3 6 405245006.1 0.1020 27 7 405245007 .1 0.1020 22.2 8 405245008.1 0.1070 23.3 9 405245009.1 0.1030 20.3 10 405245010.1 0.1060 19.4 11 405245011.1 0.1000 22.2 12 405245012.1 0.1050 24.3 13 405245013.1 0.1050 21.7 14 405245014.1 0.1020 22 15 405245015.1 0.1070 28.7 16 405245016.1 0.1050. 28.3 17 1203625471.1 0.1090 0.3 18 1203625472.1 0.1090 23.4 19 1203625473.1 0.0990 21.1 20 1203625474.1 0.1020 21 21 1203625475.1 0.1090 0.6 Sample Aliquot StDev. G 3.2300E-03 3.2302E-03 3.2304E-03 . 3.2297E-03 3.2304E-03 3.2297E-03 3.2297E-03 3.2302E-03 3.2°298E-03
  • 3.2301 E-03 4.3713E-04 3.2300E-03 3.2300E-03 3.2297E-03 3.2302E-03 3.2300E-03 3.2304E-03 3.2304E-03 4.3283E-04 3.2297E-03 3.2304E-03 AB1597819r1 Gross Alpha/Beta Solid Count Raw Data Sample Delector Date/Time ID 12115/2015 10:14 8D -12115/2015 10:19* 4D 12115/2015 10:18 1D 12115/2015 10:21 9C 12115/201511:42 3D 12115/201511:46 1C 12115/2015 12:17 2B 12115/2015 12:20 38 12115/201512:31 2A 121151201512:35 BA 1211512015 12:53 1B 12115/201512:56 9D 12115/201511:04 5D 12115/201511:08 108 12115/2015 14:02 SC 1211512015 14:06 4A 9/2212016 0:00 48 121151201510:18 58 12115/201510:18 1A 12115/201510:18 1C 9/2212016 0:00 9A Page1 Procedure Code : GFCGANBS Pannname1 : Alpha Pannname2 : Beta Required Alpha MDA : 4 Required Beta MDA : 10 Counting Time Gross Counts (min.) Alpha Beta 140 85 458 150 85 367 130 96 438 120 75 275 130 85 400 130 105 466 140 76 286 140 107 470 150 88 390 140 115 393 130 73 397 160 102 510 150 117 446 140 71 345 140 93 450 130 87 428 60 5 *77 160 102 418 60 343 3093 60 375 2961 60 494 3392 pCi/G pCi/G Count Start Date/Time 9/26/2016 13:58 9/2612016 13:59 9/26/2016 13:59 9126/201613:59 9/26/2016 13:59 912612016 13:59 9/26/201613:59 9/261201613:59 9/2612016 13:59 9/2612016 13:59 9/26/2016 13:59 912612016 14:04 91261201613:59 91261201614:04 9/2612016 13:59 912612016 14:00 91261201613:58 9126/2016 13:58 9/2612016 13:58 9/27/2016 10:14 912612016 13:58 P-ipet, 0.1 ml Stdev : +/-0.000200 ml Pipet, 0.5 ml Stdev: +/-0.001000 ml Pipe!, 1 ml Stdev : +/-0.002000 ml Analytical SOP: GL-RAD-A-001B Instrument SOP: GL-RAD-1-016 Calibration Data Alpha I Calibration Calibration Detector Counted Calibration Due Source Efficiency Pos. on Date Date Used (cpm/dpm) 1 PIC 12/1/2015 11/3012016 Th230 0.1828 2 PIC 12/1/2015 11/30/2016 Th230 0.1624 3 PIC 12/112015 11/3012016 Th230 0.1615 4 PIC 12/1/2015 11/3012016 Th230 0.1597 5 PIC 12/1/2015 11/30/2016 Th230 0.1453 6 PIC 12/1/2015 11/30/2016 Th230 0.1508 7 PIC 12/1/2015 11/3012016 Th230 0.1239 8 PIC 12/1/2015 11/30/2016 Th230 0.1573 9 PIC 12/1/2015 11/30/2016 Th230 0.1564 10 PIC 12/1/2015 11/30/2016 . Th230 0.1824 11 PIC 12/112015 11/3012016 Th230 0.1537 12 PIC 121112015 11/30/2016 Th230 0.1648 13 PIC 12/112015 11/30/2016 Th230 0.1885 14 PIC 1211/2015 11130/2016 Th230 0.1444 15 PIC 12/1/2015 11/30/2016 Th230 0.1688 16 PIC 1211/2015 1113012016 Th230 0.1405 17 -PIC 121112015 11130/2016 Th230 0.2561 18 PIC 1211/2015 1113012016 Th230 0.1842 19 PIC 1211/2015 11/30/2016 Th230 0.1542 20 PIC 1211/2015 11/30/2016 Th230 0.1711 21 PIC 1211/2015 11/3012016 Th230 0.2729 I Del.Elf. Error Calibration (cpm/dpm) X-Talk Date 0.00794 0.06858 12/1/2015 0.00613 0.06303 12/1/2015 0.00996 0.06570 12/1/2015 0.01265 0.08495 1211/2015 0.00657 0.07604 12/1/2015 0.00967 0.06165 1211/2015 0.02011 0.32365 12/1/2015 0.00853 0.06198 1211/2015 O.D1946 0.15836 1211/2015 0.01473 0.08229 12/1/2015 0.01356 0.10478 1211/2015 0.02427 0.07694 1211/2015 0.00639 0.06687 1211/2015 0.00844 0.19141 121112015 0.01161 0.06207 121112015 0.01036 0.07287 121112015 0.00704 0.11205 12/1/2015 0.01152 0.05910 121112015 0.00667 0.10371 1211/2015 0.00967 0.05749 1211/2015 0.00726 0.10251 1211/2015 AB1597819r1 Beta I Weekly Background Calibration Calibration Detector Del.Elf. Count Count Due Source Efficiency Error CPM Start TI me Date Used (cpm/dpm) (cpm/dpm) X-Talk Alpha Bela Dalemme (min.) 11/30/2016 Sr90 0.4951 0.00609 0.00243 0.222 0.888 9/23/2016 18:14 500 11/3012016 Sr90 0.4692 0.00773 0.01310 0.182 0.716 9/2312016 18:18 500 11/30/2016 Sr90 0.4858 0.00692 0.00767 0.158 1.392 9/2312016 18: 17 500 11/30/2016 Sr90 0.4874 0.00584 0.00209 0.126 0.808 9/2312016 18:14 500 11/30/2016 Sr90 0.46)8 0.02297 0.00259 0.124 0.630 9/23/2016 18:17 500 11/30/2016 Sr90 0.4860 0.00847 0.01123 0.114 0.722 9/231201618:17 500 11/30/2016 Sr90 0.4547 0.02111 0.00019 O.Q76 0.464 9/23/2016 18:17 500 11/30/2016 Sr90 0.4662 0.01614 0.01009 0.162 1.378 9123/2016 18:17 500 11/30/2016 Sr90 0.4858 0.01914 0.00045 0.160 0.470 9/231201618:17 500 11/30/2016 Sr90 0.4892 0.01579 0.00165 0.228 1.076 9/23/2016 18:14 500 11130/2016 Sr90 0.4876 0.00711 0.00168 0.114 1.118 912312016 18:17 500 11/30/2016 Sr90 0.4855 0.02610 0.00286 0.158 1.200 9/231201618:15 500 11/30/2016 Sr90 0.4947 0.00925 0.00363 0.248 o.no 9/23/2016 18:18 . 500 11/30/2016 Sr90 0.4636 0.00652 0.00072 0.120 0.560 9/23/2016 18:15 500 11/30/2016 Sr90 0.4974 0.00657 0.00367 0.182 0.794 9/2312016 18:18 500 11/30/2016 Sr90 0.4688 0.01123 0.00431 0.104 0.770 9/2312016 18:18 500 11/30/2016 Sr90 0.4941 0.01519 0.00026 0.152 1.540 9/23/2016 18:18 500 11/30/2016 Sr90 0.4979 0.00426 0.00379 0.272 0.506 9/23/2016 18:18 500 11/30/2016 Sr90 0.4780 0.00738 0.00079 0.290 0.848 9/23/2016 18:17 500 11/30/2016 Sr90 0.4886 0.00847 0.01123 0.114 0.722 9/2312016 18:17 500 11/30/2016 Sr90 0.5005 0.00758 0.00085 0.228 0.796 9/2312016 18:14 500 Page2 Notes: 1 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date Alpha Results Decision Critical Required Sample Act. Sample Act. Level Level MDA MDA Cone. Error Pos. pCl/G pCiiG pCl/G pCi/G pCl/G % 1 2.4636 1.7393 4 3.9815 8.8526 18.23% 2 2.3989 1.6937 4 3.9058 9.1411 17.01% 3 2.3338 1.64n 4 3.8860 14.1960 13.70% 4 2.3248 1.6413 4 3.9740 13.6661 15.20% 5 2.2970 1.6217 4 3.8996 14.8400 14.04% 6 2.2681 1.6013 4 3.8784 19.1357 12.03% 7 2.1886 1.5452 4 3.8539 16.6220 14.10% 8 2.3997 1.6942 4 3.9619 15.2117 13.01% 9 2.4255 1.7124 4 3.9839 11.8948 15.69% 10 2.4784 1.7498 4 3.9988 13.7174 13.82% 11 2.2698 1.6025 4 3.8812 12.9654 15.14% 12 2.1894 1.5458 4 3.5795 12.2427 14.23% 13 2.4587 1.7359 4 3.9270 11.8635 14.53% 14 2.3600 1.6662 4 3.9876 11.7842 16.38% 15 2.3707 1.6738 4 3.8820 11.7358 15.17% 16 2.2594 1.5952 4 3.8952 16.8302 13.35% 17 2.0029 1.4140 4 3.6349 -1.1135 60.00% 18 2.4765 1.7485 4 3.9176 7.9789 18.68% 19 5.0588 3.5716 4 8.6186 158.9361 5.76% 20 2.7735 1.9581 4 5.2064 144.0328 6.22% 21 2.3019 1.6252 4 4.0076 120.5044 5.55% AB 1597819r1 Alpha Spike SIN : Spike Exp Date : Spike Activity (dpm/ml): Net Count Rale CPM 0.3851 0.3847 0.5805 0.4990 0.5298 0.6937 0.4669 0.6023 0.4267 0.5934 0.4475 0.4795 0.5320 0.3871 0.4823 0.5652 -0.0687 0.3655 5.4267 6.1360 8.0053 Spike Volume Added; Spike Nuclide: Alpha LCS SIN : LCS Exp Date : LCS Activity (dpmlml): LCS Volume Added: LCS Nuclide: 2SIGMA Net Count Counting Rate Error Uncertainty CPM pCi/G 0.0691 3.1805 0.0644 3.2700 o.on4 3.8848 0.0739 4.0049 0.0726 4.0490 0.0803 4.6065 0.0635 4.4335 0.0760 3.9888 0.0650 3.5640 0.0795 3.6311 0.0674 3,8735 0.0656 3.3453 0.0755 3.3670 0.0621 3.7249 0.0715 3.4944 0.0732 4.3811 0.0411 1.3014 0.0673 2.9594 0.3096 17.9074 0.3231 16.3410 0.3711 11.0135 Page3 1493-B 618/2017 266.08 0.10 Th-230 1493-B 6/8/2017 266.08 0.10 Th-230 2SIGMA Total Prop. Uncertainty pCl/G 3.6243 3.7875 4.8190 4.8155 4.9708 6.0506 5.5053 5.0485 4.2606 4.5111 4.5639 4.1548 4.0920 4.3691 4.1928 5.5009 1.3024 3.3533 34.2831 34.6690 25.6922 Sample QC 405245003.1 405245003.1 405245003.1 Sample Nominal Type RPO RER pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE .SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP 56.1% MS 121.0665 119.6% MSD 9.8% 117.5057 110.5% LCS 109.9595 109.6%

Notes: 1 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date Beta Results Decision Critical Required Sample Act. Sample Act Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 1.7986 1.2698 10 2.7253 20.4651 7.30% 2 1.6467 1.1626 10 2.5046 15.2068 8.30% 3 2.3020 1.6253 10 3.4468 16.4056 9.09% 4 1.9291 1.3620 10 2.9504 12.9623 10.22% 5 1.6292 1.1502 10 2.5070 21.4506 7.46% 6 1.7713 1.2505 10 2.7108 25.5fi19 6.79% 7 1.4740 1.0407 10 2.2895 13.6286 8.76% 8 2.3617 1.6673 10 3.5282 17.4442 8.94% 9 1.3387 0.9451 10 2.0703 18.3382 7.33% 10 2.0077 1.4174 10 3.0210 14.4518 9.27% 11 2.2407 1.5820 10 3.3771 17.3404 8.33% 12 2.0487 1.4464 10 3.0585 17.1304 8.53% 13 1.6508 1.1655 10 2.5044 18.6566 7.37% 14 1.5880 1.1212 10 2.4465 17.2140 7.88% 15 1.6803 1.1863 10 2.5540 20.1370 7.17% 16 1.8421 1.3006 *10 2.8123 22.6372 7.28% 17 3.3040 2.3327 10 5.0835 -2.2247 61.04% 18 1.2494 0.8821 10 1.9198 17.1702 6.93% 19 2.7904 1.9700 10 4.4160 476.9753 2.02% 20 2.4447 1.7260 10 3.9039 436.2564 3.77% 21 2.3449 1.6555 10 3.7238 453.2070 3.52% AB1597819r1 . Beta Spike SIN : Spike Exp Date : Spike Activity (dpm/ml): 1243-0 12118/2016 483.29 0.10 Sr-90 Spike Volume Added: Spike Nuclide: Beta LCS SIN : 1243-0 LCS Exp Date : 12118/2016 LCS Activity (dpm/ml): 483.29 LCS Volume Added: 0.10 LCS Nuclide: Sr-90 2SIGMA 2SIGMA Net Count Net Count Counting Total Prop. Rate Rate Error Uncertainty Uncertainty CPM CPM pCi/G pCi/G 2.4034 0.1584 2.6909 3.9307 1.7307 0.1332 2.3423 3.1684 1.9772 0.1694 2.8244 3.6427 1.4837 0.1439 2.5560 3.1608 2.4469 0.1579 2.7691 4.1858 2.8626 0.1703 3.0342 4.7172 1.5789 0.1246 2.3716 3.2397 1.9791 0.1635 2.8940 3.8278 2.1300 0.1352 2.3851 3.6284 1.7311 0.1490 2.5372 3.2996 1.9358 0.1604 2.9043 3.6560 1.9875 0.1494 2.5878 3.6468 2.2033 0.1462 2.4845 3.6266 1.9043 0.1368 2.5545 3.5821 2.4203 0.1567 2.5992 3.8280 2.5223 0.1639 2.9401 4.3488 -0.2567 0.1564 2.5642 2.5643 2.1065 0.1317 2.1421 3.2050 50.7020 0.9278 17.3102 62.4055 48.6280 0.9077 16.0798 63.1053 55.7373 0.9715 15.7208 64.9367 Page4 Sample Sample Nominal QC Type RPO RER pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB 405245003. 1 DUP 4.6% 405245003.1 MS 439.7982 104.7% 405245003. 1 MSD 8.9% 426.8629 98.4% LCS 399.4497 113.5%

'"d !IJ (IQ (l) 1597819rl VI VI 00 0 H) SamplelD Instr Time (min.) Alpha Counts Beta Counts Count Start Time Count End Time Machine Batch ID 0\ ........ 405245001 80 140 85 458 9/26/2016 13:58 9/26/2016 16:18 PIC 1597819 +:-405245002 40 150 85 367 9/26/2016 13:59 9/26/2016 16:29 PIC 1597819 405245003 10 130 96 438 9/26/201613:59 9/26/2016 16:09 PIC 1597819 40S245004 9C 120 75 27S 9/26/2016 13:59 9/26/2016 1S:S9 PIC 1S97819 40524500S 30 130 8S 400 9/26/2016 13:59 9/26/2016 16:09 PIC 1S97819 40S245006 1C 130 105 466 9/26/2016 13:59 9/26/2016 16:09 PIC 1597819 40524S007 2B 140 76 286 9/26/2016 13:59 9/26/2016 16:19 PIC 1S97819 40524S008 3B 140 107 470 9/26/2016 13:S9 9/26/2016 16:19 PIC 1S97819 40524S009 2A 150 88 390 9/26/2016 13:59 9/26/2016 16:29 PIC 1597819 40S245010 8A 140 llS 393 9/26/2016 13:S9 9/26/2016 16:19 PIC 1S97819 40S24S011 lB 130 73 397 9/26/2016 13:59 9/26/2016 16:09 PIC 1597819 40S245012 90 160 102 SlO 9/26/2016 14:04 9/26/2016 16:44 PIC 1597819 405245013 SD lSO 117 446 9/26/2016 13:S9 9/26/2016 16:29 PIC 1597819 405245014 10B 140 71 345 9/26/2016 14:04 9/26/2016 16:24 PIC 1597819 40524501S SC 140 93 450 9/26/2016 13:59 9/26/2016 16:19 PIC 1597819 405245016 4A 130 87 428 9/26/2016 14:00 9/26/2016 16:10 PIC 1597819 1203625471 4B 60 5 77 9/26/201613:58 9/26/2016 14:58 PIC 1597819 1203625472 SB 160 102 418 9/26/2016 13:58 9/26/2016 16:38 PIC 1597819 1203625473 lA 60 343 3093 9/26/2016 13:58 9/26/2016 14:58 PIC 1597819 1203625474 1C 60 375 2961 9/27 /2016 10:14 9/27/201611:14 PIC 1S97819 120362547S 9A 60 494 3392 9/26/2016 13:58 9/26/2016 14:58 PIC 1597819 Page 559of614 Continuing Calibration

  • Data Gas Flow Proportional Counter Checks for 26-Sep-2016 Detectors LB4100 A1 through J4 and PIC 1A through 140 Short Name Status Parmname Run Time Count CPMor Low Limit Migh Limit Stdev Time dee LB4100A3 Below Alpha eff 26-Sep 09:40 5 8817 9142 11120 -3.99 LB4100B2 Above Beta bkg 26-Sep 06:43 60 2.650 0.992 2.051 +6.39 LB4100B3 need 2nd* Beta bkg 26-Sep 06:43 60 1.767 0.965 1.943 +1.92 LB4100C1 need 2nd Alpha bkg 26-Sep 07:20 60 0.267 0.149 0.367" +0.24 LB4100C3 Below Alpha eff 26-Sep 11 :05 5 5767 6624 9128 -5.05 LB4100C3 Above Alpha XTalk 26-Sep 11 :05 5 0.422 0.248 0.368 +5.68 LB4100C4 Above Beta bkg 26-Sep 07:20 60 13.950 0.686 2.113 +52.75 LB4100E1 Above Beta bkg 26-Sep 06:43 60 9.667 0.637 2.392 +27.87 .. LB4100E2 Above Beta bkg 26-Sep 06:43 60 2.900 1:061 2.316 +5.79 LB4100E3 Above Beta bkg 26-Sep 06:43 60 3.367 0.463 2.359 .+6.19 LB4100E4 Above Beta bkg 26-Sep 06:43 60 2.317 0.650 2.302 +3.05 LB4100F1 Below Alpha eff 26-Sep 07:45 5 10513 10840 11730 -5.21 LB4100F1 Above Alpha XTalk 26-Sep 07:45 5 0.266 0.224 0.265 +3.14 LB4100F2 Below Beta eff 26-Sep 10:15 5 18371 18400 19480 . -3.16 LB4100H2 Above Beta bkg 26-Sep 08:02 60 1.750 0.650 1.491 +4.85 LB4100H4 Below Alpha eff 26-Sep 07:52 5 10619 11490 13890 -5.18 LB4100H4 Above Alpha XTalk 26-Sep 07:52 5 0.411 0.307 0.379 +5.68 LB4100H4 Below Beta eff 26-Sep 07:45 5 34161 35210 . 36600 -7.53 LB4100l3 Above Beta bkg
  • 26-Sep 08:21 60 2.400 0.091 2.093 +3.92 LB410013 Below Beta eff 26-Sep 07:59 5 17142 17160 17920 -3.14 LB410014 Below Alpha eff 26-Sep 08:09 5 11615 12310 13620 -6.18 LB410014 Below Alpha XTalk 26-Sep 08:09 5 0.187 0.189 0.219 -3.22 LB410014 Below Beta bkg 26-Sep 06:44 60 0.883 0.958 1.734 -3.58 LB410014 need 2nd Beta eff 26-Sep 07:59 .5 20442 20380 21610 -2.70 PIC3A Above Alpha XTalk 26-Sep 11 :15 5 0.267 0.240 0.267 +3.03 PIC3A Below Beta XTalk 26-Sep 06:38 5 9.65E-4 0.011 0.029 -6.55 PIC10A Below Alpha eff 26-Sep 11 :14 5 8812 8854 10610 -3.14 Page 1of2 Page 560of614 PIC10D Below Alpha eff 26-Sep 10:10 5 11812 15350 16570 PIC10D Above Alpha XTalk 26-Sep 1O:10 5 0.771 0.303 0.427 PIC10D Below Beta eff 26-Sep 07:11 5 31169 40190 43320 PIC12B Above Alpha bkg 26-Sep 08:56 60 0.317 5.80E-4 0.380 PIC12C Above Alpha bkg 26-Sep 07:21 60 0.683 0.010 0.413 INSTRUMENTS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS LB4100D1 LB4100D2 LB410003 LB4100D4 PIC6D PIC13C The following detectors may not have properly transferred to the LIMS system Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Reviewed ____________ _ Date __ a_f /_i_& _j f_{p _____ _ GEL Laboratories LLC Page 2 of 2 Page561 of614 -20.40 +19.62 -20.29 '+2.00 +7.03 Gas Flow Proportional Counter Checks for 27-Sep-2016 Detectors LB4100 A1 through J4 and PIC 1A through 140 Short Name Status Parmname Run Time Count CPMor Low Limit High Limit Stdev Time dee LB4100A3 Below Alpha eff 27-Sep 06:17 5 8876 9142 11120 -3.81 LB4*100B2 need 2nd Beta bkg 27-Sep 05:03 60 1.917 0.992 2.051 +2.24 LB4100B3 Above Alpha bkg 27-Sep 05:03 60 0.383 0.121 0.383 +3.00 LB4100C3 Below Alpha eff 27-Sep 06:46 5 5995 6624 9128 . -4.51 LB4100C3. Above Alpha XTalk 27-Sep 06:46 5 0.416 0.248 0.368 +5.36 LB4100C4 Above Beta bkg 27-Sep 05:06 60 13.633 0.686 2.113 +51.42 LB4100E1 Above Beta bkg 27-Sep 05:03 60 8.733 0.637 2.392 +24.68 LB4100E2 Above Beta bkg 27-Sep 05:03 60 3.217 1.061 . 2.316 +7.31 LB4100E3 Above Alpha bkg 27-Sep 05:03 60 0.350 -8.16E-2 0.346 +3.05 LB4100E3 Above Beta_bkg 27-Sep 05:03 60 0.463 2.359 +8.14 LB4100E4 Above Beta bkg 27-Sep 05:03 60 2.417 0.650 2.302* +3.42 LB4100F1 Below Alpha eff
  • 27-Sep 06:59 5 10464 10840 11730 -5.53 LB4100F1
  • Above Alpha XTalk 27-Sep 06:59 5 0.268 0.224 0.265 +3.42 LB4100H4 Below Alpha eff Sep 06:24 5 10622 11490 13890 -5.17 LB4100H4 Above Alpha XTalk 27-Sep 06:24 5 0.418 0.307 0.379 +6.23 LB4100H4 Below Beta eff 27-Sep 06:31 5 34394 35210 36600' -6.52 LB410013 Above Beta bkg 27-Sep .05:03 60 2.450 0.091 2.093 +4.07* LB4100l3 Below Beta eff 27-Sep 06:17 5 17122 17160 17920 -3.30 LB4100l4 Below Alpha eff 27-Sep 06:10 5 11565 12310 13620 -6.41 LB410014 need 2nd Alpha XT alk 27-Sep 06:10 5 0.191 0.189 0.219 *-2.52 LB410014 Below Beta bkg 27-Sep 05:03 60 0.767 0.958 1.734 -4.48 LB410014 Below Beta eff 27-Sep 06:17 5 20345 20380 21610 -3.17 PIC3A need 2nd. Alpha XTalk 27-Sep 05:09 5 0.265 0.240 0.267 +2.75 PIC3A Below Beta XTalk 27-Sep 05:03 5 0.001 0.011 0.029 -6.40 PIC3D Above Alpha bkg 27-Sep 06:30 60 Q.317 -6.75E-2 0.338 +2.69 PIC5B Above Alpha bkg 27-Sep 06:38 60 0.383 0.107 0.374 +3.22 PIC5C Above Alpha bkg 27-Sep 06:39 60 0.350 -1.81E-2 0.382 +2.52 . PIC7D Above Alpha bkg 27-Sep 07:40 60 . 0.383 -1.11E-2 0.349 +3.58 Page 1of2 Page 562of614 PIC10A need 2nd Alpha eff 27-Sep 05:27 5 8986 8854 10610 PIC10A Below Beta eff 27-Sep 05:34 5 44152 44740 53240 PIC10D Below Alpha eff 27-Sep 05:27 5 11828 15350 16570 PIC10D Above AlphaXTalk 27-Sep 05:27 5 0.771 0.303 0.427 PIC1'0D Below Beta eff 27-Sep 05:34 5 31335 40190 43320 PIC11A Above Alpha bkg 27-Sep 07:01 60 0.383 0.029 0.365 PIC12A Above Alpha bkg 27-Sep 07:02 60 0.333 0.067 0.379 PIC12C need 2nd Alpha bkg 27-Sep 05:51 60 0.283 O.o10 0.413 PIC12C need 2nd Beta bkg 27-Sep 05:51 60 0.917 -3.86E-2 2.074 INSTRUMENTS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS LB4100D1 LB4100D2 LB4100D3 LB4100D4 PIC6D PIC13C The following detectors may not have properly transferred to the LIMS system Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, B.eta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk GEL Laboratories LLC Page 2 of 2 Page 563 of 614 -2.55 -3.42 -20.32 +19.62 -19.97 +3.34 +2.12 +1.07 -0.29 Page 564of614 .
  • Background and Efficiency Data a.. (.) a.. (.) a.. (.) 0.33 0.29 0.25 0.22 0.18 0.15 0.11 0.0736 0.0377 0.00174 9690 9520 9360 9190 9030 8870 8700 8540 f--------------------------_,i+-------------------------------+r---2 Sigma 8480 8370 f-+--+_,'-+--+---+-t-+--+_,-+--+---+-t-+--+-f-+--+---,f-+--+--+-+-+---+-f-+--+_,f-+--+_,-+--+---+-t-+--+-f-+--+--+--ill'--3 Sigma 8209 PIC1 OB BETA BKG 1.47 1.33 1.2 1.06 0.92 0.78 0.64 0.51 0.37 0.23 Page 565of614 20370 19980 0.000785 0.000679 0.000469 0.000363 0.000152 e Denotes Outlier Page 566of614 2 a.. u 2 a.. u 0.37 PIC1A ALPHA BKG Generated 09/26/2016 +3 Sigma 0.37 0.33 +2 Sigma 0.3 0.29 0.24 0.2 0.16 0.12 0.0732 0.03045 } J I II.I. r Ji ii "' l\ 1 ! M IT '1 A .. 11 Mean 0.16 -2 Sigma 0.02 -0.0123 -3 Sigma -0.055 10822 10482 10414 10346 1------------------------------ll-l----+++-l'--'--+----ll-------------'"-H!l-"'"-+---2Sigma10300 10278 t--+---+---;t-+--+---+-t-+--+---+-t-+--+---+-+--+---+---;t-+--+---+-+--+---+---;t-+--+---+-t-+--+----;-+--+---+-t-+--+----;-+--+---+---;t-+--+--3 Sigma 10210 *PIC1A BETA BKG 1.95 1.74 1.53 1.32 1.1 0.89 . 0.68 0.47 0.26 0.0479 Page 567 of 614 0.. (.) 0.00118,-----------------------------------------------:----------------+3Sigma00 0.001063 0.00083 0.000714 0.0004809 0.000365 0.000248 0.000132
  • Denotes Outlier Page 568of614 a.. u a.. u a.. u 0.45 PIC1 B ALPHA BKG Generated09/26/2016 ,------------------=--=--=---=--=----------------------------------------*3Sigma0.45 0.4 0.34 t----------------------------------------------------------+2Sigma0.36 0.29 0.24 0.18 0.13 0.0748 0.0213 f----------------------------------------------------------4Slgma00 -0.0322 t--+---t-+--+_,r-+--+-t--+--+-t--+--+-+--+---t-+--+-t--+--+-+--+--t-+--+_,r-+--+-t--+---t-+--+-t--+--+-+--+--+-+--+-.-3 Sigma -0.086 il#ll!!!i#!li!!!illlillllli!illlllt!lff!ill DATE PIC1 B ALPHA EFF 13370 +3 Sigma 13370 13332 +2Sigma13300 13294 13142 v I ! \ ..II ! l I I I A A r\ l 13256 13218 13180 Mean 13180 13104 13066 -2 Sigma 13100 13028 -3Sigma12990 0.28 0.28 0.28 0.28 0.27 0.27 0.27 0.27 PIC1B BETA BKG 2.08 1.87 1.67 1.46 1.25 1.05 0.84 0.64 0.43 r-----------------------------------------------------------2Sigma0.36 0.22 t--t--+-t--+--+-t-+--+--t-+--+--+-t--+--+-t-+--+-t-+--+-t-+--+--t-+--+--+-+--+---+-t-+-+-+--+--+-t--+--+-t-+--+--+-3 Sigma 0.02 Page 569of614 22460 PIC1B BETA EFF Generated 09/2612016 +3 Sigma 22460 22388 -+2 Sigma 22300 22316 22244 a_ 22172 (...) 22100 22028 21956 21884 21812 f I v j J I\ \ A ' .fl II IA v\ I\ II I JV V I Yj I v u " Mean 22100 -2 Sigma 21900 -3 Sigma 21740
  • Denotes Outller Page 570 of 614 0.38 PIC1C ALPHA BKG Generated 0912712016 +3 Sigma 0.38 0.35 +2 Sigma 0.32 0.31 0.27 0... 0.24 u 0.2 0.16 0.13 \ d r j A N A. I I I 'II I\ M Mean 0.2 0.0882 -2 Sigma 0.08 0.0512 -3 Sigm.a 0.01 PIC1 C ALPHA EFF 9980 9910 9840 9770 0.27 0.27 0.26 0.26 0.26 0.26 0.26 0.25 0.25 PIC1C BETA BKG 2.41 2.16 1.9 1.65 1.39 1.13 0... 0.88 u 0.62 0.37 0.11 Page 571of614 a.. (.)
  • Denotes Outlier Page 572of614 0.37 PIC1 D ALPHA BKG Generated 09/26/2016 +3 Sigma 0.37 0.33 +2 Sigma 0.31 0.3 2 0.26 a.. 0.22 u 0.18 0.14 0.11 J II M It 1'11 I h I\ w11 i I l \ I I\ 1) J N Mean 0.18 0.0688 -2 Sigma 0.06 0,03086 -3 Sigma -0.007 PIC1 D ALPHA EFF 11130 +3Sigma11130 11095 +2Sigma11100 11060 11025 2 10990 a.. 10955 u 10920 10885 J "'I 11, J I I I u ) ii 'l J ii vi r l IV v Mean 10960 10850 -2 Sigma 10800 10815 -3 Sigma 10780 0.27 +3 Sigma 0.27 0.27 +2 Sigma 0.26 0.26 0.26 1111!! Ji " ,!I 1 I\ I! .I A l A 1/ u 'I 1 'V I\ N A j '! N I/ 0.26 0.26 Mean026 0.26 0.26 ' 0.25 -2 Sigma 0.25 025 -3 Sigma 0.25 PIC1D BETA BKG 2.09 1.92 1.76 1.6 1.44 2 1.27 a.. 1.11 u 0.95 0.79 0.62
  • Denotes Outlier Page 573 of 614 PIC1D BETA EFF 25760 25619 25478 25055 A I vii \ \ J I' I 25337 25196 24914 24773 24632 24491 e Denotes Outlier Page 574 of 614 v I\/ \1 I ll l--M u Generated 0912612016 +3 Sigma 25760 +2 Sigma 25500 \ Mean 25060 \ -2 Sigma 24600 -3 Sigma 24350 0.36 PIC2A ALPHA BKG Generated09/26/2016 .---------------------------------------------------------41t--+3Sigma0.36 0.32 0.28 0.24 a_ 0.2 (.) 0.16 0.12 0.08107 0.04072 0.000377 f--+--+---l'-+--+---+-f-+--+--+-f--+--+--+-f--+--+---l-+--+---+-+--+--+---lf-+--+---+-f-+--+--+-+--+--+---lf-+--+---+-+--+--+---l-+--+--3 Sigma -0.04 PIC2A ALPHA EFF 11140 -,------------------------------------t._.t-----------------------+3Sigma 11140 11069 10998 10927 10856 a_ 10785 (.) 10714 10643 10572 10501 f--+--+-f--+--+---lf-+--+---l-+--+---+-+--+--+-f--+---+-+--+---+-+--+---+-f--+--+---lf-+--+---l-+--+----lf-+--+----l'-+--+----l-+--+---+--3Sigma10430 PIC2A BETA BKG 1.58 1.41 1.23 1.05 0.88 0.7 a_ 0.52 (.) 0.34 0.17 -0.01089 Page 575of614 53338 52916 0.00571 0.00469 0.00367 ' 0.00265 0,000616 -0.0004034 -0.00244
  • Denotes Outlier Page 576of614 0.38 0.34 0.29 0.25 0.. 0.21 u 0.17 0.13 0.0872 0.0456 PIC2B ALPHA EFF 9220 9070 0.. 8917 u 8770 8620 8470 8320 ::: 0.46 0.44 l---------------------------------------------------------+-+2Sigma0.42 0.42 0.4 0.38 0.36 +---------------------------------------------------------H-Mean0.36 0.34 0.32 0.3 0.28 !l ,§' {? § :.:? & :.:? § l!f f !l ,§' <! § :.:? t; ro of? i<i i<i i<i i<i ra ra ii:' i<i i<i II <!' " " " " " " " " " <:::i c c;::, c " " " " " " " " " DATE PIC2B BETA BKG 1.13 0.. 0.84 U' 0.54 0.25 -0.0452 Page 577 of 614 0.000554 0.000512 0.0004701 0.000428 0.000345 0.0003028 0.000219
  • Denotes Outlier Page 578 of.614 Cl. u Cl. u Cl. u 0.37 PIC3B ALPHA BKG Generated 09/2612016 +3 Sigma 0.37 0.33 +2 Sigma 0.31 0.29 0.26 0.22 0.19 0.15 0.11 Ar In II I I/ I u I u ' ..,, i Mean 0.19 0.07608 -2 Sigma 0.06 0.0397 -3 Sigma 00 13500 13500 13455 13410 13365 13320 13275 13230 13185 13140 13095 0.26 0.25 0.25 025 0.25 025
  • 0.24 0.24 0.24 2.08 1.96 1.85 1.73 1.62 1.5 1.39 1.27 1.16 1.04 +3 Sigma 0.26 +2 Sigma'0.25 I I r \ l v h v \ I WN !! N n ' II Mean 0.25 N j r I i y -2 Sigma 0.24 PIC3B BETA BKG +3 Sigma 2.08 +2 Sigma 1.89 v I\ t ! j ' Mean 1.5 'i u "" I *1 11 11 \ V\ w u v u -2 Sigma 1.12 -3 Sigma 0.93 Page 579of614 PIC38 BETA EFF 21960 21817 21674 21245 1fu! t I n ti A Ii ill i v., I 21531 21388 21102 20959 20816 20673 n ii u N ! .t I\ j 1 Generated 0912612016 +3 Sigma 21960 +2 Sigma 21700 Mean 21250 111/I -2 Sigma 20800 -3 Sigma 20530 0.75 -,--------------------------------------------,---------------+3Sigma0.75 0.6 0.46 t---------------------o+-------------------------------------*2Sigma0.51 0.31 0.17 0.0243+=-===-"""====-======-=====.H."===-=========================-=======Mean 0.02 -0.12 -0.264 -0.409 t----------------------------------------------------------*2Sigma-0.457 -0.553 t-+--+-+-+-+--+--!-+-+--+-t-+--+--!-+-+--+--!-+-+--+-!-+-+--+__,-+--+-+-t-+--+-!-+-+--+__,f-+--+-+-t-+--+__,-+--3 Sigma -0.697
  • Denotes Outlier Page 580 of 614 0.34 PIC3D ALPHA BKG Generated09/26/2016 0.3 0.26 Sigma 0.27 2 0.22 a.. 0.18 (.) 0.14 0.0946 0.05408 0.0136 -0.027 PIC3D ALPHA EFF 10860 10816 10772 1-1111--+------,,---------------.,------------------------------------+2Sigma10800 10728 2 10684 a.. 10840 (.) 10596 10552 10508 10464 l--+-1--+--+-1---l---"-+--+-l--+-1--+---l--l--+---"-+--+-+--+---'1-+--+-+--+l-l-+--+-+--+-1--+---"-+--+---<a--+--"'--+it-+-3Sigma10420 0.27 0.27 0.27 0.26 0.26 0.26 0.25 0.25 0.25 PIC3D BETA BKG 1.37 1.23 1.09 0.95 0.81 2 0.67 a.. 0.54 (.) 0.4 0.26 0.12 Page 581 of 614 a.. (.) 24730 24538 24346 24154 23962 23770 23578 23386 23194 23002 PIC3D BETA EFF .I :\ 1 A !! 111 11 II It\ J II N*u 11 i 11 N Generated 0912612016 +3 Sigma 24730 +2 Sigma 24400 imi Mean 23770 iri -2 Sigma 23100 -3 Sigma 22810 0.00115 f--------------------------------------------------------'---+-2si9maOO 0.000828
  • Denotes Outlier Page 582of614 a.. () a.. () a.. () 0.38 PIC4A ALPHA BKG Generated09/26/2016 .--------------------'----------------------------------------+3Sigma0.38 0.34 0.3 0.25 0.21 0.17 0.13 0,086 0.0439 0.00189 PIC4A ALPHA EFF 10980 10880 10780 10680 10480 10380 10180 0.28 0.28 0.27 0.27 0.27 0.26 0.26 0.26 PIC4A BETA BKG 1.81 1.62 1.43 1.25 1.06 0.87 0.68 0.49 0.3 0.12 Page 583 of 614 PIC4A BETA EFF Generated09/26/2016 55066 54782 52794
  • Denotes Outlier Page 584 of 614 a.. u a.. u a.. u 0.38 0.34 0.3 0.27 0.23 0.19 0.16 0.12 0.08351 0.047 2.24 2.12 1.89 1.77 1.65 1.53 1.41 1.29 1.17 Page 585of614 PIC4B ALPHA BKG I l II r l!!ll'I! ! u PIC4B ALPHA EFF PIC4B BETA BKG I '11
  • Generated 09/26/2016 +3 Sigma 0.38 +2 Sigma 0.31 .I M \ " I\ I\ Ii Mean 0.19 -2 Sigma 0.07 -3 Sigma 0.01 +3 Sigma 2.24 +2 Sigma 2.04 !" w A 1lk1!! 11 u Mean 1.65 II ljl ni1111 II I I i -2 Sigma 1.25 -3 Sigma 1.05 0... u PI C4B BET A E FF Generated 09126/2016 22610,.----------------------------------------------------------+3S!gma22610 22444 22278 f----------------------------------------------------------+2Sigma22300 22112 21946 21614 21448 21282 f--'l----------+-------H-----------ll---+--11------+l-+-+f---+--ll-----+----2 Sigma 21200 21116 f--+---+-+--+-f--t----1-+---+-+--+-f--+---+-+--+-f--+---t-+--+-+--+---1+-+---+-+-_.-le--t----1-+--+-+-Y--f--+----1++--+--3 Sigma 20950 0.00057 +3 Sigma 00 0.0005303 IV +2Sigma00 0.0004908 d r II 1 I/ I \{ I Ill I! n ,r J A1 k I I j' '\ I IJ i\ ,, 0.000451 0.000412 0.0003721 Mean 00 0.000332 0.000293 0.000253 -2 Sigma 00 0.000214 -3 Sigma 00
  • Denotes Outlier Page 586of614 0.37 PIC4D ALPHA BKG Generated 09/2612016 +3 Sigma 0.37 0.34 +2 Sigma 0.31 0.3 2 0.27 a.. 0.23 (.) 0.2 0.16 0.13 0.0919 v Ii ii 1! A ,.., i i 'I .. f l n i II Ill \ 'Ii ' Mean 0.2 -2 Sigma 0.08 l I 0.0568 -3 Sigma 0.02 17340 17272 17204 17136 2 17068 a.. 17000 (.) 16932 16864 16796 l---------+----------------------------------------------------2Slgma16800 16728 t-+--+--+-+--+--+---+-+--+--+---+-+--+--+--+-+--+--+-t-+--+--+-+--+--+---+-+--+--+---+-+--+--+-t-+--+--+-+--+--+--<f--+--+--+-1--3 Sigma 16660 0.27 +3 Sigma 0.27 027 +2 Sigma 0.27 0.26 \ ' I!/ I I \ If. j I .I M I w I L,i 1J . I !! f i \ v I ' Ni '\ 0.27 0.27 0.26 0.26 Mean 0.26 0.26 0.26 -2 Sigma 0.26 0.26 -3 Sigma 0.26 PIC4D BETA BKG 2.49 2.28 2.08 1.87 1.67 2 1.47 a.. 1.26 (.) 1.06 0.85 0.65 111111111.1111111111111111111111111111111 DME . Page 587of614 0... () DATE PIC4D BETA EFF Cross Talk 0.0114 0.01036 0.'00836 0.00736 0.00537
  • Denotes Outlier Page 588 of 614 0.37 0.35 PIC58 ALPHA BKG Generated 09/2612016 +3 Sigma 0.37 \ rr +2 Sigma 0.33 0.32 0.29 a.. 0.27 u 0.24 0.21 0.19 ! 0 ! n Ir f ! 11 I ll I IU II .l 11 ,t* I N Mean 0.24 0.16 -2 Sigma 0.15 0.13 : -3 Sigma 0.11 PIC58 ALPHA EFF 13950 13893 13836 13779 13722 a.. 13665 u 13608 13551 13494 13437 0.27 0.26 0.26 0.26 0.26 0.26 0.26 026 0.26 PIC5B BETA BKG 1.47 1.31 1.15 0.99 0.82 0.66 Mean 0.66 a.. 0.5 u 0.34 0.18 f----------------------------------------------------------*2Sigma0.12 0.0141 Page 589of614 PICSB BETA EFF Generated09/26/2016 23110*----------------------------------------------------------+3Sigma23110 23032 22642 22564 22408 l--+--+-IC--Ht+-l-+--+--l-+--+--l-+--+--+-+--+--+-IC-+--+--1-+--+--+-+--+--+-+--+--+-t--+--+-r--+--+-IC-+--+-IC-+--+---+-3 Sigma 22330
  • Denotes Outlier Page 590of614 Cl.. 0 Cl.. 0 Cl.. 0 0,38 PIC5C ALPHA BKG Generated 09/2612016 +3 Sigma 0.38 0,34 +2 Sigma 0.32 0.3 0.26 0.22 0.18 0.14. 0.1 J I! 1m1 ! A 1! II 11 ijp 'l\ l: I I" Mean 0.18 0.06201 -2 Sigma*o.os 0.022 -3 Sigma -0.018 PIC5C ALPHA EFF 10690 10629 10568 10507 10446 10385 10324 10263 10202 10141 , , zy zy zy c c c c .& & e & & e & & & § § DATE P!C5C ALPHA EFF Cross Talk 0.26 ,-------------,------------------------------------------------.-+3Sigma0.26 0.26 0.26 t----+-:+--+---------------t----+-----------+-----+-----------------++2Sigma 0.26 0.26 0.26 0.25 025 0.25 Sigma 0.25 0.25 t--+---+-+--+---+-+--+---+-+--+---+-+--+---+-+--+---1---1+--+--t--+---+-+--+---+-+--+---+-+--+---1-+--+-f-+--+--f--+---+-<._-+---+--3 Sigma 0.25 PIC5C BETA BKG. ,----.--:----------------.,--------------------------------.---------,-+3Sigma 1.87 1.87 1.67 1.47 1.26 1.06 0.86 0.66 0,45 0.25 0.04804 Page 591of614
?! a.. (.)
  • Denotes Outlier Page 592of614 0.36 PICSD ALPHA BKG Generated 09/2612016 +3 Sigma 0.36 0.33 +2 Sigma 0.31 0.29 0.26 a.. 0.22 u 0.19 0.15 0.12 \"' ! AN 1 1"/\1 11 l 1 I\ 1111@1\I ii \ / v I !j" I Mean 0.19 0.0799 -2 Sigma 0.07 0.0443 -3 Sigma 0.01 PICSD ALPHA EFF 11610 11494 11378 11262 11146 a.. 11030 u 10914 10798 10682 10566 0.21 0.27 0.25 Sigma 0.25 2.07 1.87 1.66 1.46 1.25 1.05' a.. 0.84 (.) 0.63 0.43 0.22 Page 593of614 a.. u
  • Denotes Outlier Page 594of614 0.37 PICBA ALPHA BKG Generated 0912612016 +3 Sigma 0.37 0.34 +2 Sigma 0.32 0.31 2 0.28 a.. 0.24 (.) 0.21 0.18 0.15 If \ 1 II, -I rrl n ! I Np I\ I y Mean 0.21 0.12 -2 Sigma 0.11 0.08604 -3 Sigma 0.05 11320 11276 11232 11188 2 11144 a.. 11100 (.) 11056 11012 10968 10924 PICBA BETA BKG 1.59 +3 Sigma 1.59 1.47 +2 Sigma 1.39 M ii rl '\I fu r! ' Jill , 'Vi !\ I if r ' qrr 'I I I u fl' l v 1.35 1.23 '1.11 2 0.99 a.. *0.87 (.) 0.75 Mean 0.99 0.63 -2 Sigma 0.59 0.51 -3 Sigma.0.39 Page 595 of 614 a.. () 55669 55438 55207 54976 54514 54283 0,00137 0.00121 0.0009007 0.000745 0.0004341
  • Denotes Outlier Page 596of614 0.4 PIC8D ALPHA BKG Generated09/26/2016 0.36 0.32 r-------------------------------------------------------"T"'l-+-t-+2Sigma0.33 0.28 0... 0.24 () 0.2 0.16 0.12 0,08311 0.0433 18050 17888 17726 17564 17402 0... 17240 () 17078 16916 16754 16592 0.28 0.28 . 0.25 t--+---l-+--+-l--+---l-+--+--r--+---+-+--+--r--itl--f-+--+--1--+---f-+--+--r--+---+-+--+--l--+---l-+--+-t--+---l-+--+--r--+--3 SiQma 0.25 PICBD BETA BKG 2.73 .----------------------------------------------------------*3Slgma2.73 2.42 2.11 1.81 1.5 1.19 0... 0.89 () 0.58 0.27 t----------------------------------------------------------*2Sigma0.17 -0.0341' t-+--+---l--l+--+---l-+--+--+-l-+--+--if-+--+--if-+--+--li--+--+---l-+--+--+-t-+--+-l-+--+-l-+--+-f-+--+--if-+--+---l-t--+---3Sfgma-0.341 Page 597of614 a_ u
  • Denotes Outlier Page 598of614 0.38 PIC9A ALPHA BKG Generated 09126/2016 +3 Sigma 0.38 0.34 +2 Sigma 0.31 0.3 0.27 a_ 0.23 (.) 0.19 0.15 0.12 1! ! 11 wi! !I ! I I \ 'i 11 n J\ l v Mean 0.0783 -2 Sigma o.07 0.04093 -3 Sigma 00 PIC9A ALPHA EFF 11100 11038 10976 10914 10852 a_ 10790 (.) 10728 10666 10604 10542 0.32 -r---------------------------------------------------------....-+3Sigma0.32 0.31 ,_ ____ _,,__ __________________________________________________ .,,_+2Sigma0.31 0.3 0.3 0.29 0.28 0.27 0.27 0.26 t-+--+--+-t--+--+--+-t--+--+--+-t--+--+--+-+--T---+-t--+--+--+-+--+--+--+-+--T---+--+t-+--+--+-+--+--+--+-+--T---+--+t-+--T---+-t--3 Sigma 0.26 PIC9A BETA BKG 1.74 +3 Sigma 1.74 1.57 +2Sigma 1.46 1.4 1.24 1.07 0.9 a_ 0.74 (.) 0.57 0.41 1l T TI ! iJ rvp1 I '\I i Mean 0.91 -2 Sigma 0.35 0.24 -3 Sigma 0.07 Page 599of614 PIC9A BETA EFF Generated09/26/2016 217901,-----------------------------------------------------------+3S!gma21790 0.. u 21690 20890
  • Denotes Outlier f-+--+-f-+--+-f-+--+_,_,+--+_,_,+--+_,-+--+--+-+--+--+-+-+--+-f-+--+-f-+--+_,f-+--+_,'--+--+-j-+--+---l-+--+---l._-3 Sigma 20790 Page_600of614 0.36 PIC9C ALPHA BKG Generated 09126/2016 +3 Sigma 0.36 0,33 +2 Sigma 0.3 0,29 0.25 a.. 0.21 () 0.17 0.13 J l n/ 1lli1 A ! ' I I ' M ,,. di I! N II ! II w I Mean 0.17 0.0917 0.0527 -2 Sigma 0.04 0.0137 --3 Sigma -0.025 10420 10400 10300 10200 10100 a.. 10100 () 10000 9940 9880 9810 0.27 0.27 0.26 0.26 0.26 0.25 0.25 0.25 0.24 PIC9C BETA BKG 1.76 1.59 1.42 1.25 1.08 0.91 a.. 0.74 () 0.57 0.4 0.24 Page 601 of 614 a.. (.)
  • Denotes Outlier Page 602 of 614 0.37 PIC9D ALPHA BKG Generated 09/26/2016 +3 Sigma 0.37 0.33 +2 Sigma 0.31 0.3 2 0.26 c.. 0.23 (.) 0.19 0.16 0.12 I ff II l!n I II !1 ' I I y l J f J Mean 0.19 0.085008 -2 Sigma 0.07 0.0497 -3 Sigma 0.01 PIC9D ALPHA EFF 11110 11070 11030 10990 2 10950 c.. 10910 (.) 10870 10830 10790 10750 0.28 +3 Sigma 0.28 0.27 I +2 Sigma 0.27 0.27 I n n .! U1 j ' v 1J\ ' 1/ fl I ,J N v 0.27 0.27 0.27 Mean 0.27 0.26 0.26 0.26 -2 Sigma 0,26 0.26 -PIC9D BETA BKG 2.01 1.83 1.65 1.47 1.29 2 1.11 c.. 0.93 (.) 0.75 0.57 0.39 Page 603of614 25920 PIC9D BETA EFF Generated 09/2612016 +3 Sigma 25920 25821 , +2 Sigma 25700 25722 :2! 25623 a.. 25524 () 25425 25326 25227 J j I } i 1J ! ! ,/ rl ,, I " i 11 W\ Ir A JI I\ I i Mean 25420 25128 -2 Sigma 25100 25029 -3 Sigma 24930 e Denotes Outlier Page 604of614 Page 605of614 RAD Standards Traceability gff(._, \a Eckert & Ziegler -Analytics Customer: P.O. No.: CERTIFICATE OF CALIBRATION Standard Radionuclide Source 78352-278 Sr-90 10 mL Liquid in Flame Sealed Vial General Engineering Labs/Charleston, SC 7312 RD, Item 3 1380 Seaboard Industrial Blvd. Atlanta, (;eorgla ::1031 B Tel 404*352*8677 Fax 404*352*2837 www.analyticsinc.com This standard radionuclide source was prepared gravirnetrically from a calibrated master solution. The master solution was calibrated by liquid scintillation counting. Radionuclide purity and calibration were checked by germanium gamma-ray spectrometry and liquid scintillation counting. The nuclear decay rate and assay date for this s.ource are given below. ANALYTICS maintains traceability to the National Institute of Standards and Technology through Measurements Assurance Programs as described in USNRC Reg. Guide 4.15, Revision 1. Isotope: Activity (Bq): Half-Life: Sr-90 3.856 E5 28.79 years Calibration Date: October 1, 2008 12:00 EST Comments: Relative Expanded Uncertainty. (k=2): Impurities: y-impurities <0.1 % 1.7% 10.41484 grams 0. lM HCl solution with 30 Sr carrier. NOTE: This source also contains Y-90 in secular equilibrium with Sr-90. The Y-90 activity is equal to the Sr-90 activity. Since Sr-90 and Y-90 both decay 100% by beta emission, the total beta emission rate for the source is twice the certified Sr-90 activity. The half-life for Y-90 is 64.08 hours9.259259e-5 days <br />0.00222 hours <br />1.322751e-5 weeks <br />3.044e-6 months <br />. ' Source Prepared By: f1/ ./"-"" ' . QA Approved: W. Mao, Radiochemist A-lr!--1 Date: /

Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Parent Code: 1243 Prepared By: Daniel Roy Prepared By: Daniel Roy Prep Date: 12/19/2008 Carrier Cone: O.lMHCL Verification Date: 09/27/2016 Reference Date: 10/01/2008 Expiration D_ate: 09/27/2017 Ampoule Mass (g): 10.41484 g Primary Code: 1243-A Uncertainty: +!-.85 % Dilution(mL): lOOmL LogBookNo: RC-S-048-124 Mass of Parent(g): 10.2164 g Derisity(g/mL): 0.9991 Balance ID: 38080204 Calculations Converting parent activity to dpm/mLjdpm/g (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (Bq)) *.(conversion dpm to Bq) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity (dpm/g) (10.2164 g) * (385600 Bq) * (60 dpm/Bq) I (10.41484 g

  • 100 mL) = 226951.7634 dpm/mL . (10.2164 g) * (385600 Bq) * (60 dpm/Bq) I ( 0.9991 g/mL)/ (10.41484 g
  • 100 mL) = 227146.2010 dpm/g Secondary Standards Prep Date Preparer Mass Dilution Code Concdpm/mL Verification Expiration Primary (mL) Date Date 01/21/2010 Bethany 2.2467 1000 1243-B 510.329369 01/21/2010 01/21/2011 Fiem dpm/mL 08/03/2010 Bethany 2.5604 1000 1243-C 581.5851 08/03/2010 08/03/2011 Fiem dpm/mL Bethany.-566.6389 01/12/2011 Fi em 2.4946 1000 1243-D dpm/mL 01/12/2011 01/12/2012 08/12/2011 Tim 3.3115 100 1243-G 18.7877 03/26/2014 03/25/2015 Chandler dpm/mL 08/17/2011 Tim 2.5541 100 1243-H 14.49064 03/26/2014 03/25/2015 Chandler dpm/mL 06/21/2011 Tim .0235 100 1243-E 53.37936 03/19/2014 06/20/2014 Chandler dpm/mL 07/05/2011 Bethany 2.6072 1000 1243-F 592.2156 07/05/2011 07/05/2012 Fi em dpm/mL 01/31/2012 Gregory 2.6792 1000 1243-I 608.5701 01/31/2012 01/31/2013 Ramsay dpm/ml Page 607of614 08/29/2012 Bethany Fiem 02/12/2013 Gregory Ramsay 12/04/2013 Gregory Ramsay 08/11/2014 Gregory Ramsay 05/06/2015 Gregory Ramsay 12/18/2015 Gregory I Ramsay 08/30/2016 Christina Kimball 09/27/2016 Bethany Fiem GEL Laboratories LLC Version 1.0 9/18/2000
  • Page 608of614 2.6799 1000 2.'6526 1000 2.5347 1000 2.7006 1000 2.5102 1000 2.5762 1000 .068 250 2.6337 1000 1243-J 608.729104 09/14/2012 09/11/2013 dpm/mL 1243-K 602.528 01/15/2014 01/15/2015 dpm/ml 1243-L 575.747476 12/04/2013 12/04/2014 dpm/ml 1243-M 613.431 08/12/2014 08/12/2015 dpm/mL 1243-N 570.1824 05/06/2015 05/06/2016 dpm/mL 1243-0 585.174 12/18/2015 12/18/2016 dpm/mL 1243-P 61.7838 09/07/2016 09/07/2017 dpm/mL 1243-Q 598.235 09/27/2016 09/27/2017 dpm/mL Verification for Sr-90 Standard 1243-0 v1.0.2 Instrument BLUE Analvst BXF1 Verification Prep Date 12/18/2015 Standard Information Quench Gross Bkg dpm/mL 509.17 2.755468033 Isotope Serial Number Isotope Halflife Reference. Date Ref. Act. (DPM/mL) Amount of Std. (ml) Standard Prep Date Sr-90 Std # Count Date 1243-0 1 12/30/2015 28.9000 y 2 12/30/2015 10/1/2008 3 12/30/2015 585.174 1.0 Net 12/18/2015 Std # cpm 1 1033.40 2 1023.00 3 1024.80 Verification Rules Number cpm 88.50 1073.20 90.20 1062.80 89.60 1064.60 Calculated Standard Avg. Eff. dpm/ml 2.017144 512.31 2.017144 507.15 2.017144 508.04 cpm 39.80 39.80 39.80 Measured. dpm 512.31 507.15 508.04 Mean Value= Stdev= Certificate.Value*= Two sigma= 10 %of Mean= Rule A (Pass/Fail) % Recovery Rule B (Pass/Fall) Expiration Date Rule A = The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. . Rule B = The determined mean value shall be within 5% of the certificate value.
  • Value is decay corrected to Count Date. 491.8 5.511 50.917 Pass 103.52% Pass 12/18/2016 The analyst prepared three standard verification sources for Sr-90 source 1243-0 by transferring 1 ml portions of the standard into glass liquid scintillation vials. 10 ml of Ecoscint Ultra liquid scintillation cocktail was added to each vial and the vials were shaken to mix. A Blank vial was prepared in a similar fashion using 1 o ml of Ecoscint Ultra liquid scintillation cocktail. *The standard verification vials and background source were dark adapted for at least two hours and counted on LSCBLUE for_ Sr-90 source standard verification. The Sr-90 efficiency calibration which was used for verification calculations was. performed on 12/18/2015 using Sr-90 source 1244-A.
  • Standard results for each verification source was calculated as follows: RAD-M-001 Source dpm/mL = (A -B)/(C)(D) where: A = Ver. source cpm, B BKGcpm, C System efficiency (cpm/dpm), and D volume used for standard verification.

-. 9 Eckert & Ziegler Analytics Customer: GEL Labs, LLC P.O. No.: 7344 RD, Item 1 CERTIFICATE OF CALIBRATION Standard Radionuclide Source 82898-278 5 mL Liquid in Flame Sealed Vial 1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 Tel 404*352*8677 Fax 404*352*2837 www.analyticsinc.com This standard radionuclide source was prepared gravimetrically from a master solution, calibrated by Eckert & Ziegler Analytics. The master solution was calibrated by liquid scintillation counting. Radionuclide purity and calibration were checked by germanium gamma-ray spectrometry and liquid scintillation counting. The nuclear decay rate and reference date for this source are given below. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of Standards and Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15, Revision 1, February, 1979, and compliance with ANSI N42.22-1995, "Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for the production of NIST-traceable sources, and this source was produced in accordance with the HPS accreditation requirements. Customers may report any concerns with the accreditation program to the HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA 2210 I. Uncertainty* , % Half-Life, Activity . Type Reference Date Isotope Days (Bq) UA Us u (12:00 PM EST) Th-230 2.753E+0.7 3.942E+04 0.1 0.9 1.8 07/29/2010 *Uncertainty: U -Relative expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines for Evaluating and Expressing the Uncert<ilnty of NIST Mea5urement Results." Comments: Impilrities: r-impurities < 0.1 %, a-impurities< 0.04 %. 5.10422 grams 0.5M HN03 solution. h/L--.,,,,..--Source Prepared W. Mao, Radiochemist QA Approved: Single Isotope Certificate, Rev 1 9/28/2009 Corporate Office Date: -:J. ... ... JfJ RC.-S* O(.,o-o'-10 Laboratory Page 610 Valencia, California 91355 1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318 Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Thorium-230 Parent Code: 1493 Prepared By: Bethany Fiem Prepared By: Gregory Ramsay Prep Date: 06/24/2015 Carrier Cone: 0.5MHN03 Verification Date: 09/2712016 Reference Date: 07/29/2010 Expiration Date: 09/2712017 Ampoule Mass (g): 5.10422 g Primary Code: 1493-A Uncertainty: +/-1.8 % Dilution(mL): IOOmL LogBookNo: RC-S-060-040 Mass of Parent(g): 5.0802 g Density(g/mL): 1.0011 Balance ID: 38080204 Calculations Converting parent activity to dpm/mLldpm/g (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity (dpm/g) (5.0802 g) * (39420 Bq) * (60 dpm/Bq) I (5.10422 g

  • 100 mL) = 23540.6958 dpm/mL (5.0802 g) * (39420 Bq) * (60 dpm/Bq) I ( 1.0011 g/mL)/ (5.10422 g
  • 100 mL) = 23515.7691 dpm/g Prep Date Preparer 06/24/2015 Bethany Fiem 09/27/2016 Bethany Fiem GEL Laboratories LLC Version 1.0 9/18/2000 Page 611 of 614 Mass Primary 11.3156 11.4091 Secondary Standards Dilution Code Cone Verification Expiration (mL) dpm/mL Date Date 1000 1493-B 266.095 06/08/2016 06/08/2017 dpm/mL 1000 1493-C 268.294 09/27/2016 09/27/2017 dpm/mL Verification for th-230 Standard 1493-B v1.0.2 Instrument BLUE Analvst TC1 Verification Prep Date 6/8/2016 Standard Information Quench Gross Bkg dpm/mL Isotope Serial Number Isotope Halflife Reference Date Ref. Act. (DPM/ml) Amount of Std. (mll Standard Prep Date Th-230 Std# Count Date Number cpm cpm Mean Value= 1493-B 1 6/8/2016 95.10 312.60 38.67 Stdev= 7.5380E+04 Y 2 6/8/2016 95.30 306.40 38.67 7/29/2010 3 6/8/2016 95.20 312.20 38.67 Certificate Value* = 266.095 Two sigma= 1.0 Net Ca.lculated Standard Measured 10%of Mean= 6/24/2015 Std# cpm Avg. Eff. dpm/ml dpm Rule A (Pass/Fail) 1 273.93 1.007294 271.95 271.95 % Recovery 2 267.73 1.007294 265.79 265.79 Rule B (Pass/Fail) 3 273.53 1.007294 271.55 271.55 Expiration Date Verification Rules Rule A= The two sigma value used for the 95% confidence interval shall not exceed 10% of the inean value of the three verification measurements. Rule B =The determined mean value shall be within 5% of the certificate value. " Certificate Value is decay corrected to Count Date. 269.76 3.444745088 266.1 6.889 26.976 Pass 101.38% Pass 6/8/2017 The analyst prepared three standard verification sources for Th-230 source 1493-B by transferring 1 ml portions of the standard into glass liquid scintillation vials. 1 O ml of Ecoscint Ultra liquid scintillation cocktail was added to each vial and the vials were shaken to mix. A Blank vial was prepared in a similar fashion using 1 o ml of Ecoscint Ultra liquid scintillation* cocktail. The standard verification vials and background source were dark adapted for at least two hours and counted on LSCBLU E for Th-230 source standard verification. The Th-230 efficiency calibration which was used for verification calculations was performed on 6/8/2016 using Th-230 source 1759-A.
  • Standard results for each verification source was calculated as follows: RAD-M-001 Source dpm/ml = (A -B)/(C)(D) where: A B c D Ver. source cpm, BKGcpm, . System efficiency (cpm/dpm), and volume used for standard verification.

Runlogs Page 613of614.

Instrument Run Log Instrument Type: GFPC Batch ID: 1597819 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 1203625471 MB JXC9 PIC48 SEP-26-16 13:58:44 DONE 2 inch Planchett 01-DEC-15 00:01 1203625475 LCS JXC9 PIC9A SEP-26-16 13:58:4 7 DONE 2 inch Planchett 01-DEC-15 00:01 12036254 73 MS Jxc9* PIC1A SEP-26-16 13:58:52 DONE 2 inch Planchett 01-DEC-15 00:01 1203625472 DUP JXC9 PIC58 SEP-26-16 13:58:54 DONE 2 inch Planchett 01-DEC-15 00:01 405245001 SAMPLE JXC9 PIC8D\ SEP-26-16 13:58:58 DONE 2 inch Planchett 01-DEC-15 00:01 405245002 SAty1PLE JXC9 PIC4D SEP-26-16 13:59:01 DONE 2 inch Planchett 01-DEC-15 00:01 405245003 SAMPLE JXC9 PIC1D SEP-26-16 13:59:05 DONE 2 inch Planchett 01-DEC-15 00:01 405245004 SAMPLE JXC9 PIC9C SEP-26-16 13:59:09 DONE 2 inch Planchett 01-DEC-15 00:01 405245005 SAMPLE JXC9 PIC3D SEP-26-16 13:59:10 DONE 2 inch Planchett 01-DEC-15 00:01 405245006 SAMPLE JXC9 PIC1C SEP-26-16 13:59:15 DONE 2 inch Planchett 01-DEC-15 .00:01 405245010 SAMPLE JXC9 PIC8A SEP-26-16 13:59:17 DONE 2 inch Planchett 01-DEC-15 00:01 405245007 SAMPLE JXC9 PIC2B SEP-26-16 13:59:19 DONE 2 inch Planchett 01-DEC-15 00:01 405245008. SAMPLE JXC9 PIC3B SEP-26-16 13:59:25 DONE 2 inch Planchett 01-DEC-15 00:01 405245009 SAMPLE JXC9 . PIC2A SEP-26-16 13:59:30 DONE 2 inch Planchett 01-DEC-15 00:01 405245011 SAMPLE JXC9 PIC1B SEP-26-16 13:59:35 DONE 2 inch Planchett 01-DEC-15 00:01 405245013 SAMPLE JXC9 PIC5D SEP-26-16 13:59:41 DONE 2 inch Planchett 01-DEC-15 00:01 405245015 SAMPLE -JXC9 PIC5C SEP-26-16 13:59:57 DONE 2 inch Planchett 01-DEC-15 00:01 405245016 SAMPLE JXC9 PIC4A SEP-26-16 14:00:01 DONE 2 inch Planchett 01-DEC-15 00:01 405245012 SAMPLE JXC9 PIC9D SEP-26-16 14:04:16 DONE 2 inch Planchett 01-DEC-15 00:01 405245014 SAMPLE JXC9 PIC10B SEP-26-16 14:04:25 DONE 2 inch Planchett 01-DEC-15 00:01 1203625474 MSD JXC9 PIC1C SEP-27-16 10:14:36 DONE 2 inch Planchett 01-DEC-15 00:01 Page 614of614

Retrieved from "https://kanterella.com/w/index.php?title=ML16364A068&oldid=667444"