ML18331A012

Restoration Project, FSS Final Report - Phase 1. FSS Release Record, South Beach Area Survey Unit 10224

ML18331A012
Person / Time
Site:	Zion  File:ZionSolutions icon.png
Issue date:	03/28/2018
From:	Yetter R F ZionSolutions
To:	Office of Nuclear Material Safety and Safeguards
Shared Package
ML18331A015	List: ML18331A003 ML18331A004 ML18331A005 ML18331A006 ML18331A007 ML18331A008 ML18331A009 ML18331A010 ML18331A011 ML18331A012 ML18331A013 ZS-2018-0093, Submittal of Final Status Survey (FSS) Final Report - Phase 1
References
ZS-2018-0093
Download: ML18331A012 (199)

Text

=ZION SOLUTIONS LLC-An E n ergySolutions Company FSS RELEASE RECORD SOUTH BEACH AREA SURVEY UNIT 10224 PREPARED BY /DATE: REVIEWED BY/ DATE: APPROVED BY I DATE: [1] =ZlON SOLUTIONS~ M Et~*o,~*~IPIS~ (I) !. zo,g

(1)Based on maximum percent of total activity from Table 20 of TSD 14-019, normalized to one for the dose significant radionuclides. (2)Does not include dose significant radionuclides for activated concrete (H-3, Eu-152, Eu-154).

Table 3 - Base Case DCGLs for Surface Soils (BcDCGL SS) Table 4 - Base Case DCGLs for Subsurface Soils (BcDCGL SB)

Table 5 - Operational DCGLs for Surface Soils (OpDCGL SS) Table 6 - Operational DCGLs for Subsurface Soils (OpDCGL SB)

Table 7 - Surrogate Ratios

Table 8- Action Levels for Survey Unit L310219B

1: Ni-63 and Sr-90 are inferred concentrations using the maximum HTD ratio.

44-10 PR316938 293136 10224 GS007 4/21/2016 9:02 4480 3918 5121 No 44-10 PR316938 293136 10224 GS007 4/21/2016 9:02 4280 3918 5121 No 44-10 PR316938 293136 10224 GS007 4/21/2016 9:03 4530 3918 5121 No 44-10 PR316938 293136 10224 GS007 4/21/2016 9:03 4290 3918 5121 No 44-10 PR316938 293136 10224 GS007 4/21/2016 9:04 4530 3918 5121 No 44-10 PR316938 293136 10224 GS007 4/21/2016 9:04 3800 3918 5121 No 44-10 PR320649 304726 10224 GS014 6/2/2016 10:42 3270 2973 3556 No 44-10 PR320649 304726 10224 GS014 6/2/2016 10:46 3200 2973 3556 No 44-10 PR320649 304726 10224 GS011 6/2/2016 13:34 3090 2850 3420 No 44-10 PR320649 304726 10224 GS011 6/2/2016 13:35 3320 2850 3420 No 44-10 PR320649 304726 10224 GS011 6/2/2016 13:36 2890 2850 3420 No 44-10 PR320649 304726 10224 GS011 6/2/2016 13:37 3380 2850 3420 No 44-10 PR320649 304726 10224 GS011 6/2/2016 13:39 3410 2850 3420 No 44-10 PR320649 304726 10224 GS011 6/2/2016 13:42 3350 2850 3420 No 44-10 PR320649 304726 10224 GS011 6/2/2016 13:45 3060 2850 3420 No 44-10 PR321892 304708 10224 GS001 6/2/2016 9:34 3040 2514 3050 No 44-10 PR321892 304708 10224 GS001 6/2/2016 9:35 2840 2514 3050 No 44-10 PR321892 304708 10224 GS001 6/2/2016 9:37 2850 2514 3050 No 44-10 PR321892 304708 10224 GS001 6/2/2016 9:38 2850 2514 3050 No 44-10 PR321892 304708 10224 GS001 6/2/2016 9:40 2930 2514 3050 No 44-10 PR321892 304708 10224 GS002 6/2/2016 9:46 2420 2514 3050 No 44-10 PR321892 304708 10224 GS002 6/2/2016 9:48 2490 2514 3050 No 44-10 PR321892 304708 10224 GS002 6/2/2016 9:50 2460 2514 3050 No 44-10 PR321892 304708 10224 GS002 6/2/2016 9:51 2340 2514 3050 No 44-10 PR321892 304708 10224 GS002 6/2/2016 9:53 2410 2514 3050 No 44-10 PR321892 304708 10224 GS003 6/2/2016 10:19 4090 3590 4231 No 44-10 PR321892 304708 10224 GS003 6/2/2016 10:21 3480 3590 4231 No 44-10 PR321892 304708 10224 GS003 6/2/2016 10:23 3450 3590 4231 No 44-10 PR321892 304708 10224 GS003 6/2/2016 10:25 2710 3590 4231 No 44-10 PR321892 304708 10224 GS003 6/2/2016 10:28 2440 3590 4231 No 44-10 PR321892 304708 10224 GS003 6/2/2016 10:29 2380 3590 4231 No 44-10 PR321892 304708 10224 GS004 6/2/2016 10:33 3660 3590 4231 No 44-10 PR321892 304708 10224 GS004 6/2/2016 10:36 3750 3590 4231 No 44-10 PR321892 304708 10224 GS004 6/2/2016 10:37 3590 3590 4231 No

44-10 PR321892 304708 10224 GS004 6/2/2016 10:39 3680 3590 4231 No 44-10 PR321892 304708 10224 GS004 6/2/2016 10:40 3600 3590 4231 No 44-10 PR321892 304708 10224 GS004 6/2/2016 10:41 3480 3590 4231 No 44-10 PR321892 304708 10224 GS004 6/2/2016 10:43 3780 3590 4231 No 44-10 PR321892 304708 10224 GS004 6/2/2016 10:45 3710 3590 4231 No 44-10 PR321892 304708 10224 GS005 6/2/2016 12:43 2990 3590 4231 No 44-10 PR321892 304708 10224 GS005 6/2/2016 12:44 3030 3590 4231 No 44-10 PR321892 304708 10224 GS005 6/2/2016 12:46 3080 3590 4231 No 44-10 PR321892 304708 10224 GS005 6/2/2016 12:47 2910 3590 4231 No 44-10 PR321892 304708 10224 GS005 6/2/2016 12:49 2810 3590 4231 No 44-10 PR321892 304708 10224 GS005 6/2/2016 12:50 2890 3590 4231 No 44-10 PR321892 304708 10224 GS006 6/2/2016 12:53 2910 3590 4231 No 44-10 PR321892 304708 10224 GS006 6/2/2016 12:55 2900 3590 4231 No 44-10 PR321892 304708 10224 GS006 6/2/2016 12:56 2820 3590 4231 No 44-10 PR321892 304708 10224 GS006 6/2/2016 12:58 3060 3590 4231 No 44-10 PR321892 304708 10224 GS006 6/2/2016 12:59 3180 3590 4231 No 44-10 PR321892 304708 10224 GS007 6/2/2016 13:01 3680 3590 4231 No 44-10 PR321892 304708 10224 GS007 6/2/2016 13:03 4030 3590 4231 No 44-10 PR321892 304708 10224 GS007 6/2/2016 13:04 3840 3590 4231 No 44-10 PR321892 304708 10224 GS007 6/2/2016 13:06 3120 3590 4231 No 44-10 PR321892 304708 10224 GS007 6/2/2016 13:07 2970 3590 4231 No 44-10 PR321892 304708 10224 GS008 6/2/2016 13:10 3000 3590 4231 No 44-10 PR321892 304708 10224 GS008 6/2/2016 13:12 3050 3590 4231 No 44-10 PR321892 304708 10224 GS008 6/2/2016 13:13 2930 3590 4231 No 44-10 PR321892 304708 10224 GS008 6/2/2016 13:14 2900 3590 4231 No 44-10 PR321892 304708 10224 GS008 6/2/2016 13:16 2760 3590 4231 No 44-10 PR321892 304708 10224 GS009 6/2/2016 13:18 3280 3590 4231 No 44-10 PR321892 304708 10224 GS009 6/2/2016 13:19 3760 3590 4231 No 44-10 PR321892 304708 10224 GS009 6/2/2016 13:20 3650 3590 4231 No 44-10 PR321892 304708 10224 GS009 6/2/2016 13:22 3410 3590 4231 No 44-10 PR321892 304708 10224 GS009 6/2/2016 13:23 3380 3590 4231 No 44-10 PR321892 304708 10224 GS009 6/2/2016 13:25 3340 3590 4231 No 44-10 PR321892 304708 10224 GS014 6/2/2016 13:28 2980 3590 4231 No 44-10 PR321892 304708 10224 GS014 6/2/2016 13:29 2930 3590 4231 No

44-10 PR321892 304708 10224 GS014 6/2/2016 13:31 3300 3590 4231 No 44-10 PR321892 304708 10224 GS014 6/2/2016 13:32 2900 3590 4231 No 44-10 PR321892 304708 10224 GS014 6/2/2016 13:35 2660 3590 4231 No 44-10 PR321892 304708 10224 GS010 6/2/2016 13:40 2570 2514 3050 No 44-10 PR321892 304708 10224 GS010 6/2/2016 13:41 2300 2514 3050 No 44-10 PR321892 304708 10224 GS010 6/2/2016 13:43 2220 2514 3050 No 44-10 PR321892 304708 10224 GS010 6/2/2016 13:44 2250 2514 3050 No 44-10 PR321892 304708 10224 GS010 6/2/2016 13:46 2210 2514 3050 No 44-10 PR321892 304708 10224 GS010 6/2/2016 13:47 2170 2514 3050 No 44-10 PR321892 304708 10224 GS010 6/2/2016 13:49 2220 2514 3050 No 44-10 PR321892 304708 10224 GS010 6/2/2016 13:49 2190 2514 3050 No 44-10 PR311756 266669 10224 GS012 6/2/2016 10:34 2670 2440 2968 No 44-10 PR311756 266669 10224 GS012 6/2/2016 10:35 2780 2440 2968 No 44-10 PR311756 266669 10224 GS012 6/2/2016 10:37 2640 2440 2968 No 44-10 PR311756 266669 10224 GS012 6/2/2016 10:38 2660 2440 2968 No 44-10 PR311756 266669 10224 GS012 6/2/2016 10:39 2560 2440 2968 No 44-10 PR311756 266669 10224 GS012 6/2/2016 10:41 2870 2440 2968 No 44-10 PR311756 266669 10224 GS012 6/2/2016 10:45 2860 2440 2968 No 44-10 PR311756 266669 10224 GS013 6/2/2016 13:05 2340 2242 2748 No 44-10 PR311756 266669 10224 GS013 6/2/2016 13:07 2500 2242 2748 No 44-10 PR311756 266669 10224 GS013 6/2/2016 13:08 2410 2242 2748 No 44-10 PR311756 266669 10224 GS013 6/2/2016 13:11 2420 2242 2748 No 44-10 PR311756 266669 10224 GS013 6/2/2016 13:13 2470 2242 2748 No 44-10 PR311756 266669 10224 GS013 6/2/2016 13:14 2380 2242 2748 No 44-10 PR311756 266669 10224 GS013 6/2/2016 13:16 2640 2242 2748 No 44-10 PR311756 266669 10224 QGS006 6/2/2016 13:39 2940 2652 3203 No 44-10 PR311756 266669 10224 QGS006 6/2/2016 13:41 3180 2652 3203 No 44-10 PR311756 266669 10224 QGS006 6/2/2016 13:43 2950 2652 3203 No 44-10 PR311756 266669 10224 QGS006 6/2/2016 13:45 3100 2652 3203 No 44-10 PR311756 266669 10224 QGS006 6/2/2016 13:47 3060 2652 3203 No 44-10 PR311756 266669 10224 QGS006 6/2/2016 13:50 2910 2652 3203 No

6/61~. o 1 : 46:40PM Analysis Report for 06-Jun-16-10002 L310224AFRGS001SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels}

Identification Energy Tolerance Energy Calibration Used Done On Effic i ency Calibration Used Done On Efficiency Calibration Description Sample Number : 06-J un-16-10002

L310224AFRGS001SS (DR IE D) : Miscellaneous 1.583E+03 grams Default 6/2/2016 1 0: 00: 00AM 6/6/2016 1 :3 6:01PM

• 130G 1 L Sand Sam pie JWelch

• P11314X2

• 130G Sand 600.0 seconds : 600.5 seconds : 0.09% : 2.80 : 120 -8192 :120-8192 : 1.000FWHM

1/27/2016

11/26/2012

15068 PEAK WITH NID REPORT Peak Analysis Performed on : 6/6/2016 1: 46:0SPM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default

\Library\Zion Lib-BNL.NLB

1.000FWHM Page I of8 Analysis Report for 06-Jun-16-10002 L310224AFRGS001SS (DRIED) Peak Energy ROI No. (keV) start 1 76.88 305 -2 186.18 742 -.) 238.70 950 -4 295.26 1175 -5 351.95 1398 -6 583.30 2325 -7 609 .13 2428 -8 911. 28 3638 -9 969.45 3869 -10 1120.52 4475 -11 1461. 09 5836 -M ;;;; First peak in a multiplet regio n m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 315 749 961 1187 1415 2337 2441 3650 3882 4486 5854 6/6/:t...,.

J 1 :46:40PM Peak Net Peak Net Area Centroid Area Uncertainty 308.73 5.85E+O l 29.91 745.33 1.95E+Ol 18.09 955 .11 1.39E+02 31.55 1181.10 6.18E+01 20.45 1407.59 1.22E+02 26.29 2332.19 3.53E+Ol 15.79 2435.45 7.47E+Ol 19.44 3643.64 3.36E+01 14.01 3876.31 2.81E+Ol 12.82 4480.66 1.84E+Ol 10.51 5843.67 l.55E+02 26.24 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defauft\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Page 2 of 8 Continuum Tentative Counts Nuclide 1.1 3E+02 Pb214-XR Pb212-XR 6.09E+Ol Ra-226 U-235 8.42E+Ol Pb-212 3.25E+Ol Pb-214 Eu-152 3.60E+Ol Pb-214 Bi-211 2.34E+Ol Tl-208 1.65E+Ol Bi-214 l.49E+Ol Ac-228 l.18E+Ol Ac-228 9.13E+OO Bi-214 1. 52E+Ol K-40 Activity Coinc Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 0.99 1 460.82

• 10.66 5.48E+OO 1. 04E+OO miss Tl-208 0.99 583.19

• 85.00 8.39E-02 3.89E-02 miss Pb-212 1. 00 115.18 0.60 238.63

• 43.60 3.49E-01 9.73E-02 miss 300.09 3.30 Pb212-XR 0.99 74.82 10.28 77 .11

• 17.10 6.50E-01 3.58E-01 miss 87.35 3.97 89.78 1. 46 Bi-214 0.99 609.32

• 45.49 3.42E-01 9.80E-02 miss 768.36 4.89 806.18 1.26 934.06 3 .11 6/6/~v .O 1 :46:40PM Page 3 of8 Analysis Report for 06-Jun-16-10002 L310224AFRGS001SS (DRIED) Nuclide Id Energy Yield(%) Activity Activity Coinc Name Confidence (keV) (pCi/grams)

Uncertainty Corr B i-214 0.99 11 20. 29

• 14.92 3.8 7E-01 2.2 2E-01 miss 1155.2 1 1. 63 1238.12 5.83 1280.98 1. 43 13 77.67 3.99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2 .13 1661.2 7 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2 1 18.51 1.16 Pb-214 1. 00 241.99 7.25 295.22 18.42 4.23 E-0 1 l.5 6E-0 1 mis s 351.93

• 3 5.60 4.86E-01 1.31E-01 miss 785. 96 1. 06 Pb214-XR 0.99 74.82 5.80 77.11

• 9.70 1.15E+OO 6.40E-01 m i s s 87.35 2.24 89.78 0.82 Ra-226 1. 00 186.21

• 3.64 5.15 E-01 4.84E-01 miss Ac-228 0.99 129.07 2.42 209.2 5 3.89 2 7 0.24 3.46 328.00 2.9 5 33 8.32 11.27 409.46 1. 92 463.00 4.40 794.95 4.25 911. 20

• 25.8 0 3.55E-01 1. SlE-01 miss 964. 77 4.99 968.97

• 15.8 0 5.0 6E-01 2.35E-01 m is s 1588.20 3.22 U-235 0.99 143.76 10. 96 163.3 3 5.08 185.71 -*-57.20 3.28E-02 3.0 SE-0 2 m i ss 202 .11 1. 08 205.31 5.01 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

6/6/21.., .., 1 : 46: 40PM Page4 of8 Analysis Report for 06-Jun-16-10002 L310224AFRGS001SS (DRIED) INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCi!grams)

Uncertainty K-40 0. 996 5.48E+OO 1.04E+OO Tl-208 0.999 8.39E-02 3.89E-02 X Bi-211 0.953 Pb-212 1. 000 3.49E-01 9.73E-02 ? Pb212-XR 0.998 6.SOE-01 3.58E-01 Bi-214 0.999 3.49E-01 8.97E-02 Ph-214 1. 000 4.60E-01 1.00E-01 ? Pb214-XR 0.998 1.15E+OO 6.40E-01 ? Ra-226 1.000 5.15E-01 4.84E-01 Ac-228 0.997 3.99E-01 1. 27E-01 ? U-235 0.990 3.28E-02 3.0SE-02 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 6/6/, ,,6 1 :46:40PM Ana,ysis Report for 06-Jun-16-10002

+ + + + + + + + + L310224AFRGS001 SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy {keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/6/2016 1 : 46:08PM : 120 : 8192 Peak CPS {°A,) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield("Ai)

Activity NuclideMDA LineMDA Name (keV) (pCVgrams) (pCl/grams) (pCi/grams)

K-40 1460.82

• 10.66 5.48E+OO 5.69E-01 5.69E-01 Cr-51 320.08 9.91 -2.47E-02 2.91E-01 2.91E-01 Mn-54 834.85 99.98 6.06E-03 3.66E-02 3. 66E-02 Co-58 810.76 99.45 -1.03E-02 2.46E-02 3.46E-02 1674.73 0.52 8.38E-01 6.17E+OO Co-60 1173.23 99.85 6.16E-03 3.48E-02 3.48E-02 1332.49 99.98 6.72E-03 4.60E-02 Nb-94 702.65 99.81 -4.29E-03 2.85E-02 3.0lE-02 871.09 99.89 5.00E-03 2.85E-02 Ag-108m 79.13 6.60 1. 20E-01 3.37E-02 8.16E-01 433.94 90.50 -7.28E-04 3.43E-02 614.28 89.80 -9.33E-04 3.70E-02 722. 94 '.30. 80 -2.57E-03 3.37E-02 Sn-113 255.13 2 .11 5.49E-01 4.72E-02 1.39E+OO 391.70 64. 97 8.27E-03 4. 72E-02 Cs-134 475.36 1. 48 -3. 96E-01 3.00E-02 1.56E+OO 563.25 8.34 6.08E-02 4.14E-Ol 569.33 15.37 3.32E-02 2.26E-01 604. 72 97.62 3.41E-03 3.00E-02 Page 5 of 8 Tolerance Nuclide Coinc Co" miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss miss 6/6/°L_. ci 1: 46: 40PM Page 6 of8 Analysis R eport fo r 06-Jun-16-10002 L310224AFRGS001SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

Corr Cs-134 795.86 85.46 n.OlE-03 3.00E-02 4.13E-02 miss 801.95 8.69 1.08E-01 4.59E-01 miss 1038.61 0.99 5.03E-02 2.80E+OO miss 1167. 97 1. 79 -1.29E-01 l.94E+OO miss 1365.1 9 3.02 2.26E-02 1.28E+OO m i ss + Cs-137 661.66 85.10 -2.SOE-03 3.39E-02 3.39E-02 miss + Eu-152 121.78 28.6 7 -2.16E-02 8.75E-02 8.75E-02 miss 244.70 7.61 -9. llE-02 3.12E-01 miss 295.94 0.45 1.0 l E+Ol 1.07 E+O l miss 344.28 26.60 -1.39E-02 9.54E-02 miss 367.79 0.86 -8.51E-01 2.04E+D0 miss 411.12 2.2 4 -3.76E-01 1.24E+D0 miss 443. 96 2.83 6.57E-03 9.86E-01 miss 488.68 0.4 2 6.39E-02 6.76E+OO m i ss 563.99 0.49 2.84 E+OO 7.58E+OO miss 586.26 0.4 6 -1.68E+OO 5.78E+OO miss 678.62 0.47 -6.33E-02 6.22E+OO miss 688.67 0.86 1.40E+OO 4.39E+O O miss 719.35 0.28 -1.25E+OO 1.00E+Ol miss 778.90 12.96 -6.21E-02 2.04E-01 miss 8 10.45 0.32 -3.27E+OO 1.03E+D1 miss 867.37 4.26 '7.23E-0 2 6.67E-01 miss 919.33 0.43 ~.32 E+OO 9.06E+OO miss 964.08 14.65 9.69E-03 2.91E-01 m i ss 1085.87 10.24 -3.21E-02 2.78E-01 m i ss 1 089.7 4 1. 73 -1.02E-01 1.65E+00 m i ss 1112.0 7 13.69 -8.56 E-02 2.4 5 E-01 miss 1212.95 1. 43 3.63E-01 3.85E+00 miss 1249.94 0.19 -9.65E+OO 2.14E+Ol miss 1299.14 1. 63 4.55E-01 2.55E+D0 miss 1408.01 21. 07 2.48E-03 1.28E-01 m i ss 1 457.64 0.50 -9.76E+OO 1.18E+O l miss 1528.10 0.28 1.38E+OO 1.02 E+Ol miss + Eu-154 123.07 40.40 2.70E-02 6.72E-02 6.72 E-02 miss 247.93 6.89 1.68E-01 4.0lE-01 miss 591.76 4.95 -1.82E-02 5.41E-01 m i ss 692.42 1. 78 -4.05E-01 1.38E+OO m i ss 723.30 20.06 1.36E-02 1.7 5 E-01 miss 756.80 4.52 1.78E-02 5.7 4E-01 miss 873.1 8 12.08 -6.83E-D2 2.36E-01 miss 996.29 10.48 7.85E-02 3.33E-01 miss 1 004.76 18.01 -1.08E-02

1. 74E-01 m i ss 1274.43 34.80 l.35E-D2 1.05E-D1 miss 1596.48 1. 80 O.OOE+OO 6.06E-01 miss + Eu-155 45.30 1. 31 9.88E-01 1.60E-01 6.90E+OO miss 60.01 1. 22 -5.52E+D0

6. 96E+D0 miss 86.55 30.7 0 6.02E-02 1.60E-01 miss 105.31 2 1.10 1.41E-02 1.60E-01 m i ss + Tl-208 583.1 9

• 85.00 8.39E-0 2 4.71E-D2 4.71E-0 2 m i ss + Bi-211 351.07

• 13.02 1. 33E+OO 2.85E-01 2.85E-01 miss + Pb-211 404.85 3.78 -3. llE-01 6.24E-01 6.24E-01 miss 6/6/~.., ,o 1:46:40PM Page 7 of8 Analysis Report for 06-Jun-16-10002 L310224AFRGS001SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCUgrams) (pCilgrams) (pCi/grams)

Corr Pb-211 427.09 1. 76 6.26E-01 6.24E-01 1.74E+OO miss 832.01 3.52 -1.94E-01 7.84E-01 miss + Bi-212 39.86 1. 06 3.86E+OO 8.08E-01 1.0lE+Ol miss 727. 33 6.67 4.28E-01 8.08E-01 miss 785.37 1.10 2.24E-01 3.16E+OO miss 1620.50 1. 47 3.46E-01 2. 98E+OO miss + Pb-212 115 .18 0.60 l.65E+OO 9.35E-02 5. 04E+OO miss 238.63

• 43.60 3.49E-01 9.35E-02 miss 300.09 3.30 6.38E-01 1.02E+OO miss + Pb212-XR 74.82 10.28 5.97E-01 5.00E-01 8.33E-01 miss 77 .11

• 17.10 6.50E-01 5.00E-01 miss 87.35 3.97 5.61E-01 1.27E+OO miss 89.78 1. 45 -3.53E-01

2. 59E+OO miss + Bi-214 609.32

• 45.49 3.42E-01 7.93E-02 7.93E-02 miss 768.36 4.89 2.71E-01 9.36E-01 miss 806.18 1. 26 1. 03E-01 3.31E+OO miss 934.06 3.11 3.65E-01 1.26E+OO miss 1120.29

• 14.92 3.87E-01 2.66E-01 miss 1155. 21 1. 63 4.55E-01 2.93E+OO miss 12 38.12 5.83 3.50E-02 8.59E-01 miss 12 80.98 1. 43 2.72E-01 2.56E+OO miss 1377.67 3.99 4.12E-01 l.43E+OO miss 1385.31 0.79 7.37E-01 4.90E+OO m i ss 1401. 52 1.33 -3.91 E-01 2.0lE+OO miss 1407.99 2.39 2.18E-02 1.12E+OO miss 1509.21 2 .13 3.79E-01 l.95E+OO miss 1 661. 27 1. 05 5.44E-01 4.26E+OO miss 1729.59 2.88 l.22E+OO 2. 48E+OO miss 1764.49 15.30 2.84E-01 4.94E-01 miss 1847.43 2.03 2.76E-02 2.05E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss Pb-214 241. 99 7.25 4.87E-01 1. 04E-01 5.43E-01 miss 295.22

• 18.42 4.23E-01 l.66E-01 miss 351.93

• 35.60 4.86E-01 1.04E-01 miss 785.96 1. 06 1. llE+OO 3.70E+OO miss + Pb214-XR 74.82 5.80 1.06 E+OO 8.81E-01 1.48E+OO miss 77 .11 .,. 9.70 l.15E+OO 8.81E-01 miss 87.35 2.24 9.94E-01 2.25E+OO miss 89.78 0.82 -6.28E-01 4.60E+OO miss + Ra-226 186.21

• 3.64 5.15E-01 7.55E-01 7.55E-01 miss + Ac-228 129.07 2.42 3.69E-03 1.66E-01 1.14E+OO miss 209.25 3.89 3.65E-01 8.53E-01 miss 270.24 3.46 2.BOE-01 9.40E-01 m i ss 328.00 2.95 3.55E-01 1.08E+OO miss 338.32 11. 27 3.71E-01 4.03£-01 miss 409.46 1. 92 -1.23E-01 1.61E+00 miss 463.00 4.40 -7.05E-02 6.52E-01 miss 794.95 4.25 3.83E-01 1.02E+OO miss 911. 20

• 25.80 3.55E-01 1.66E-01 miss 964.77 4.99 3.06E-01 9.02E-01 m i ss 968. 97

• 15.80 5.06E-0 1 2.63E-01 miss 6/6J"L.v 10 1:46:40PM Page 8 of8 Ai'1alysis Report for 06-Jun-16-10002 L310224AFRGS001SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCilgrams)

Corr Ac-223 1588.20 3.22 2.84E-01 1.66E-01 1.49E+OO miss + Pa-231 27.36 10.30 O.OOE+OO 1.08E-01 1.08E-01 miss 283.69 1. 70 -3.45E-01 l.41E+OO miss 300.07 2.47 8.53E-01 1.37E+OO miss 302.65 2.20 1.58E-01 l.21E+OO miss 330.06 1. 40 -3.64E-01 1.83E+OO miss + Th-234 92.38 2.13 4.02E-01 2.29E+OO 2.29E+OO miss 92.80 2.10 1. 27E+OO 2.43E+OO miss 112. 81 0.21 7.75E-01 1.57E+Ol miss + U-235 143.76 10. 96 9.59E-02 4.81E-02 2. 61E-Ol miss 163.33 5.08 -7 .13E-02 4.53E-01 miss 185.71

• 57.20 3.28E-02 4.81E-02 miss 202.11 1. 08 7.84E-01 2.54E+OO miss 205.31 5.01 9.04E-03 5.15E-01 miss + Am-241 59.54 35.90 l.22E-01 3.08E-01 3.08E-01 miss + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed. free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45-.. 40 35 V'l ..... C: 8 30 "" >;< ;'!; "' ..0 "" 25 >;< CL 20 15 10 5 0 1000 0000015068.CNF :~ ,~wl 2000 3000 4000 5000 channel Live Time : 600.000 sec Real Time :600.530 sec sta r t: 1: -0.2(kev) stop : 8192: 2047 .4(kev) Acq. start : M on Jun 06 13:36: 01 2016 6000 7000 8000 6/6/2_ ., 1:47:17PM am 111a Analysis Report for 06-Jun-16-10003 L310224AFRGS002SS (DRIED} GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real lime Dead lime Peak Locate Threshold Peak Locate Range (in channels}

Peak Area Range (in channels}

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number , 06-Jun-16-10003 , L310224AFRGS002SS (DRIED} ; Miscellaneous 1.889E+03 grams Default : 6/2/2016 10:17:00AM

6/6/2016 1 :36:23PM : 130G 1 L Sand Sample : JWelch : P40818B : 130G Sand : 600.0 seconds : 600.9 seconds : 0.15 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 15069 PEAK WITH NID REPORT Peak Analysis Performed on : 6/6/2016 1 :46:46PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance ~~Vo .x,,,u : C:\Canberra\Apex

\Root\Default\Library\Zion Lib-BNL.NLB

1.0 00FWHM Page 1 of7 Analysis Report for 06-Jun-16-10003 L310224AFRGS002SS (DRIED) Peak Energy ROI No. (keV) start 1 238.59 949 -2 295.24 117 3 -3 351.89 1401 -4 583.08 2327 -5 609.25 2429 -6 1460.1 8 5834 -7 1764.27 7053 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 960 1190 1414 2338 2444 5855 7066 6/6/2l,. 1:47:17PM Peak Net Peak Net Area Centroid Area Uncertainty 954.86 7.40E+O l 27.27 1181. 28 3.65E+Ol 22.16 1407.75 6.48E+Ol 21.73 2332.11 3.26E+Ol 12.32 2436.76 4.85E+01 18.00 5844.10 2.38E+02 31.05 7059.45 1.23E+Ol 7.89 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDE S Nuclide Id Energy Yield(%) Activity Page 2 of7 Continuum Tentative Counts Nuclide 8.79E+Ol Pb-212 5.30E+Ol Pb-21 4 Eu-152 4.43E+Ol Pb-214 Bi-2 11 4.80E+OO Tl-208 2.50E+Ol Bi-214 2.84E+00 K-40 3.50E+OO Bi-2H Activity Caine Name Confidence (keV) (pCi/grams)

Uncertainty Corr K-40 1. 00 1 460.82 ~** 10.66 7.79E+OO 1. 22E+OO miss Tl-208 0.99 583.19 ... 85.00 7.20E-02 2.86E-02 miss Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 1.76E-01 7.06E-02 miss 300.09 3.30 Bi-214 0.99 609.32

• 45.49 2.06E-Ol 8.04E-02 miss 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155. 21 1.63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2 .13 1 661. 27 1. 05 Analysis Report for 06-Jun-16-10003 L310224AFRGS002SS (DRIED) Nuclide Id Energy Name Confidence

{keV} Bi-214 0.99 1729.59 1764.49 1847.43 2118.51 PL-2 1 4 1. 00 241.99 295.22 351.93 785.96 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required. Yield(%) 2.8 8 15.30 2.03 1.16 7.25 1 8.4 2 35.60 1. 0 6 miss = Nuclide energy was not found in the coincidence library. 6/6/21., . .., *1 :47:17PM l'age 3 of7 Activity Activity Caine (pCi/grams)

Uncertainty Corr 3.24E-01 2.lOE-01 m iss 2.3 4E-0 1 1. 4 7E-01 m iss 2.41E-01 8.9 4E-02 m i ss INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Tl-208 X Bi-211 Pb-21 2 Bi-214 Pb-2 14 Nuclide Id Confidence

1. 000 0.9 99 0. 960 1. 000 0.9 99 1. 000 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 7.79E+OO 7.20E-02 1.76E-01 2.21E-01 2.39E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty l.22E+OO 2.86E-02 7.06E-02 7. SlE-02 7.64E-02 6/6/2v ,\J 1 :47:17PM Analysis Report for 06-Jun-16-10003

+ + L310224AFR GS002SS (DRIED) Peak Locate Performed o n Peak Locate From Chann el Peak Locate To Channel Peak No. Energy (keV) All peaks were identified. M = First peak in a multiplet regio n m "'Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/6/2016 1 :46:46PM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCilgrams) (pCilgrams)

K-4 0 1460.8 2

• 10.66 7.79E+OO 2.89 E-01 2.89E-01 Cr-51 320.08 9.91 2.25E-0 2 3.0SE-01 3.0SE-01 Page4 of7 Tolerance Nuclide Coinc Corr miss free + Mn-54 834.85 99.98 l.29 E-02 4.02E-02 4.02E-02 miss + Co-58 810.76 99.45 -2.04E-03 2.95E-02 2.95E-02 miss 1674.73 0.52 6.83E-01 5,74E+OO m i ss + Co-60 1173.2 3 99.85 8.59E-04 3.6 1E-02 3.61E-02 miss 1332.49 99.98 9.33E-03 4.28E-02 miss + Nb-94 702.65 99.81 9.95E-03 2.28E-02 4.02E-02 miss 871. 09 99.89 -1. 31E-02 2.28E-02 mL,s + Ag-108m 79.13 6.60 2.84E-01 2.84E-02 l.13E+OO miss 433.94 90.50 1. 54E-02 3.30E-02 miss 614.28 89.80 -5.98E-03 2.84E-02 miss 722. 94 90.80 -9.16E-03 3 .13E-02 miss + Sn-113 255.13 2 .11 3.38E-01 2.95E-02 1.23E+OO free 3 91. 70 64. 97 -5.23E-03 2.95E-02 f ree + Cs-134 475.36 1. 48 -1.27E-01 2.79E-02 1.76E+OO miss 563.25 8.34 l.06E-01 3.68E-01 miss 569.33 15.37 -5.SOE-02 2.lOE-01 miss 604.72 97.62 -1.19E-03 2.79E-02 miss 6/6/21., ,.J 1 :47:17PM Page 5 of7 Analysis Report for 06-Jun-16-10003 L310224AFRGS002SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCilgrams) (pCi/grams)

Corr Cs-134 795.86 85.46 -4.35E-03 2.79E-02 3.56E-02 miss 801.95 8.69 -9.40E-02 2.89E-01 miss 1038.61 0.99 6.08E-01 3.37E+OO miss 1167.97 1. 79 l.13E+00 2.79E+OO miS$ 1365.19 3.02 O.OOE+OO 1.03E+OO miss + Cs-137 661. 66 85.10 -9.82E-03 3.81E-02 3.SlE-02 miss + Eu-152 121. 78 28.67 -2.08E-02 8.90E-02 9.38E-02 miss 244.70 7.61 -8.74E-02 3.39E-01 miss 295.94 0.45 9.lOE+OO 9.07E+OO miss 344.28 2 6. 60 1. 96E-03 8.90E-02 miss 367.79 0.86 2.63E-01 3.09E+OO miss 411.12 2.24 -3.43E-01 1.20E+OO miss 443.96 2.83 1. 58E-01 9.17E-01 miss 488.68 0.42 3.64E+OO 7.18E+OO miss 563.99 0.49 1.22E+OO 6.23E+OO miss 586.26 0.46 3.0lE-01 6.83E+OO miss 678.62 0.47 1. 71E-01 4.75E+OO miss 688.67 0.86 -1.02E-02 3.88E+OO miss 719.35 0.28 1.68E+OO 9.32E+OO miss 778.90 12.96 -2.64E-02 2.llE-01 miss 810.45 0.32 -1.78E+OO 7.86E+OO miss 867.37 4.26 2.05E-01 9.13E-01 miss 919.33 0.43 -4.28E+OO 6.42E+OO miss 964.08 14.65 1.14E-01 3.13E-01 miss 1085.87 10.24 6.07E-02 4.42E-01 miss 1089.74 1. 73 -1.19E+OO 1.78E+OO miss 1112.07 13.69 -2. 72E-02 2.77E-01 miss 1212.95 1. 43 -9.21E-01 2.82E+OO miss 1249.94 0.19 2.06E+OO 2.48E+Ol miss 1299.14 1. 63 1.13E-01 1.83E+OO miss 1408.01 21. 07 -2.31E-02 1.74E-01 miss 1457.64 0.50 -1.50E+Ol 1.26E+Ol miss 1528.10 0.28 1.83E-01 9.45E+OO miss + Eu-154 123.07 40.40 -9.68E-04 7.lSE-02 7.15E-02 miss 247.93 6.89 1.17E-01 4.34E-01 miss 591.76 4.95 O.OOE+OO 6.08E-01 miss 692.42 1. 78 -2.85E-01 1.56E+OO m i ss 723. 30 20.06 -1.99E-02 1.53E-01 miss 756.80 4.52 -2.28E-01 5.33E-01 miss 873.18 12.08 -2.21E-02 1.89E-01 miss 996.29 10.48 -1.29E-02 L.39E-01 miss 1004.76 18.01 6.52E-02 2.12E-01 miss 1274.43 34.80 1. 43E-02 1. 28E-01 miss 1596.48 1. 80 O.OOE+OO 5.64E-01 miss + Eu-155 45.30 1.31 1.63E+OO 1.SSE-01 1.91E+Ol miss 60.01 1. 22 1.75E+OO 1. 85E+Ol miss 86.55 30.70 3.32E-02 1.85E-01 miss 105.31 21.1 0 1.lOE-01 2.16E-01 miss + Tl-208 583.19

• 85.00 7.20E-02 2.28E-02 2.28E-02 miss + Bi-211 351.07

• 13.02 6.58E-01 2. 71E-01 2.71E-01 miss + Pb-211 404.85 3.78 4.51E-03 7.2 7 E-01 7.27E-01 miss 6ta120. _ 1 :47:17PM Page 6 of7 Analysis Report for 06-Jun-16-10003 L310224AFRGS002SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCi!grams) (pCi!grams)

Corr Pb-211 427.09 1. 76 2.51E-01 7.27E-01 1. 43E+OO miss 832.0 1 3.52 l.58E-01 9.54E-01 miss + Bi-212 39.86 1. 06 -2.61E+OO 6.15E-01 l. 94E+01 miss 727. 33 6.67 l.03E-01 6.15E-01 miss 785.37 1.10 l.94E+OO 4. 05E+OO miss 1620.50 1. 47 2.58E-01 2. 39E+OO miss + Pb-212 115 .18 0.60 2.62E+OO 8.89E-02 6.18E+OO miss 238.63 .. 43.60 l.76E-01 8.89E-02 miss 300.09 3.30 8.00E-01 1. llE+OO miss + Pb212-XR 74.82 10.28 3.BlE-01 6.48E-01 1.09E+00 miss 77 .11 17.10 4.88E-01 6.48E-01 miss 87.35 3.97 3.7 4E-01 l.39E+00 miss 89.78 1. 46 1.33E+OO 3.43E+OO miss + Bi-214 609.32

• 45.49 2.06E-01 9.12E-02 9.12E-02 miss 768.36 4.89 3 .13E-01 8.69E-01 miss 806.18 1. 26 O.OOE+OO 2.60E+OO miss 934.06 3.11 -1.00E-01 l.32E+OO miss 1120.29 14.92 2.30E-01 4.27E-01 miss 1155.21 1. 63 2.92E-01 2.88E+OO miss 1238.12 5.83 -2.18E-01 8.44E-01 miss 1280.98 1. 43 1.9 5E-01 3.12E+OO miss 1377. 67 3.99 -2.20E-02 l.18E+OO miss 1385.3 1 0.79 6.05E-02 3. llE+OO miss 1401.52 1. 33 -2.18E-01 2.36E+00 miss 1407.99 2.39 -2.03E-01 1.53E+OO miss 1509.21 2.13 3. 77E-01 1.81E+OO miss 1661.27 1. 05 8.75E-01 4.43E+00 miss 1729.59 2.88 4.74E-01 l.81E+OO miss 1764.49 ,i.r 15.30 3.24E-01 2.29E-01 miss 1847.43 2.03 1.54E-01 1.51E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 3.31E-01 9.92E-02 5.03E-01 miss 295.22

• 18.42 2.34E-01 2.14E-01 m i ss 351. 93

• 35.60 2.41E-01 9.92E-02 miss 785.96 1. 06 2.31E+OO 4.22E+OO miss + Pb214-XR 74.82 5.80 6.76E-01 1.1 4E+OO l.92E+OO miss 77 .11 9.70 8.60E-01 1.14E+OO miss 87.35 2.24 6.63E-01 2.46E+OO miss 89.78 0.82 2.37E+OO 6. llE+OO miss + Ra-226 18'5.21 3.64 2.96E-01 8.58E-01 8.58E-01 misl" + Ac-228 129.07 2.42 1. 53E-01 2.55E-0 1 1.37E+OO miss 209.25 3.89 4.44E-01 8.39E-01 miss 270.24 3.46 '.2.00E-01 9.25E-01 miss 328.00 2.95 3.54E-01 1. 07E+OO miss 338.32 11.27 1.87E-01 3.08E-01 miss 409.46 1. 92 1.38E-01 1. 63E+OO miss 463.00 4.40 2.53E-01 7.55E-01 miss 794.95 4.25 -3.02E-02 7.67E-01 miss 911.20 25.80 1. 83E-01 2.55E-01 miss 964. 77 4.99 4.40E-01 9.94E-01 miss 968. 97 15.80 2.40E-01 3.76E-01 m i ss 6/6h-,o 1 :47: 17PM Page7 of7 Analysis Report for 06-Jun-16-10003 L310224AFRGS002SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCi/grams) (pCi!grams) (pCl!grams)

Corr A.c-228 1588.20 3.22 -7.23E-02 2.SSE-01 8.52E-01 miss + Pa-231 27.36 10.30 l.19E-01 1.lOE+OO 2.39E+OO miss 283.69 1. 70 2.16E-01 l.76E+OO miss 300.07 2.47 1.07E+OO l, 48E+OO miss 302.65 2.20 -4.12E-01

.lOE+OO miss 330.06 1. 40 -1.14E-01 l.99E+OO miss + Th-234 92.JB 2.13 1.66E+OO 2.SSE+OO 2.75E+OO miss 92. 80 2.10 8.33E-02 2.55E+OO miss 112. 81 0.21 9.04E-01 l.83E+Ol miss + U-235 143.76 10.96 1.38E-01 5.40E-02 3.09E-01 miss 163.33 5.08 -1. 20E-01 4. 79E-01 miss 185. 71 57.20 1.87E-03 5.40E-02 miss 2 02 .11 1. 08 5.54E-0 1 2.6 1 E+OO m i ss 205.31 5.01 3.lOE-02 5.17E-01 miss + Am-241 59.54 35.90 1.65E-01 6.94E-01 6.94E-01 miss + "' Nuclide identified during the nuclide identification

.. "' Energy line found in the spectrum > "' MDA value not calculated

@ "" Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

Ill +-' C ::s 60 55 50 40 3 5 8 30 2 5 20 15 10 5 1000 2000 3000 0000015069

.CNF 4000 channel 5000 L i ve Time :600.000 sec Rea 1 Time :600. 930 sec start: 1: -0.l(kev)

Stop : 8192: 2047.0(keV) Acq. start :Mon Jun 06 13:36:23 2016 6000 7000 8000 6/6i.c.v 16 2.19:20PM Analysis Report for 06-Jun-16-10004 L310224AFRGS003SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 06-Jun-16-10004

L310224AFRGS003SS (DRIED) : Miscellaneous 1.830E+03 grams : Default : 6/2/2016 10:36:00AM

6/6/2016 2:08:42PM

130G 1 L Sand Sample : JWeJch : P11314X2 : 130G Sand : 600.0 seconds 600.5 seconds 0.09% 2.80 120-8192 120-8192 1.000FWHM 1/27/2016

• 11/26/2012

' 15070 PEAK WITH NID REPORT Peak Analysis Performed on : 6/6/2016 2: 18:47PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BN L.NLB : 1.000FWHM Page I of8 Analysis Report for 06-Jun-16-10004 L310224AFRGS003SS (DRIED) Peak Energy ROI No. (keV) start 1 77.09 305 -2 238.57 946 -3 295.15 1176 -4 351.85 1402 -5 510.66 2037 -6 583.09 2324 -7 609.35 2429 -8 860.29 3434 -9 911. 38 3640 -10 968.87 3868 -11 1120.58 4475 -12 1237.92 4945 -13 1461. 01 5832 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 313 960 1186 1413 2046 2339 2445 3445 3649 3879 4486 4956 5853 6/6/2v ,u 2:19:20PM Peak Net Peak Net Area Centroid Area Uncertainty 309.60 4.41E+Ol 28.22 954. '60 1. 58E+02 34.55 1180.63 5.26E+Ol 21.93 1407.19 1.04E+02 23 .11 2041.85 1. lOE+Ol 13. '72 2331.36 6.58E+Ol 18.93 2436.33 7.83E+Ol 20.23 3439.69 l.41E+Ol 9. "7 8 3644.02 1.97E+Ol 10.17 3873.96 2.09E+Ol 11.93 4480.87 1.68E+Ol 9.93 4950.41 9.29E+OO 7.07 5843.36 l.77E+02 26.61 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNLNLB IDENTIFIED NUCLIDE S Nuclide Id Energy Yield(%) Activity Page2 of8 Continuum Tentative Counts Nuclide 1.22E+02 Pb214-XR Pb212-XR 9.80E+Ol Pb-212 5.69E+Ol Pb-214 Eu-152 2.67E+Ol Pb-214 Bi-211 3.60E+Ol 1.85E+Ol Tl-208 1. 74E+Ol Bi-214 9.81E+OO 6.67E+OO Ac-228 l.42E+Ol Ac-228 8.46E+OO Bi-214 3.43E+OO Bi-2 14 O.OOE+OO K-40 Activity Caine Name Confidence (keV) (pCi/grams)

Uncertainty Corr K-40 0.99 1 460.82

• 10.66 5.39E+OO 9.36E-01 miss Tl-208 0.99 583.19

• 85.00 1.35E-01 4.22E-02 miss Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 3.43E-01 9.34E-02 miss 300.09 3.30 Pb212-XR 1. 00 74.82 10.28 77 .11

• 17.10 4.20E-01 2.83E-01 miss 87.35 3.97 89.78 1. 46 Bi-214 0.99 609.32

• 45.49 3.lOE-01 8.83E-02 miss 768.36 4.89 806.18 1. 26 Analysis Report for 06-Jun-16-10004 L310224AFRGS003SS (DRIED) Nuclide Name Bi-214 Pb-214 Pb214-XR Ac-228 Id Confidence 0.99 1. 00 1. 00 0.99 Energy (keV) 934.06 1120.29

• 1155.21 1238.12

• 1280.98 1377.67 1385.31 1401.52 1407.99 1509.21 1661. 27 1729.59 1764.49 1 847.43 2118. 51 241. 99 295.22

• 351. 93

• 785. 96 74.82 77.11

• 87.35 89.78 129.07 209.25 27 0.24 3 2 8.00 338.3 2 409.46 463.0 0 794.95 911.20 964. 77 968.97

• 1588.20 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWH M Nuclide confidence index thres hold = 0.30 Errors quoted at 2.000sigma Coincidence correction performed, free = No coincidence correction required.

Yield(%) 3.11 14.92 1. 63 5.83 1. 43 3.99 0.79 1. 33 2.39 2 .13 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 5.80 9.70 2.24 0.82 2.42 3.89 3.46 2.95 11. 27 1. 92 4.40 4.25 25.80 4.99 15.80 3.22 miss = Nuclide energy was not found in the coincidence library. 6/6/2-.. J 2:19:20PM Page3 of8 Activity (pCilgrams) 3.04E-01 4.60E-01 3.12E-D1 3.57E-01 7.41E-01 1. 80E-01 3.26E-01 Activity Uncertainty 1.82E-01 3.52E-01 l.39E-01 9.8 1E-02 5.0 3 E-01 9.44E-02 1.88E-01 Caine Corr miss miss miss miss miss miss miss 6/6/2u 10 2:19:20PM Analysis Report for 06-Jun-16-10004 L310224AFRGS003SS (DRIED) INTERFERENCE CORRECTED REPORT X ? ? Nuclide Name K-40 Tl-2 0 8 Bi-211 P b-2 1 2 P b212-XR Bi-214 P b-2 1 4 P b2 14-XR Ac-22 8 Nuclide Id Confidence 0.998 0.999 0. 963 1. 00 0 1.00 0 0.999 1. 000 1. 000 0.999 ? "" nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCi/grams) 5.39E+OO 1.35E-01 3.43E-01 4.20E-01 3.16E-01 3.42E-01 7.41E-01 2.09E-01 @ " nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty 9.36E-01 4.22E-02 9.34E-02 2.83E-Ol 7.75E-0 2 8.02E-02 5.0 3 E-01 8.44E-02 Page4 of8 Comments 6/6/2L ,,., 2:19:20PM Analysis Report for 06-Jun-16-10004

+ + + + + + + + L310224AFRGS003SS (DRIED) Peak Locate Performed o n Peak Locate From Chann el Peak Locate To Channel Peak No. 5 8 Energy (keV) 510.66 860.29 M "' First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/6/2016 2: 18:47PM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 1.83333E-02 2.34942E-02 62.35 34.70 Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name {keV) (pCi/grams) (pCilgrams) (pCilgrams)

K-40 1460.82

• 10.66 5.39E+OO 8.25E-02 8.25E-02 Cr-51 320.08 9.91 -1.19E-01 2.34E-01 2.34E-01 Mn-54 834.85 99.98 5.67E-03 3.3':'E-02 3.37E-02 Co-58 810.76 99.45 2.21E-03 2.99E-02 2.99E-02 1674.73 0.52 1.31E+OO 6.73E+OO Co-60 1173.23 99.85 6.33E-03 3.2;E-02 4.20E-02 1332. 49 99.98 8.67E-04 3.27E-02 Nb-94 702 .. 65 99.81 -1.18E-03 2.75E-02 2. 98E-02 871. 09 99.89 2.48E-03 2.75E-02 hg-108m 79.13 6.60 2.43E-01 1.8"7E-02 7.41E-01 433.94 90.50 4.20E-03 2. 96E-02 614.28 89.80 -1.41E-02 1.87E-02 722. 94 90.80 3.71E-03 3.14E-02 Sn-113 255.13 2.11 2.89E-02 3.94E-02 1.25E+OO 391. 70 64.97 3.46E-03 3.94E-02 Page::, of8 Tolerance Nuclide Coinc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free + Cs-134 475.36 1. 48 -1. 20E-01 3.82E-02 1.80E+OO miss 6/6/2(, ,.., 2:19:20PM Page 6 of8 Analysis Report for 06-Jun-16-10004 L310224AFRGS003SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCilgrams) (pCi!grams)

Corr Cs-134 563.25 8.34 8.39E-02 3.82E-02 3.09E-01 miss 569.33 15.37 2.56E-02 1.47E-01 miss 604.72 97.62 1.26E-02 3.82E-02 miss 795.86 85.46 2.14E-02 4.59E-02 miss 801.95 8.69 5.84E-02 3.53E-01 miss 1038.61 0.99 4.35E-02 3.42E+OO miss 1167.97 1. 79 -2.58E-01 2.04E+00 miss 1365.19 3.02 -6.31E-01 7.56E-01 miss + Cs-137 661.66 85.10 -4.97E-03 2.41E-02 2.41E-02 miss + Eu-152 1 2 1.78 28.67 -1. llE-02 8.8 7 E-02 9.37E-02 miss 244.70 7.61 -1.14E-01 2.84E-01 miss 295.94 0.45 -9.7'7E-02 9.97E+OO miss 344.28 26.60 6.44E-03 8.87E-02 miss 367.79 0.86 -2.06E-01 2.56E+OO miss 411.12 2.24 -4.99E-01 8.66E-01 miss 443.96 2.83 -3.58E-01 4.75E-01 miss 488.68 u. 4 2 1. 7 6E+OO 6.42E+OO miss 563.99 0.49 -1.39E-01 4.56E+OO miss 586.26 0.46 -2.90E+OO 4.58E+OO miss 678.62 0.47 -1.05E+OO 5.38E+OO miss 688.67 0.86 -6.36E-01 2.74E+OO m i ss 719.35 0.28 -2.77E+OO l.02E+Ol miss 778. 90 12.96 2.19E-02 2.15E-01 miss 810.45 0.32 -9.06E-01 8.16E+OO miss 867.37 4.26 O.OOE+OO 1.45E-01 misE' 919.33 0.43 1.85E-01 6.67E+OO miss 964. 08 14.65 2.Sl E-0 2 2.52E-01 miss 1085.87 10.24 -1.16E-01

3. llE-01 miss 1089.74 1. 73 6.59E-01 2.44E+OO miss 1112. 07 13.69 -3.56E-02 2.12E-01 miss 1212.95 1. 43 1.69E+OO 3.89E+OO miss 1249.94 0.1 9 -7.91E+OO 1.43E+Ol miss 1299.14 1. 63 -3.87E-01 2.20E+OO miss 1408.01 21. 07 -1.82E-02 1.39E-01 m i ss 1457.64 0.50 O.OOE+OO 8.46E+00 miss 1528.10 0.28 -1.70E-01 8.78E+OO miss Eu-154 123.07 ~0.40 -2.60E-02 6.31E-02 6.31E-02 miss 2 47.93 6.89 l.SSE-02 3.32E-01 miss 591.76 4.95 -2.00E-02 4.68E-01 miss 692.42 1. 78 7.37E-02 l.75E+OO miss 723.30 20.06 -6.72E-04 1.32E-01 miss 756.80 4.52 2.59E-01 7.69E-01 miss 873.18 12.08 2.32E-0~ 2.04E-01 miss 996.29 10.48 7.98E-03 2.88E-01 miss 10 04.7 6 18.01 4.44E-02 1.98E-01 miss 1 2 74.43 34.80 -1.98E-02

1. llE-01 miss 1596.48 1. 80 -5.33E-01 l.43E+OO miss + Eu-155 45.30 1. 31 1.62E+OO 1.18E-01 6.41E+OO miss 60.01 1. 22 -1.74E+OO 8.20E+OO miss 86.55 30.70 -6.33E-03 1.18E-01 m i ss 105.31 21.10 -1. 49E-02 1.36E-01 miss 6/6/2l., ,v 2:19:20PM Page 7 of8 Analysis Report for 06-Jun-16-10004 L310224AFRGS003SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCi/grams) (pCi!grams)

Co" + Tl-208 583.19

• 85.00 1. 35E-01 3.86E-02 3.86E-0~ miss + Bi-211 351. 07

• 13.02 9.77E-01 1.95E-01 1. 95E-01 miss + Pb-211 404.85 3.78 -2.87E-02 5.70E-01 5.70E-01 miss 427.09 1. 76 3.68E-02 1.39E+OO miss 832.01 3.52 -1.63E-01 5.85E-01 miss + Bi-212 39.86 1. 06 3.60E+OO 6.30E-01 8.25E+OO miss 727.33 6.67 3.73E-01 6.30E-01 miss 785.37 1.10 8. 72E-01 3.23E+OO miss 162 0.50 1. 47 8.73E-01 3.14E+OO miss + Pb-212 115 .18 0.60 -9.86E-02 9.06E-02 4.29E+00 miss 238.63

• 43.60 3.43E-01 9. 06E-02 miss 300.09 3.30 6.23E-01 9.85E-01 miss + Pb212-XR 74.82 10.28 7.lOE-01 4.l-:'E-01 7.79E-01 miss 77 .11

• 17.10 4.20E-01 4.17E-01 miss 87.35 3.97 1.12E-01 9.79E-01 miss 89.78 1. 46 :.09E+OO 3.0lE+OO miss + Bi-2 14 609.32

• 45.49 3.lOE-01 7.46E-02 7.46E-02 miss 768.36 4.89 -1.60E-01 7.16E-01 miss 806.18 1. 26 6.49E-01 2.86E+OO miss 934.06 3.11 1. 76E-01 1.09E+OO miss 1120.29 ... 14.92 3.04E-01 2.16E-01 miss 1155.21 1. 63 8.69E-01 2.54E+OO miss 1238.12 *'* 5.83 4.60E-01 4.25E-01 miss 1280.98 1. 43 1.22E+OO 3.09E+OO miss 1377.67 3.99 6.91E-01 1. 36E+OO miss 1385. 31 0.79 l.18E+OO 4.24E+OO miss 1401.52 1. 33 6.85E-01 2.84E+OO miss 1407.99 2.39 -1.60E-01 1.23E+OO miss 1509.21 2.13 2.75E-01 1. 68E+OO miss 1661.27 1. 05 1. 71E-01 2.52E+OO miss 1729.59 2.88 7.85E-01 1.93E+OO miss 1764.49 15.30 3.70E-01 5.23E-01 miss 1847.43 2.03 5.72E-01 2.05E+OO miss > 2118.51 1.16 O.OOE+OO 0.00E+OO miss Pb-214 241.99 7.25 3.90E-01 7.14E-02 4.99E-01 miss 295.22

• 18.42 3.12E-01 1.76E-01 miss 351.93

• 35.60 3.57E-01 7.14E-02 miss 785.96 1. 06 1. 44E+OO 3.66E+OO miss + Pb214-XR 74.82 5.80 1.26E+OO 7.34E-01 1.38E+00 miss 77.11

• 9.70 7.41E-01 7.34E-01 miss 87.35 2.24 l.99E-01 1.73E+OO miss 89.78 0.82 3. 72E+OO 5.36E+00 miss + Ra-226 186.21 3.64 4.66E-01 7.97E-01 7.97E-01 miss + .hc-228 129.07 2.42 5.14E-01 9.98E-02 1.17E+OO miss 209.25 3.89 5.84E-01 7.86E-01 miss 270.24 3.46 6.17E-01 9.78E-01 miss 328.00 2.95 6.34E-01 1.12E+OO miss 338.32 11. 27 3.88E-01 3.67E-01 miss 409.46 1. 92 6.07E-01 1.48E+OO miss 463.00 4.40 5.66E-01 8.79E-01 miss 6/6/21.J ,., :l:19:20PM Page 8 of8 Analysis Report for 06..Jun-16-10004 L310224AFRGS003SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCilgrams)

Corr Ac-228 794.95 4.25 2.79E-01 9.98E-02 9.19E-01 miss 911. 20

• 25.80 1.80E-01 9.98E-02 miss 964.77 4.99 2.62E-01 8.20E-01 miss 968.97

• 15.80 3.26E-01 2.38E-01 miss 1 588.20 3.22 2.15E-01 9. 99E-01 miss + Pa-231 2 7.36 10.30 O.OO E+OO 9.36E-02 9.36E-02 miss 283.69 1. 70 -1.25E-01

1. 33E+OO miss 300.0 7 2.47 8.32E-01 1. 32E+OO miss 302.65 2.20 2.75E-01 1.13E+OO miss 330.06 1. 4 0 -1.09E+OO l.52E+00 miss + Th-2 34 92.38 2 .13 1.03E-01 1.98E+0() l.98E+00 miss 92.80 2.10 1.llE+OO 2.17E+OO miss 112. 81 0.2 1 -5.31E+OO 1.42E+Ol miss + U-235 143.76 1 0.96 2.46E-03 5.21E-02 2.26E-01 miss 163.33 5.08 3.48E-02 4.77E-01 miss 185.71 57.20 3.20E-02 5.21E-02 miss 202 .11 1. 08 -9.37E-02 1.93E+OO miss 205.31 5.01 -9.36E-02 4.61E-01 miss + Am-241 59.54 35.90 -3.76E-02 2.95E-01 2. 95E-01 miss + = Nuclide identified during the nuclide identification

• = Energy line fo u nd in the spectrum > = MDA value not calculated

@ ;;;; Half-life too short to be able to perform the decay correction

? ;;;; CAUTION: MDA value is inconsistent with Currie MDA at 95% conf i dence level Coincidence correction performed. free = No coincidence correction required. miss = Nuclide energy was not found in the co i nc i dence library.

60 55 50 45-.. 40 35 ..,., 1 C ::II 8 30 ... "" ,_. >;< ..... 1:, ;:!; <>. ..... 25 .Q "" >< ..!.. ,_. ... 20 15 10 5 0 1000 2000 3000 0000015070.CNF 4000 channel I a, 5000 L iv e Tim e :600.000 sec Re a l Time : 600.53 0 sec s ta r t: 1: -0.2(kev) sto p : 819 2: 2 047 .4 (kev) Acq. S ta rt :Mo n J un 0 6 1 4: 08: 4 2 20 16 6000 7000 8000 6/6, ... .,16 2:19:57PM

~-Gamma Analysis Report for 06-Jun-16-10005 L310224AFGRS004SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type U ni t Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 06-Jun-16-10005

L310224AFGRS004SS (DRIED) : Miscellaneous 1.627E+03 grams : Default : 6/2/2016 12:40: 00PM : 6/6/2016 2:09:00PM

130G 1 L Sand Sample : JWelch . P40818B

• 130G Sand

• 600.0 seconds

• 600.9 seconds : 0.15% : 2.80 : 120-8192 : 120-8192 : 1.000FWHM : 1/27/2016

1/5/2015 : 15071 PEAK WITH NID REPORT Peak Analysis Pertormed on : 6/6/2016 2: 19:26PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Ca nberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.0 00FWHM P age 1 of8 Analysis Report for 06-Jun-16-10005 L310224AFGRS004SS (DRIED) Peak Energy ROI No. (keV) start 1 238.71 948 -2 295.06 1174 -3 338.44 1349 -4 351.93 1398 -5 583.14 2325 -6 609.15 2430 -7 911. 12 3637 -8 1460.85 5835 -9 1764.37 7053 -M = First peak in a multiplet regio n m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 960 1188 1359 1415 2340 2442 3650 5853 7066 6/6/~,.,, 6 2:19:57PM Peak Net Peak Net Area Centroid Area Uncertainty 955.33 1.55E+D2 35.94 1180. 55 3.64E+Ol 23. 62 1353.9 7 3.33E+Ol 15.93 1407.92 1. 0 2 E+02 22.56 2332.34 4.91E+Ol 19. -:-2 2436.36 8.32E+Ol 20 .11 3644.18 3.49E+Ol 14.49 5844.38 1.12E+02 21.77 7059.86 1.24 E+Ol 8.32 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDE S Nuclide Id Energy Yield(%) Activity Page 2 of8 Continuum Tentative Counts Nuclide 1.28E+02 Pb-212 6.92E+Ol Pb-214 Eu-152 2.74E+Ol Ac-228 1.BOE+Ol Pb-214 Bi-2 11 3.58E+Ol Tl-208 1.56E+Ol Bi-214 1.63E+Ol Ac-228 5.22E+OO K-40 5.17E+OO Bi-214 Activity Caine Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 1. 00 1 460.82

• 10.66 4.28E+OO 9.08E-01 miss Tl-208 1. 00 583.19

• 85.00 1.26E-01 5.28E-02 miss Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 4.27E-01 1.21E-0 1 miss 300.09 3.30 Bi-214 0.99 609.32

• 45.49 4. llE-01 1. llE-01 miss 768.36 4.89 806.18 1. 26 934.06 3.11 1120.29 14.92 1155.21 1. 63 1238.12 5.83 128 0.98 1. 43 1377.67 3.99 138 5. 31 0.79 1 401.52 1. 33 1407.99 2.39 Analysis Report for 06-Jun-16-10005 L 310224AFGRS004SS (DR I ED) Nuclide Id Energy Name Confidence (keV) Bi-2 1 4 0.99 1509.21 1661.27 1729.59 1764.49 1847.43 2118.51 Pb-214 0.99 241.99 295.22 351.93 785. 96 Ac-228 0.74 129.07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911. 20 964. 77 968. 97 1588.20 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield{°/a) 2 .13 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 2.42 3.89 3.46 2.95 11. 27 1. 92 4.40 4.25 25.80 4.99 15.80 3.22 miss = Nuclide energy was not found in the coincidence library. 6/6/'Lv 10 2:19:57PM Page 3 of8 Activity Actlvifl.1 Coinc (pCi/grams)

Uncertainty Corr 3.81E-O l 2.57E-01 miss 2. 71E-01 1. 81E-01 miss 4.40E-01 1.20E-01 miss 4.42E-01 2.24E-01 miss 3.98E-0 1 l.69E-01 miss INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean wt mean Comments Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 1.000 4.28E+OO 9.08E-01 Tl-208 1. 000 1.26E-01 5.28E-02 Analysis Report for 06-Jun-16-10005 X L310224AFGRS004SS (DRIED) Nuclide Nuclide Name Id Confidence B i-211 0.955 Pb-212 1. 000 Bi-214 0.999 Pb-214 0.999 Ac-2 28 0.744 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis 6/6/L-,6 Wt mean Activity (pCilgrams) 4.27E-01 4.06E-01 3.88E-01 4.14E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 2:19:57PM Page 4 of8 Wt mean Comments Activity Uncertainty 1.21E-01 1.02E-01 1. OOE-01 1.35E-01 6/61.c.v 16 2:19:57PM Analysis Report for 06-Jun-16-10005

+ + + + + + + + + L310224AFGRS004SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/6/2016 2:19:26PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C: \Canberra\Apex\Root\Defau lt\Library\2 ION LI B-BN L. NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCUgrams) (pCilgrams) (pCi/grams)

K-40 1460.82

• 10.66 4.28E+OO 4.12E-01 4.12E-01 Cr-51 320.08 9.91 -1.41E-01 3.04E-Ol 3.04E-01 Mn-54 834.85 99.98 9.09E-03 3.95E-02 3.95E-02 Co-58 810.76 99.45 9.72E-03 4.51E-02 4.51E-02 1674.73 0.52 -5.66E-01 6.66E+OO Co-60 1173.23 99.85 1.50E-03 4.92E-02 4.92E-02 1332.49 99.98 8.66E-03 5.69E-02 Nb-94 702.65 99.81 -6.88E-05 3.49E-02 3.49E-02 871.09 99.89 1.45E-02 4.53E-02 Ag-108m 79.13 6.60 -1.88E-01 2.58E-02 1.35E+OO 433.S4 90.50 1.12E-02 3.95E-02 614.28 89.80 5.03E-04 4.19E-02 722.94 90.80 4.62E-04 2.58E-02 Sn-113 255.13 2 .11 4.02E-01 5.26E-02 1. 69E+OO 391.70 64.97 l.04E-02 5.26E-02 Cs-134 475.36 1. 48 -l.16E+OO 3.83E-02 l.82E+OO 563.25 8.34 4.36E-02 4.82E-01 569.33 15.37 5.73E-02 2.73E-01 604. 72 97.62 6.99E-03 3.83E-02 Page 5 of8 Tolerance Nuclide Caine Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss miss 6/6/'.£.., ,d 2:19:57PM Page 6 of8 Analysis Report for 06-Jun-16-10005 L310224AFGRS004SS (DRIED) Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCi!grams)

Corr Cs-134 795.86 85.46 1. 84E-02 3.83E-02 5.49E-02 miss 801.95 8.69 -l.09E-01 2.90E-01 miss 1038.61 0.99 -3.39E-01 3.91E+OO miss 1167. 97 1. 79 -3.40E-01 2.34E+OO miss 1365.1 9 3.02 -3.66E-01

. . l 9E+O O miss + Cs-137 661.66 85.10 2.73E-02 6.llE-02 6.llE-02 m i ss + Eu-152 121.78 28.67 1. 03E-02 1. llE-01 l.34E-01 miss 244.70 7.61 -1. 29E-01 3.77E-01 miss 295.94 0.45 6.07E+OO l.08E+Ol miss 344.28 26.60 -3.24E-03

1. llE-01 miss 367.79 0.8S -2.30E-01 3.46E+OO miss 411.12 2.24 -9.97E-02 1.54E+OO miss 443.96 2.83 -4.77E-01 9.0lE-01 miss 488.68 0.42 2.66E+OO 8.0lE+OO m i ss 563.99 0.49 -1.30E+OO 7.24E+OO miss 586.26 0.46 .-3. 65E+OO 7.93E+OO miss 67 8. 62 0.47 2.99E-01 7.22E+00 miss 688.67 0.86 -3.22E-01 3.72E+00 miss 719.35 0.28 -1.95E+OO l.08E+Ol m i ss 778.90 12. 96 3.75E-02 2.4GE-Ol miss 810.45 0.32 -2.06E+OO

1. llE+Ol miss 867.37 4. 2 6 -2.12E-01 6.20E-01 miss 919.33 0.43 1.lSE-01 6.43E+OO miss 964. 08 14.65 1.58E-01 4.07E-01 miss 1085.87 10.24 -3.69E-02 3.00E-01 miss 1089.74 1. 73 4.l lE-01 2.30E+OO miss 1112. 07 13.69 -2.81E-02

2. 64E-01 m i ss 1212.95 1. 43 -7.84E-01 2.32E+OO miss 1249.94 0.19 -5.21E+OO 1.41E+Ol miss 1299.14 1. 63 O.OOE+OO 2.13E+OO miss 1408.01 21.07 -8.57E-02 1.38E-01 miss 1457.64 0.50 -2.0lE+OO 1.06E+Ol miss 1528.10 0.28 -l.28E+OO 1.lOE+Ol miss + Eu-154 123.07 40.40 -2.21E-02 7.78E-02 8.66E-02 miss 247.93 6.89 4.88E-02 4.72E-01 miss 591.76 4.95 2.08E-01 8.0BE-01 miss 692.42 1. 78 -2.25E-01 1.81E+OO m i ss 723. 30 20.06 -5.45E-02 9.25E-02 miss 756.80 4.52 -3.02E-01 5.34E-01 miss 873.18 12.08 -5.13E-02 3.34E-01 miss 996.29 10.48 6.22E-02 3.59E-01 miss 1004.76 18.0 1 3.79E-02 2.lOE-01 miss 1274.43 34.80 1.06E-02 7.78E-02 miss 1596.48 1. 80 -6.0SE-01 2.25E+OO miss + Eu-155 45.30 1. 31 -1.08E+OO 2.04E-01 2.26E+Ol miss 60.0 1 1.22 -1.91E-01 2.19E+Ol miss 86.55 30.70 1. 96E-02 2.06E-01 miss 105.31 21.10 -5.65E-02 2.04E-D1 miss + Tl-208 583.19

• 85.00 1.26E-01 6.SSE-02 6.55E-02 miss + Bi-211 351.07

• 13. 02 1.20E+OO 2.27E-01 2.27E-01 miss + Pb-211 404.85 3.78 -1. 26E-01 7.82E-01 7.82E-01 miss 6/6,,., 16 2:19: 57PM Page 7 of8 Analysis Report for 06-Jun-16-10005 L310224AFGRS004SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCVgrams) (pCVgrams) (pCi!grams)

Corr Pb-2 1 1 42"7.09 1. 76 -3.00E-01 7.82E-0 1 1.41E+OO miss 832.0 1 3.52 8.51E-0 2 9.44E-01 miss + Bi-212 39.86 1. 06 -2.82E+OO 9.49E-01 2.41E+Ol miss 727.33 6.67 6.81E-01 9.49E-01 miss 785.37 1.10 1.73 E-01 3.63E+OO miss 1620.50 1. 47 1.0l E+OO 3.59 E+OO miss + Pb-212 115 .18 0.60 9.15E-01 1. 25E-01 6.53E+00 miss 238.63 *-43.60 4.27E-01 l.25E-01 m i ss 300.09 3.30 4.94E-01 1.15E+OO miss + Pb212-XR 74.82 10.28 1. 05E+OO 7.63E-01 1.41E+00 miss 7 7 .11 17.10 4.84 E-01 7.63E-01 miss 87.35 3.97 3.41E-01 1.63E+OO m i ss 89.78 1. 46 -9.58E-01 3.98E+OO miss + Bi-214 609.32

• 45.4 9 4. llE-01 8.21E-02 8.21E-0 2 miss 768.36 4.89 4.91E-01 9.72E-01 miss 80fi .18 1. 26 3.21E-01 3.22E+OO m i ss 934.06 3.11 2.87E-01 1.36E+OO mi.3S 1120.29 14.92 2.55E-01 4.55E-01 miss 1155. 21 1. 63 4.lOE-01 2.77E+OO miss 1 238.12 5.83 5.03E-01 l.28E+OO miss 1280.98 1. 43 -1.54E+OO 2.77E+OO m i ss 137 7. 6 7 3.9 9 5.0lE-01 l.46E+OO m i ss 1385. 31 0.79 1.47E+OO 5.29 E+OO miss 1401. 52 1. 33 5.41E-01 3.88E+OO miss 1407.99 2.39 -7.53 E-01 1.21E+OO miss 1 509.21 2.13 -8.37E-02 2.35E+OO m i ss 1 661.27 1. 05 -2.67E-01 3.15E+OO miss 1 729.59 2.88 O.OO E+OO 4.35E-01 miss 1764.49

• 15.30 3.81E-01 3.06 E-01 miss 1847.43 2.03 2.39E-01 1.76E+OO miss > 2118.5 1 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 4.28E-01 8.30E-02 6.16E-01 miss 295.22

• 18.42 2.71E-01 2.69E-01 miss 351.93

• 35.60 4.40E-01 8.30E-0 2 m i ss 785.96 1. 06 -4.19E-01 3.54E+O O miss + Pb214-XR 74.82 5.80 l.86E+OO 1.35E+OO 2.50E+OO m i ss 77.11 9.70 8.53E-01 1.35E+OO miss 87.35 2.24 6.04E-01 2.39E+OO miss 89.78 0.82 -1.71E+OO 7.09E+OO miss + Ra-226 186.21 3.64 1.lOE-01 9.44E-0 1 9.44E-01 miss + Ac-228 129.07 2.42 5.71E-01 l.89E-0 1 1.6 1 E+OO m i ss 209.25 3.89 3.65E-02 7.80E-01 miss 270.24 3.46 6.36E-01 1.07E+OO miss 328.00 2.95 2.84 E-01 1. 27E+OO miss 338.32 -*-11. 27 4.42E-01 2.76E-01 miss 409.46 1. 92 6. 96E-01 2.00E+OO m i ss 463.00 4.40 3.lOE-01 9.0 l E-01 miss 794.95 4.25 4.21E-01 l.1 9E+OO miss 911. 20

• 25.80 3.98E-01 1.89E-01 miss 964. 77 4.99 3.99E-01 1.15E+OO miss 968. 97 15.80 2.88E-01 4.36E-Ol m i ss Analysis Report for 06-Jun-16-10005

+ + + + + * > L310224AFGRS004SS (DRIED) Nuclide Energy Yield(%) Activity Name (keV) (pCi/grams)

Ac-228 1588.20 3.22 5.88E-02 Pa-231 27.36 10.30 -2.87E-01 2 83.69 1. 70 -5.64E-01 300.0 7 2.47 6.60E-01 302.65 2.20 1.59 E-0 2 330.06 1. 4 0 -7.42E-01 Th-234 92.38 2 .13 1.57E-01 92.80 2.10 1.32E+OO 112.81 0.2 1 4.83E+OO U-235 143.76 10.96 -9.06E-02 163.33 5.08 7.16E-0 2 1 85. 71 57.20 -3.50E-0 3 2 02 .11 1. 08 -9.07E-01 205.31 5.01 -2.84E-01 Am-241 59.54 35.90 -1. OlE-01 -Nuclide identified during the nuclide identification

= Energy line found in the spectrum = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction 6/6/<.,; 16 Nuclide MDA (pCilgrams) 1.89E-01 1.49E+O O 3.38E+OO 6.00E-02 7.52E-01 ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 2:19:57PM Page 8 of 8 Line MD.4. Coinc (pCi/grams)

Corr 1.25E+OO miss 2.58E+OO miss 1.58E+OO miss l.54E+OO miss l.49E+OO m i ss 2.24E+OO m i ss 3.38E+OO miss 3.53E+00 miss 2.23E+01 m i ss 2.98E-01 miss 6.7 6E-01 miss 6.00E-02 miss 2.36E+OO m i ss 5.48E-01 miss 7.52 E-01 miss 60 55 50 45 --+0 35 V> ,1-1 C: =3 8 30 25 I .c Q.. 20 ..1.5 10 5 0 1000 DO I I-2000 3000 0000015071.CNF 4000 channel 5000 Li v e T i me : 600.000 se c Real r i me : 600.900 sec Start: 1: -0.l(kev) Stop : 8 192: 2 047. O(keV) A c q. Sta r t :M o n Jun 06 14:09: 00 2 016 6000 7000 8000 617/~,., , o 10:24:42AM

• _ J\pex-Gamma Analysis Report for 07-Jun-16-10002 L310224AFR GS005SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time DeadTime Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 07-Jun-16-10002

L310224AFRGS005SS (DRIED) : Miscellaneous

1. 771 E+03 grams : Default : 6/2/2016 1 :OO:OOPM : 6/7/2016 10:13:43AM

130G 1 L Sand Sample : JWelch : P40818B '. 130G Sand 600.0 seconds 600.9 seconds 0.14 % 2.80 120-8192 120 -8192 1.000FWHM . 1/27/2016 . 1/5/2015 : 15084 PEAK WITH NID REPORT Peak Analysis Performed on : 617/2016 10:24:11AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Defaul t\Library\Zion Lib-BNL.NLB

1.000FWHM Page I of8 6/7/20*,~ 10:24:42AM Page 2 of8 Analysis Report for 07-Jun-16-10002 L310224AFRGS005SS (DRIED) Peak Energy RO! No. (keV) start 1 238.54 948 -2 295.17 1176 -3 351.84 1401 -4 583.22 2325 -5 609.23 2430 -6 911. 06 3639 -7 1120. 52 4476 -8 1460.86 5832 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma RO! end 960 1187 1413 2340 2445 3651 4488 5853 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 954.66 1. l 7E+02 30.74 9.00E+Ol 1180.99 4.88E+Ol 21. 94 5.65E+Ol 1407.54 6.47E+O l 21.63 4.47E+Ol 2332.65 4.57E+Ol 17.34 2.25E+01 2436.67 6.76E+Ol 18.01 1.08E+Ol 3643.95 3.20E+Ol 12. 93 7.97E+OO 4482.05 2.21E+Ol 10. 96 7.80E+OO 5844.39 1. 38E+02 24.12 5.93E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 1. 00 146 0.82

• 10.66 4.8 3 E+OO 9.42E-01 Tl-208 1. 00 583.19

• 85.00 1.0BE-01 4.29E-02 Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 2. 96 E-0 1 9 .13E-0 2 300.0 9 3.30 Bi-214 0.99 609.32

• 4 5.49 3.0 7 E-01 8.96E-02 768.36 4.89 806.18 1.26 934.0 6 3.11 11 20.29

• 14.92 4.60E-01 2.31E-01 1155. 21 1. 63 1 238.12 5.83 1280.9 8 1. 43 13 77. 67 3.99 1385.3 1 0.79 140 1.52 1. 3 3 14 0 7.99 2.39 1509.2 1 2 .13 Tentative Nuclide Pb-212 Pb-21'1 Eu-152 Pb-214 Bi-211 Tl-208 Bi-214 Ac-228 Bi-214 K-40 Caine Corr m iss mis s miss miss mi ss An~lysis Report for 07-Jun-16-10002 L310224AFRGS005SS (DRIED) Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1661. 27 1729.59 1764.49 1847.43 2118.51 Pb-214 1. 00 ~4 1. 99 295.22 351. 93 785.96 Ac-228 0.95 129.07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911. 20 964.77 968. 97 1588.20 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance:

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 2.42 3.89 3.46 2.95 11. 27 1. 92 4.40 4.25 25.80 4.99 15.80 3.22 miss = Nuclide energy was not found in the coincidence library. 617/2\rnJ 10*24:42AM Page3 of8 Activity Activity Caine (pCi/grams)

Uncertainty Corr 3.34E-01 1. 60E-01 miss 2.56E-01 9.50E-02 miss 3.36E-01 l.39E-01 miss INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 1. 000 4.83E+O O 9.42E-01 Tl-208 1. 000 1.08E-0 1 4.29E-02 X Bi-211 0. 964 An1;:1lysis Report for 07-Jun-16-10002 L310224AFRGS005SS (DRIED) Nuclide Nuclide Name Id Confidence Pb-212 1. 000 Bi-21 4 0.999 Pb-214 1. 000 Ac-228 0.956 ? = nuclide i s part of an undetermined solution X = nuclide rejected by the interference analysis 6/7/2v . .., Wt mean Activity (pCilgrams) 2.96E-01 3.27E-0 1 2.77E-0 1 3.36E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10:24:42AM Page4 of 8 Wt mean Comments Activity Uncertainty 9.13E-02 8.36E-02 8.16E-02 l.39E-01 6/7/20 "' 10:24:42AM Anralysis Report for 07-Jun-16-10002

+ + + + + + + + L310224AFRGS005SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy {keV) All peaks were id entified.

M = First peak in a multiplet region m = Other peak in a multiplet reg ion F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6f7/2 0 16 10: 24:10AM : 120 : 8192 Peak CPS {°.to) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (keV) (pCi!grams) (pCi!grams) (pCilgrams)

K-40 1460.82

• 10. 66 4.83E+OO 4.08E-01 4.08E-01 Cr-51 320.08 9.91 6.36E-02 3.14E-Ol 3.14E-01 Mn-54 834.85 99.98 -l.42E-02

1. 90E-02 1.90E-02 Co-58 810.76 99.45 2.75 E-03 3 .17E-02 3.17E-02 1674.73 0.52 -7.34E-01 6.17E+OO Co-60 1173.23 99.85 -9.17E-04 3.24E-02 5.35E-02 1332.49 99.98 3.98E-03 3.24E-02 Nb-94 702.65 99.81 -2.24E-02 l.6 7 E-02 l.67E-02 871. 09 99.89 4.37E-04 2.44E-02 Ag-108m 79 .13 6.60 4.19E-01 l.94E-02 1.41E+OO 433.94 90.50 3.61E-04 1.94E-02 614.28 89.80 l.16E-02 3.03E-02 722. 94 90.80 -3.40E-03 3.60E-02 Sn-113 255 .13 2.1 1 -2. llE-01 3.63E-02 1. 35E+OO 391.70 64.97 1.79E-03 3.63E-02 Page 5 of8 Tolerance Nuclide Caine Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free + Cs-134 475.36 1. 48 -6.96E-01 2.77E-02 l.55E+OO miss 563.25 8.34 l.18E-01 4.27E-01 miss 569.33 15.37 8.58E-03 l.82E-01 miss 604. 72 97.62 -1. OlE-02 2. 77E-02 miss 6/7/2() IV 10: 24:42AM Page 6 of8 Analysis Report for 0 7-Jun-16-1 0 002 L310224AFRGS005SS (DRIED) Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCi!grams) (pCi!grams)

Corr Cs-134 795.86 85.46 2.13E-02 2.77E-02 5.05E-02 miss 801.95 8.69 2.39E-02 3.44E-01 miss 1038.61 0.99 3.00E-01 2.21E+OO miss 1167.97 1. 79 3.32E-01 2.84E+OO miss 1365.19 3.02 8.42E-02 l.2 7E+OO m i ss + Cs-137 661.66 85.10 1.69E-02 4.6 5E-02 4. 65E-02 miss + Eu-152 121. 78 28.67 -8.63E-03

1. 08E-01 l.13E-01 miss 244.70 7.61 -7.51E-02 3.69E-01 miss 295.94 0.45 9.21E+OO 1.08E+Ol miss 344.28 26.60 9.14E-03 1.08E-01 miss 367.79 0.86 -2.03E+OO 2.38E+OO miss 411.12 2.24 -2.33E-01 l.17E+00 miss 443. 96 2.83 8.95E-02 9.32E-01 miss 488.68 0.42 -3.17E-02 6.71E+OO miss 563.99 0.49 -2.lOE+OO 5.63E+OO miss 586.26 0.46 2.19E-01 6.57E+OO miss 678.62 0.47 1.73E-01 6.17E+OO miss 688.67 0.86 -1.96E-01 3.68E+OO miss 719.35 0.28 -2.62E+OO 1.17E+Ol miss 778.90 12.96 8.61E-03 2.26E-01 miss 810.45 0.32 9.09E-01 9.35E+OO miss 867.37 4.26 -3.41E-03 6.61E-01 miss 919.33 0.43 1. 06E+00 5.91E+OO miss 964.08 14.65 l.56E-01 3.48E-01 mi s s 1085.87 10.24 -3.49E-02 2.76E-01 miss 1089.74 1. 73 5.23E-01 2.12E+OO miss 1112.07 13.69 l.68E-02 2. 96E-01 miss 1212.95 1. 43 8.43E-01 3.44E+OO miss 1249.94 0.19 7.57E+OO 2.65E+Ol miss 1299.1 4 1. 63 -3.0lE-02 l.96E+OO miss 1408.01 21. 07 7.13E-02 2.43E-01 miss 1457.64 0.50 O.OOE+OO 1.49E+Ol miss 1528.10 0.28 O.OOE+OO 3.71E+OO miss + Eu-154 123.07 40.40 6.41E-03 7.43E-02 7.63E-02 miss 247.93 6.89 6.95E-02 4.70E-01 miss 591. 7 6 4.95 l.29E-01 7.42E-01 miss 692.42 1. 78 -4.48E-01 1.66E+OO miss 7.23.30 20.06 -6.42E-02 1.24E-01 miss 756.80 4.52 -9.25E-02 6.35E-01 miss 873.18 12.08 1.45E-02 2.34E-Ol miss 996.29 10.48 0.00E+OO 7.43E-02 miss 100 4.76 18.01 6.96E-02 2.55E-01 miss 1274.43 34.80 6.94E-04 9.02E-D2 miss 1596.48 1. 80 -l.39E-01 1.64E+OO miss + Eu-155 45.30 1. 31 1.0 7E+01 1. 95E-01 1.94E+Ol miss 60.01 1. 22 -5.08E+00 1.91E+Ol miss 86.55 30.70 -7.42E-03 2. llE-01 miss 105.31 21.10 3.49E-02 1.95E-01 miss + Tl-208 583.19

• 85.00 1. OBE-01 4.85E-02 4.BSE-02 miss + Bi-211 351.07

• 13.02 7.0lE-01 2.87E-01 2.87E-01 miss + Pb-211 404.85 3.78 1.28E-02 6.8-;'E-01 6.87E-01 miss 6/7/20 ,.., 10:24:42AM Page 7 of8 Analysis Report for 07..Jun-16-10002 L310224AFRGS005SS (DRIED) Nuclide Er.ergy Yield{%) Activity NuclideMDA LineMDA Coir.c Name (keV) (pCilgrams) (pCilgrams) (pCi!grams)

Corr Pb-211 427.09 1. 76 -8.14E-02 6.87E-01 l. 38E+OO miss 832.01 3.52 1. 41E-01 l. 08E+OO miss + Bi-212 39.86 1. 06 -1.14E+Ol 6.32E-01 l. 80E+Ol miss 727.33 6.67 2.0lE-02 6.32E-01 miss 785.37 1.10 9.99E-01 3.33E+OO miss 1 620.50 1. 47 4.47E-01 2. 96E+00 miss + Pb-212 115 .18 0.60 -6.30E-01 9.77E-02 5.51E+OO miss 238.63

• 43.60 2. 96E-01 9.77E-02 miss 300.09 3.30 2.64E-01 l.15E+OO miss + Pb212-XR 74.82 10.28 5.44E-01 6.86E-01 l.16E+OO miss 77 .11 17.10 4.48E-01 6.86E-01 miss 87.35 3.97 1. 02E+OO 1. 68E+OO miss 89.78 1. 46 8.91E-01 3.88E+OO miss + Bi-214 609.32

• 45.49 3.07E-01 6.71E-02 6.71E-02 miss 768.36 4.89 1.91E-01 8. 94E-01 miss 806.18 1.26 -1.48E-01

2. 37E+OO miss 934.06 3.11 6.SOE-01 1.54E+OO miss 1120.29

• 14.92 4.60E-01 2. 4 9E-01 miss 1155.21 1. 63 2.40E-01 2. 7 3E+00 miss 1238.12 5.83 -3.25E-01 6.llE-01 miss 1280.98 1. 43 1.18E+00 3.lOE+OO miss 1377.67 3.99 -5.llE-02 9.63E-01 miss 1385.31 0.79 6.45E-02 3.32E+OO miss 1401.52 1. 33 -1.16E-01 2.00E+OO miss 1407.99 2.39 6.28E-01 2.14E+OO miss 1509.21 2.13 2.0SE-01 1.93E+00 miss 1661.27 1. 05 9.83E-02 2.89E+00 miss 1729.59 2.88 8.85E-01 2.08E+OO miss 1764.49 15.30 3.16E-01 5.31E-01 miss 1847.43 2.03 4.38E-01 2.04E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 6.20E-01 l.05E-01 5.95E-01 miss 295.22

• 18.42 3.34E-01 2.09E-01 miss 351.93

• 35.60 2.56E-01 1.05E-Ol miss 785.96 1. 06 1. OOE+OO 3.66E+OO miss + Pb214-XR 74.82 5.80 9.64E-01 1.21E+OO 2.0SE+OO miss 77 .11 9.70 7.90E-01 1.21E+D0 miss 87.35 2.24 l.80E+OO 2. 97E+D0 miss 89.78 0.82 1.59E+OO 6.91E+OO miss + Ra-226 186.21 3.64 3.54E-01 9.25E-01 9.25E-01 miss + Ac-228 129.07 2.42 -5.38E-02

1. 36E-01 1.28E+00 miss 209.25 3.89 l.07E-01 7.63E-01 miss 270.24 3.46 5.60E-01 9.58E-01 miss 328.00 2.95 -2.35E-01 1.05E+OO miss 338.32 11. '.27 3.43E-01 3.97E-01 miss 409.46 1. 92 8.91E-01 1.79E+OO miss 463.00 4.40 9.80E-02 8.72E-01 miss 794.95 4.25 4.33E-01 1.0SE+OO miss 911. 20

• 25.80 3.36E-01 1.36E-01 miss 964. 77 4.99 2.lOE-01 9.82E-01 miss 968.97 15.80 2.43E-01 3.91E-01 miss 617/2l,,-, 10:24:42AM Page 8 of8 Analysis Report for 07-Jun-16-10002 L310224AFRGS005SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCilgrams) (pCilgrams) (pCi/grams)

Corr Ac-228 1588.20 3.22 O.OOE+OO l.36E-0 1 3.34E-01 miss + Pa-231 27.36 10.30 4.63E-01 1.49E+OO 2. 33E+OO miss 283.69 1. 70 -7.84E-02 l.50E+OO miss 300.07 2.47 3.53E-01 l.54E+OO miss 302.65 2.20 -l.18E-01 l.49E+OO miss 330.06 1. 4 0 l.20E+00 2.47E+OO miss + Th-234 92.38 2 .13 9.24E-01 3.41E+OO 3.41E+00 miss 92.80 2.1 0 9.lOE-01 3.41E+OO miss 112. 81 0.21 -4.33E+00 1.77E+Ol miss + U-23 5 143.76 10.96 -2.40E-02 5.70E-02 2.74E-01 miss 163.33 5.08 -8.51E-02 5.53E-01 miss 185. 71 57.20 1.23E-02 5.70E-02 miss 202 .11 1. 08 -4.12E-01 2.70E+OO miss 205.31 5.01 7.44E-02 5.23E-01 miss + Arn-241 59.54 35.90 1. 05E-01 7.04E-01 7.04E-01 miss + = Nuclide identified during the nuclide identification

• "' Energy line found in the spectrum > -"' MDA value not calculated

@ _,._ Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed. free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

V) +-' C: :::I 60 55 50 40 35 8 30 25 20 15 10 5 ~\ 1000 2000 3000 0000015084.CNF 4000 channel 5000 Live Time 600.000 sec Real Time 600.870 sec start: 1 -0. l(kev) stop : 8192 2047 .O(kev) Acq. Start Tue >un 07 10:13:43 2016 6000 7000 8000 6/7!"Lv 16 10:57:07AM I _pex-Gamma Analysis Report for 07-Jun-16-10003 L310224AFRGS006SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 07-Jun-16-10003

L310224AFRGS006SS (DRIED)

Miscellaneous 1.714E+03 grams : Default : 6/2/2016 2:26:00PM

6/7/2016 10:46:29AM

130G 1LSand Sample : JWelch : P11314X2 : 130G Sand : 600.0 seconds : 600.5 seconds : 0.09% : 2.80 : 120 -8192 : 120-8192 : 1.000FWHM

! 1/27/2016

! 11/26/2012 . 15085 PEAK WITH NID REPORT Peak Analysis Performed on : 6/7/2016 10:56:35AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Ca nberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page 1 of&

6/7/2(; o',) 10:57:07AM Page 2 of8 Analysis Report for 07-Jun-16-10003 L310224AFRGS006SS (DRIED) M m Peak Energy ROI No. (keV) start 1 74.81 295 -2 77.00 295 -3 185.85 740 -4 238.69 950 -5 295.20 1176 -6 338.41 1348 -7 352.05 1401 -8 498.73 1990 -9 583.21 2325 -10 609.25 2428 -11 726.92 2902 -12 794.96 3174 -13 860.63 3437 -14 911. 30 3637 -15 969 .11 3868 -16 1120.32 4474 -17 1460.81 5834 -M = First peak in a multiplet regio n m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 315 315 751 960 1187 1360 1415 1999 2340 2444 2911 3183 3446 3653 3880 4487 5852 Peak. Net Peak Net Area Continuum Centroid Area Uncertainty Counts 300.48 7.90E+Ol 21.50 1.14E+02 309.21 8.85E+Ol 22.32 1.17E+02 743.99 4.32E+Ol 24.40 8.17E+Ol 955.09 2.20E+02 36.68 9.56E+Ol 1180.86 8.38E+Ol 23.81 4.63E+Ol 1353.51 4.79E+Ol 18.46 3.22E+Ol 1407.99 1.42E+02 26.99 3.24E+Ol 1994.17 9.64E+00 9.31 1. 07E+Ol 2331.85 9.21E+Ol 22.14 2.37E+Ol 2435.92 1.26E+02 24.35 1. 68E+Ol 2906.38 1. 85E+Ol 10.03 6.91E+00 3178.42 1. 44E+Ol 9.69 9.30E+OO 3441.03 l.26E+Ol 7.83 2.86E+OO 3643.70 4.95E+O l 16.78 1.70E+Ol 3874.92 2.35E+O l 12.17 1. 30E+Ol 4479.84 3.02E+O l 12.88 9.60E+OO 5842.59 1.23E+02 23.57 1. 32E+Ol NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 1. 00 1 460.82

• 10.66 4.0lE+OO 8.42E-01 Tl-208 1. 00 583.19

• 85.00 2.02E-01 5.43E-02 Bi-212 0.99 39.86 1. 06 727. 33

• 6.67 6.02E-01 3.33E-01 785.37 1.10 Tentative Nuclide Pb214-XR Pb212-XR Pb214-XR Pb212-XR U-235 Ra-226 Pb-212 Pb-214 Eu-152 Ac-'.228 Pb-214 Bi-211 Tl-208 Bi-2 14 Bi-212 Ac-228 Cs-134 Ac-228 Ac-228 Bi-214 K-40 Caine Corr miss miss miss 617/21.J,u 10:57:07AM Pagc3 of 8 Analysis Report for 07-Jun-16-10003 L310224AFRGS006SS (DRIED) Nuclide Id Energy Yield(%) Activity Activity Caine Name Confidence (keV) (pCilgrams)

Uncertainty Co" Bi-212 0.99 1620.50 1. 47 Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 5. llE-01 l.19E-01 miss 300.09 3.30 Pb212-XR 0.77 74.82

• 10.28 l.45E+O O 4.95E-01 miss 77 .11

• 17.10 9.04E-01 2.94E-01 miss 87.35 3.97 89.78 1. 46 Bi-214 1. 00 609.32

• 45.49 5.31E-01 1.21E-01 miss 768.36 4.89 806.18 1. 26 934.06 3.11 1120.29

• 14.92 5.85E-01 2.54E-Ol miss 1155. 21 1. 63 1238.12 5.83 1280.98 1. 43 1 377.67 3.99 1385. 31 0.79 1 401.52 1. 33 1 407.99 2.39 1 509.21 2.13 1661.27 1. 05 1729.59 2.88 1 764.49 15.30 1847.43 2.03 2118. 51 1.16 Pb-214 1. 00 241.99 7.25 295.22 .-18.42 5. 31E-D1 1.73E-01 miss 351.93

• 35.60 5.22E-Ol 1.30E-01 miss 785. 96 1. 06 Ra-226 0.99 186.21

• 3.64 l.05E+OO 6.17E-01 miss Ac-228 1. 00 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 ,.. 11. 27 5.43E-Ol 2.27E-01 miss 409.46 1. 92 463.00 4.40 794.95

• 4.25 7.76E-01 5. 31E-01 miss 911. 20

• 25.80 4.84E-01 1.69E-Ol miss 964.77 4.99 968. 97

• 15.80 3.91E-01 2.05E-01 miss 1 588.20 3.22 U-235 0.99 143.76 10. 96 163.33 5.08 185.71

• 57.20 6.68E-02 3.93E-02 miss 202.11 1. 08 205.31 5.01 Analysis Report for 07-Jun-16-10003 L310224AFRGS006SS (DRIED) * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activ i ty Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 6/7/20,., 10:57:0?AM INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Name Id Activity Activity Confidence (pCi/grams)

Uncertainty K-40 1. 000 4.0lE+OO 8.42E-01 Tl-208 1. 000 2.02E-01 5.43E-02 X Bi-211 0.943 Bi-212 0.993 6.02E-01 3.33E-01 Pb-212 1.000 5. llE-01 1.19E-0 1 Pb212-XR 0.775 1. OSE+OO 2.53E-Ol Bi-214 1. 000 5.41E-01 1. 09E-Ol Pb-214 1. 000 5.25E-0 1 1.04E-01 X Pb214-XR 0.776 ? Ra-226 0.992 1.0SE+OO 6.17E-01 Ac-228 1. 000 4.84E-01 1.llE-01 ? U-235 0.999 6.68E-02 3.93E-02 ? = nuclide is part of an undetermined solution X -nuclide rejected by the interference analysis @ :::; nuclide contains energy Jines not used in Weighted Mean Activity Errors quoted at 2.000sigma Page 4 of8 Comments 6/7/2u,., 10:57:0?AM Page 5 of8 Analysis Report for 07-Jun-16-10003

+ + + + + + + + + L310224AFRGS006SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. 8 13 Energy (keV) 498.73 860.63 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/7/2016 10:56:35AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty l.60667E-02 2.09524E-02 48.30 31.14 Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCVgrams) (pCi/grams)

Corr K-40 1460.82

• 10.66 4.0lE+OO 5.09E-01 5.09E-Ol miss Cr-51 320.08 9.91 6.66E-02 3.44E-01 3.44E-01 free Mn-54 834.85 99.98 3.33E-03 3.39E-02 3.39E-02 miss Co-58 810.76 99.45 -3.85E-03 3.22E-02 3.22E-02 miss 1674.73 0.52 O.OOE+OO 2. llE+OO miss Co;.....60 1173.23 99.85 -2.56E-03 2.20E-02 2.20E-02 miss 1332.49 99.98 9.26E-05 4.25E-02 miss Nb-94 702.65 99.81 9.26E-03 3.21E-02 3.69E-02 miss 871.09 99.89 5.30E-03 3.21E-02 miss Ag-108m 79 .13 6.60 -4.56E-03 2.93E-02 8.26E-01 miss 433.94 90.50 -1.34E-03 2.93E-02 miss 614.28 89.80 l.52E-02 3.90E-02 miss 722. 94 90.80 3.04E-03 3.35E-02 miss Sn-113 255.13 2.1 1 6.52E-01 5.16E-02 1. 29E+OO free 391.70 64.9'7 1.03E-02 5.16E-02 free Cs-134 475.36 1. 48 1.14E-01 1. 83E-02 2.00E+OO m i ss 6/7/2u ,v 10:57:0?AM Page 6 of 8 Analysis Report for 07-Jun-16-10003 L310224AFRGS006SS (DRIED) Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCilgrams)

Corr Cs-134 563.25 8.34 1. 43E-01 l.83E-02 4.28E-01 miss 569.33 15.37 -l.23E-02 2.00E-01 miss 604. 72 97.62 -7.09E-03 1.83E-02 miss 795.36 85.46 -9.46E-03

5. 92E-02 miss 801.95 8.69 -8.55E-02 3.SOE-01 miss 1038.61 0.99 -1. 09E-01 3. 94E+OO miss 1167.97 1. 79 -8.92E-02 2.00E+OO miss 1365.19 3.02 4.70E-02 8.07E-01 miss + Cs-137 661.66 85.10 1.21E-02 4.50E-02 4.SOE-02 miss + Eu-152 121. 78 28.67 2.45E-02 9.4:E-02 l.03E-01 miss 244.70 7.61 9.60E-02 3.58E-01 miss 295.94 0.45 1.87E+Ol 1 . .23E+01 miss 344.28 26.60 -1.62E-02 9.47E-02 m i ss 367.79 0.86 -9.95E-01 2.62E+OO miss 411.12 2.24 -1.70E-01 l.47E+OO miss 443.96 2.83 l.08E-01 9.91E-01 miss 488.68 0.42 -2.60E+OO 6.24E+00 miss 563.99 0.49 2.0lE+OO 7.00E+OO miss 586.26 0.46 -8.26E-01 6.79E+OO miss 67 8. 62 0.47 1. 51E+00 6.18E+OO miss 688.67 0.86 1. 88E+OO 4.41E+OO miss 719.35 0.28 4.79E+OO 1.SOE+Ol miss 778.90 12. 96 5.83E-02 2.63E-01 miss 810.45 0.32 -2.42E+OO 8.72E+OO miss 867.37 4.26 -1.62E-01 5.31E-01 miss 919.33 0.43 -1.98E+OO 7 .13E+OO miss 964. 08 14.65 8.29E-02 3.12E-01 m i ss 1085.87 10.24 -8.69 E-02 2.04E-01 miss 1089.74 1. 73 -2.81E-01 l.77E+OO miss 1112. 07 13.69 6.60E-02 3.16E-01 miss 12 12.95 1. 43 -1.22E-01 2.30E+OO miss 1249.94 0.19 5.87E+OO 2.32E+Ol miss 1299.14 1. 63 1.40E-01 2.llE+OO miss 1408.01 21. 07 l.OlE-01 2.79E-01 miss 1457.64 0.50 -1.03E+Ol 9.71E+OO miss 1528.10 0.28 1. 82E-01 1.18E+Ol miss + Eu-154 12 3.07 40.40 1.76E-03 7.0?E-02 7.07E-02 miss 247.93 6.89 2.08E-01 3.92E-01 miss 591. 76 4.95 -7.62E-02 6.35E-01 miss 692.42 1. 78 -5.31E-01 l.67E+OO miss 723. 30 20.06 3.59E-03 l.41E-01 miss 756.80 4.52 2.94E-01 8.93E-01 miss 873.18 12.08 -1.91E-02 2.lBE-01 miss 996. 29 10.48 -7.39E-02 2.75E-01 miss 1004.76 18.01 -6.48E-02 1.lOE-01 miss 127 4.43 34.80 -3.44E-03 9.73E-02 miss 1596.48 1. 80 -1.03E-01 1.52E+OO miss + Eu-155 45.30 1. 31 -1.76E+00 1.50E-01 6.99E+OO miss 60.01 1. 22 -3.19E+OO 8.24E+D0 miss 86.55 30.70 -1.74E-02 1. 50E-Ol miss 105.31 21.10 l.BlE-03 1.65 E-01 m i ss 6/7/2u ,v 10:57:07AM Page 7 of8 Analysis Report for 07-Jun-16-10003 L310224AFRGS006SS (DRIED) Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCi/grams)

{pCi!grams) (pCilgrams)

Corr + Tl-208 583.1 9

• 85.00 2.02E-Ol 4.57E-02 4. 57E-02 miss + Bi-211 351.07

• 13.02 1.43E+OO 2.37E-01 2.37E-01 miss + Pb-211 404.85 3.78 -1.23E-01 5.76E-01 5. 76E-01 miss 427.09 1. 76 -1.44E-01 1.42E+OO miss 832.01 3.52 -3.36E-02

8. 08E-01 miss + Bi-212 39.86 1. 06 -3.61E+OO 3.63E-01 7. 65E+00 miss 727. 33

• 6.67 6.02E-01 3.63E-01 miss 785.37 1.10 -1.84E-Ol 3.45E+OO m i ss 162 0.50 1. 47 5. 96E-01 2. 75E+OO miss + Pb-212 115.1 8 0.60 2.25E+OO 8.86E-02 5.13E+OO miss 238.63

• 43.60 5. llE-01 8. 86E-02 miss 300.09 3.30 4. 71E-01 1. 09E+OO miss + Pb212-XR 74.82 .L 10.28 1. 45E+00 3.91E-01 6. 93E-01 miss 77 .11

• 17.10 9.04E-01 3.91E-01 miss 87.35 3.97 5.67E-01 l .19E+OO miss 89.78 1. 46 4.21E-01 2.76E+OO miss + Bi-214 609.32

• 45.49 5.31E-01 7.75E-02 7.75E-02 miss 768.36 4.89 4.73E-01 9.51E-01 miss 806.18 1. 26 -2.lOE-01 2. 76E+OO miss 934.06 3 .11 8.52E-01 1. 50E+OO miss 1120.29

• 14.92 5.85E-01 2. 66E-01 miss 1155.21 1. 63 8.90E-01 3.27E+OO miss 1238.12 5.83 3.47E-01 l.06E+OO miss 1280.98 1. 43 6.28E-01 3.66E+00 miss 1377. 67 3.99 2.06E-01 l.17E+OO miss 1385. 31 0.79 9.00E-01 5.0SE+OO miss 1401.52 1. 33 1. 62E+OO 4.0lE+OO miss 1407.99 2.39 8.85E-01 2. 45E+OO miss 1 509.21 2.13 3.67E-01 2 .19E+OO miss 1 661. 27 1. 05 3.66E-01 3.39E+OO miss 1729.59 2.88 5.59E-01 l.80E+OO miss 1764.49 15.30 6.87E-01 7.27E-01 miss 1847.43 2.03 1.66E+OO 3.39E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss Pb-214 241.99 7.25 5.36E-01 8.68E-02 5.71E-01 miss 295.22

• 18.42 5.31E-01 1.76E-Ol miss 351.93

• 35.60 5.22E-01 8.68E-02 miss 785. 96 1. 06 l.62E+OO 4.0SE+OO miss + Pb214-XR 74.82

• 5.80 2.57E+OO 6.89E-01 l.23E+OO miss 77 .11

• 9.70 1.59E+OO 6.89E-01 miss 87.35 2.24 1. OlE+OO 2. llE+OO miss 89.78 0.82 7.50E-01 4.92E+OO miss + Ra-226 186.21

• 3.64 1. 05E+OO 8.88E-0 1 8.88E-01 miss + Ac-228 129.07 2.42 2.64E-01 1.73E-01 l.27E+OO miss 209.25 3.89 4.05E-01 7.88E-01 miss 270.24 3. 46 7.92E-Ol l.07E+OO miss 328.00 2.95 6.93E-01 l.21E+OO miss 338.32 11. 27 5.43E-01 2.58E-01 miss 409.46 1. 92 7.34E-01 l.90E+OO miss 463.00 4.40 2.63E-01 8.31E-01 miss 6/7/2{J IV 10:57:0?AM Pag.: 8 of8 Analysis Report for 07-Jun-16-10003 L310224AFRGS006SS

{DRIED) 1-lucllde Energy Yield(%) Activity Nuclide MDA LlnellJDA Caine Name (keV) (pCUgrams) (pCUgrams) (pCi/grams)

Corr Ac-228 794.95

• 4.25 7.76E-01 l.73E-01 6.83E-01 miss 911. 20

• 25.80 4.84E-01 1.73E-01 miss 964. 77 4.99 3.84E-01 9.88E-01 miss 968. 97

• 15.80 3.91E-01 2.46E-01 miss 1588.20 3.22 1.86E-01 1.24E+OO miss + Pa-231 27.36 10.30 O.OOE+OO 9.99E-02 9. 99E-02 miss 283.69 1. 70 2.44E-01 l.46E+OO miss 300.07 2.47 6.29E-01 l.46E+OO miss 302.65 2.20 7.91E-02 l.15E+OO miss 330.06 1. 40 -1.28E+OO l.86E+OO miss + Th-234 92.38 2 .13 1.15E-02 2.35E+OO 2.35E+OO miss 92.80 2.10 l.77E+OO 2. 60E+OO miss 112. 81 0.21 -1. 57E-01 l.65E+01 miss + U-235 143.76 1 0. 96 -3.26E-02 5.65E-02 2.29E-01 miss 163.33 5.08 6.99E-02 5.42E-01 miss 185.71

• 57.20 6.68E-02 5.65E-D2 miss 202 .11 1. 08 l.14E+OO 2.59E+OO miss 205.31 5.0 1 1. 44E-01 5.25E-01 miss + Am-241 59.54 35.90 2.39E-03 3.02E-0 1 3.02E-01 miss + :::; Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? =-CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free :::; No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

120 100 90 80 70 Vl .µ C: :::s 0 60 u 50 "" 1 40 0.. "" 1 30 20 10 0 1000 2000 3000 0000015085.CNF 4000 channel 5000 Live Ti m e 600.000 sec Real Time 600.S20 sec start: 1 -0. 2(kev) stop : 8192 2047. 4(kev) Acq. Start Tue l un 07 10: 46: 29 2016 6000 7000 8000 6/7/~v 16 10:24:04AM ex-Gamma Analysis Report for 07-Jun-16-10001 L310224AFRGS007SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number

• 07-Jun-16-10001 L310224AFRGS007SS (DRIED) Miscellaneous 1.899E+03 grams : Default : 6/2/2016 1:00:00PM

6/7/2016 10:13:27AM

130G 1 L Sand Sample : JWelch : P11314X2 : 130G Sand : 600.0 seconds : 600.5 seconds : 0.08 % : 2.80 :120-8192

120 -8192 : 1.000FWHM

1/27/2016

11/26/2012

15083 PEAK WITH NID REPORT Peak Analysis Performed on : 6/7/2016 10:23:32AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Z ion Lib-BNL.NLB

1.000FWHM Page 1 of8 6/7/20,o 10:24:04AM Page 2 of8 Analysis Report for 07-Jun-16-10001 L310224AFRGS007SS (DRIED) M m M m Peak Energy ROI No. (keV) start 1 74.79 297 -2 76.84 297 -3 238.66 949 -4 241.91 949 -5 295.26 1175 -6 338.30 1347 -7 351.86 1400 -8 4 62. 8 1 184 '7 -9 510.83 2036 -10 583.16 2326 -11 609.23 2428 -12 727.42 2904 -13 860.37 3435 -14 911. 61 3637 -15 1120.38 4474 -16 1460.94 5833 -M = First peak in a multiplet region m "' Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 313 313 974 974 1186 1357 1413 1854 2047 2336 2442 2913 3445 3653 4486 5853 Peak NetPeak Net Area Continuum Centroid Area Uncertainty Counts 300.39 5.45E+Ol 19. 88 1. 19E+02 308.58 7.98E+Ol 23.15 1. 55E+02 954.94 2.44E+02 32.16 6.22E+Ol 967. 96 6.28E+Ol ::;_g .21 7.06E+Ol 1181.07 7.55E+Ol 27. 68 9.09E+Ol 1353. 07 3.73E+Ol -7. 64 3.73E+Ol 1407.24 1. 43E+02 29.03 5.62E+Ol 1850.62 9.40E+OO 9.46 1. 32E+Ol 2042.53 2.86E+O l 1 6. 39 3.49E+01 2331.65 5.55E+Ol 1 9.58 3.71E+Ol 2435.84 l.12E+02 24.82 3.31E+Ol 2908.36 l.33E+Ol 10.58 l.53E+Ol 3440.02 1.82E+Ol 10.17 7.61E+OO 3644.93 6.49E+Ol 17.29 8.24E+OO 4480.08 3.17E+Ol 13.84 1.66E+Ol 5843.08 1.49E+02 25 .27 8.89E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams)

Uncertainty K-40 0.99 1460.82

• 10.66 4.36E+OO 8.33E-01 Tl-208 1. 00 583.19

• 85.00 1.lOE-01 4.lOE-02 Bi-212 1. 00 39.86 1. 06 727. 33 6.67 3.91E-0 1 3.13E-01 785.37 1.10 1 620.50 1. 47 Tentative Nuclide Pb214-XR Pb212-XR Pb214-XR Pb212-}'.R Pb-212 Pb-214 Pb-214 Eu-152 Ac-228 Pb-214 Bi-211 Cs-138 Ac-228 Sb-125 Tl-208 Bi-2 1,J Bi-212 Ac-228 Bi-2 14 K-40 Caine Corr miss miss miss 6/7/2010 10:24:04AM Pa g e J of& Analysis Report for 07-Jun-16-10001 L310224AFRGS007SS (DRIED) Nuclide Id Energy Yield(%) Activity Activity Coinc Name Confidence (keV) (pCi/grams)

Uncertainty Corr Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 5. llE-01 l.07E-01 miss 300.09 3.30 Pb212-XR 0.99 74.82

• 10.28 9.03E-01 3.78E-01 miss 77 .11

• 17.10 7.40E-01 2.63E-01 miss 87.35 3.97 89.78 1. 46 Bi-214 1. 00 609.32

• 45.49 4.29E-01 1.08E-D1 mi s s 768.36 4.89 806.18 1. 26 934.06 3.11 1120.29

• 14. 92 5.54E-0 1 2.4 6 E-0 1 miss 1155. 21 1. 63 1238.12 5.83 1280.98 1. 43 13 77. 67 3.9 9 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1 5og.21 2.13 1661.27 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2 11 8.51 1.16 Pb-~14 1. 00 2 4 1.99

• 7.25 7.98E-01 2.64E-01 miss 295.22

• 18.42 4.32E-01 1.73E-01 miss 35 1.93

• 35.60 4.75E-01 1.23 E-01 miss 785. 96 1. 06 Ac-228 0.99 129.0 7 2.4 2 209.25 3.89 270.24 3.46 328.00 2.95 338.32

• 11.27 3.82E-01 1.91E-01 miss 409.46 1. 92 463.00

• 4.40 3.07E-Ol 3.12E-01 miss 794.95 4.25 911.20

• 25.80 5.73E-01 1.60E-0 1 miss 964. 7 7 4.99 968. 97 15.80 1588.2 0 3.22 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWH M Nuclide confidence index thres hold = 0.30 Errors quoted at 2.000sigma Analysis Report for 07-Jun-16-10001 L310224AFRGS007SS (DRIED) Coincidence correction performed.

free :a: No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 6/7/21.J 1d 10:24:04AM INTERFERENCE CORRECTED REPORT X X X Nuclide Name K-40 Sb-125 Tl-208 Bi-211 Bi-212 Pb-212 Pb212-XR Bi-214 Pb-214 Pb214-XR Ac-228 Nuclide Id Confidence 0.999 0.419 1. 000 0.962 1. 000 1. 000 0.998 1. 000 1. 000 0.998 0.997 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 4.36E+OO 1.lOE-01 3.91E-01 5. llE-01 7.93E-01 4.49E-01 5.02E-01 4.68E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty 8.33E-01 4.lOE-0 2 3.1 3E-01 1. 07E-01 2.16E-01 9.87E-02 9.36E-02 1.14E-01 Page 4 of8 Comments 6/7/2u 1ti 10:24:04AM An alysis Report for 07-Jun-16-10001

+ + + + + + + + + L310224AFRGS007SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. 9 1 3 Energy (keV) 5 1 0.83 8 6 0.37 M::: F i rst peak in a multiplet regi on m = Other peak in a m u ltiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/7/2016 10: 23:32AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 4.7 6087 E-0 2 3.03283E-02 28.7 0 2 7.93 Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCUgrams) (pCi/grams)

K-40 1460.82

• 10.66 4.36E+OO 4.0lE-01 4.0lE-01 Cr-5 1 3 2 0.08 9.91 -7.50E-02 2.47E-0 1 2.47E-01 Mn-54 834.85 99.98 ~.96E-03 2.84E-02 2.84E-0 2 Co-58 810.76 99.45 9.23E-03 3 .13E-02 3.13E-02 1674.73 0.52 O.OOE+OO l.90E+OO Co-60 117 3.23 99.85 -7.12E-03 2.SOE-02 2.SOE-02 1332.49 99.98 9.19E-03 3.83E-02 Nb-94 702.65 99.81 -5.92E-03 2.87E-02 2.87E-02 871.09 99.89 5.52E-03 3.SOE-02 Ag-108m 79.13 6.60 1.20E-01 2.64E-02 7.54E-01 433.94 90.50 5.88E-03 2.64E-02 614.28 89.80 -7.56E-03 3.52E-02 722. 94 90.80 -1.16E-02 2.81E-02 Sn-113 255.13 2 .11 1.52E-02 3.22E-02 1.23E+OO 391.70 64.97 9.63E-04 3.22E-02 Cs-134 475.3 6 1. 48 -4.57E-0 1 3.09E-02 l.58E+OO Page 5 of8 Tolerance Nuclide Caine Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss 6/7/2ln6 10:24: 04AM Page 6 of8 Analysis Report for 07-Jun-16-1 0001 L310224AFRGS007SS (DRIED) Nuclide Energy Yie!d{°/o)

Activity Nuc!idcMDA LineMDA Caine Name (keV) (pCl/grams) (pCilgrams) (pCilgrams)

Co" Cs-134 563.25 8.34 5.15E-02 3.09E-02 3.14E-01 miss 569.33 15.37 1.14E-02 l. 63E-01 miss 604. 72 97.62 2.13E-03 3. 09E-02 miss 795.86 85.46 8 .13E-03 3.66E-02 miss 801.95 8.69 -5.93E-02

2. 90E-01 m i ss 1 038.61 0.99 -4.20E-01 2.34E+OO miss 1167. 97 1. 79 1. 89E-01 1. 97E+OO miss 1365.19 3.02 -2.26E-01 7.28E-01 miss + Cs-137 661.66 85.10 8.03E-03 3.59E-02 3.59E-02 m i ss + Eu-152 121.78 28.67 -8.14E-03 7.31E-02 8. 60E-02 miss 244.70 7.61 1.16E-01 3.23E-01 miss 295.94 0.45 2.62E-01 l.15E+Ol miss 344.28 26.60 -2.12E-02 7.3 1 E-02 m i ss 367.79 0.86 1.47E-Ol 2. 94E+OO miss 411.12 2.2 4 5.03E-01 1.39E+OO miss 443.96 2.83 -4.04E-01 7.82E-01 miss 488.68 0.42 -7.lOE-03 6.18E+OO miss 563.99 0.49 -4.02E-01 4.73E+OO miss 586.26 0.46 -4.78E+OO 5.19E+OO miss 678.62 0.47 1.60E+OO 6.89E+OO miss 688.67 0.86 -1.42E+OO

2. 64E+OO miss 719.35 0.28 4.43E+00 1.26E+Ol m i ss 778.90 12.96 -2.63E-02 1.47E-01 miss 810.45 0.32 1.89E+OO 9.24E+OO miss 867.37 4.26 -9.46E-02

4. 79E-01 miss 919.33 0.43 7.81E-01 6.43E+OO m i ss 964. 08 14.65 1.49E-01 3.25E-01 miss 1085.87 10.24 4.28E-02 3.27E-01 miss 1089.74 1. 73 3.68E-01 1.94E+00 miss 1112.07 13.69 -2. 71E-02 2. 67E-Ol miss 1212.95 1. 43 -3.58E-01 2.31E+OO miss 1249.94 0.19 5.65E-01 2.09E+Ol miss 1299.14 1. 63 2.90E-01 2.12E+OO miss 1408.01 21. 07 4.67E-02 1. 90E-01 miss 1457.64 0.50 -1.78E+OO 9.33E+OO miss 1528.1 0 0.28 -4.93E-01 1.07E+Ol miss + Eu-154 123.07 40.40 -9.29E-03 5.93E-02 5.93E-02 miss 247.93 6.89 -3.25E-02 3.20E-01 miss 591. 76 4.95 -1. 46E-01 4.85E-01 miss 692.42 1. 78 3.30E-01 l.86E+OO miss 723.30 20.06 3.93E-03 1.46E-01 miss 756.80 4.52 1.26E-01 7.05E-01 miss 873.18 12.08 1.32E-02 2.58E-01 miss 996.29 10.48 -5.00E-02 l.70E-01 miss 1004.76 18.01 7.85E-02 2.03E-01 miss 1274.43 34.80 -1. 28E-02 6.00E-02 miss 1596.48 1. 80 -5.83E-01

1. 37E+OO miss + Eu-155 45.30 1. 31 9.28E-01 1.34E-01 7.18E+OO miss 60.01 1. 22 -1.93E+OO 7.79E+OO miss 86.55 30.70 -4.42E-02 l.34E-01 miss 105.31 21.10 -3.20E-02 l.52E-01 miss 6/7/2u*16 10:24: 04AM Page 7 of8 Analysis Report for 07-Jun-16-10001 L310224AFRGS007SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCUgrams) (pCilgrams) (pCilgrams)

Corr + Tl-208 583.19

• 85.00 l.lOE-01 4.68E-02 4. 68E-02 miss + Bi-211 351.07

• 13.02 1.30E+00 2.71E-01 2.71E-01 mi$S + Pb-211 404.85 3.78 -5.59E-02 4.4-:'E-01 6.51E-01 m i ss 427.09 1. 76 1.75E-01 1.29E+OO miss 832.0 1 3.52 -1. 62E-01 4.47E-01 miss + Bi-212 39.86 1. 06 -1.73E+OO 4.48E-01 7.62E+OO miss 727.33

• 6.67 3.91E-01 4.48E-01 miss 785.37 1.10 6.73E-01 2. 96E+OO miss 1620.50 1. 47 2.31E-01 2.14E+00 miss + Pb-2 1 2 115 .18 0.60 4.lOE-01 6.00E-02 4. 88E+00 miss 238.63

• 43.60 5. llE-01 6.00E-02 miss 300.09 3.30 6.20E-01 9.74E-01 miss + Pb212-XR 74.82

• 10.28 9.03E-01 4.04E-01 6.39E-01 miss 77.11

• 17.10 7.40E-01 4.04E-01 miss 87.35 3.97 4.83E-01 1.17E+OO miss 89.78 1. 46 -5.30E-03 2.79E+00 miss + Ei-214 609.32

• 45.49 4.29E-01 9.1 2 E-02 9.12E-02 miss 768.36 4.89 2.28E-01 8.59E-01 miss 806.18 1. 26 5.87E-01 2. 63E+OO miss 934.06 3 .11 6.21E-01 1.40E+OO miss 1120.29

• 14.92 5.54E-01 2.78E-01 miss 1155.21 1. 63 4.07E-01 2.58E+OO miss 1238.12 5.83 3.15E-01 9.59E-01 miss 1280.98 1. 43 -5.67E-02 2.80E+OO miss 1377.67 3.99 3.75E-01 9.84E-01 miss 1385. 31 0.79 3. llE-01 4.55E+OO miss 1401.52 1. 33 4. 72E-01 2.74E+OO miss 1407.99 2.39 4.lOE-01 l.67E+OO miss 1509.21 2 .13 1. 35E-01 1.81E+OO miss 1661. 27 1. 05 7.0lE-01 3.96E+OO miss 1729.59 2.88 3.60E-01 l.49E+OO miss 1764.49 15.30 4.98E-01 5. 92E-01 miss 1847.43 2.03 O.OOE+OO 1.35E+OO miss > 2118. 51 1.16 O.OOE+OO O.OOE+OO miss Pb-214 241.99 *'* 7.25 7.98E-01 9.90E-02 3.86E-01 miss 295.22

• 18.42 4.32E-01 2.18E-01 miss 351.93

• 35.60 4.75E-01 9.90E-02 miss 785.96 1. 06 6.39E-01 3.08E+OO miss + Pb214-XR 74.82

• 5.80 1.60E+OO 7.13E-01 1 .13E+OO miss 77.11

• 9.70 1.30E+OO 7.13E-01 miss 87.35 2.24 8.55E-01 2.08E+OO miss 89.78 0.82 -9.44E-03 4.96E+OO miss + Ra-226 186.21 3.64 7.83E-01 8. 96E-01 8. 96E-01 miss + Ac-228 129.07 2.42 2.16E-01 1.lSE-01 l.lOE+OO miss 209.25 3.89 3.99E-01 7.27E-01 miss 270.24 3.46 4.30E-01 9.52E-01 miss 328.00 2.95 2.75E-01 1.03E+OO miss 338.32

• 11. 27 3.82E-01 2.42E-01 miss 409.46 1. 92 -1.06E-01 1.46E+OO miss 463.00

• 4.40 3.07E-01 4.74E-01 miss 6/7/2u16 10:24:04AM Page8of8 Analysis Report for 07-Jun-16-1000 1 L310224AFRGS007SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCVgrams) (pCUgrams) (pCilgrams)

Corr Ac-228 794.95 4.25 2.90E-02 1.15E-0 1 7.33E-01 miss 911. 20

• 25.80 5.73E-01 l.15E-01 miss 964.77 4.99 2.SOE-01 9.53E-01 miss 968. 97 15.80 3.40E-01 4.23E-01 miss 1588.20 3.22 8.14E-01 1.73E+OO miss + Pa-231 27.36 10.30 O.OOE+OO 9.02E-02 9.02E-02 miss 283.69 1. 70 -5.58E-01 1.35E+OO miss 300.07 2.47 8.29E-01 1.30E+OO miss 302.65 2.20 -4.44E-01 8.82E-01 miss 330.06 1. 40 2.24E-01 1.95E+OO miss + Th-234 92.38 2.13 8.91E-01 2.24E+OO 2.24E+OO miss 92.80 2.10 l.90E+OO 2.41E+OO miss 112. 81 0.21 3.21E+OO 1.72E+Ol miss + U-235 143.76 10. 96 4.56E-02 5.53E-02 2.41E-01 miss 163.33 5.08 3.44E-02 4.83E-01 miss 185.71 57.20 3.66E-02 5.53E-02 miss 202 .11 1. 08 -3.09E-01 l.82E+OO miss 205.31 5.01 7.13E-02 4.60E-01 miss + Am-241 59.54 35.90 -4.77E-02 2.69E-01 2.69E-01 miss + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

VI +-' C: ::3 60 55 50 40 35 8 30 25 20 15 10 5 0000015083.CNF j Live Time :600.000 sec Real Ti m e : 600.490 sec Start: 1: -0.2(kev) stop : 8192: 2047. 4(kev) Acq. Star t : Tue Jun 07 10: 13:27 2016 0--1.......1....--'--

,.....____._---l-l----l...-...l....,......--'---+-

I ....J.........J----l...----'--+---'--...L........1..--'-'---lj..l........ll...1...J.......U............U......j....J.IJI.JL.......J........ILLll..l.ll..J..LILjU...LJllll..lll.lL.LIWlllUWll.lllllll..li.i.l..L.J..I.IIWWJ.lWl!U.JILll.l.lUllllWIIJl..lUI.IWIIII 1000 2000 3000 4000 5000 6000 7000 8000 channel 6/712u16 11:56:56AM Analysis Report for 07-Jun-16-10005 L310224AFRGS008SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done O n Efficiency Calibration Description Sample Number : 07-Jun-16-10005

L310224AFRGS008SS (DRIED) : Miscellaneous 1.875E+03 grams

• Default : 6/2/2016 1:25:00PM . 6/7/2016 11:46:18AM 130G 1 L Sand Sample JWelch P11314X2 130G Sand 600.0 seconds 600.5 seconds

• 0.09% : 2.80 : 120-8192 : 120 -8192 : 1.0 0 0FWHM : 1/27/2016

11/26/2012

15087 tL PEAK WITH NID REPORT Peak Analysis Performed on : 6/7/2016 11:56:23AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page 1 of 8 6/7/2010 11:56:56AM Page 2 of8 Analysis Report for 07-Jun-16-10005 L310224AFRGS008SS (DRIED) Peak Energy R"' ..,, No. (keV) start 1 76. 96 305 -2 87.02 343 -3 185.93 738 -4 238.66 949 -5 295.38 1175 -6 338.18 1346 -7 352.00 1400 -8 583.09 2326 -9 609.33 2430 -10 911. 43 3638 -11 1120.14 4474 -12 1460.99 5834 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 315 353 749 961 1186 1359 1414 2339 2444 3652 4486 5854 Peak Net Peak NetA;ea Continuum Centroid Area Uncertainty Counts 309.04 4.29E+Ol 31. 08 1.36E+02 349.23 4.64E+Ol 26. 94 9.52E+Ol 744.31 3. llE+O l 23.22 7.98E+Ol 954.97 1. 44E+02 35. 72 1. 29E+02 1181. 58 6.20E+Ol 21.42 4.20E+Ol 1352.57 4.87E+Ol 1 9. 26 3.65E+Ol 1407.78 1.12E+02 25.98 4.50E+Ol 2331.35 4.82E+Ol 1 7.21 2.15E+Ol 2436.27 8.90E+Ol 21. 70 2.20E+Ol 3644.20 3.76E+Ol 15.52 1.87E+Ol 4479.13 2.59E+Ol 11.74 8.17E+OO 5843.29 1.51E+02 25.18 6.00E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams)

Uncertainty K-40 0.99 1 460.82

• 10.66 4.49E+OO 8.44E-01 Eu-155 0.31 45.30 1. 31 60.01 1.22 86.55

• 30.70 1.75E-01 1. 07E-01 105.31 2 1.10 Tl-208 0.99 583.19

• 85.00 9.68E-02 3.64E-02 Pb-212 1. 00 115.18 0.60 238.63

• 43.60 3.06E-01 9.05E-02 300.09 3.30 Pb212-XR 0.99 74.82 10.28 Tentative Nuclide Pb214-XR Pb212-;~R Pb214-XR Pb212-XR Eu-155 U-235 Ra-226 Pb-212 Pb-214 Eu-152 Ac-228 Pb-2 14 Bi-2 11 Tl-208 Bi-21-1 Ac-228 Bi-214 K-40 Coinc Corr miss miss miss miss 6/7/21.J. -11:56:56AM Page 3 of8 Analysis Report for 07-Jun-16-10005 L310224AFRGS008SS (DRIED) Nuclide Id Energy Yield(%) Activity Activity Coinc Name Confidence (keV) (pCilgrams)

Uncertainty Corr P b2 1 2-XR 0.99 77 .11

• 1 7.1 0 4. OlE-01 3.02E-01 miss 87.3 5

• 3.97 1.35E+OO 8.30E-01 miss 8 9.78 1. 46 Bi-214 1. 00 6 0 9.32

• 45.4 9 3.44E-01 9.35E-02 miss 7 6 8.36 4.89 8 06.1 8 1. 26 9 34.06 3.11 1120.2 9

• 1 4.9 2 4.59E-Ol 2.llE-01 miss 1155. 2 1 1. 6 3 1238.1 2 5.83 1280.98 1. 43 1377.67 3.99 138 5. 31 0.79 1401.52 1. 3 3 1407.99 2.39 1 509.21 2.1 3 1661.27 1. 05 1 7 29.59 2.88 1764.49 15.30 1 847.43 2.0 3 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22

• 18.4 2 3.59E-Ol 1.37E-01 miss 351.93

• 35.60 3.79 E-01 1.06E-01 miss 7 8 5.96 1. 06 Ra-226 0.99 186.21

• 3.64 6.92 E-0 1 5.28E-0 1 miss Ac-22 8 0.74 1 29.07 2.42 209.25 3.8 9 270.24 3.46 328.00 2.95 338.32

• 11. 27 5.05E-01 2.16E-01 miss 409.46 1. 92 463.00 4.40 7 94.95 4.2 5 9 11. 20

• 25.8 0 3.36E-0 1 l.42E-0 1 m i ss 964.77 4.99 968.97 15.80 1 58 8.20 3.22 U-235 0.99 143.76 10. 96 163.33 5.08 185.71

• 5 7.2 0 4.40E-02 3.36E-02 miss 202.11 1. 08 205.31 5.01 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.3 0 Errors quoted at 2.000sigma Analysis Report for 07-Jun-16-10005 L310224AFRGS008SS (DRIED) Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 6/7/'-'.~ 11 :56:56AM INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 0.998 4.49E+OO 8.44E-01 Eu 155 9.316 1. 23E 01 l. l4E 01 Tl-208 0.999 9.68E-02 3.64E-02 X Bi-211 0.948 Pb-212 1.000 3.06E-01 9.0SE-02 Pb212-XR 0.998 4.0lE-01 3.02E-01 Bi-214 1. 000 3.63E-01 8.55E-02 Pb-Ll4 0.999 3.71E-01 8.39E-02 X Pb214-XR 0.998 ? Ra-226 0.995 6.92E-01 5.28E-01 Ac-228 0.74 4 3.87E-01 1.18E-01 ? U-235 0.998 4.40E-02 3.36E-02 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Pagc4 of 8 Comments f b-*z.rf 111,:,11'(

617/~.., ,d 11: 56:56AM Page 5 of8 Analysis Report for 07-Jun-16-10005

+ + + + + + + + + L310224AFRGS008SS (DRIED) Peak Locate Performed o n Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet regio n m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000s i gma UNIDENTIFIED PEAKS : 6/7/2016 11 :56:23AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Lib r ary\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCi/grams) (pCilgrams)

Corr K-40 1460.82

• 10.66 4.49E+OO 3.49E-01 3.49E-01 miss Cr-51 320.08 9.9 1 1. 88E-01 3.45E-01 3.45E-01 free Mn-54 834.85 99.98 1.lOE-03 3.30E-02 3.30E-02 miss Co-5 8 810.76 99.45 -1.20E-02 1.65E-02 1.65E-02 miss 16 74.73 0.52 O.OOE+OO 5.25E+OO miss Co-60 1173.23 99.85 1.09E-03 3.58E-02 3.58E-02 miss 1 332.49 99.98 1.16E-02 3.88E-02 miss Nb-94 702.65 99.81 -4.93E-03 2.33E-02 2.33E-02 miss 871.09 99.89 7.08E-03 2.93E-02 miss Ag-108m 79 .13 6.60 3.75E-02 2.31E-02 6.05E-01 miss 433.94 90.50 -.2.02E-03 2.31E-02 miss 614.28 89.80 -6.38E-03 2.58E-02 miss 722.94 90.80 -4. 71E-03 2.34E-02 miss Sn-113 255.13 2 .11 -7.31E-03 3.08E-02 1.13E+OO free 391.70 64.97 S.34E-03 3.08E-02 free Cs-134 475.36 1. 48 -7.86 E-01 3.13E-02 1.2 1E+OO miss 563.25 8.34 1. OOE-01 3.64E-01 miss 569.33 15.37 -4.75E-03 1. 55E-01 miss 604.72 97.62 8.31E-03 3 .13E-02 miss 6ll/2016 11:56:56AM Page 6 of8 Analysis Report for 07-Jun-16-10005 L310224AFRGS008SS

{DRIED) Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCi!grams)

Corr Cs-134 795.86 85.46 1.89E-02 3 .13E-02 4. 97E-02 miss 801.95 8.69 6.24E-02 2.63E-01 miss 1038.61 0.99 -4.68E-01 2.75E+OO miss 1167.97 1. 79 5.93E-01 2.42E+OO miss 1365.19 3.02 O.OOE+OO 2.71E-01 miss + Cs-137 661.66 85.10 -l.64E-03 2.62E-02 2.62E-02 miss + Eu-152 121. 78 28.67 1. 55E-02 8.49E-02 8.49E-02 miss 244.70 7.61 5.34E-02 3.03E-01 miss 295.94 0.45 -7.75E-01 9.73E+OO miss 344.28 26.60 3.02E-02 8.93E-02 miss 367.79 0.86 1.17E+OO 3.06E+OO miss 411.12 2.24 -1.68E-01 9.50E-01 miss 443. 96 2.83 -2.80E-01 7.50E-01 miss 488.68 0.42 -1.89E+OO 3.87E+OO miss 563.99 0.49 1.73E+OO 5.66E+00 miss 586.26 0.46 -1.77E+OO 4.88E+OO miss 678.62 0.47 2.58E+00 6.68E+OO miss 688.67 0.86 -3.15E-01 2.67E+OO miss 719.35 0.28 3.82E+00 l.17E+Ol miss 778.90 12. 96 -8.62E-02 1.72E-01 miss 810.45 0.32 -2.76E-01 7.97E+OO miss 867.37 4.26 2.09E-01 6.28E-01 miss 919.33 0.43 1.81E-01 7. llE+OO miss 964.08 14.65 l.68E-02 2.97E-01 miss 1085.87 10.24 -3.61E-03 2.72E-01 miss 1089.74 1. 73 6.22E-01 2.12E+OO miss 1112. 07 13.69 8.23E-02 3.05E-01 miss 1212.95 1. 43 -l.SlE-01 2.93E+OO miss 1249.94 0.19 4.83E+OO 2.12E+Ol miss 1299.14 1. 63 2.30E-01 2.35E+OO miss 1408.01 21. 07 5.73E-02 1.92E-01 miss 1457.64 0.50 -1.79E+Ol 7.56E+OO miss 1528.10 0.28 -6.49E+OO 8.57E+OO miss + Eu-154 123.07 40.40 -3.35E-03 2.24E-02 5.59E-02 miss 247.93 6.89 2.18E-02 2.60E-01 miss 591.76 4.95 -1.42E-01 4.91E-01 miss 692. 42 1. 78 -1.37E-01 1.42E+OO m i ss 723. 30 20.06 -2.95E-02 1.06E-01 miss 756.80 4.52 -9.15E-02 5.90E-01 miss 873.18 12.08 -4.53E-02 1.99E-01 miss 996.29 10.48 -4.81E-02 2.52E-01 miss 1004.76 18.01 1.88E-02 1.64E-01 miss 1274.43 34.80 O.OOE+OO 2.24E-02 miss 1596.48 1. 80 O.OOE+OO 5.12E-01 miss + Eu-155 45.30 1. 31 8.33E-01 1.53E-01 6.25E+OO miss 60.01 1.22 2.62E+OO 8.44E+00 miss 86.55

• 30.70 l.75E-01 1.54E-01 miss 105.31 21.10 7.65E-02 1. 53E-01 miss + Tl-208 583.19

• 85.00 9.68E-02 3.90E-02 3.90E-02 miss + Bi-211 351.07

• 13.02 l.04E+OO 2.52E-01 2.52E-01 miss + Pb-211 404.85 3.78 2.00E-01 6.36E-01 6.36E-01 miss 6/7/20-10 11: 56:56AM Page 7 of8 Analysis Report fo r 07-Jun-16-10005 L310224AFRGS008SS (DRIED) Nuclide Energy Yield(-/;,)

Activity Nuc!ideMDA Lir.cMDA Caine Name (keV) (pCl/grams) (pCi/grams) (pCi!grams)

Corr Pb-211 427.09 1. 76 6.04E-01 6.36E-01 1.62E+00 miss 832.0 1 3.52 3.59E-02 7.39E-01 miss + Bi-212 39.86 1. 06 -~.80E+OO 6.98E-01 5.95E+OO miss 727.33 6.67 4.55E-01 6.98E-01 miss 785.37 1.10 1. 25E+OO 3.15E+OO miss 1620.50 1. 47 2.63E-01 2.17E+OO miss + Pb-212 115 .18 0.60 -3.09E-01 9.80E-02 3.95E+00 miss 238.63

• 43.60 3.06E-01 9.80E-02 miss 300.09 3.30 4.33E-01 9.06E-01 miss + Pb212-XR 74.82 10.28 6.67E-01 4.59E-01 7.12E-01 miss 77 .11

• 17.10 4.0lE-01 4.59E-01 miss 87.35

• 3. 97 1.35E+OO 1.19E+OO miss 89. 78 1. 46 1.54E+OO 2.63E+00 miss + Bi-214 609.32

• 45.49 3.44E-01 7.86E-02 7.86E-02 miss 768.36 4.89 1.89E-01 7. 61E-01 miss 806.18 1. 26 -4.0lE-01 1.81E+OO miss 934.06 3.11 6.29E-01 1.42E+00 miss 1120.29

• 14.92 4.59E-01 2.18E-01 miss 1155.21 1. 63 2.17E-01 2.16E+OO miss 1238.12 5.83 3.73E-01 l.06E+OO m i ss 1280.98 1. 43 -4.88E-01 2.83E+OO miss 1377. 67 3.99 5.51E-01 1. 2 1 E+OO miss 1 385.31 0.79 2.19E-01 2.83E+OO m i ss 1401.52 1. 33 -3.30E-01 2.14E+OO miss 1 407.99 2.39 5.04E-01 1. 69E+OO miss 1 509.21 2 .13 2.18E-02 1.42E+OO miss 1661.27 1. 05 1.25E-01 2.46E+OO miss 1729.59 2.88 5.02E-01 1.51E+OO miss 1764.49 15.30 3.88E-01 5.38E-01 miss 1847.43 2.03 5.59E-01 2.00E+OO miss > 2118.51 1.16 O.OOE+OO 0.00E+OO miss Pb-214 241.99 7.25 3.82E-01 9.22E-()2 4.71E-01 miss 295.22

• 18.42 3.59E-01 1.54E-01 miss 351.93

• 35.60 3.79E-01 9.22E-02 miss 785.96 1. 06 8.81E-01 3.28E+OO miss + Pb214-XR 74.82 5.80 1.18E+OO 8.09E-01 1.26E+OO miss 77 .11

• 9.70 7.07E-01 8.09E-01 miss 87.35

• 2.24 2.39E+OO 2. llE+OO miss 89.78 0.82 2.75E+OO 4.68E+OO miss + Ra-226 186.21

• 3.64 6.92E-01 8.0SE-01 8.0SE-01 m i ss + Ac-228 129.07 2.42 2.77E-01 1.64E-01 1.lOE+OO miss 209.25 3.89 1.38E-01 6.52E-01 miss 270.24 3.46 6.32E-01 8.89E-D1 miss 328.0 0 2.95 3.40E-D1 9.31E-01 miss 338.32

• 11. 27 5.05E-01 2.54E-01 miss 409.46 1. 92 7.46E-01 1. 52E+OO miss 463.00 4.40 4.54E-01 7.60E-01 miss 794.95 4.25 4.67E-01 1.05E+OO miss 911. 20

• 25.80 3.36E-01 1.64E-01 miss 964.77 4.99 -2.20E-02 9.04E-01 m i ss 968.97 15.80 4.06E-01 4.35E-01 m i ss 6/7/2\J 16 11:56:SSAM Page 8 of8 Analysis Report for 07-Jun-1R-10005 L310224AFRGS008SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCi!grams) (pCilgrams)

Corr Ac-228 1588.20 3.22 1.SOE-01 1.64E-01 9.75E-01 miss + Pa-231 27.36 10.30 O.OOE+OO 9.14E-02 9.14E-02 miss 283.69 1. 7Q -3.21E-01 1.37E+OO miss 300.07 2.47 5.78E-01 1. 21E+OO miss 302.65 2.20 4.32E-01 1. 21E+OO miss 330.06 1. 4 0 -3.57E-01 l.70E+OO miss + Th-234 92.38 2.13 1.02E+00 2.19E+OO 2.19E+OO miss 92.80 2.10 1.53E+OO 2.31E+OO miss 112. 81 0.2 1 5.40E+00 1.55E+Ol miss + U-235 143.76 10. 96 4.73E-02 5.12E-02 2.23E-01 miss 163.33 5.08 -3.27E-02 4.39E-01 miss 185.71

• 57.20 4.40E-02 5.12E-02 miss 202 .11 1. 08 1. 07E+OO 2.21E+OO miss 205.31 5.01 6.84E-02 4.SBE-01 miss + Am-241 59.54 35.90 9.SSE-02 2. 96E-0 1 2. 96E-01 miss + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ -Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 40 35 V) µ C ::, 8 30 25 i::i ' 20 )e "' ' "' "" V, 15 ::, 10 1000 .... ;::::J -k "" 2000 3000 0000015087.CNF co u < 4000 channel 5000 Live Time : 600.000 sec Rea1 Tiae : 600.5 30 sec Start: 1: -0.2(kev) stop : 8192: 2047.4(kev)

Acq. Start : Tue Jun 07 11:46:18 2016 6000 7000 8000 6/7,--16 11:57:33AM

~,l\pex-C3amma Analysis Report for 07-Jun-16-10006 L310224AFRGS009SS (DRIED) GAMMA SPECTRUM ANAL YS/S Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 07-Jun-16-10006 L310224AFRGS009SS (DRIED) Miscellaneous

• 1.774E+03 grams : Default : 6/2/2016 1 : 35: 00PM : 6/7/2016 11 :46:34AM : 130G 1 L Sand Sample : JWelch : P40818B : 130G Sand : 600.0 seconds : 601.0 seconds : 0.16 % : 2.80 : 120-8192 : 120-8192 : 1.000FWHM

1/27/2016

1/5/2015 : 15088 PEAK WITH NID REPORT Peak Analysis Performed on : 6/7/2016 11 :57:02AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Roo t\Default\Library\Zion Lib-BNL.N LB 1.000FWHM (c;-7-/l.t? Page I of8 617/~. ,d 11:57:33AM Page2 of8 Analysis Report for 07 -Ju n-16-10006 L310224AFRGS009SS (DRIED) Peak Energy ROI No. (keV) start 1 77.26 306 -2 238.61 949 -3 295.06 1176 -4 351. 81 1399 -5 583.20 2327 -6 609.13 2430 -7 1460.44 5833 -M :: First peak in a multiplet region m = Other peak in a multiplet reg ion F :: Fitted singlet Errors quoted at 2.000sigma ROI end 316 961 1186 1414 2340 2443 5353 Peak Net Peak NetArea Continuum Centroid Area Uncertainty Counts 310.12 3.73E+Ol 26.37 9.53E+Ol 954.95 l.31E+02 34.67 1.26E+02 1180. 59 3.37E+Ol 20.50 5.86E+Ol 1407.41 7.02E+Ol 24.09 5.76E+Ol 2332.59 5.08E+Ol 1 6.18 1. 25E+Ol 2436.28 7.08E+O l 19. 2 7 1.83E+Ol 5842.74 1.11E+02 22.44 1.19E+Ol NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi!grams)

Uncertainty K-40 0.99 1 460.82

• 10.66 3.88E+OO 8.53E-01 Tl-208 1. 00 583.19

• 85.00 l.19E-01 4.07E-02 Pb-212 1. 00 115.18 0.60 238.63

• 43.60 3.31E-01 1.03E-01 300.09 3.30 Pb212-XR 0.99 74.82 10.28 77 .11

• 17.10 6.59E-01 4.85E-01 87.35 3.97 89.78 1. 46 Bi-214 0.99 609.32

• 45.49 3. 21E-01 9.54E-02 768.36 4.89 806.18 1.26 934.06 3 .11 1120. 29 14.92 1155. 21 1. 63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99 Tentative Nuclide Pb214-XR Pb212-XR Pb-212 Pb-214 Eu-152 Pb-214 Bi-211 Tl-208 Bi-214 K-40 Coinc Corr miss miss miss miss miss Analysis Report for 07-Jun-16-10006 L310224AFRGS009SS (DRIED) Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1385.31 1401.52 1407.99 1509.21 1661.27 1729.59 1764.49 1847.43 2118.51 Pb-214 0.99 241.99 295.22 351.93 785.96 Pb214-XR 0.99 74.82 77 .11 87.35 89.78 * = Energy line found in the spectrum. -= Manually added nuclide. ? ;;; Manually edited nuclide. .,. * ... @ = Energy line not used for Weighted Mean Activity Energy Tolerance:

1.000FWH M Nuclide confidence index threshold

0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%j 0.7 9 1. 33 2.39 2.13 1. 05 2.88 15.30 2.03 1.1 6 7.25 18.42 35.60 1. 06 5.80 9.70 2.24 0.82 miss = Nuclide energy was not found in the coincidence library. 6/7/L_ .d 11:57:33AM Page 3 of8 Activity Activity Caine (pCUgrams)

Uncertainty Coll 2 , 30E-01 1.45E-01 miss 2.78E-0 1 1. OSE-01 miss 1.16E+OO 8.61E-01 miss INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 0.991 3.88E+OO 8.53E-01 Tl-208 1. 000 1.19E-0 1 4.07E-02 X Bi-211 0. 967 Pb-212 1. 000 3.31E-01 1.03E-01 ? Pb212-XR 0.999 6.59E-01 4.85E-01 Bi-214 0.999 3.21E-01 9.54E-02 Pb-214 0.999 2.61E-01 8.SlE-02 Analysis Report for 07-Jun-16-10006

? L310224AFRGS009SS (DRIED) Nuclide Nuclide Name Id Confidence Pb214-XR 0.999 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interfere n ce analysis 617/,.._ .0 Wt mean Activity (pCilgrams) l.1 6E+OO @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000s i gma 11:57:33AM Page 4 of8 Wt mean Comments Activity Uncertainty 8.61E-01 6/7/,.._ .d 11:57:33AM Analysis Report for 07-Jun-16-10006

+ + + + + + + + L310224AFRGS009SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/7/2016 11: 57: 02AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCi!grams) (pCi/grams)

K-40 1460.82

• 10.66 3.88E+OO 5.3..,E-01 5.37E-Ol Cr-51 320.08 9.91 -6.l OE-02 2.52E-0 1 2.52E-01 Mn-54 834.85 99.98 l.16E-02 4.48E-02 4.48E-02 Co-58 810.76 99.45 -6.58E-03 2.83E-02 2.83E-02 1674.73 0.52 8.38E-01 7. 78E+OO Co-60 1173.23 99.85 9.15E-04 3.85E-02 3.85E-02 1332. 49 99.98 1.90E-02 5.22E-02 Nb-94 702.65 99.81 2.84E-03 3.lSE-02 3.20E-02 871.09 99.89 3.05E-03 3.lSE-02 Ag-108m 79.13 6.60 9.70E-02 3.00E-02 l.29E+OO 433.94 90.50 7.0lE-03 3.00E-02 614.28 89.80 l.58E-03 3.46E-02 722. 94 90.80 2.30E-03 3.82E-02 Sn-113 255.13 2.11 -2.06E-01 3.82E-02 l.1 3E+OO 391. 70 64. 97 -2.03E-02 3.82E-02 Page 5 of8 Tolerance Nuclide Coinc Corr m is s free miss miss miss miss miss miss miss miss miss m i ss m i ss free free + Cs-134 475.36 1. 48 -1.41E+OO 2.53E-02 1.55E+OO miss 563.25 8.34 -l.41E-01 3.08E-01 miss 569.33 15.37 3.47E-02 2.04E-01 miss 604.72 97.62 -l.12E-02 2.53E-02 m i ss 6/7, __ ,6 11:57: 33AM Page 6 of8 Analysis Report for 07-Jun-16-10006 L310224AFRGS009SS (DRIED) Nuclide Ene;gy Yield(%j Activity Nuclide MDA LineMDA Coinc Name (keV) (pCUgrams) (pCilgrams) (pCilgrams)

Corr Cs-134 795.86 85.46 2.58E-02 2.53E-02 6.00E-02 miss 801.95 8.69 1. 43E-02 4.04E-01 miss 1038.61 0.99 -6.98E-01 2.78E+OO miss 1167.97 1. 79 -2.30E-01 2.15E+OO miss 1365.19 3.02 O.OOE+OO 3.19E-01 miss + Cs-137 661.66 85.10 1.18E-02 4.64E-02 4. 64E-02 miss + Eu-152 121. 78 28.67 -2.02E-02 1.05E-01 ::i...05E-01 miss 244.70 7.61 9.71E-02 4.15E-01 miss 295.94 0.45 1.13E+OO l.07E+Ol miss 344.28 26.60 3 .13E-02 l.05E-01 miss 367.79 0.86 -1. llE+OO 2.81E+OO miss 411.12 2.24 l.43E-01 1.28E+OO miss 443.96 2.83 -4.76E-01 7.68E-01 miss 488.68 0.42 -9.45E-01 5.53E+OO miss 563.99 0.49 -3.78E+OO 5.22E+OO miss 586.26 0.46 -4.93E+OO 5.24E+OO miss 678.62 0.47 1. 03E+OO 6.16E+OO miss 688.67 0.86 8.73E-01 4.54E+OO miss 719.35 0.28 6.lOE-01 l.24E+Ol miss 778.90 12. 96 -8.75E-03 2.4GE-01 miss 810.45 0.32 2.59E-01 9.34E+D0 miss 867.37 4.26 -l.63E-01 4.51E-01 miss 919.33 0.43 -8.83E-01 6.84E+OO miss 964. 08 14.65 1.09E-01 3.48E-01 miss 1 085.87 10.24 2.36E-02 4.45E-01 miss 1089.74 1. 73 2.SlE-01 2.64E+OO miss 1112. 07 13.69 2.25E-02 3.18E-01 miss 1212.95 1. 43 -6.54E-02 2.46E+OO miss 1249.94 0.19 -5.54E+OO 1.30E+Ol miss 1299.14 1. 63 8. 71E-01 2. 96E+OO miss 1408.01 21.07 5.16E-02 1.85E-Ol miss 1457.64 0.50 -1.97E+OO 1.34E+Ol miss 1528.10 0.28 -1.17E+OO 1.0lE+Ol miss + Eu-154 123.07 40.40 7.12E-03 7.13E-02 7.73E-02 miss 247.93 6.89 -1. 72E-01 3.09E-01 miss 59 1. 76 4.95 2.68E-01 7. ll E-01 miss 692.4 2 1. 78 -3.75E-02 2.llE+OO miss 723. 30 20.06 5.77 E-03 1.63E-01 miss 756.80 4.52 -1.23E-01 6.92E-01 miss 873.18 12.08 -1. 72E-02 2.61E-01 miss 996.29 10.48 -5.02E-02 2.54E-01 miss 1004.76 18.01 -1.78E-03 l.73E-01 miss 1274.43 34.80 6.93E-03 7 .13E-02 miss 1596.48 1. 80 O.OOE+OO 6.0lE-01 miss + Eu-155 45.30 1. 31 -4.59E+OO l.94E-01 2.0lE+Ol miss 60.01 1. 22 2.74E+OO 2.04E+Ol miss 86.55 30.70 -8.15E-02 l.94E-01 miss 105.31 21.1 0 3.21E-02 2.00E-01 miss + Tl-208 583.19

• 85.0 0 1.19E-01 3.61E-02 3. 61E-02 miss + Bi-211 351.07

• 13.02 7.59E-01 3.37E-01 3.37E-01 miss + Pb-211 404.85 3.78 -3.27E-01 7.46E-01 7.46E-01 miss 6!71~_,o 11:57:33AM Page 7 of8 Analysis Report for 07-Jun-16-10006 L310224AFRGS009SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCl/grams) (pCUgrams) (pCi/grams)

Corr Pb-211 427.09 1. 76 -8.97E-02 7.46E-01 1.53E+OO miss 832.01 3.52 3.60E-02 9.45E-01 miss + Bi-212 39.86 1. 06 7.19E+OO 6.SSE-01 2.47E+Ol miss 727.33 6.67 2.26E-01 6.55E-01 m i ss 785.37 1.10 1. 23E+OO 3.86E+OO miss 1620.50 1. 47 2.74E-01 2.02E+OO miss + Pb-212 115 .18 0.60 -l.44E+00 1.15E-01 5.24E+OO miss 238.63

• 43.60 3.31E-01 l.15E-01 miss 300.09 3.30 7.SOE-01 1.14E+00 miss + Pb212-XR 74.82 10.28 8.35E-01 7.26E-01 1.22E+OO miss 77.11

• 17.10 6.59E-01 7.26E-01 miss 87.35 3.97 7.83E-01 l.68E+OO miss 89.78 1. 46 l.98E+OO 4.09E+OO miss + Bi-214 609.32

• 45.49 3.21E-01 8.22E-02 8.22E-02 miss 768.36 4.89 2.87E-02 9.25E-01 miss 806.18 1. 26 -9.17E-01 l.45E+OO miss 934.06 3.11 8.19E-01 1.66E+OO miss 1120.29 14. 92 5.02E-01 5.39E-01 miss 1155.21 1. 63 6.68E-01 2.73E+OO miss 1 238.12 5.83 8.lOE-01 1.27E+OO miss 1280.98 1. 43 7.08E-01 2.54E+OO miss 1377.67 3.99 5.44E-01 l.49E+OO miss 1385.31 0.79 l.93E-01 3.32E+OO miss 1401.52 1. 33 5.29E-01 2.92E+OO miss 1407.99 2.39 4.54E-01 l.63E+OO miss 1509.21 2 .13 6.27E-01 2.15E+OO m i ss 1661. 27 1. 05 O.OOE+OO l.06E+00 miss 1729.59 2.88 2.95E-01 1.37E+OO miss 1764.49 15.30 2.57E-01 5.lOE-01 miss 1847.43 2.03 -7.66E-01 1.61E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss I* Pb-214 241.99 7.25 5.00E-01 1.23E-01 5.98E-01 miss 295.22

• 18.42 2.30E-01 2.09E-D1 miss 351.93

• 35.60 2.78E-01 l.23E-D1 miss 785. 96 1. 06 4.42E-01 3.66E+OO miss + Pb214-XR 74.82 5.80 1.48E+OO 1.28E+OO 2.16E+OO miss 77 .11

• 9.70 1.16E+OO 1.28E+OO miss 87.35 2.24 1. 39E+OO 2.97E+OO miss 89.78 0.82 3.52E+OO 7.28E+OO miss + Ra-226 186.21 3.64 5.89E-01 9.23E-01 9.23E-01 miss + Ac-228 129.07 2.42 -1.33E-03 2.81E-01 l.41E+00 m is s 209.25 3.89 4.53E-01 8.84E-01 miss 270.24 3.46 6.03E-01 9.85E-01 miss 328.00 2.95 -5.llE-02 1.07E+OO miss 338.32 11. 27 3.lOE-01 3.82E-01 miss 409.46 1. 92 2.17E-01 1.59E+OO miss 463.00 4.4 0 -1.57E-01 5.08E-01 miss 794.95 4.25 5.51E-D1 1. 23E+D0 miss 911. 20 25.80 2.03E-01 2.81E-01 miss 964. 77 4.99 3.67E-01 1.02E+OO miss 968. 97 15.80 4.85E-01 5.17E-01 miss 6/7,-.. 16 11:57:33AM Page 8 of8 Analysis Report for 07-Jun-16-1 0006 L310224AFRGS009SS (DRIED) Nuclide Ene;gy Yiefd(%) Activity NucUde MDA LineMDA Coinc Name (keV) (pCilgrams) (pCi!grams) (pCilgrams)

Corr Ac-228 1588.20 3.22 1.02E+OO 2.81E-01 2.05E+OO miss + Pa-231 27.36 10.30 -l.86E-01 1.1 7E+00 2.SOE+OO miss 283.69 1. 70 3.26E-01 1.74E+OO miss 300.07 2.47 1. OOE+OO l.52E+00 miss 302.65 2.20 3.74E-02 l.17E+00 miss 330.06 1. 40 5.99E-01 2.32E+OO miss + Th-234 92.38 2 .13 l.18E+OO 2.90E+OO 2. 90E+OO miss 92.80 2.10 1.79E+00 3.0lE+OO miss 112. 81 0.21 6.61E+OO 2.18E+Ol miss + U-235 143.76 10. 96 -3.83E-02 5.98E-02 2.SOE-01 miss 163.33 5.08 -3.94E-02 5.35E-01 miss 185. 71 57.20 3.12E-02 5.98E-02 miss 202 .11 1. 08 1.17E+OO 2.89E+OO miss 205.31 5.0 1 1. 72E-01 5.60E-01 miss + ~-241 59.54 35.90 -1.36E-01 6.77E-01 6.77E-Ol miss + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No _coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45 -+0 35 V> +-' C :::::, 8 30 a:: 25 'i' .... ;::j ..0 "' 1 ;::j ..0 20 0.. 15 10 '.~ s 0 ;::! I ..0 a.. .... ;:j I ..0 a.. ..0 a.. 1000 2000 3000 0000015088.CNF 4000 channel 5000 l iv e Tim e :60 0.0 00 sec Real Tiae :600.970 se c S t a rt: 1: -0.l(kev) sto p : 81 92: 2 04 7 .O(ke v) Acq. Start :Tu e Jun 07 11:46:34 2 016 6000 7000 8000 617/,,., 16 12: 19: 56PM ~3~pex-Gamma Analysis Report for 07-Jun-16-10007 L310224AFRGS010SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels}

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number 07-Jun-16-10007

• L310224AFRGS010SS (DRIED) Miscellaneous 1.832E+03 grams Default 6/2/2016 1:50:00PM 6/7/2016 12:09:18PM 130G 1 L Sand Sample JWelch

• P11314X2 : 130G Sand : 600.0 seconds : 600.4 seconds : 0.07% : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

11/26/2012

15089 PEAK WITH NID REPORT Peak Analysis Performed on : 6/7/2016 12: 19:23PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance C:\Canberra\Apex\Root\Default\Library\Zion Lib-BN L.NLB 1.000FWHM Pag1: I of7 6171~ .... .., 12:19:56PM Page 2 of7 Analysis Report for 07-Jun-16-10007 L310224AFRGS010SS (DRIED) Peak Energy R"' VI No. (keV) start 1 238.53 950 -2 352.02 1402 -3 583.24 2326 -4 609.22 2430 -5 1461. 04 5834 -M = First peak in a multiplet regio n m == Other peak in a multiplet region F == Fitted singlet Errors quoted at 2.000sigma ROI end 960 1415 2337 2443 5853 Peak Net Peak NetArea Continuum Centroid Area Uncertainty Counts 954.43 7.18E+Ol 23.40 4.83E+Ol 1407.88 6.02E+Ol 17.49 1. 36E+Ol 2331.95 3 .13E+Ol 12.63 7.30E+OO 2435.80 4.48E+Ol 13.78 2.36E+OO 5843.47 1. 31E+02 23.14 2.68E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-B NL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1 460.82 -** 10.66 3.98E+OO 7.84E-Ol Tl-208 1. 00 583.19

• 85.00 6.44E-02 2. 71E-02 Bi-211 0.94 351.07 ... 13. 02 5.67E-0l l.88E-01 Pb-212 0.99 115 .18 0.60 238.63

• 43.60 1.56E-01 5.67E-02 300.09 3.30 Bi-214 1. 00 609.32

• 45.49 1.77E-01 5.85E-02 768.36 4.89 806.18 1. 26 934.06 3.11 1120.29 14.92 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 1 401.52 1. 33 1407.99 2.39 1509.21 2.13 1661. 27 1. 05 1729.59 2.88 1764.49 15.30 Tentative Nucllde Pb-212 Pb-214 Bi-211 Tl-208 Bi-214 K-40 Coinc Corr miss miss miss miss miss Analysis Report for 07-Jun-16-10007 L 3 10 224 AF RGS 0 1 0SS (DRIED) Nuclide Id Energy Name Confidence (keV) Bi-214 1. 00 1 847.43 2118.51 Pb-214 0.51 241.99 295.22 35 1.93 7 85.96 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 2.03 1.16 7.25 18.42 35.60 l.. 0 6 miss = Nuclide energy was not found in the coincidence library. 617/'L..., *" 12:19:56PM Page 3 of7 Activity Activity Coinc (pCi/grams)

Uncertainty Corr 2.07E-01 6.88 E-02 mi s s INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Tl-208 ? Bi-211 Pb-212 Bi-214 ? Pb-214 Nuclide Id Confidence 0.997 1. 000 0.946 0.999 1.000 0. 5 13 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 3.98E+OO 6.44E-02 5.67E-01 l.56E-0 1 1.77E-01 2.0:E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty 7.84E-01 2.71E-02 1.88E-01 5.67E-02 5.85E-0 2 6.88 E-02 6/7h~. o 12:1 9:56PM Analysis Report for 07-Ju n-16-10007 L310224AFRGS0 10SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/7/2016 12:19:23PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LI B-BNL. NLB Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCi/grams) (pCi!grams)

+ K-40 1460.8 2

• 10.66 3.98E+OO 2.60E-01 2.60E-01 + Cr-51 320.08 9.91 5.64E-02 2.56E-01 2.56E-01 + Mn-54 834.85 99.98 -3.37E-03 2.09E-02 2.09E-02 + Co-58 810.76 99.45 5. llE-04 2.47 E-0 2 2.47E-02 1674.73 0.52 7.30E-01 5.37E+OO + Co-60 1173.23 99.85 -4.79E-03 2.59E-02 2.59E-02 1332.49 99.98 6.35E-03 3.26E-02 + N b-94 70';:.. 65 99.81 -7.16E-04 2.75E-02 2.80E-02 871.09 99.89 l.91E-0 3 2.75E-02 + Ag-108m 79 .13 6.60 -2. llE-01 1. 69E-02 5.04E-01 433.94 90.50 -4.09E-03

1. 69E-0~ 614.28 89.80 -8.06E-04 2.42E-02 722. 94 90.80 1. llE-03 2.67E-02 + Sn-113 255.13 2 .11 -3.29E-01 3.1 6E-02 9.lOE-01 3 91. 70 64.97 -1.0S E-03 3.16E-02 + Cs-134 475.36 1. 48 2.06E-02 l.86E-02 l.45E+OO 563.25 8.34 -8.21E-03 1.9 1E-01 569.33 15.37 -l.25 E-02 l.69E-01 604. 72 9,. 62 -3.38E-03 2.60E-02 Page 4 of7 Tolerance Nuclide Caine Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free m iss m is s miss miss 617fL~ ,d 12:19:56PM Page 5 of7 Analysis Report for 07-Jun-16-10007 L310224AFRGS010SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCi!grams) (pCi!grams)

Corr Cs-134 795.86 85.46 -8.0lE-03 1.86E-02 l.86E-02 miss 801.95 8.69 -8.75E-02 2.32E-01 miss 1038.61 0.99 8.70E-01 3.68E+OO miss 1167. 97 1. 79 l.95E-01 l.87E+00 miss 1365.19 3.02 3.59E-01 1. 23E+00 miss + Cs-137 661.66 85.10 5.22E-03 3.15E-02 3.15E-02 miss + Eu-152 121.78 28.67 2.62E-02 7.21E-02 7.29E-02 miss 244. -;'0 7.61 -1. 09E-01 2.30E-01 miss 295.94 0.45 1.87E+OO 6.34E+OO miss 344.28 26.60 -1.48E-02 7.21E-02 miss 367.79 0.86 2.35E-02 1.93E+OO miss 411.12 2.24 -6.13E-02 9.73E-01 miss 443. 96 2.83 -7.57E-02 6.70E-01 miss 488.68 0.42 1.22E+OO 4.83E+OO miss 563.99 0.49 -1.32E+OO 2.56E+OO miss 586.26 0.46 -2.82E+OO 3.54E+OO miss 678.62 0.47 2.0SE-01 5.38E+00 miss 688.67 0.86 -9.86E-01

2. llE+OO miss 719.35 0.28 -2.65E+OO 6.70E+00 miss 778.90 12. 96 3.55E-02 l.97E-01 miss 810.45 0.32 -5.66E-01 7.31E+OO miss 867.37 4.26 1.69E-01 7.02E-01 miss 919.33 0.43 7.40E-01 7.28E+00 miss 964. 08 14.65 8.72E-02 2.66E-01 miss 1085.87 10.24 2.lOE-02 2.79E-01 miss 1089.74 1. 73 -3.73E-01 1.65E+OO miss 1112. 07 13.69 -1.lOE-01

1. 45E-01 miss 1212.95 1. 43 5.71E-02 2.40E+OO miss 1249.94 0.19 -2.63E+OO

1. 43E+Ol miss 1299.14 1. 63 -7.86E-02

1. 35E+OO miss 1408.01 21. 07 -1.28E-02

1. lOE-01 miss 1457.64 0.50 -3.96E+OO 7.74E+OO miss 1528.10 0.28 1.19E+OO 8.77E+OO miss + Eu-154 123.07 40.40 1. llE-02 4.SlE-02 4.51E-02 miss 247.93 6.89 -7.06E-04 2.92E-01 miss 591. 76 4.95 O.OOE+OO 4.68E-01 miss 692.42 1. 78 5.89E-01 1.56E+OO miss 723. 30 20.06 -2.35E-02 1.08E-01 miss 756.80 4.52 7.68E-03 4.28E-01 miss 873.18 12.08 2.69E-02 2.28E-01 miss 996.29 10.48 O.OOE+OO 6.47E-02 miss 1004.76 18.01 4.43E-02 1. 84E-01 miss 1274.43 34.80 -3.62E-03 7.85E-02 miss 1596.48 1. 80 2.42E-02 l.42E+OO miss + Eu-155 45.30 1. 31 -8. 51E-01 1.28E-01 4.32E+00 miss 60.01 1. 22 -1.25E-02 5.85E+OO mis::: 86.55 30.70 5.56E-02 1.28E-01 miss 105.31 21.10 3.61E-02 1. 31E-01 miss + Tl-208 583.19

• 85.00 6.44E-02 2.53E-02 2.53E-02 miss + Bi-211 351.07

• 13.02 5.67E-01 1.50E-01 1.SOE-01 miss + Pb-211 404.85 3.78 l.26E-01 5.69E-01 5.69E-01 miss 6171,~,o 12:19: 56PM Page 6 of7 Analysis Report for 07-Jun-16-10007 l310224AFRGS010SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCilgrams) (pCUgrams) (pCi!grams)

Corr Pb-211 427.09 1. 76 -9.60E-02 5.69E-01 l.13E+OO miss 832.01 3.52 2.44E-01 9.45E-01 miss + Bi-212 39.86 1. 06 -l.38E+OO 5.51E-01 6.32E+OO miss 727.33 6.67 2.42E-01 5.51E-01 miss 785.37 1.10 4.19E-01 2.32E+OO miss 1620.50 1. 47 O.OOE+OO 6.47E-01 m i ss + Pb-:12 115 .18 0.60 2.28E+OO 6.35E-02 3.97E+OO miss 238.63

• 43.60 1.56E-01 6.35E-02 miss 300.09 3.30 2.85E-01 6. 72E-01 miss + Pb212-XR 74. 8::::'. 10.28 3.37E-01 3.33E-01 6.17E-01 miss 77.1 1 17.10 2.59E-01 3.33E-01 miss 87.35 3.97 3.57E-01 8.90E-01 miss 89.78 1. 46 8.99E-01 2.20E+OO miss + Bi-214 609.32

• 45.49 1.77E-01 3.18E-02 3.18E-02 miss 768.36 4.89 3.84E-01 7.79E-01 miss 806.18 1. 26 -2.58E-01 2.06E+00 miss 934.06 3.11 2.38E-01 9.28E-01 miss 1120.29 14.92 8.02E-02 3.16E-01 miss 1155. 21 1. 63 4.24E-01 2.21E+OO miss 1 2 38.12 5.83 2.54E-01 7.4 2 E-01 m i ss 1280.98 1. 43 2.94E-02 2.47E+00 miss 1377.67 3.99 4.08E-02 8.38E-01 miss 1385.31 0.79 7.72E-01 4.72E+OO miss 1401.52 1. 33 1.08E+OO 3.55E+OO miss 1407.99 2.39 -1.13E-01 9.70E-01 miss 1509.21 2 .13 2.79E-01 l.88E+OO miss 1661.27 1. 05 3.42E-01 2.52E+OO miss 1729.59 2.88 4.05E-01 1.54E+OO miss 1764.49 15.30 5.09E-02 3.21E-01 miss 1847.43 2.03 l.91E-01 l.40E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss Pb-214 241. 99 7.25 1.35E-01 5.SOE-02 3.72E-01 miss 295.2~ 18.42 1. llE-01 l.67E-01 miss 351.93

• 35.60 2.07E-01 5.SOE-02 miss 785.36 1. 06 3.19E-01 2.42E+00 miss + Pb214-~:R 74.82 5.80 5.97E-01 5.8 1 E-Ol 1.09E+OO miss 77.1 1 9.70 4.56E-01 5.87E-01 miss 87.35 2.24 6.32E-01 l.58E+OO miss 89.78 0.82 l.60E+OO 3.92E+00 miss + Ra-226 186.21 3.64 5.43E-01 7.40E-01 7.40E-01 miss + Ac-228 129.07 2.42 3.25E-01 2.24E-01 8.52E-01 miss 209.25 3.89 1.92E-01 5.21E-01 miss 270.24 3.46 4.46E-02 6.16E-01 miss 328.00 2.95 -6.61E-03 7.47E-01 miss 338.32 11. 27 1.99E-01 2.BOE-01 miss 409.46 1. 92 2.38E-01 1.13E+OO miss 463.00 4.40 2.36E-01 6.13E-01 miss 794.95 4.25 5.90E-02 5.45E-01 miss 91 1.20 25.80 1. 72E-01 2.24E-01 miss 964.77 4.99 2.46E-02 6.93E-01 m i ss 968.97 15.80 3.93E-02 2.34E-01 m i ss Analysis Report for 07-Jun-16-10007

+ + + + + * > L310224AFRGS010SS (DRIED) f./uclide

,:.,....,r.,,_., Yield(%) Activity ... ., ...... :,, Name (keV) (pCl/grams)

Ac-'.228 1588.20 3.22 2.69E-01 Pa-231 27.36 10.30 O.OOE+OO 283.69 1. 70 -4.12E-02 300.07 2.47 3.80E-01 302.65 2.20 6.30E-02 330.06 1. 40 -l.68E-01 Th-234 92.38 2.13 l.20E+OO 92.80 2.10 1.45E+OO 112. 81 (). 21 1.52E+OO U-235 143.76 10. 96 -2.42E-02 163.33 5.08 -1.97E-01 185.71 57 . .:20 2.36E-02 202 .11 1. 08 3.40E-01 205.31 5.01 -l.63E-01 Am-241 59.54 35.90 -1.19E-01

.. Nuclide identified during the nuclide identification Energy line found in the spectrum = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction 6/7,_J 16 Nuc!ideMDA (pCi/grams) 2.24E-Ol 9.35E-02 2.03E+OO 4.49E-02 l.G5E-01 ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 12:19:56PM Page 7 of7 LineMDA Caine (pCi/grams)

Corr l.29E+OO miss 9.35E-02 miss 1 .13E+OO miss 8. 98E-01 miss 9.49E-01 miss l.46E+OO miss 2.03E+OO miss 2.09E+OO miss l.21E+Ol miss l.57E-01 miss 2.89E-01 miss 4.49E-02 miss 1.84E+OO miss 2.77E-01 miss 1.65E-01 miss VI ...... C: :::::s 60 55 50 45 40 35 8 30 25 20 15 10 5 1000 2000 3000 0000015089.CNF 4000 channel 5000 Live Time :600.000 sec Real Time :600.420 sec start: 1: -0.Z (kev) stop : 8192 :2047. 4(kev) Acq. sta r t :Tue Jun 07 12:09:18 2016 6000 7000 8000 6/7/21, . .: 12:20:33PM Analysis Report for 07-Jun-16-10008 L310224AFRGS011SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 07-Jun-16-10008

L310224AFRGS011SS (DRIED) : Miscellaneous 1.939E+03 grams : Default : 6/2/2016 1:55:00PM

6/7/2016 12:09:35PM

130G 1 L Sand Sample : JWelch : P40818B : 130G Sand : 600.0 seconds : 600.9 seconds : 0.16 % : 2.80 : 120-8192 : 120-8192 : 1.000FWHM

1/27/2016

1/5/2015 : 15090 PEAK WITH NID REPORT Peak Analysis Performed on : 6/7/2016 12:20:02PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.N LB : 1.000FWHM Pnge 1 of8 6/7/20, _ 12:20: 33PM Page2 of8 Analysis Report for 07-Jun-16-10008 L310224AFRGS011SS (DRIED) Peak Energy ROI No. (keV) start 1 238.56 950 -2 295.19 1173 -3 351.79 1398 -4 583 .13 2326 -5 609.54 2431 -6 726.80 2902 -7 910.92 3636 -8 968. 67 3869 -9 1119.78 4474 -10 1460.73 5833 -M ;;; First peak in a multiplet regio n m = Other peak in a multiplet region F ;;; Fitted singlet Errors quoted at 2.000sigma ROI end 960 1188 1414 2339 2444 2911 3650 3880 4485 5853 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 954.75 1.61E+02 33.54 9.87E+Ol 1181. 08 5.19E+Ol 25. 64 7.02E+Ol 1407.35 1. 08E+02 28.09 6.65E+Ol 2332.30 5.43E+Ol 1 8.67 2.74E+Ol 2437.91 6.67E+Ol 1 9. 90 2.66E+01 2906.87 1. 45E+Ol 10.64 1. 50E+Ol 3643.39 3.94E+Ol 15.12 1. 51E+Ol 3874.43 2.00E+O l 11.66 1. 39E+Ol 4479.09 1.16E+O l 9.76 1.29E+Ol 5843.88 1. 24E+02 22.27 O.OOE+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDE S Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-4 0 0.99 1 460.82

• 10.66 3.96E+00 7.90E-01 Tl-2 0 8 1. 0 0 5 83.1 9

• 85.00 1. l 7E-01 4.2 6E-0 2 Bi-21 2 0.98 39.86 1. 06 72 7.33

• 6.67 4.61E-01 3.43E-01 7 85.37 1.10 1 62 0.5 0 1. 47 Pb-212 1. 00 11 5 .1 8 0.60 238.63

• 43.60 3.71E-Ol 9.80 E-0 2 300.0 9 3.30 Bi-214 0.99 609.32

• 45.49 2.76E-Ol 8.89 E-02 7 68.36 4.89 8 06.18 1. 26 9 3 4.06 3.11 1120.29

• 14.92 2.19E-01 1.86E-01 1155.2 1 1. 63 1 23 8.1 2 5.83 Tentative Nuclide Pb-212 Pb-214 Eu-152 Pb-214 Bi-211 Tl-208 Bi-214 Bi-212 Ac-228 Ac-228 Bi-~14 K-40 Coinc Corr miss miss miss miss miss miss Analysis Report for 07-Jun-16-10008 L310224AFRGS011SS (DRIED) Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1 280.98 13 77. 67 1385. 31 1401.52 1407.99 1509.21 1661.27 1 729.59 1764.49 1847.43 2118. 51 Pb-21 4 0.99 241.99 295.22 351.93 785.96 Ac-228 0.99 12 9. 07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911.20 964. 77 968. 97 1588.20 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 1. 43 3.99 0.79 1. 33 2.39 2.1 3 1. 05 2.88 1 5.30 2.03 1.16 7.25 18.42 35.60 1. 06 2.42 3.89 3.46 2.95 11.27 1. 92 4.40 4.25 25.80 4.99 1 5.80 3.22 miss = Nuclide energy was not found in the coincidence library. 6/7/2(). -12:20:33PM Page 3 of8 Activity Activity Coinc (pCilgrams)

Uncertainty Corr 3.25E-0l l.69E-01 miss 3.90E-01 l.19E-01 miss 3.78E-0 1 1.48E-01 miss 3.26E-0 1 1. 92E-01 miss INTERFERENCE CORRECTED REPORT Analysis Report for 07-Jun-16-10008 X L310224AFRGS011 SS (DRIED) t.Juclide

., .. ,.,,,.,,.

l'l'W"UM'lw" Name Id Confidence K-4 0 0.99 9 Tl-2 0 8 1. 000 B i-2 11 0. 96 9 B i-2 1 2 0.9 8 9 Pb-21 2 1. 000 B i-214 0.9 97 P b-2 1 4 0.99 9 A c-228 0.99 7 ? = nuclide is part of an undetermined solution X = nuclide rejected by the i n terference analysis 6/7/20 *-Wt mean Activity (pCilgrams)

3. 96E+OO l.1'7E-0 1 4.GlE-01 3.71E-01 2.66E-01 3.68E-01 3.59E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 12: 20:33PM Page4 of8 Wtmaan Comments Activity Uncertainty 7.90E-01 4.26E-02 3.43E-01 9.80E-02 8.02E-02 9.74E-02 l.17E-01 6/7/20,. 12:20:33PM Page 5 of8 Analysis Report for 07-Jun-16-10008

+ + + + + + + + + L310224AFRGS011SS (DRIED) Peak Locate Performed o n Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified. M = First peak in a multiplet region m = Other peak in a multiplet region F "' Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAK S : 6/7/2016 12:20:02PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCilgrams) (pCilgrams)

Corr K-40 1460.82

• 10.66 3.96E+OO 8.64E-02 8.64E-02 miss Cr-51 320.08 9.9 1 -1.13E-01 3.40E-01 3.40E-01 free Mn-54 834.85 99.98 3.53E-03 3.53E-02 3.53E-02 miss Co-58 810.76 99.45 -3.SlE-03 2.89E-02 2.89E-02 miss 1674.73 0.52 O.OOE+OO 2.07E+OO miss Co-60 1173.23 99.85 -2.59E-03 2.95E-02 3.84E-02 miss 1332.49 99.98 4.54E-04 2.95E-02 miss Nb-94 702.65 99.81 -l.34E-03 3.12E-02 3.12E-02 miss 871.09 99.89 -9.58E-04 3.14E-02 miss Ag-lORm 79 .13 6.60 3.52E-02 2.99E-02 l.16E+OO miss 433.94 90.50 -4.71E-03 2.99E-02 m i ss 614.28 89.80 7.60E-03 3.35E-02 miss 722. 94 90.80 -l.SOE-03 3.SOE-02 miss Sn-113 255.13 2.11 -4.87E-01 4.44E-02 1.26E+OO free 391.70 64.97 5.42E-03 4.44E-02 free Cs-134 475.36 1. 48 7.57E-02 2.32E-02 1. 88E+OO miss 563.25 8.34 -9.38E-02 2.82E-01 miss 569.33 15.37 2.47E-02 2.05E-01 miss 604.72 97.62 -1.68E-02 2.32E-02 miss a1112u. 12:20:33PM Page 6 of8 Analysis Report for 07-Jun-16-10008 L310224AFRGS011SS (DRIED) Nuclide Energy Yie!d("/u)

Activity Nuclide MD.4. Lir.eMDA Caine Name (keV) (pCi/grams) (pCi/grams) (pCi!grams)

Co" Cs-134 795.86 85.46 2.43E-02 2.32E-02 4. 80E-02 miss 801.95 8.69 8.73E-03 3.15E-01 miss 1038.61 0.99 1.13E+OO 3.59E+OO miss 1167.97 1. 79 -5.25E-02

1. 96E+OO miss 1365.19 3.02 -2.62E-01

7. 92E-01 miss + Cs-137 661.66 85.10 1.13E-02 4.56E-02 4.56E-02 miss + Eu-152 121. 78 28.67 -7.36E-02

1. OOE-01 1.00E-01 miss 244.70 7.61 -1.65E-02 3.74E-01 miss 295.94 0.45 8.12E+00 1.02E+Ol miss 344.28 26.60 2.39E-04 l.02E-01 miss 367.79 0.86 -3.63E-01 2.45E+OO miss 411.12 2.24 1.16E-01 l.48E+OO miss 443. 96 2.83 -2.14E-02 8.51E-01 miss 488.68 0.4 2 -1.41E+OO 5.44E+OO miss 563.99 0.49 -1. 09E+OO 4.78E+OO m i ss 586.26 0.46 -2.25E+00 6.34E+OO m i ss 67 8. 62 0.47 -1.92E+00 5.16E+OO miss 688.67 0.86 -3.18E-01 3.36E+OO miss 719.35 0.28 -4.41E-01 1.07E+Ol miss 778.90 12.96 7.06E-02 2.58E-01 m i ss 810.45 0.32 -3.08E+OO 7.65E+OO miss 867.37 4.26 -6.0lE-02 8.42E-01 miss 919.33 0.43 -7.17E-01 7.62E+OO miss 964. 08 14.65 l.71E-01 3.63E-01 miss 1085.87 10.24 -5.81E-02 2.00E-01 miss 1089.74 1. 73 3.45E-01 1.93E+OO miss 1112. 07 13.69 -3.73E-02 2.22E-01 miss 1212.95 1. 43 -4.34E-01 2.52E+OO miss 1249.94 0.19 4.28E+OO 2.42E+Ol miss 1299.14 1. 63 -4.81E-01 l.79E+OO miss 1408.01 21. 07 3.48E-02 1.89E-01 miss 1457.64 0.50 O.OOE+OO 9.54E+OO miss 1528.10 0.28 1. 34E+OO l.16E+Ol miss Eu-154 123.07 40.40 l.83E-02 7.74E-02 7.74E-02 miss 247.93 6.89 1.13E-01 3.96E-01 miss 5 91. 7 6 4.95 -9.34E-02 4.49E-01 miss 692.42 1. 78 -4.31E-01 1.25E+OO miss 723. 30 20.06 -3.52E-03 1.58E-01 m i ss 756.80 4.52 -1.17E-0 1 6.81E-01 miss 873.18 12.08 -5.57E-02 2.BOE-01 miss 996.29 10.48 -7.52E-02 2.33E-01 miss 1004.76 18.01 -3.91E-02 1.36E-01 miss 1274.43 34.80 -l.31E-02 9.55E-02 miss 1596.48 1. 80 -3.64E-01 2.19E+OO n t iss + Eu-155 45.30 1. 31 3.70E+00 1.83E-01 2.12E+Ol miss 60.01 1. 2 2 4.6 1 E+OO 1.90E+Ol miss 86.55 30.70 4.0BE-02 1.90E-01 miss 105.31 21.10 -8.31E-02 1.83E-01 m i ss + Tl-208 583.19

• 85.00 1.17E-01 4.64E-02 4.64E-02 miss + Bi-211 351.07

• 13.02 1. 07E+OO 3.35E-0 1 3.35E-01 miss + Pb-211 404.85 3.7 8 -3.46E-01 5.65E-01 5.65E-01 miss 6/7/20. 12:20:33PM Page 7 of8 Analysis Report for 07-Jun-16-10008 L310224AFRGS011SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCl/grams) (pCl/grams) (pCilgrams)

Corr Pb-211 427.09 1.76 6.6 ffi-02 5 , 6 5E-01 l.84E+OO miss 832.01 3.52 J.57i:i-02 7.92E-01 miss + Bi-212 39.86 1. 06 -l.18E+Ol 4.75E-01 2.07E+Ol miss 727.33 * . 6'i' 4.61E-01 4.75E-01 miss 785.37 1.10 3.lSE-01 2.86E+OO miss 1620.50 1. 47 4.91E-01 2.70E+OO miss + Pb-212 115.18 0.60 3.26E+00 8.97E-02 6.40E+OO miss 238.63 43.60 3.71E-01 8.97E-02 miss 300.09 3.30 2.59E-01 1.04E+OO miss + Pb212-XR 74.82 10.28 1.08E-02 6.59E-01 1.0SE+OO miss 77.1 1 1 7.10 6.19E-01 6.59E-01 miss 87.35

• _g ~t 4.43E-01 l.48E+OO miss 89.78 1. 46 1.20E+OO 3.96E+00 miss + Bi-214 609.32

• 45. 4 91 2.76E-01 8.87E-02 8.87E-02 miss 768.36 4..89 4.25E-01 9.32E-01 miss 806.18 1. 26 -l.32E-01 2.36E+OO miss 934.06 3.11 1.86E-01 1.06E+OO miss 1120. 29

• 14.92 2.19E-01 2.70E-01 miss 1155.21 1. 63 -1.20E-01 2 .13E+00 miss 1238.12 5.83 3.56E-01 9.76E-01 m i ss 1280.98 1. 43 2.85E-01 2.59E+00 miss 1377. 67 3.99 1.1 7E-02 7.58E-01 miss 1385. 31 0.79 3.31E+OO 6.87E+00 miss 1401.52 1. 33 O.OOE+OO 6. 71E-01 miss 1407.99 2.39 3.06E-01 1. 66E+OO miss 1509.21 2.13 1.76E-01 1.97E+OO miss 1661. 27 1. 05 O.OOE+OO 9. 72E-01 miss 1729.59 2.88 5.42E-01 1.77E+OO miss 1764.49 15.30 2.95E-01 4.84E-01 miss 1847.43 2.03 4.00E-01 1.86E+OO miss > 2118. 51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 4.05E-01 1.22E-01 5.47E-01 miss 295.22

• 18.42 3.25E-01 2.35E-01 miss 351. 93

• 35.60 3.90E-01 1.22E-01 miss 785.96 1. 06 1.97E-01 2.76E+OO miss + Pb214-XR 74.82 5.80 1.92E-02 1.16E+OO 1.86E+OO miss 77 .11 9.70 1.09E+00 1.16E+OO miss 87.35 2.24 7.86E-01 2.62E+OO miss 89.78 0.82 2.13E+OO 7.04E+00 miss + Ra-226 186.21 3.64 5.78E-01 9.69E-01 9.69E-01 miss + Ac-228 129.07 2.42 2.65E-01 1. 59E-01 1.47E+00 miss 209.25 3.89 2.59E-01 8.26E-01 miss 270.24 3.46 5.57E-01 1.00E+OO miss 328.00 2.95 6.34E-02 1. 02E+OO miss 338.32 11.27 3.62E-01 3.82E-01 miss 409.46 1. 92 1.57E-01 l.68E+00 miss 463.00 4.40 ~.02E-01 7.96E-01 miss 794.95 4.25 4.43E-01 9.97E-01 miss 91 1.20

• 25.80 3.78E-01 1.59E-01 miss 964. 77 4.99 6.31E-01 l.13E+00 miss 968. 97

• 15.80 3.26E-01 2.44E-01 miss 6/7/2(, 12:20:33PM Page 8 of8 Analysis Report for 07-Jun-16-10008 L310224AFRGS011SS (DRIED) Nuclide Energy Yield(%} Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

Corr Ac-228 1588.20 3.22 9.87E-02 l.59E-01 l.21E+OO miss + Pa-231 27.36 10.30 -5.25E-01 1.33E+OO 2.41E+OO miss 283.69 1. 70 4.98E-01 l.92E+OO miss 300.07 2.47 3.45E-01 l.39E+OO miss 302.65 2.20 5.50E-02 l.33E+OO miss 330.06 1. 40 -2.65E-01 2.12E+OO miss + Th-234 92.38 2.13 1.90E+OO 3. 27E+OO 3.27E+OO miss 92.80 2.10 2.38E+OO 3.34E+OO miss 11~. 81 0.21 -5.47E+O O 2.06E+01 miss + U-235 143.76 10. 96 -2.60E-02 6.16E-02 2.75E-01 miss 163.33 5.08 -2.98E-01 4.74E-01 m i ss 185. 71 57.20 2.69E-02 6.16E-02 m i ss 202 .11 1. 08 l.04E-01 2.20E+OO miss 205.31 5.01 l.33E-01 5.74E-01 miss + Am-241 59.54 35.90 -3.14E-01 5.82E-01 5.82E-01 miss + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > ... MDA value not calculated

@ -= Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

40 35 V) C 8 30 ;:!; "' I = CL 25 20 15 a, = 7~ 'i= 10 5 0 1000 2000 3000 0000015090.CNF 00 ..... ';' u < u < 4000 channel 5000 Live Time : 600.000 sec Real Time :600.940 sec start: 1: -0.l(kev) stop : 8192:2047.0(kev)

Acq. start :Tue Jun 07 12: 09: 35 2 016 C> ""r" "" 6000 7000 8000 6ntL.-. . ., 12:43:33PM Analysis Report for 07-Jun-16-10009 L310224AFRGS012SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 07-Jun-16-10009

L310224AFRGS012SS (DRIED) : Miscellaneous 1.731E+03 grams : Default : 6/2/2016 2:16:00PM

6/7/2016 12:32:55PM

130G 1 L Sand Sample : JWelch ; P11314X2

• 130G Sand 600.0 seconds 600.5 seconds 0.08% . 2.80

• 120-8192 : 120-8192 : 1.000FWHM : 1/27/2016

11/26/2012

15091 PEAK WITH NID REPORT Peak Analysis Performed on : 6/7/2016 12:43:00PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Ca nberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page J of8 6/7/20 I u 12:43:33PM Page 2 of8 Analysis Report for 07-Jun-16-10009 l310224AFRGS012SS (DRIED} Peak Energy ROI No. {keV) start 1 238.66 947 -2 295.25 1175 -3 352.01 1400 -4 583.04 2325 -5 609.22 2429 -6 911.10 3637 -7 1120.28 4474 -8 14 61. 09 5833 -M "' First peak in a multiplet regio n m "' Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 960 1186 1415 2336 2444 3648 4485 5853 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 954.98 1.08E+02 29 .10 7.54E+Ol 1181.06 4.61E+Ol 19. 97 4.19E+Ol 1407.83 7.04E+Ol 20. 31 2.52E+Ol 2331.1 7 3.14E+Ol 14.57 1. 91E+Ol 2435.81 5.37E+O l 17.63 1.86E+Ol 3642.92 2.90E+Ol 11.51 3.98E+OO 4479.68 1.65E+Ol 9.21 5.lOE+OO 5843.68 1.69E+02 27.12 1.19E+Ol NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1 460.82

• 10.66 5.45E+OO 9.94E-01 T l-208 0.99 583.19

• 85.00 6.83E-02 3.27E-02 Pb-212 1. 00 115.18 0.60 238.63

• 43.60 2.49E-01 7.81E-02 300.09 3.30 Bi-214 1. 00 609.32

• 45.49 2.25E-Ol 7.86E-02 768.36 4.89 806.18 1.26 934.06 3 .11 1120.29

• 14.92 3.lSE-01 1. 7 8E-01 11 55.21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 140 1.52 1. 33 1 407.99 2.39 1 509.21 2.13 Tentative Nucllde Pb-212 Pb-2U Eu-152 Pb-214 Bi-21l Tl-208 Bi-214 Ac-228 Bi-214 K-40 Coinc Corr miss miss miss miss miss Analysis Report for 07-Jun-16-10009 L310224AFRGS012SS (DRIED) Nuclide Id Energy Name Confidence (keV) Bi-214 1. 00 1661. 27 1729.59 1764.49 1847.43 2118.51 Pb-214 l. 00 241.99 295.22 351.93 785.96 Ac-228 1. 00 129.07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911. 20 964.77 968.97 1 588.20 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * @=Energy line not used for.Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 1. 05 ~.88 1 5.30 2.03 1.16 7.25 18.42 35.60 1. 06 2.42 3.89 3.46 2.95 11. 27 1. 92 4.40 4.25 25.80 4.99 15.80 3.22 miss = Nuclide energy was not found in the coincidence library. 6!7/2u. 12:43:33PM Page 3 of8 Activity Activity Coinc (pCilgrams)

Uncertainty Corr 2.89E-01 l.33E-01 miss 2.57E-0 l 8.47E-02 miss 2.BlE-01 1.1 4E-01 miss INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCi/grams)

Uncertainty K-40 0. 996 5.45E+OO 9.94E-01 Tl-208 0.999 6.83E-02 3.27E-02 X Bi-211 0.947 Analysis Report for 07-Jun-16-10009 L310224AFRGS012SS (DRIED) Nuclide Nuclide Name Id Confidence P b-2 1 2 1. 000 B i-21 4 1. 000 Pb-214 1. 000 A c-228 1. 000 ? = nuclide is part of an undetennined solution X = nuclide rejected by the interference analysis 6/7/20, -Wt mean Activity (pCilgrams) 2.49 E-01 2.39E-01 2.66 E-01 2.8 1 E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 12:43:33PM Page 4 of8 Wt mean Comments Activity Uncertainty 7.81E-02 7.19E-02 7.lSE-02 1.14E-01 6/7/20. 12:43:33PM Analysis Report for 07-Jun-16-10009

+ + + + + + + + + L310224AFRGS012SS (DRIED) Peak Locate Performed o n Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet regio n m;;; Other peak in a multiplet region F ;;; Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : .6/7/2016 12:43:00PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (keV) (pCilgrams) (pCi!grams) (pCilgrams)

K-40 1460.82

• 10.6 6 5.45E+OO 4. 96E-01 4. 96E-01 Cr-51 320.08 9.91 -1. 50E-01 2.21 E-01 2.21E-01 Mn-54 834.85 99.98 2.21E-02 4.48E-02 4.48E-02 Co-58 810.76 99.45 -2.43E-03 2.26E-02 2.26E-02 1674.73 0.52 -4.83E-Ol 5.69E+OO Co-60 1173.23 99.85 1. 09E-03 2.98E-02 4.44E-02 1332.49 99.98 5.04E-03 2. 98E-02 Nb-94 702.65 99.81 -1.33E-02

1. 55E-02 1.55E-02 871. 09 99.89 4.04E-04 2.25E-02 Ag-108m 79.13 6.60 -1.60E-01 2.64E-02 6.lOE-01 433.94 90.50 -8.16E-03 2.64E-02 614.28 89.80 1. 62E-02 4.0lE-02 722. 94 90.80 7.23E-03 3.53E-02 Sn-113 255.13 2 .11 4.38E-02 3.34E-02 1. 23E+OO 391.70 64.97 -2.45E-02 3.34E-02 Cs-134 475.36 1. 48 -5.35E-01 2.34E-02 1.73E+OO 563.25 8.34 6.27E-02 3.26E-01 569.33 15.37 (;,51E-02 2.07E-01 604. 72 97. 62 -4.87E-03 2.34E-02 Page 5 of8 Tolerance Nuclide Caine Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss miss 6/7/2(J 12:43:33PM Page 6 of8 Analysis Report for 07-Jun-16-10009 L310224AFRGS012SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pC i lgrams) (pC i/grams) Corr Cs-134 '795.86 85.46 5.65E-03 2.34E-02 2.88E-02 miss 801.95 8.69 l.lOE-03 3.18E-01 m i ss 1038.61 0.99 3.68E-01 2. 98E+OO miss 1167. 97 1. 7 9 -2.36E-01 i.78E+00 miss 1365.19 3.02 l.55 E-02 1.0lE+OO m i ss + C s-137 661.66 85.10 2.49E-02 5.05E-02 5.05E-0 2 m i ss + Eu-152 121.78 28.67 2.06E-02 7.86E-02 7.86E-02 miss 244.70 7.61 1.69E-01 3.08E-01 miss 295.94 0.45 3.0lE-01 9.77E+OO miss 3 44.2 8 26.60 1.66E-02 8.73E-02 m i ss 367.79 0.86 4.67E-01 2.93E+OO m i ss 411.12 2.2 4 -3.12E-01 9.1 5E-01 miss 443. 96 2.83 O.OOE+OO 7.63E-01 miss 488.68 0.4: -l.34E-01 5.85E+OO miss 563.9 9 0.49 -2.06E+OO 3.96E+OO m i ss 586.26 0.46 -2.2 6 E+OO 4.85E+OO m i ss 678.62 0.4 7 -8.44E-02 6.12E+OO miss 688.67 0.86 -9.24E-01 2.24E+00 miss 719. 35 0.28 -1.19E+OO 8.22E+00 miss 778.90 12. 96 -l.36E-02 2.60E-01 miss 810.45 0.32 8.38E-01 7.74E+OO miss 867.37 4.26 -l.18E-01 5.26E-01 miss 919.33 0.43 1.23E+OO 7.70E+OO miss 964. 08 14.65 -1.65E-02 2.66E-Ol m i ss 1 08'1.87 10.24 -3.78E-02 2.95E-01 miss 1089.7 4 1. 73 4.49E-01 2.2 9E+OO miss 1112.07 13.69 -2.53E-02 2.50E-01 miss 12 1 2.95 1. 43 -4.35E-01 2.77E+OO miss 1249.94 0.19 -4.59E+OO 1.95E+Ol m i ss 1299.1 4 1. 63 -6.93E-Ol

1. 80E+OO miss 1408.01 21. 07 2.27E-03 l.47E-01 miss 1 457.64 0.50 -1.0lE+Ol l.02E+Ol miss 1528 .10 0.28 4.81E-01 1.36E+Ol miss + Eu-154 123.07 40.40 -2.68E-03 5.76E-02 5.76E-02 miss 247.93 6.89 1.82E-01 3.35E-Ol miss 591. 76 4.95 6.79E-02 4.53E-01 miss 692.42 1. 78 -9.74E-03 1.86E+OO miss 723. 30 20.06 -2.lOE-02 1.40E-01 m i ss 756.80 4.52 -2.4 4 E-02 3.59E-01 m i ss 873.1 8 12.08 -5.02E-02

1. 86E-01 miss 996.29 10.48 O.OOE+OO 6.85E-02 miss 1004.76 18.0 1 4.97 E-02 2.35E-01 miss 1274.43 34.80 1.79E-02 8.31 E-02 miss 1596.48 1. 80 O.OOE+OO 5.54E-01 miss + Eu-155 45.30 1. 31 -1. 46E+OO 1.32E-01 5.23E+OO miss 60.01 1. 22 -1.87E-01 6.54E+OO miss 86.5 5 30.70 :.09E-0 2 1. 43E-01 miss 105.31 21.10 2.89E-02 :i...32E-01 miss + Tl-208 583.19

• 85.00 6.83E-0 2 3.9 2 E-02 3.92E-02 miss + Bi-211 351.07

• 13. 02 7.02E-01 2.15E-0 1 2.15E-01 m iss + Pb-211 404.85 3.78 -3.lSE-02 5.70E-0 1 5.70E-01 miss 617/2(,,_

12:43:33PM Page 7 of8 Analysis Report for 07-Jun-16-10009 L310224AFRGS012SS (DRIED) Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Caine Name (keV) (pCUgrams) (pCi/grams) (pCi/grams)

Corr Pb-211 427.09 1. 76 1. 85E-01 5.70E-01 l.47E+OO miss 832.01 3.52 -4.22E-01 6.19E-01 miss + Bi-212 39.86 1. 06 -l.68E+OO 7.56E-01 5.92E+OO miss 727.33 6.67 4.5 4E-01 7.56 E-01 miss 785.37 1.10 6.83E-01 3. 08E+OO miss 1620.50 1. 47 5.48 E-01 2. 72E+OO miss + Pb-212 115 .18 0.60 -7.65E-01 8.31E-02 3.76E+OO m i ss 238.63 43.60 2.49E-0 1 8.31E-02 miss 300.09 3.30 4.43E-:-01 8.50E-01 miss + Pb212-XR 74.82 10.2 8 3.37E-01 4.52E-0 1 6.65E-Ol miss 77 .11 17.10 6. llE-01 4.52E-01 miss 87.35 3.97 5.63E-01 l. llE+OO miss 89.78 1. 46 -l.48E-02 2.40E+OO miss + Bi-214 609.32

• 45.49 2.25E-01 7.88E-02 7.88E-02 miss 768.36 4.89 6.30E-01 l.02E+OO miss 806.18 1. 26 2.12E-01 L.96E+OO miss 934.06 3.11 3.41E-01 l.15E+OO miss 1120.29

• 14.92 3.lSE-01 l.90E-01 miss 1155. 21 1. 63 2.85E-01 2.52E+OO m i ss 12 38.12 5.83 2.24E-01 8.30 E-01 miss 1280.98 1. 43 -8.09E-01

1. 60E+OO miss 13 7 7. 67 3.99 -3.41E-01 6.06E-01 miss 1385. 31 0.79 0.00E+OO l.13E+OO miss 1401.52 1. 33 l.07E-01 2. 32E+OO miss 1407.9 9 2.39 1. 99E-02 l.30E+OO miss 15 09.21 2.13 -3.78E-Ol l.54E+OO miss 1 661.27 1. 05 O.OOE+OO 9.80E-01 miss 1729.59 2.88 8.49E-02 l.OOE+OO miss 1764.49 15.30 2.60E-0 1 4. 71E-01 miss 1847.43 2.03 6.05E-01 2.17E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss Pb-214 241.99 7.25 3.26E-01 7.85E-02 4.43E-01 miss 295.22

• 18.42 2.89E-01 1. 68E-01 m i ss 351.93

• 35.60 2.57E-01 7.85E-02 miss 785.96 1. 06 1.17E+OO 3.38E+OO miss + Pb214-XR 74.82 5.80 5.97E-01 7.97E-01 l.18E+OO miss 77.11 9.70 1.08E+OO 7.97E-01 miss 87.35 2.24 9.98E-01 l.97E+OO miss 89.78 0.82 -2.64E-02 4.27E+OO miss + Ra-226 186.21 3.64 6.19E-01 7.74E-01 7.'74E-01 miss + Ac-228 129.0 7 2.42 -3.69 E-02 9.08E-02 8.84E-01 miss 209.25 3.89 1. 42E-01 6.35E-01 miss 270.24 3.46 4.54E-01 8.73E-Ol miss 328.00 2.95 3.88E-01 9.19E-0 1 miss 338.32 11. 27 l.69E-01 3.02E-01 miss 409.46 1. 92 9.45E-02 1. 37E+OO miss 463.00 4.40 2.28E-01 7.20E-01 miss 794.95 4.25 1.78E-01 7.02E-01 miss 911. 20

• 25.80 2.81E-01 9.08E-02 miss 964.77 4.99 3.59E-01 9.0oE-01 miss 968.97 15.80 1. 48E-01 3.21E-01 miss 6/7/2L 12:43:33PM Page 8 of8 Analysis Report for 07-Jun-16-10009 L310224AFRGS012SS (DRIED) Nuclide Energy Yield{°/o)

Activity NuclideMDA LineMDA Caine Name (keV) (pCilgrams) (pCi/grams) (pCi/grams)

Corr Ac-228 1 588.20 3.22 5.69E-01 9.08E-02 1.49E+OO miss + Pa-231 27.36 10.30 O.OOE+OO 9.90E-02 9.90E-02 miss 283.69 1. 70 5.38 E-01 1.52E+OO m i ss 300.0 7 2.47 5.92E-01 1.14E+OO miss 302.65 2.20 1.71E-01 9.68E-01 m i ss 330.06 1. 40 -5. llE-01 1. 55E+OO m i ss + Th-234 92.38 2.13 1.56E+OO 2.29E+OO 2.29E+OO miss 92.80 2.10 l.64E+OO 2.35E+OO miss 112. 81 0.21 -3.48E+OO 1.33E+01 miss + U-235 143.76 10. 96 6.29E-02 4.45E-02 2.20E-01 miss 163.33 5.08 8.29E-02 4.61E-01 miss 1 85.71 57.20 1.60E-02 4.45E-02 miss 202 .11 1. 08 -2.09E-01 l.95E+OO miss 205.31 5.01 -4.lSE-0 2 4.04E-01 m i ss + Am-241 59.54 35.90 -6.20E-03 2.35E-01 2.35E-01 m i ss + = Nuclide identified during the nuclide identification

• "' Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performe d. free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45** -40 35 Vl ..... C ::::, 8 30 25 20 15 ... ..Q <L 10 5 0 1000 ..... ;:;:: I 2000 3000 0000015091.CNF 4000 channel 5000 Live Time 600. 000 sec Rea 1 Time 600. 500 sec Start: 1 -0.2(kev) Stop : 8192 2047.4(kev)

Acq. Start Tue Jun 07 12: 32: 55 2016 6000 7000 8000 6171~ .... J 12:44:11PM

.amma Analysis Report for 07-Jun-16-10010 L310224AFRGS013SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live lime Real lime Dead Time Peak Locate Threshold Peak Locate Range {in channels)

Peak Area Range {in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done O n Efficiency Calibration Description Sample Number : 07-Jun-16-10010

L310224AFRGS013SS

{DRIED) : Miscellaneous 1.644E+03 grams 1 Default : 6/2/2016 2:12:00PM

6/7/2016 12:33:09PM . 130G 1 L Sand Sample : JWelch : P408188 : 130G Sand : 600.0 seconds : 600.9 seconds : 0.15% : 2.80 : 120-8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 15092 PEAK WITH NID REPORT Peak Analysis Performed on : 6/7/2016 12:43:39PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page I of8 6/7/20,_ 12:44:11PM Page 2 of8 AnalY,sis Report for 07-Jun-16-10010 L310224AFRGS013SS (DRIED) Peak Energy ROI No. (keV) start 1 238.57 947 -2 295.25 1175 -3 351.92 1402 -4 609.10 2431 -5 911. 01 3639 -6 1460.77 5834 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 960 1185 1413 2441 3650 5853 Peak Net Peak NetArea Continuum Centroid Area Uncertainty Counts 954.78 1. 06E+02 28.38 6.92E+Ol 1181. 32 3.23E+Ol 18 .11 4.14E+Ol 1407.88 6.33E+Ol 20.00 3.33E+Ol 2436.17 3.92E+Ol 15.01 1.55E+01 3643.77 2.24E+Ol 10.10 3.14E+OO 5844.04 1. 41E+02 24.00 2.81E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi!grams)

Uncertainty K-40 1. 00 1 460.82 *'* 1 0.66 5.30E+O O 1.0lE+OO Pb-212 1. 00 115.18 0.60 238.63

• 43.60 2.90E-01 9.04E-02 300.09 3.30 Bi-214 0.99 609.32

• 45.49 1.92E-01 7.69E-02 768.36 4.89 806.18 1.26 934.06 3 .11 1120.29 14.92 1155. 21 1. 63 1 238.12 5.83 1 280.98 1. 43 1377.67 3.99 1385. 31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2.13 1 661.27 1. 05 1 729.59 2.88 1764.49 15.30 Tentative Nuclide Pb-212 Pb-214 Eu-152 Pb-214 Bi-211 Bi-214 Ac-228 K-40 Coinc Corr miss miss miss Analysis Report for 07-Jun-16-10010 L310224AFRGS013SS (DRIED) Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1847.43 2118.51 Pb-214 1. 00 241.99 295.22 351.93 785. 96 Ac-228 0.99 129.07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911.20 964.77 968.97 1588.20 * -Energy line found in the spectrum.

--Manually added nuclide. ? -Manually edited nuclide. * * *A* @ == Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWH M Nuclide confidence index threshold

0.30 Errors quoted at 2.000sigma Coincidence correction performed. free = No coincidence correction required.

Yield(%) 2.03 1.16 7.25 18.42 35.60 1. 06 2.42 3.89 3.46 2.95 1 1. 27 1. 92 4.40 4.25 25.80 4.99 15.80 3.22 miss = Nuclide energy was not found in the coincidence library. 6/7/2u ,.., 12:44:11PM Page 3 of8 Activity Activity Coinc (pCi/grams)

Uncertainty Corr 2.38E-01 1. 39E-01 miss 2.70E-0 1 9.57E-02 miss 2.53E-01 1.16E-01 miss INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCi!grams)

Uncertainty K-40 1. 000 5.30E+OO 1.0lE+OO X Bi-211 0.956 Pb-212 1. 000 2.90E-Ol 9.04E-0 2 Bi-214 0.999 1. 92E-01 7.69E-02 Pb-214 1.000 2.60E-01 7.38E-02 Ac-228 0.999 2.53E-0 1 1.16E-01 Analysis Report for 07-Jun-16-10010 L310224AFRGS013SS (DRIED) ? = nuclide is part of an undetermined solution X = nuclide rejected by the i nterference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 6/7/2!.J ,u 12:44:11PM Page 4 of8 617/20,v 12:44:11PM Analysis Report for 07-Jun-16-10010

+ + + + + + + + + L310224AFRGS013SS (DRIED) Peak Locate Performed o n Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified. M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 617/2016 12: 43:39PM : 120 : 8192 Peak CPS {°/a) Peak Size {CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Ape x\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (keV) (pCilgrams) (pCi/grams) (pCi!grams)

K-40 1 460.82

• 10.66 5.30E+OO 3.30E-0 1 3.30E-01 Cr-51 320.08 9.9 1 4.34E-02 2.59E-01 2.59E-01 Mn-54 834.85 99.98 -l.62E-02 2.58E-02 2.58E-02 Co-58 810.76 99.45 -5.68E-03 2.09E-02 2.09E-02 1674.73 0.52 5.65E-01 6.65E+OO Co-60 1173.23 99.85 2.04E-02 4.92E-02 5.19E-02 1332.49 99.98 1.55E-02 4.92E-02 Nb-94 702.65 99.81 8.35E-03 3.70E-02 4.0BE-02 871.09 99.89 -2.73E-03 3.70E-02 Ag-108m 79.13 6.60 4.49E-02 2.74E-02 l.25E+OO 433.94 90.50 -2.33E-03 2.74E-02 614.28 89.80 1. 50E-02 4.34E-02 722. 94 90.80 -4.12E-03 3.30E-02 Sn-113 255.13 2.11 -l.51E-02 4.90E-02 1.42E+OO 391.70 64. 97 3.81E-03 4.90E-02 Cs-134 475.36 1. 48 4.67E-01 2.73E-02 2.22E+OO 563.25 8.34 1.81E-01 4.60E-01 569.33 15.37 5.19E-02 2.08E-01 604. 72 97.62 -3.87E-03 2.73E-02 Page :'i of8 Tolerance Nuclide Coinc Co" miss free m i ss miss miss miss miss miss miss miss miss m i ss miss free free miss miss miss miss 6/7/20*1 12:44:11PM Page 6 of8 Analysis Report for 07-Jun-16-10010 L310224AFRGS013SS (DRIED) Nuclide Energy Yield(%) Activity Nuclide MnJ1 Une MD,4 Caine Name (keV) (pCi!grams) (pCUgrams) (pCi!grams)

Corr Cs-134 795.86 85.46 1.98E-02 2.73E-02 5.44E-02 miss 801.95 8.69 4.12E-02 4.0 SE-01 m is s 1038.61 0.99 9.68E-01 4.55E+00 miss 1167.97 1. 79 3.26E-01 2. 72E+OO miss 1365.19 3.02 2.09E-01 1.53E+OO miss + Cs-137 661.66 85.10 3.76E-03 3.90E-02 3.90E-02 miss + Eu-152 121.78 28.67 -8.45E-03

1. 02E-01 1.17E-01 miss 244.70 7.61 -2.64E-01 3.47E-01 miss 295.94 0.45 -1.58E+OO 9.88E+00 miss 344.28 26.60 -9.02E-03 1.02E-01 miss 367.79 0.86 -6.0'7E-01 3.03E+OO miss 411.12 2.24 2.37E-01 1.48E+OO miss 443.96 2.83 2.87E-01 9.49E-01 miss 488.68 0.42 -1. 46E+OO 6.42E+OO miss 563.99 0.49 7.64E-01 7 .16E+OO miss 586.26 0.46 -1.45E+OO 9.lBE+OO miss 678.62 0.47 6.97E-01 6.09E+00 miss 688.67 0.86 -4.22E-01 3.38E+D0 miss 719. 35 0.28 5.0lE+OO 1.55E+Ol miss 778.90 12. 96 l.OlE-02 2.85E-01 miss 810.45 0.32 -6.99E-01 6.17E+OO miss 867.37 4.26 3.53E-01 1.lOE+OO miss 919.33 0.43 -2.86E+O O 6.37E+OO miss 964. 08 14.65 3.22E-02 2.92E-01 miss 1 085.87 10.24 3.20E-0 2 3.84E-01 miss 1089.74 1. 73 -5.97E-01 l.40E+OO miss 1112. 0.7 13. 69 -8.68 E-02 2.26E-01 miss 1212.95 1. 43 -3.88 E-01 2. 97E+OO miss 1249.94 0.19 6.25E+OO 2.85E+Ol miss 1299.14 1. 63 7.94E-01 3.60E+OO miss 1408.01 21. 07 9.27E-02 2.43E-01 miss 1457.64 0.50 -6.27E+OO l.33E+Ol mi s s 1528.10 0.28 -1.05E+OO 1.09E+Ol miss + Eu-154 123.07 40.40 1.02E-02 8.46E-0 2 8.46E-D2 miss 247.93 6.89 6.75E-02 4.75E-01 miss 591. 76 4.95 1.59E-01 6.99E-01 miss 692.42 1. 78 2.27E-0 1 2.38E+O O miss 723.30 20.06 -6.7 4E-03 1.49E-01 miss 756.80 4.52 -9.17E-02 6.13 E-01 m i ss 873.18 12.08 -1. 56E-01 1.72E-01 miss 996.29 10.48 1.0SE-01 4.17E-01 miss 1004.76 18.01 -6.06E-02 l.27E-01 miss 1274.43 34.80 1.lOE-02 1.48E-Ol miss 1596.48 1. 80 -1.20E-01 1.76E+OO miss + E u-155 45.30 1. 31 -7.63E-0 1 1.8:E-01 1.85E+Ol m i ss 60.01 1. 22 7.14E-01 2.0 5 E+Ol miss 86.55 30.70 -2.53E-02 l.99E-01 miss 105.31 21.10 6.lOE-03 1.87E-0 1 miss + Tl-208 583.19 85.00 6.73E-02 7. 77 E-02 7.77E-02 miss + B i-211 351.07

• 13.02 7.3 9E-01 2.64E-01 2.64E-01 m i ss + Pb-211 404.85 3.78 ?.99E-02 7.40E-0 1 7.40E-01 m iss 6/7/20 1-.., 12:44:11PM Page 7 of8 A n a l~si s Report for 07-Jun-16-10010 L310224AFRGS013SS (DRIED) Nuclide Energy Yield(%) Activ i ty NuclideMDA LineMDA Caine Name (keV) (pCUgrams) (pCi!grams) (pCi/grams) Corr Pb-211 427.09 1. 76 3.39E-02 7.40E-01 1.49E+OO miss 832.01 3.52 3.89E-01 l.46E+OO miss + Bi-212 39.86 1. 06 2.7 5E+OO 8.00E-0 1 2.28E+Ol miss 727. 33 6.67 4.30E-01 8.00E-01 miss 785.37 1.10 3.39E-0 1 3.37E+OO m i ss 1620.50 1. 47 O.OOE+OO 8.0lE-01 miss + Pb-212 115 .18 0.60 -2.54E+OO 9.47E-02 5.45E+OO miss 238.63

• 43.60 2.90E-01 9.47E-02 miss 300.09 3.30 -7 .13E-02 9.79E-01 m i ss + Pb212-XR 74.82 10.28 3.37E-01 7.02E-0 1 1.16E+OO m iss 7 7 .11 17.10 3.94E-01 7.02E-01 miss 87.35 3.97 -1.59E-01 l.54E+OO m i ss 89.78 1. 4 6 -9.86E-01 4.09E+OO m i ss + Bi-2 1 4 609.3 2

• 45.4 9 1.92E-Ol 7.97E-02 7.97E-02 miss 768.36 4.89 -1.77E-02 7.97E-01 miss 806.18 1. 26 3.00E-01 2.55E+OO miss 934.06 3.11 -9.54E-02 1.35E+OO miss 11 2 0.29 1 4.92 -1.65E-02 3.16E-01 miss 1155.21 1. 63 1. 08E+00 3.64E+OO miss 1238.12 5.83 2.lS E-01 l.02E+OO miss 1 280.98 1. 43 -4.12E-01 3.59E+OO miss 1 3 77.67 3.99 4.95E-01 l.36E+OO miss 1385. 31 0.79 5.91E-01 4.52E+OO miss 1401. 52 1. 33 6.27E-01 3.51E+OO miss 1407.99 2.39 8.15E-01 2.14E+0 0 miss 1509.21 2.13 1. 38E-01 1.42E+OO m iss 1661.27 1. 05 O.OOE+OO l.lSE+OO miss 1729.59 2.88 -1. 39E-01 1.17E+OO miss 1 764.49 15.30 2.45E-01 5.06E-01 miss 1 847.43 2.03 7.38E-01 3.09E+OO m i ss > 2118.51 1.16 O.OOE+OO O.OOE+OO m i ss + Pb-214 241. 99 7.25 4.25E-01 9.65E-02 5.66E-01 m iss 295.22

• 18.42 2.38E-01 1.91E-01 miss 351.93

• 35.60 2.70E-01 9.65E-02 miss 785.96 1. 06 -4.31E-01 3.26E+OO miss + Pb214-XR 7 4.82 5.80 5.97E-01 1.24E+OO 2.05E+OO miss 77 .11 9.70 6.95E-01 1. 24E+OO miss 87.35 2.24 -2.82E-01 2.73E+OO miss 89.78 0.82 -1.76E+OO 7.28E+OO miss + Ra-226 186.21 3.64 1.79E-01 9.23E-01 9.23E-01 miss + Ac-228 129.07 2.4 2 3.22E-01 9.58E-02 l.40E+OO miss 209.25 3.89 -3.67E-02 6.29E-01 miss 270.24 3.46 2.36E-01 9.99E-01 miss 328.00 2.95 7.21E-01 1. 30E+OO miss 338.32 1 1. 27 2.39E-01 3.87E-01 miss 409.46 1. 92 -2.llE-01

1. 53E+00 miss 463.00 4.4 0 2.87E-01 8.15E-01 miss 794.95 4.25 1.02E-01 9.91E-01 m i ss 911.20 25.80 2.53E-01 9.58E-02 miss 964. 7 7 4.99 -7.89E-02

7. 96E-Ol miss 968.97 15.80 8.65E-02 3.20 E-01 miss 6/7/20 ,o 12: 44: 11PM Page 8 of8 Analysis Report for 07-Jun-16-10010 . ' L310224AFRGS013SS (DRIED} Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCi/grams) (pCi!grams)

Corr Ac-228 1588.20 3.22 2.66E-01 9.58E-02 l.23E+OO m is s + Pa-231 27.36 10.30 7.79E-02 l.18E+OO 2.46E+OO miss 283.69 1. 70 6.48E-01 l.83E+OO miss 300.0 7 2.47 -9.52E-02

.. 31E+OO miss 302.65 2.20 -1.88E-Ol l.18E+OO miss 330.06 1. 40 -1.14E-Ol 2.03E+OO m i ss + Th-234 92.38 2.13 4.27E-01 3.35E+OO 3.36E+OO miss 92.80 2.10 -4.lBE-01 3.35E+OO miss 112.81 0.2 1 -6.69E+OO

..94E+Ol miss + U-235 143.76 10. 96 4.77E-02 5.87E-02 2.70E-01 miss 163.33 5.08 -l.16E-01 6.04E-01 miss 185.71 57.20 l.98E-02 5.87E-02 miss 202.11 1. 08 -8.19E-01

2. llE+OO miss 205.31 5.01 1.45E-01 5.20E-01 miss + Am-241 59.5 4 35.90 -2.17E-01 6.55E-0 1 6.SSE-01 miss + :; Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > :; MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence l evel Coincidence correction performed. free = No co i ncidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45 40 35 V) .µ C: ::::I 8 30 25 20 i:5 ' .a ... 15 10 5 0 1000 .... .... . "' 2000 3000 0000015092.CNF 4000 channel 5000 L ive Ti m e : 600.000 sec Real Ti m e :6 0 0.910 sec sta r t: 1: -0. l(keV) stop : 8192 :2 04 7. O (kev) Acq. S tart : Tue Jun 07 1 2: 33: 09 2 016 6000 7000 8000 61712v ,o 2:25: 50PM ex Gamm , a Analysis Report for 07-Jun-16-10011 L310224AFRGS014SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live lime Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 07-Jun-16-10011

L310224AFRGS014SS (DRIED) : Miscellaneous 1.933E+03 grams : Default

• 6/2/2016 2:00:00PM 6/7/2016 2:15:14PM 130G 1 L Sand Sample JWelch P11314X2 130G Sand 600.0 seconds : 600.6 seconds : 0.10 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM 1/27/2016

11/26/2012

• 15093 PEAK WITH NID REPORT Peak Analysis Performed on : 6/7/2016 2:25:18PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page I of8 617/20*,v 2:25:50PM Analysis Report for 07-Jun-16-10011 M m M m L310224AFRGS014SS (DRIED) Peak Energy ROI No. (keV) start 1 74.89 294 -2 76.97 294 -3 238.67 949 -4 241. 59 949 -5 295.22 1176 -6 338.35 1 347 -7 351. 88 1 398 -8 583.16 2326 -9 609.29 2429 -10 768.36 3068 -11 911.18 3636 -12 1120.55 4475 -L:i 1460.97 5835 -14 1764.60 7053 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 324 324 974 974 1188 1360 1414 2340 2444 3077 3652 4486 585 1 7066 Peak Nat PA:tlc N,:,f JtreR Centroid Area Uncertainty 300.79 4.99E+Ol 20.69 309.09 7.67E+O l 23.38 955.02 2.77E+02 34. 72 966. 66 6.87E+Ol 19.04 1180. 94 9.07E+Ol 27.32 1353.27 6.38E+O l 22.31 1407.33 1.90E+02 36 .12 2331.62 9 .13E+Ol 23.06 2436.10 1. 29E+02 26 .24 3072. 07 1.48E+Ol 9.62 3643.23 6.63E+Ol 17.90 4480.77 2.19E+01 :!.2. 29 5843.21 9.07E+Ol 20. 68 7059.10 2.55E+Ol 11.33 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Roo t\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDE S Nuclide Id Energy Yield(%) Activity Page2 of8 Continuum Tentative Counts Nuclide 1.90E+02 Pb214-XR Pb212-XR 1.76E+02 Pb214-XR Pb212-XR 9.78E+Ol Pb-2 1 2 8.95E+Ol Pb-2H 7.26E+Ol Pb-214 Eu-152 5.04E+Ol Ac-228 9. 96E+Ol Pb-21<! Bi-2 11 3.34E+Ol Tl-208 3.31E+Ol Bi-2 1 4 8.46E+OO Bi-214 1.13E+Ol Ac-228 1.61E+Ol Bi-2 14 l.46E+Ol K-40 7.UOE+OO Bi-214 Activity Coinc Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 0.99 1 460.82

• 10.66 2.62E+OO 6.38E-01 m i ss Tl-208 1. 00 583.19

• 85.0 0 1.78E-O: 4.97E-02 miss Pb-212 1. 00 115.18 0.60 238.63

• 43.60 5.70E-0 1 1.1 7E-01 mi ss 300.09 3.30 Pb212-XR 0.99 74.82

• 10.28 8.lOE-01 3.75E-01 miss 77 .11

• 1 7.10 6.95E-O l 2.56E-01 miss 87.35 3.97 89.78 1. 46 Bi-21 4 0.9 9 609.32

• 45.49 4.85E-O::.

1.14E-01 miss Analysis Re~ort for 07-Jun-16-10 011 L310224AFRGS014SS (DRIED) Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 768.36 806.18 934.06 1120.29 1155. 21 1238.12 1280.98 1377.67 1385.31 1401.52 1 407.99 1509.21 1661.27 1729.59 1764.49 1847.43 2118.51 Pb-214 0.99 241.99 295.22 351.93 785.96 Ac-228 0.74 129.07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911. 20 964.77 968. 97 1588.20 * = E ner gy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * * * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence.index threshold=

0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 4.89 1.26 3 .11 14.92 1. 63 5.83 1. 43 3.99 0.79 1. 33 2.39 2.13 1. 05 2.88 15.30 2.03 1.1 6 7.25 18.42 35.60 1. 06 2.42 3.89 3.46 2.95 11.27 1. 92 4.40 4.25 25.80 4.99 15.80 3.22 miss = Nuclide energy was not found in the coincidence library. 6/7/20 ,.., 2:25:SOPM Page 3 of8 Activity Activity Coinc (pCilgrams)

Uncertainty Corr 6.0lE-0 1 3.97E-01 miss 3.77E-0 1 2 .13E-01 miss 5.92E-01 2.67E-01 miss 8.57E-01 2.74E-01 miss 5.0SE-Ol 1. 74E-01 miss 6.21E-01 1.54E-01 miss 6.41E-O l 2.47E-01 miss 5.75E-01 1.63E-01 miss 617/20 , -2:25:SOPM Analysis Report for 07-Jun-16-10011 L310224AFRGS014SS (DRIED) I N',ER rrR rN'"' r "'"" nRE"' Tern Rc~"QQT I I' re Cl vC vVI"'\ V, u ,-, 'I X X Nuclide Name K-40 Tl-2 0 8 Bi-2 11 Pb-2 1 2 Pb 2 1 2-X R Bi-21 4 P b-21 4 P b214-XR A c-228 Nuclide Id Confidence 0.9 9 9 1. 000 0. 96 0 1. 000 0.999 0.999 0.9 99 0.9 99 0.745 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 2.62E+OO 1.78E-01 5.70E-01 7.32E-0 1 4.84E-0 1 6.14E-01 5.9 5 E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty 6.38E-01 4.97E-02 1.17E-01 2. llE-01 9.17E-02 1.06E-01 1.36E-01 Page .i of 8 Comments 6/7/20. Analysis Report for 07-Jun-16-10011 L310224AFRGS014SS (DRIED) Peak Locate Performed o n Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet regio n m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/7/2016 2: 25:18PM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 2:25:50PM Peak Type Page 5 of& Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCilgrams) (pCilgrams)

Corr + K-40 1460.82

• 10.66 2.62E+OO 4.60E-01 4.60E-01 miss + Cr-51 320.08 9.9 1 8.16E-02 3.46E-01 3.46E-01 free + Mn-54 834.85 99.98 1.27E-02 4.0lE-02 4.0lE-02 miss + Co-58 810.76 99.45 2.18E-03 3.27E-02 3.27E-02 miss 1674.73 0.52 O.OOE+OO l.87E+00 miss + Co-60 1173.23 99.85 -9.83E-03 2.46E-02 2.46E-02 miss 1 332.49 99.98 1.07E-02 4.0SE-02 miss + Nb-94 702.65 99.81 l.41E-02 2.33E-02 3.66E-02 miss 871.09 99.89 -9.39E-03 2.33E-02 miss + Ag-108m 79 .13 6.60 1.80E-01 1.95E-02 8.32E-01 miss 433.94 90.50 -1.04E-02 1.95E-02 miss 614.28 89.80 -3.73E-03 3.18E-02 miss 722. 94 90.80 -2.23E-02 2.97E-02 m i ss + Sn-113 255.13 2 .11 -5.70E-01 4.13E-02 1. 03E+OO free 391. 70 64.97 -3.93E-03 4.13E-02 free + Cs-134 475.36 1. 48 -6.30E-01 2.91E-02 l.63E+OO miss 563.25 8.34 1.19E-01 3.53E-01 miss 569.33 15.37 2. 71E-02 l.93E-01 miss 604. 72 97.62 -1. 28E-02 2.91E-02 miss 6/7/2i.,.

2:25:50PM Page 6 of8 Analys i s Report for 07-Jun-16-1001 1 L310224AFRGS014SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCUgrams) (pCilgrams)

Corr Cs-134 795.86 85.46 -9.22E-04 2.91E-02 4.67E-02 miss 801.95 8.69 -5.79E-02 2.55E-01 miss 1038.61 0.99 -3.71E-01 2.30E+OO miss 1167. 97 1. 79 -5.48E-01 1.77E+OO miss 1365.19 3.02 -2.64E-01 7.16E-Ol miss + Cs-137 661.66 85.10 -5.65E-03 3.36E-02 3.36E-02 miss + Eu-152 121.78 28.67 1.72E-03 9.64E-02 9.64E-02 miss 244.70 7.61 -l.40E-01 3.00E-01 miss 295.94 0.45 l.76E+01 l.15E+01 miss 344.28 26.60 1. 35E-02 l.06E-01 miss 367.79 0.86 -l.40E+OO 2.21E+OO miss 411.12 2.24 -l.08E-02 l.17E+OO miss 443.96 2.83 -4.57E-01 6.35E-01 miss 488.68 0.42 l.28E+OO 5.24E+OO miss 563.99 0.49 -9.37E-01 5.49E+OO miss 586.26 0.46 1.44E-01 6.55E+OO miss 678.62 0.47 6. 2 6E-01 6.48E+OO miss 688.67 0.86 8.73E-02 3.24E+OO miss 719. 35 0.28 3.16E+OO l.24E+Ol miss 778.90 12.96 7.40E-02 2.70E-01 miss 810.45 0.32 4.20E+OO l.12E+Ol miss 867.37 4.26 1.73E-01 8.05E-01 miss 919.33 0.43 -4.38E-01 6.32E+0()

miss 964. 08 14.65 2.61E-01 3.81E-01 miss 1085.87 10.24 -2.lOE-02 2.28E-01 miss 1089.74 1. 73 7.46E-01 2.31E+OO miss 1112. 07 13.69 5.37E-02 2.63E-Ol miss 1212.95 1. 43 -1.08E+00 2.48E+OO miss 1249.94 0.19 -2. llE+OO 2.19E+Ol miss 1299.14 1. 63 8.27E-02 1.87E+OO miss 1408.01 21. 07 1. 72E-02 1.32E-01 miss 1457.64 0.50 -1.03E+01 9.17E+OO miss 1528.10 0.28 O.OOE+OO 3.06E+OO miss + Eu-154 123.07 40.40 2.23E-02 3.59E-02 6.75E-02 miss 247.93 6.89 -2.23E-01 3.14E-01 miss 591.76 4.95 1.17E-01 6.13E-01 miss 692. 42 1. 78 l.42E-01 1.74E+OO miss 723. 30 20.06 -7.28E-02

1. 51E-01 miss 756.80 4.52 -2.07E-01 5.24E-01 miss 873.18 12.08 1.48E-01 2. 99E-01 miss 996.29 10.48 l .13E-02 3.20E-01 miss 1004.76 18.01 O.OOE+OO 3.59E-02 miss 1274.43 34.80 -1.83E-02 5.90E-02 miss 1596.48 1. 80 -9.17E-01 l.35E+OO miss + Eu-155 45.30 1. 31 -1.28E+OO

1. SOE-01 6.58E+OO miss 60.01 1. 22 1.76E+00 9.52E+OO miss 86.55 30.70 -2.82E-03 1.54E-01 miss 105.31 21.10 -2.19E-02 1.50E-01 miss + Tl-208 583.19

• 85.00 l.78E-01 4.66E-02 4.66E-02 miss + Bi-211 351.07

• 13 .02 l.70E+OO 3.66E-01 3.66E-01 miss + Pb-211 404.85 3.78 -2.83E-01 5.67E-01 5.67E-01 miss 6/7/20. 2:25:SOPM Page 7 of8 Analysis Report for 07-Jun-16-10011 L310224AFRGS014SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCilgrams) (pCi/grams)

Corr Pb-211 427.09 1. 76 -5.30E-02 5.67E-01 ::..20E+00 miss 832.01 3.52 -1. 79E-01 9.47E-01 miss + Bi-212 39.86 1. 06 -l.38E+OO 7.99E-01 8. llE+OO miss 727.33 6.67 5.36E-01 7.99E-01 miss 785.37 1.10 6.92E-01 3.69E+OO miss 1620.50 1. 47 -5.66E-02

1. 67E+OO miss + Pb-212 115 .18 0.60 2.39E+OO 7.25E-02 5.08E+OO miss 238.63

• 43.60 5.70E-01 7.25E-02 miss 300.09 3.30 7.97E-01 1.08E+OO miss + Pb212-XR 74.82 .,. 10.28 8.lOE-01 4.21E-01 7.80E-01 miss 77.11

• 17.10 6.95E-01 4.21E-01 miss 87.35 3.97 1.19E+OO 1.. 29E+OO miss 89.78 1. 46 2.44E+00 3.25E+OO miss + Bi-214 609.3 2

• 45.49 4.85E-01 9.07E-02 9.07E-02 miss 768.36

• 4.89 6.0lE-01 4.97E-01 miss 806.18 1. 26 8.23E-01 2. 95E+00 miss 934.06 3.11 6.88E-01 l.52E+OO miss 1120.29

• 14.92 3.77E-01 2.71E-01 miss 1155.21 1. 63 3.69E-01 2.40E+OO miss 1238.12 5.83 6.86E-01 9.99E-01 miss 1280.98 1. 43 7.15E-01 3.25E+OO miss 1377.67 3.99 2.21E-01 1.04E+OO miss 1385.31 0.79 3.37E-01 5.25E+OO miss 1401.52 1. 33 4.16E-01 2.41E+OO miss 1407.99 2.39 1.52E-01 l.16E+OO miss 1509.21 2.13 8.46E-02 1.37E+OO miss 1661. 27 1. 05 -1.42E-01 3.0lE+OO miss 1729.59 2.88 6.08E-01 1.59E+OO miss 1764.49

• 15.30 5.92E-01 2.59E-01 miss 1847.43 2.03 9.03E-01 2.37E+00 miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99

• 7.25 8. 57E-*01 1.34E-01 4.22E-01 miss 295.22

• 18.42 5.09E-01 1. 96E-01 miss 351.93

• 35.60 6.21E-01 1.34E-01 miss 785.96 1. 06 2.04E+OO 4.07E+OO miss + Pb214-J~R 74.82

• 5.80 l.44E+OO 7.42E-01 l.38E+OO miss '77, 11

• 9.70 1. 23E+OO 7.42E-01 miss 8 7.35 2.24 2.lOE+OO 2.29E+OO miss 89.78 0.82 4.34E+00 5.79E+OO miss + Ra-226 186.21 3.64 9.69E-01 1.0lE+OO 1. OlE+OO miss + Ac-228 129.07 2.42 2.69E-01 1.29E-01 1. 23E+OO miss 209.25 3.89 7.48E-01 9.07E-01 miss 270.24 3.46 5.14E-01 1. OlE+OO miss 328.00 2.95 2.84E-01 1. llE+OO miss 338.32

• 11.27 6.41E-01 2.84E-01 miss 409.46 1. 92 6.83E-01 1.69E+OO miss 463.00 4.40 4.55E-01 8.32E-01 m i ss 794.95 4.25 4. llE-01 9.93E-01 miss 911. 20

• 25.80 5.75E-01 1.29E-01 m i ss 964. 77 4.99 7.22E-01 l.12E+00 miss 968. 97 15.80 6.56E-01 5.25E-01 miss 6/7/20. _ 2:25:SOPM Page 8 of8 Analysis Report for 07-Jun-16-10011 L310224AFRGS014SS (DRIED) Nuclide Energy Yield{";{,)

Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCUgrams) (pCi/grams)

{pCi!grams)

Corr Ac-228 1588.20 3.22 4.61E-01 1. 29E-01 l.44E+OO miss + Pa-231 27.36 10.30 O.OOE+OO 8.86E-02 8.86E-02 miss 283.69 1. 70 7.33E-01 l.69E+OO miss 300.07 2.47 1.06E+OO 1.45E+OO miss 302.65 2.20 -1.35E-01 1.07E+OO miss 330.06 1. 40 -4.24E-01

1. 99E+OO miss + Th-234 92.38 2.13 1.05E+OO 2.44E+OO 2.44E+OO miss 92.80 2.10 2.00E+OO 2.57E+00 miss 112. 81 0.21 -1.33E-01 1.71E+D1 miss + U-235 143.76 10. 96 1.25E-01 6. llE-02 2.89E-01 miss 163.33 5.08 -9.57E-02 4.69E-01 miss 185.71 57.20 3.75E-02 6.llE-02 miss 202 .11 1. 08 -1.08E+OO 2.21E+OO miss 205.31 5.01 2.12E-01 5. 99E-01 miss + Arn-241 59.54 35.90 l.25E-01 3.43E-01 3.43E-Ol miss + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the c;lecay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

120 110 100 90 80 £1 I ..0 0.. 70 V) ,1,-1 C: :::, 0 60 u 50 40 "' X ...!.. ...... ..... ..... ..c 0.. ...... ..... I .0 0.. 30 20 10 0 1000 0000015093.CNF *..; l ',ll.l,.J~,i'

! , L uJ 2000 3000 4000 5000 channel Live Time : 600.000 sec Real Time :600.600 sec Start: 1: -0.2(kev) stop : 8192: 2047.4(kev)

Acq. start : Tue Jun 07 14:15:14 2016 0 ;;:i I "&i 6000 7000 8000 4/26/20. 1:29:16PM Analysis Report for 26-Apr-16-10003 L310224AFJGS15SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done O n Efficiency Calibration Description Sample Number : 26-Apr-16-10003

L310224AFJGS15SS (DRIED) : Miscellaneous

• 2.126E+03 grams : Default : 4/25/2016 10:30:00AM

4/26/2016 12:34:28PM

130G 1 L Sand Sample : JWelch : P40818B : 130G Sand : 1800.0 seconds : 1803.6 seconds : 0.20% : 2.80 : 120 -8192 : 120-8192 : 1.000FWHM : 1/27/2016

1/5/2015 : 14735 PEAK WITH NID REPORT Peak Analysis Performed on : 4/26/2016 1:28:37PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM I ( Page I of9 4/26/2011..

1 :29: 16PM Page 2 of9 'Analysis Report for 26-Apr-16-10003 L310224AFJGS15SS (DRIED) Peak Energy ROI ROI Peak Net Peak Net Area Continuum Tentative No. (keV) start end Centroid Area Uncertainty Counts Nuclide M 1 74.78 294 -315 300.21 1.40E+O~ 41.13 1.01E+03 Pb214-XR Pb212-};R m 2 77.05 294 -315 309.26 2.72E+02 48.95 9.80E+02 Pb214-XR Pb212-XR M 3 87.24 343 -365 349.96 1.41E+02 41.86 9.24E+02 Pb214-}~R Pb212-}~R Eu-155 Ce. a 9 m 4 89.95 343 -365 360.82 8.50E+O l 39.44 9.59E+02 Th-231 U235-XR Ac228-XR Pb214-XR Pb212-X:l.

5 154.06 613 -620 6 1 7.00 4. 77E+Ol 53. 92 6.77E+02 ..... 19-£-,:u.y 6 185.88 739 -750 74 4.18 1.41E+02 74. 66 9.98E+02 U-235 Ra-226 7 209.13 833 -84 3 837.10 1.09E+02 63.15 7.41E+02 Ac-228 M 8 238.59 94 7 -973 954.87 2.12E+03 95.53 7.86E+02 Pb-212 m 9 241.52 94 7 -973 966. 57 3.45E+02 44.90 6.50E+02 Pb-214 10 270.18 1075 -1089 1081.10 1.38E+02 61.88 5.67E+02 Ac-228 Rn-219 11 277.24 1105 -1117 1109.35 7.23E+O l 52. 62 4.69E+02 Ba-133 1-*>-2.f"'

M 12 295.17 1172 -1206 1180.99 5.57E+02 51.91 4.48E+02 Pb-2 1 4 Eu-152 m 13 299.98 1172 -1206 1200.24 1.24E+02 31.02 4.61E+02 Th-227 Pa-2 31 Pb-212 14 3 2 8.06 1307 -1319 1312.47 7.49E+O l 44.12 3.54E+02 Ac-228 15 338.21 1347 -1359 1353. 05 3.81E+02 58.76 4.18E+02 Ac-228 16 351.84 1384 -1415 1407.56 9.34E+02 107.00 8.27E+02 Pb-21 4 Bi-211 17 4 09.16 1631 -1645 1636.71 4.03E+O l 42.06 3.17E+02 Cs-138 Ac-228 18 462.78 184 1 -1857 1851.08 1.08E+02 43.12 2.63E+02 Cs-138 Ac-228 Sb-125 19 510.62 2033 -2047 2042.35 2.09E+02 48. ,4 3.05E+02 ..... ~IIH~S(I 20 583.09 2323 -2339 2332.15 6.63E+02 63.48 2.53E+02 Tl-208 21 609.19 2426 -2444 2436.51 7.37E+02 63.20 1. 8 2 E+02 Bi-214 22 727.12 290 0 -2917 2908.14 l.25E+D2 34.21 1. 34E+02 Bi-212 M 23 768.23 3063 -3093 3072.58 5.46E+Ol 18.88 1.13E+02 Bi-214 m 24 772.07 3063 -3093 3087.94 3.85E+Ol 17.40 1. 22E+D2 ..... TJ..~of( 25 785.53 3136 -3147 3 1 41.77 3.43E+Ol 22.27 8.94E+Ol Bi-212 Pb-214 2 6 794.86 3172 -3185 3179.0 9 5.40E+Ol 22.81 7.0lE+Ol Ac-228 Cs-134 27 806.24 3220 -3229 3224.63 1.79E+Ol 17.67 6.43E+Ol Bi-214 28 860.45 3431 -3448 3441.47 8.08E+Ol 26.39 7.45E+Ol ..... ;1,,,-;;o'I 29 911. 00 36 3 1 -3654 3643.72 5.30E+02 52.02 9.83E+Ol Ac-228 30 933.70 3724 -3742 3734.54 6.18E+O l 22.52 5.03E+Ol Bi-214 M 31 964.64 3850 -3885 3858.31 7.05E+Ol 19.86 1. 03E+02 Ac-228 Eu-152 m 32 968. 87 3850 -3885 3875.23 2.81E+02 34 .11 7.44E+Ol Ac-228 33 1120.06 4472 -4490 4480.21 1.39E+02 30.36 7.67E+Ol Bi-214

'An al y s is R ep o rt for 26-A p r-16-10003 L3 1 0224AFJGS15SS (D R I ED) Peak Energy ROI No. (keV) start 34 1238.01 4945 -35 1377.58 5503 -36 1460.60 5830 -37 1592.43 6365 -38 1620.62 6478 -39 1630.35 6517 -40 1764.16 705 1 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 4959 5518 5853 6378 6491 6530 :068 4/26/2011:.

1:29:16PM Peak. NetPeak Net Area Centroid Area Uncertainty 4952.30 4.93E+O l 21.14 55 1 0.98 4.79E+O l 18.39 5843.36 l.62E+02 29.17 6371.25 l.15E+Ol 14.37 6484.12 2.62E+01 13.43 6523 .11 2.66E+Ol 12.75 7059.05 1.22E+02 24.42 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Page 3 of9 Continuum Tentative Counts Nuclide 5.95E+Ol Bi-214 3.42E+Ol Bi-214 3. 72E+Ol K-40 4. llE+Ol .... 1),;or 1.97E+Ol Bi-212 l.48E+Ol ..... tfe,.J)j.j"" 2.55E+Ol Bi-214 Activity Caine Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 0.99 1 460.82

• 1 0.66 1.58E+OO 3.15E-01 m i ss T l-2 0 8 0.99 583.19

• 85.00 4.34E-01 6.67E-02 miss Bi-212 0.99 39.86 1. 06 72 7. 33 .. 6.67 1.21E+OO 3.60E-01 miss 7 85.3 7 1.10 2. llE+OO l.39E+OO miss 1 62 0.50

• 1. 47 2.00E+OO l.04E+OO miss P b-2 1 2 1. 00 11 5 .1 8 0.60 238.63

• 43.60 1.49E+OO 2.50E-01 miss 30 0.09

• 3.30 1.33E+OO 3.97E-01 miss Pb212-XR 1. 00 7 4.82

• 10.28 1.30E+OO 4.67E-01 miss 7 7 .11

• 17.10 1.35E+OO 3.69E-01 miss 8 7.35

• 3. 97 1.84E+OO 6.63E-01 miss 8 9.78 ~:: 1. 46 2.81E+OO l.43E+OO miss Bi-214 0.9 9 609.32

• 45.49 9.28E-01 1.3 7E-01 miss 76 8.36

• 4.89 7.47E-01 2.71E-01 miss 806.18

• 1. 26 9.76E-01 9. 72E-01 miss 9 3 4.06

• 3.11 1. 52E+OO 5.67E-01 miss 1120.29

• 1 4.92 8.00E-01 1.87E-01 miss 1155. 2 1 1. 63 1238.12

• 5.83 7.77E-01 3.39E-01 miss 128 0.9 8 1. 43 4/26/201_

1:29:16PM Page 4 of9 Analysis Report for 26-Apr-16-10003 L310224AFJGS15SS (DRIED) Nuclide Id Energy Yield(%) Activity Activity Coinc Name Confidence (keV) (pC//grams)

Uncertainty Corr Bi-214 0.99 1377.67

• 3.99 1.19E+OO 4.66E-01 miss 1385.31 0.79 1401.5 2 1. 33 1 407.99 2.39 1 509.21 2.13 1661. 27 1. 05 1729.59 2.88 1764.49

• 15.30 9.57E-Ol 2.06E-01 miss 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99

• 7.25 l.47E+OO 3.03E-01 miss 295.22

• 18.42 l.06E+OO 1. 96E-01 miss 351.93

• 35.60 l.03E+OC 2.02E-01 miss 785. 96 ".': 1. 06 2.20E+OC 1.45E+OO miss Ra-226 0.99 186.21

• 3.64 1. OSE+OO 5.84E-01 miss Ac-228 0.99 129.07 2.42 209.25

• 3.89 8.09E-01 4.86E-01 miss 270.24

• 3.46 1.32E+OO 6.31E-01 miss 328.00

• 2.95 9.SlE-01 5.86E-01 miss 338.32

• 11.27 1.29E+OC 2.90E-01 miss 409.46

• 1. 92 9.16E-01 9.66E-01 miss 463.00

• 4.40 l.16E+OO 4.94E-01 miss 794.95

• 4.25 8.69E-01 3.BOE-01 miss 911.20

• 25.80 1.54E+OO 2.02E-01 miss 964. 77

• 4.99 1. lOE+OO 3.26E-01 miss 968. 97

• 15.80 1. 39E+OO 2.09E-01 miss 1588.20 3.22 U-235 0.99 143.76 10. 96 163.33 5.08 185. 71

• 57.20 6.71E-02 3.72E-02 miss 202.11 1. 08 205.31 5.01 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. @ ; Energy line not used for Weighted Mean Activity Energy Tolerance:

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. INTERFERENCE CORRECTED REPORT 4/26/20*1.

1 :29:16PM Page 5 of9 Analysis Report for 26-Apr-16-10003 L310224AFJGS15SS (DRIED) Nuclide Nuclide wt mean Wt mean Comments Name Id Activity Activity Confidence (pCi/grams)

Uncertainty K-40 0.997 l.58E+OO 3.lSE-01 X

• c a 1 09 0. 962 Tl-208 0.999 4.34E-01 6.67E-02 X Bi-211 0.964 Bi-212 0.998 1. 28E+OO 3.29E-01 Pb-212 1. 000 1. 44E+OO 2.llE-01 Pb212-XR 1. 000 l.46E+OO 2.61E-01 Bi-214 0.998 9.0lE-01 8.56E-02 Pb-214 0. 998 l.12E+OO 1. 27E-Ol X Pb2 1 4-XR 1. 000 X Rn-219 0.400 ? Ra-226 0.993 1. OSE+OO 5.84E-01 Ac-228 0.999 l.29E+OO l.OSE-01 ? U-235 0.999 6. 71E-02 3. 72E-02 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 4/26/201...

1 :29:16PM Page 6 of9 Analysis Report for 26-Apr-16-10003 m + + + + + + + L310224AFJGS15SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) 5 154.06 11 277. 24 19 510.62 24 772. 07 28 860.45 37 1592.43 39 1630.35 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 4/26/2016 1 :28:37PM : 120 : 8192 Peak Size (CPS) 2.64814E-02 4.01764E-02 l.16313E-01 2.14044E-02 4.48635E-02 6.37153E-03 l.47712E-02 Peak CPS(%) Uncertainty 56.56 36.38 11. 64 22.58 1 6.34 62.64 23.97 Peak Tolerance Type Nuclide Sum fc.-~').ff rv,-oY ,t,v H-51 f T'J--),(I"' Sum r J--~" 'ti' Sum r;, ~:;,.ot" ,4.<,*;;).y' NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCUgrams) (pCilgrams) (pCi!grams)

Corr K-40 1460.82

• 10.66 1. 58E+OO 2.53E-01 2.53E-01 miss Cr-51 320.08 9.9 1 -6.74E-03 2.02E-01 2.02E-Ol free Nn-54 834.85 99.98 1.62E-02 2.64E-02 2.64E-02 miss Co-58 810.76 99.45 2.79E-03 2.16E-02 2.16E-02 miss 1674.73 0.52 -9.40E-Ol 3.16E+OO miss Co-60 1171.23 99.85 -5.72E-04

1. 79E-02 l.79E-02 miss 1332.49 99.98 7.87E-03 2.42E-02 miss Nb-94 702.65 99.81 -4.37E-03 1.89E-02 2.19E-02 miss 871.09 99.89 -5.22E-03 1.89E-02 miss Ag-108m 79.13 6.60 -5.48E-02 2.14E-02 9 .17E-01 miss 433.94 90.50 1. 47E-03 2.14E-02 miss 4/26/201 .... 1 :29:16PM Page 7 of9 Analysis Report for 26-Apr-16-10003 L310224AFJGS15SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCilgrams) (pCi!grams)

{pCilgrams)

Corr Ag-108m 614.28 89.80 -4.34E-03 2.14E-02 2.41E-02 miss 722.94 90.80 4.14E-03 2.47E-02 miss + Sn-113 255 .13 2 .11 -9.02E-02 3.09E-02 1.03E+OO free 391. 70 64.97 1.26E-03 3.09E-02 free + Cs-134 475.36 1. 48 -3.98E-01 1.92E-02 1.27E+OO miss 563.25 8.34 -7.86E-03

2. 68E-01 miss 569.33 15.37 1.91E-02 1.39E-Ol miss 604. 72 97.62 -1.25E-02

1. 92E-02 miss 795.86 85.46 -4.59E-03 3.27E-02 miss 801.95 8.69 5.33E-02 2.24E-01 miss 1038.61 0.99 -4.89E-01 1.44E+OO miss 1167.97 1. 79 -6.36E-02 l.19E+OO miss 1365.19 3.02 -3.00E-01

5. 68E-01 miss + Cs-137 661.66 85.10 7.04E-03 2.78E-02 2.78E-02 miss + Eu-152 121. 78 28.67 2.46E-02 6.94E-02 9.14E-02 miss 244.70 7.61 -9.86E-02 2.84E-01 miss 295.94 0.45 2.78E+Ol 8.89E+OO miss 344.28 26.60 -3.0lE-02 6.94E-02 miss 367.79 0.86 9.97E-01 2.46E+OO miss 411.12 2.24 1.95E-01 9.35E-01 miss 443.96 2.83 -1.50E-01 6.65E-01 miss 488.68 0.42 -1.03E+OO 4.lOE+OO miss 563.99 0.49 -3.31E-Ol 4.45E+OO miss 586.26 0.46 -8.24E+OO 5.09E+OO miss 678.62 0.47 5.48E-01 4.24E+OO mis~ 688.67 0.86 -5.72E-01 2.38E+OO miss 719.35 0.28 -4. 91E-01 8.18E+OO miss 778.90 12.96 -1.89E-02 1.49E-01 miss 810.45 0.32 2.58E-01 6.62E+OO miss 867.37 4.26 1.06E-01 4.94E-01 miss 919.33 0.43 -1. 34E-01 4.33E+OO miss 964. 08 14.65 3.54E-01 2. 68E-01 miss 1085.87 10.24 -1.96E-02 1.98E-01 miss 1089.74 1. 73 -4.34E-01 1.0lE+OO miss 1112. 07 13.69 -7.62E-02 1.37E-01 miss 1212.95 1. 43 4.00E-01 1.50E+OO miss 1249.94 0.19 -6.62E-01 1.20E+Ol miss 1299.14 1. 63 2.40E-02 1.25E+OO miss 1408.01 21. 07 1.25E-01 1.57E-01 miss 1457.64 0.50 -9.30E-01 6.37E+OO miss 1528.10 0.28 -8.47E-01 4.98E+OO miss *I Eu-154 123.07 40.40 -1. 42E-02 6.1 4E-02 6.14E-02 miss 247.93 6.89 -7.75E-02

2. 96E-01 miss 591.76 4.95 -2.18E-01 3.93E-01 miss 692.42 1. 78 2.66E-Ol 1. 26E+OO miss 723. 30 20.06 -5.90E-03 1.12E-01 miss 756.80 4.52 -1.99E-01 4.20E-01 miss 873.18 12.08 -1.63E-02 1.54E-01 miss 996.29 10.48 6.69E-02 l.87E-01 miss 1004.76 18.01 -7.43E-04

1. 02E-01 miss 1274.43 34.80 2.0SE-02 6.61E-02 miss 4/26/2 0 1 .. 1: 2 9:16 P M Page 8 of9 Analysis Report for 26-Apr-16-10003 L310224AFJGS15SS (DRIED) Nuclide Energy Yield{°/o)

Activity NuclideMDA LineMDA Caine Name (keV) (pCVgrams) (pCilgrams) (pCi/grams)

Corr Eu-154 1596.48 1. 80 -2.76E-01 6.14E-02 l.07E+OO miss + Eu-155 45.30 1. 31 2.59E+00 1.52E-01 1.SOE+Ol miss 60.01 1. 22 -2.27E+OO l.47E+Ol miss 86.55 30.70 3.0BE-02 1.58E-01 miss 105.31 21.1 0 5.lOE-02 l.52E-01 miss + Tl-208 583.1 9

• 85.00 4.34E-01 4.17E-02 4.17E-02 miss + Bi-211 351. 07

• 13. 02 2.81E+OO 4.43E-01 4.43E-01 miss + Pb-211 404.85 3.78 5.86E-02 5.47E-01 5.47E-01 miss 427.09 1. 76 3.34E-01 l.14E+OO miss 832.01 3.52 -7.91E-02 6.06E-01 miss + Bi-212 39.86 1. 06 1.56E+OO 4.38E-01 l.61E+Ol miss 727. 33 *'* 6.67 l.21E+00 4.38E-01 miss 785.37

• 1.10 2. llE+OO 2.09E+OO miss 1620.50

• 1. 47 2.00E+OO l.30E+00 miss + Pb-212 11 5 .18 0.60 2.80E+00 6.67E-02 4. 72E+OO miss 238.63

• 43.60 1.49E+OO 6.67E-02 miss 300.09

• 3.30 l.33E+OO 7.86E-01 miss + Pb212-XR 74.82

• 1 0.28 1.30E+OO 5.25E-01 9.97E-01 miss 77 .11

• 17.10 1.35E+OO 5.25E-01 miss 87.35

• 3.97 1. 84E+OO 1.34E+OO miss 89.78

• 1. 46 2.81E+OO 3.46E+OO miss Bi-21 4 609.32

• 45.49 9.28E-01 7.04E-02 7.04E-02 miss 768.36

• 4.89 7.47E-01 5.14E-01 miss 806.18

• 1. 26 9.76E-01 l.54E+OO miss 934.06

• 3.11 l.52E+OO 7.19E-01 miss 1120.29

• 14.92 8.00E-01 l.98E-01 miss 1155. 21 1. 63 3.lOE-01 1.58E+OO miss 1238.12

• 5.83 7.77E-01 4.53E-01 miss 1280.98 1. 43 8.22E-01 1.93E+OO miss 1377. 67

• 3.99 1.19E+OO 5.62E-01 miss 1385.31 0.79 5.25E-01 2.81E+OO miss 1401.52 1. 33 9.12E-01 l.92E+00 miss 1407.99 2.39 l.lOE+OO 1.38E+OO miss 1 509.21 2.13 6.86E-01 1.40E+OO miss 1661. 27 1. 05 1.18E+OO 2.45E+OO m i ss 1729.59 2.88 1.08E+OO l.30E+OO miss 1764.49

• 15.30 9.57E-01 1. 55E-01 miss 1847.43 2.03 6.26E-01 1.43E+OO miss > 2118. 51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99

• 7.25 l.47E+OO 1.38E-Ol 3.69E-01 miss 295.22

• 18.42 1.06E+OO l.38E-01 miss 351. 93

• 35.60 1. 03E+OO l.62E-01 miss 785.96

• 1. 06 2.20E+OO 2.17E+D0 miss + Pb214-XR 74.8~

• 5.80 2.31E+OO 9.25E-01 l.77E+OO miss 77 .11

• 9.70 2.38E+D0 9.25E-01 miss 87.35

• 2.24 3.26E+OO 2.37E+OO miss 89. 78

• 0.82 5.0lE+OO 6.16E+OO miss + Ra-226 186.21

• 3.64 1. OSE+OO 8.92E-01 8.92E-01 miss + Ac-228 129.07 2.42 8.23E-01 1.24E-01 1.13E+OO miss 209.25

• 3.89 8.09E-01 7.46E-01 miss 4/26/20*1-1 :29:16PM Page 9 of9 Analysis Report for 26-Apr-16-10003 L310224AFJGS15SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCUgrams) (pCilgrams) (pCi!grams)

Corr Ac-228 270.24

• 3.46 1.32E+OO 1.24E-01 9.28E-01 miss 328.00 *.': 2.95 9.51E-01 8.82E-01 miss 338.32

• 11. 27 1.29E+OO 2.54E-01 miss 409.46

• 1. 92 9.16E-01 1. 56E+OO miss 463.00

• 4.40 1.16E+OO 7.00E-01 miss 794.95

• 4.25 8.69E-01 5.06E-01 miss 911. 20

• 25.80 1.54E+OO 1.24E-01 miss 964.77

• 4.99 1. lOE+OO 5.65E-01 m i ss 968.97

• 15.80 1.39E+OO 1.54E-01 miss 1588.20 3.22 1.17E+OO 1.19E+OO miss + Pa-231 27.36 10.30 3.19E-01 8.86E-01 1.88E+OO miss 283.69 1. 70 5.14E-01 1.30E+OO miss 300.07 2.47 1.68E+OO 1.08E+OO miss 302.65 2.20 -8.84E-02 8.86E-01 miss 330.06 1. 40 -2.04E-01 1.32E+OO miss + Th-234 92.38 2.13 2.16E+OO 2.24E+OO 2.24E+OO m i ss 92.80 2.10 3.0lE+OO 2.29E+OO miss 112. 81 0.2 1 5.09 E+OO 1.41E+Ol miss + U-235 143.76 10.96 1.18E-01 5.68E-02 2.34E-01 miss 163.33 5.08 3.20E-02 4.47E-01 miss 185.71 .,. 57.20 6.71E-02 5.68E-02 miss 202 .11 1. 08 -4.69E-01 1.85E+OO miss 205.31 5.0 1 4.02E-02 4.23E-01 miss + Am-241 59.54 35.90 8.83E-02 5.40E-0 1 5.40E-01 m i ss + = Nuclide identified during the nuclide identification

• Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

0000014735.CNF 1000-900 800 700 600 t ;j VI L .µ I g 500 u 400 300 200 ! .-< ,! ;:j ..c 0.. ;!; ";' ;;;; "" X ~.-. ' 0~ r.... '° ~. .... -.t-I-~ ..... ~a:, .'.. < .\, ";' ::e I-";' "" ..c u o..~ <l ::e :::::: ";'~ J:, ";' 100+ > -* _

• J,.,""tl l\. ' , ll _.,,L , t -. 0 I I I I 1000 2000 3000 4000 Channel 5000 Live Time :1800.000 sec Real Time :1803.640 sec start: 1: -0.l(kev) stop : 8192: 2047 .O(kev) Acq. start : rue Apr 26 12:34:28 2016 6000 7000 8000 Aoex. -~amm*a*

• g i. . .. Analysis Report for 07-Jun-16-1 0004 L310224AFQGS006SS (DRIED) QC 6/7/2v 16 10:57:44AM GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range {in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 07-Jun-16-10004

L310224AFQGS006SS (DRIED) QC : Miscellaneous 1.820E+03 grams Default 6/2/2016 2:26:00PM 6/7/2016 10:46:45AM

• 130G 1LSand Sample

• JWelch : P40818B : 130G Sand : 600.0 seconds : 601. 1 seconds : 0.18 % : 2.80 : 120 -8192 : 120-8192 : 1.000FWHM ' 1/27/2016

1/5/2015 15086 PEAK WITH NID REPORT Peak Analysis Performed on : 6/7/2016 10:57:13AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page I of8 6/7/20*10 10:57:44AM Page 2 of8 Analysis Report for 07-Jun-16-10004 L310224AFQGS006SS (DRIED) QC Peak Energy ROI No. (keV) start 1 77.27 305 -2 209.27 834 -3 238.61 949 -4 295.13 1175-5 338.21 1348 -6 351.91 1401 -7 582.99 2324 -8 609.18 2430 -9 911. 09 3638 -10 968.7 9 3868 -11 1119.86 4474 -12 1460.65 5835 -13 1764.37 7053 -M = First peak in a multiplet regio n m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI Peak end Centroid 316 310.1 4 843 837.68 961 954.92 1188 1180.86 1358 1353.04 14 16 1407.82 2338 2331.72 2444 2436.45 3651 3644.08 3881 3874.92 4485 4479.42 5854 5843.58 7066 7059.89 Net Peak Net Area Continuum Area Uncertainty Counts 4.30E+Ol 33. 42 l.54E+02 3.74E+Ol 22. 63 7.73E+Ol 1.91 E+02 41.05 1.7 0E+02 7.27E+Ol 26 .13 6.86E+Ol 4.67E+Ol 19. 42 4.45E+Ol 1.17E+02 26. 62 4.66E+Ol 7.25E+Ol 22.04 3.90E+Ol 7.86E+Ol 21.17 2.67E+Ol 5.24E+Ol l S.31 5.25E+OO 2.82E+Ol 14.70 2.35E+Ol 1.74E+Ol 9.43 5.13E+OO 1.12 E+02 21. 98 7.37E+OO l.64E+Ol 9.22 5 .13E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 14 60.82

• 10.66 3.82E+OO 8.18E-01 Tl-208 0.99 583.19

• 85.00 1.66E-01 5.44E-02 Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 4.70E-01 1.26E-01 300.09 3.30 Pb212-XR 0.99 74.82 10.28 77 .11

• 17.10 7.40E-0 1 5.95E-01 87.35 3.97 89.78 1. 46 Bi-214 0.99 609.32

• 45.49 3.47E-0 1 l.02E-01 768.36 4.89 806.18 1. 26 Tentative Nuclide Pb214-XR Pb212-XR Ac-228 Pb-212 Pb-214 Eu-15 2 Ac-228 Pb-214 Bi-211 Tl-208 Bi-214 Ac-228 Ac-228 Bi-214 K-40 Bi-214 Caine Corr miss miss miss miss miss 6/7/20u; 10:57:44AM Page 3 of8 Analysis Report for 07-Jun-16-10004 L310224AFQGS006SS (DRIED) QC Nuclide Id Energy Yield(%) Activity Activity Caine Name Confidence (keV) (pCl!grams)

Uncertainty Corr Bi-214 0.99 934.06 3.11 1120.29

• 14.92 3.53E-01 1.93E-01 miss 1155. 21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509. 21 2.13 1661.27 1. 05 1729.59 2.88 1764.49 15.30 4.51E-01 2.55E-01 miss 1847.43 2.03 2118.51 1.16 Pb-214 1. 00 241.99 7.25 295.22

• 18.42 4.85E-0 1 1.91E-01 miss 351.93

• 35.60 4.50E-01 1.25E-01 miss 785.96 1. 06 Pb214-XR 0.99 74.82 5.80 77 .11

• 9.70 1.31E+OO 1. 06E+00 miss 87.35 2.24 89.78 0.82 Ac-228 0.90 1 29.07 2.42 209.25

• 3.89 9.70E-01 6.08E-01 miss 270.24 3.46 328.00 2.95 338.32

• 11.27 5.55E-01 2.48E-01 miss 409.46 1. 92 463.0 0 4.40 794.95 4.25 911.20

• 25.80 5.35E-01 1.63E-01 miss 964. 77 4.99 968. 97

• 15.80 4.91E-01 2.59E-01 miss 1588.20 3.22 * = Energy line found in the spectrum. = Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWH M Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

6/7/20-.o 10:57:44AM Analysis Report for 07-Jun-16-10004 L310224AFQGS006SS

{DRIED) QC INTERFERENCE CORRECTED REPORT X ? ? Nuclide Name K-40 Tl-20 8 Bi-211 Pb-212 Pb2 1 2-XR B i-214 Pb-214 Pb214-XR Ac-228 Nuclide Id Confidence 0.998 0.998 0.9 58 1.000 0.999 0.998 1. 000 0.9 99 0.908 ? = nuclide i s part of an undetermined solution X = nuclide r ejected by the interference analysis Wt mean Activity (pCilgrams) 3.82E+OO 1.66E-01 4.70E-01 7.40E-01 3.60E-01 4.61E-01 1.31E+OO 5.47E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty 8.18E-01 5.4 4 E-02 1.26E-01 5.95E-01 8.52E-02 1.0SE-01 1.06E+OO l.18E-01 Page 4 of8 Comments 6/7/2010 10:57:44AM Page 5 of8 Analysis Report for 07-Jun-16-10004

+ + + + + + + + + L310224AFQGS006SS (DRIED) QC Peak Locate Performed o n Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F "' Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/7/2016 10:57:13AM

120 : 8192 Peak CPS {°/o) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCilgrams) (pCilgrams) (pCilgrams)

Corr K-40 1460.82

• 10.66 3.82E+OO 4.17E-01 4.17E-01 miss Cr-51 320.08 9.91 1.69E-01 3.82E-01 3.82E-01 free Mn-54 834.85 99.98 -7.27E-03 3.29E-02 3.29E-02 miss Co-58 810.76 99.45 1. 28E-03 3.62E-02 3.62E-02 miss 1674.73 0.52 -3.06E-0 1 6.0lE+OO miss Co-60 1173.23 99.85 4.09E-03 4.40E-02 4.40E-02 miss 1332.49 99.98 1.37E-02 4.78E-02 m i ss Nb-94 702.65 99.81 5.54E-03 2.75E-02 3.51E-02 miss 871.09 99.89 2.98E-03 2.75E-02 miss Ag-108m 79.13 6.60 1. 72E-01 3.5"7E-02 1.19E+OO miss 433.94 90.50 5.41E-03 3.64E-02 miss 614.28 89.80 -2.70E-03 3.57E-02 miss 722. 94 90.80 4.31E-03 3.73E-02 miss Sn-113 255.13 2.11 4.49E-01 4.73E-02 1.52E+OO free 391. 70 64.97 5.17E-03 4.73E-02 free Cs-134 475.36 1. 48 -9.45E-01 3.58E-02 1.83E+OO miss 563.25 8.34 1.14E-01 4.47E-01 miss 569.33 15.37 5.0lE-03 1.88E-01 miss 604.72 97.62 -2.06E-03 3.58E-02 miss 6/7/2010 10:57:44AM Page 6 of8 Analysis Report for 07-Jun-16-10004 L310224AFQGS006SS (DRIED) QC Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCi/grams) (pCi/grams)

Corr Cs-134 795.86 85.46 2.12E-02 3.58E-02 5.12E-02 miss 801.95 8.69 -6.98E-02 3.00E-01 miss 1038.61 0.99 -7.29E-02 2.71E+OO miss 1167.97 1. 79 1.68E-01 2.09E+OO miss 1365.19 3.02 l.15E-01 8.44E-01 miss + Cs-137 661. 66 85.10 -2.08E-04 3.96E-02 3. 96E-02 miss + Eu-152 121.78 28.67 -5.62E-03 1.14E-01 1.20E-01 miss 244.70 7.61 -1.16E-01 3.45E-01 miss 295.94 0.45 1.45E+Ol 1.25E+Ol miss 344.28 26.60 6.90E-03 l.14E-01 miss 367.79 0.86 9.19E-01 3.31E+00 miss 411.12 2.24 4.14E-01 l.78E+OO miss 443.96 2.83 2.91E-01 l.18E+OO miss 488.68 0.42 2.26E+OO 7.46E+00 miss 563.99 0.49 -7.27E-01 7.04E+OO miss 586.26 0.46 -3.75E+00 8.29E+OO miss 678.62 0.47 2.90E+OO 7.98E+OO miss 688.67 0.86 -4.39E-01 4.61E+OO miss 719. 35 0.28 -5.37E-01 8.67E+OO miss 778.90 12. 96 -8.02E-02 l.97E-01 miss 810.45 0.32 -4.04E-01 9.93E+OO miss 867.37 4.26 6.97E-02 7.18E-01 miss 919.33 0.43 -4 .13E-01 5.75E+OO miss 964. 08 14.65 2.17E-01 4.19E-01 miss 1085.87 10.24 7.30E-02 3. llE-01 mis~ 1089.74 1. 73 5.15E-01 l.85E+OO miss 1112. 07 13.69 -3.24E-02 2.36E-01 miss 1212.95 1. 43 -l.59E-Ol 2.40E+OO miss 1249.94 0.1 9 -5.81E+00 1.85E+Ol miss 1299.14 1. 63 -l. l 7E-01 1.90E+OO miss 1408.01 21. 07 1. OlE-01 2.36E-01 miss 1457.64 0.50 -7.69E+OO 1.26E+Ol miss 1528.10 0.28 0.00E+OO 3.61E+OO miss Eu-154 123.07 40.40 -l.54E-03 8.34E-02 8.34E-02 miss 247.93 6.89 1. lOE-01 4.37E-01 miss 591.76 4.95 1. 31E-01 7.22E-01 miss 692.42 1. 78 1. 76E-01 l.85E+OO miss : 23.30 20.06 -2.66E-02

1. 47E-01 miss 756.80 4.52 2.46E-01 8.16E-01 miss 873.18 12.08 -l.09E-01 l.97E-01 miss 996.29 10.48 l.71E-01 4.24E-01 miss 1004.76 18.01 -8.93E-02 l.88E-01 miss 1274. 43 34.80 -2.90E-02

8. 78E-02 miss 1596.48 1. 80 2.71E-01 2.0lE+OO miss + Eu-155 45.30 1. 31 1.17E+Ol 2.16E-01 2.20E+Ol miss 60.0 1 1. 22 -1.09E+Ol 2.15E+Ol miss 86.55 30.'70 -8.17E-02 2.16E-01 miss 105.31 21.10 5.91E-02 2.24E-01 m i ss + Tl-208 583.19

• 85.00 l.66E-01 5.90E-02 5.90E-02 miss + Bi-211 351.07

• 13.02 l.23E+OO 2.98E-01 2.98E-01 miss + Pb-211 404.85 3.78 1. 25E-01 7.82E-01 7.82E-01 miss 6/7/2010 10:57:44AM Page 7 of8 Analysis Report for 07-Jun-16-10004 L310224AFQGS006SS (DRIED) QC Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

Corr Pb-211 427.09 1. 76 3.66E-01 7.82E-01 l.96E+OO miss 832.01 3.52 1. 95E-01 9.91E-01 miss + Bi-212 39.86 1. 06 1. 20E+OO 7.23E-01 2.33E+Ol miss 727. 33 6.67 4.54E-01 7.23E-Ol miss 785.37 1.1 0 l.42E+OO 4.35E+OO miss 1620.50 1. 47 7.13E-01 2.88E+OO miss + Pb-212 115 .18 0.60 9.07E-01 1. 30E-01 7.19E+OO miss 238.63 *J: 43.60 4.70E-01 1. 30E-01 miss 300.09 3.30 8.90E-01 1.21E+OO miss + Pb212-XR 74.32 10.28 2.21E-01 9.1:E-01 1.25E+00 miss 77.11

• 17.10 7.40E-01 9.17E-01 miss 87.35 3.97 8.43E-01 1.79E+OO miss 89. 78 1. 46 4.lOE-01 4.lOE+OO miss + Bi-214 609.32

• 45.49 3.47E-01 9.59E-02 9.59E-02 miss 768.36 4.89 3.77E-01 9.34E-01 miss 806.18 1. 26 6.19E-01 3.04E+00 miss 934.06 3.11 9.57E-01 1.84E+OO miss 1120.29

• 14.92 3.53E-01 2. OlE-01 miss 1155.21 1. 63 l.59E+OO 3.79E+OO miss 1238.12 5.83 4.94E-01 1. llE+OO miss 1280.98 1. 43 l.40E+OO 3.65E+OO miss 1377.67 3.99 5.36E-01 l.31E+OO miss 1385.31 0.79 7.91E-01 5.76E+OO miss 1401.52 1. 33 2.83E-01 3.18E+OO miss 1407.99 2.39 8.84E-01 2.08E+OO miss 1509.21 2.13 4.16E-01 1. 88E+OO miss 1661.27 1. 05 3.51E-01 4.12E+OO miss 1729.59 2.88 5.53E-01 1.88E+OO miss 1764.49

• 15.30 4.51E-01 2.72E-01 miss 1847.43 2.03 -9.33E-02 l.98E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241. 99 7.25 7.06E-01 1.09E-01 6.74E-01 miss 295.22

• 18.42 4.85E-01 2.35E-01 miss 351.93

• 35.60 4.50E-01 l.09E-01 miss 785.96 1. 06 3.12E+OO 4.79E+OO miss + Pb214-XR 74.82 5.80 3.91E-01 1.62E+OO 2.22E+OO miss 77 .11

• 9.70 1. 31E+OO 1.62E+OO miss 87.35 2.24 l.49E+OO 3.17E+OO miss 89.78 0.82 7.30E-01 7.30E+OO miss + Ra-226 186.21 3.64 2.97E-01 9.94E-01 9.94E-01 miss + Ac-228 129.07 2.42 9.15E-01 1. llE-01 1.74E+OO miss 209.25

• 3.89 9.70E-01 3.83E-Ol miss 270.24 3.46 6.38E-01 l.09E+00 miss 328.00 2.95 -4.32E-01 1.02E+OO miss 338.32 ;': 11. 27 5.55E-01 3.02E-01 miss 409.46 1. 92 1.17E+OO 2.31E+00 miss 463.00 4.40 2.54E-01 7.36E-01 miss 794.95 4.25 4.55E-01 1.14E+OO miss 911. 20

• 25.80 5.35E-01 1.llE-01 miss 964. 77 4.99 4.17E-01 1.17E+OO miss 968. 97

• 15.80 4.91E-01 3.37E-01 miss 6/7/2() ,o 10:57:44AM Page 8 of8 Analysis Report for 07-Jun-16-10004 L310224AFQGS006SS (DRIED) QC Nuclide Energy Yield{%) Activity Nuc/ideMDA LineMDA Caine Name (keV) (pCi/grams) (pCi!grams) (pCilgrams)

Corr Ac-228 1588.20 3.22 2.13E-01 l. llE-01 l.58E+00 miss + Pa-231 r: .36 10.30 -6.16E-01 l.39E+OO 2.60E+OO miss 283.69 1. 70 -8.14E-01 l.76E+OO miss 300.07 2.47 l.19E+OO l.61E+OO miss 302.65 2.20 -4.25E-02

1. 39E+OO miss 330.06 1. 40 1.1 5E+OO 2.73E+OO miss + Th-234 92.38 2 .13 2.35E+00 3.50E+OO 3.53E+OO miss 92.80 2.10 2.15E+OO 3.50E+OO miss 112. 81 0.21 3. 78E+OO 2.23E+Ol miss + U-235 143.76 10. 96 1. 02E-Ol 6.S";"E-02 3.40E-O l miss 163.33 5.08 3.54E-01 7.00E-01 miss 185.71 57.20 3.98E-02 6.57E-02 miss 202 .11 1. 08 -4.90E-01 2.67E+OO miss 205.31 5.01 8.87E-02 5.88E-01 miss + Am-241 59.54 35.90 -4.27E-01 7.44E-0 1 7.44E-01 miss + ;; Nuclide identified during the nuclide identification

• "' Energy line found in the spectrum > ;; MDA value not calculated

@ ;; Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value i s inconsistent with Currie MDA at 95% confidenc e level Coincidence correction performed. free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

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Printed: 6/18/2018 3:23 PMPage 1 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S ampleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnits17-03011-01LCSKNOWN03/03/17 00:003/3/20173/14/201717-0 3011Nickel-63ASTM 3500-Ni Modified1.51E+034.52E+01pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.52E+039.33E+009.01E+012.11E+00pCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.58E+001.27E+001.27E+002.11E+00UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified2.19E+001.39E+001.39E+002.29E+00UpCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.71E+001.37E+001.37E+002.28E+00UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified3.46E+001.39E+001.40E+002.25E+00pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified2.88E-011.36E+001.36E+002.31E+00UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified-1.69E+001.65E+001.65E+002.90E+00UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified6.89E-011.40E+001.40E+002.37E+00UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified8.22E-011.30E+001.30E+002.20E+00UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.06E+001.27E+001.27E+002.13E+00UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified3.84E+001.40E+001.42E+002.25E+00pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified2.34E+001.48E+001.49E+002.44E+00UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified1.97E+001.36E+001.37E+002.26E+00UpCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified1.09E+001.42E+001.42E+002.39E+00UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified9.12E-011.44E+001.44E+002.44E+00UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified1.02E+011.52E+001.64E+002.24E+00pCi/g17-03011-01LCSKNOWN03/03/17 00:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.43E+013.04E-01pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified6.16E+011.65E+002.15E+018.24E-01pCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified-2.14E-024.23E-014.23E-019.04E-01UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified7.78E-013.45E-014.39E-016.48E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.42E-013.48E-013.96E-016.83E-01UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified3.59E-013.59E-013.81E-017.29E-01UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified3.97E-013.66E-013.91E-017.40E-01UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.85E-014.17E-014.64E-018.27E-01UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified6.39E-023.97E-013.98E-018.41E-01UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified9.84E-013.37E-014.80E-016.09E-01pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified4.59E-013.45E-013.80E-016.86E-01UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified6.36E-013.86E-014.45E-017.54E-01UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified8.09E-014.19E-015.05E-018.12E-01UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified7.29E-013.98E-014.72E-017.75E-01UpCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified3.09E-013.90E-014.04E-018.00E-01UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified1.03E-013.61E-013.62E-017.59E-01UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.03E-013.78E-014.17E-017.53E-01UpCi/gZion, IL 60099Work Order Details:67149817-03011SOEN VIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i on Solutions101 Shiloh BlvdCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/18/2018 3:23 PMPage 2 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S ampleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i on Solutions101 Shiloh Blvd17-03011-01LCSKNOWN03/03/17 00:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified6.21E+012.48E+00pCi/g17-03011-01LCSKNOWN03/03/17 00:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified3.94E+011.58E+00pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified7.58E+015.03E+006.36E+006.59E-01pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified4.44E+014.02E+004.62E+006.97E-01pCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.74E-024.81E-024.82E-028.85E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified1.72E-022.56E-022.57E-024.39E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.29E-021.46E-021.46E-022.73E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-1.28E-041.27E-021.27E-021.91E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.40E-031.48E-021.48E-022.34E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified1.37E-011.68E-011.69E-013.28E-01UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Lead-212LANL ER-130 Modified6.28E-031.70E-021.70E-022.64E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Lead-214LANL ER-130 Modified-3.01E-032.42E-022.42E-023.65E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified-5.23E-034.16E-024.16E-026.34E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.11E-011.33E-011.34E-012.02E-01pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.84E-011.17E-011.19E-011.04E-01pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-2.54E-033.32E-023.32E-024.18E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified2.64E-041.18E-021.18E-024.72E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified5.75E-024.30E-024.31E-027.05E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified1.01E+011.11E+001.23E+004.65E-01pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified4.00E-015.25E-025.64E-028.50E-02pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.90E-011.31E-011.33E-019.32E-02pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.46E-016.92E-027.04E-025.39E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.23E-011.04E-011.06E-012.03E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.66E-011.11E-011.13E-018.49E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified4.50E-043.33E-023.33E-023.46E-02UpCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-5.96E-031.09E-021.09E-024.15E-02UpCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.04E-023.06E-023.08E-024.76E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified1.02E+011.13E+001.24E+005.53E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.75E-015.11E-025.46E-028.70E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified4.00E-011.33E-011.35E-011.11E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified1.86E-016.47E-026.54E-026.95E-02pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/18/2018 3:23 PMPage 3 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S ampleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i on Solutions101 Shiloh Blvd17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified3.95E-016.68E-026.98E-022.26E-01pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.88E-016.28E-026.59E-028.04E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.89E-022.04E-022.04E-022.86E-02UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-3.06E-031.04E-021.04E-022.78E-02UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified4.11E-016.15E-026.50E-023.88E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified6.85E+008.02E-018.76E-012.60E-01pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.45E-015.27E-025.56E-024.16E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.73E-016.08E-026.37E-027.27E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.93E-017.55E-027.82E-026.80E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified3.14E-011.00E-011.02E-011.05E-01pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.82E-017.07E-027.34E-027.96E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified2.05E-031.95E-021.95E-022.33E-02UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified4.00E-036.34E-036.34E-032.49E-02UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified2.25E-022.00E-022.01E-023.30E-02UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified8.06E+001.03E+001.11E+004.94E-01pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.61E-011.24E-011.26E-016.77E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.73E-011.30E-011.31E-016.84E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.87E-017.16E-027.31E-025.18E-02pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.85E-011.06E-011.07E-012.08E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.30E-019.29E-029.55E-021.27E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.61E-039.25E-039.25E-035.27E-02UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified8.33E-031.55E-021.55E-024.39E-02UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.93E-011.06E-011.12E-016.05E-02pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified4.65E+007.78E-018.14E-015.30E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Lead-212LANL ER-130 Modified5.59E-025.32E-025.33E-021.04E-01UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.45E-018.88E-029.05E-021.15E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.39E-018.59E-028.67E-021.47E-01pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/18/2018 3:23 PMPage 4 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S ampleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i on Solutions101 Shiloh Blvd17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.93E-011.05E-011.06E-012.39E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.41E-016.34E-026.57E-021.35E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-3.32E-024.28E-024.28E-025.98E-02UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified6.49E-032.04E-022.04E-024.57E-02UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified4.03E-017.19E-027.49E-028.51E-02pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified8.03E+001.20E+001.27E+006.92E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.68E-015.53E-025.84E-021.09E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified2.92E-016.40E-026.57E-021.03E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified4.27E-011.02E-011.04E-011.72E-01pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.67E-011.03E-011.03E-017.51E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.06E-016.14E-026.33E-026.49E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.29E-021.47E-021.47E-021.62E-02UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified1.85E-035.88E-035.88E-032.29E-02UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified5.77E-031.18E-021.18E-021.84E-02UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified4.97E+006.50E-016.98E-013.09E-01pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Lead-212LANL ER-130 Modified2.92E-019.35E-029.47E-025.97E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.26E-011.09E-011.11E-015.08E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.49E-016.26E-026.39E-026.96E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.56E-018.81E-029.11E-021.90E-01pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.52E-011.14E-011.16E-017.67E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-1.95E-032.38E-022.38E-022.96E-02UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-2.43E-031.04E-021.04E-023.39E-02UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified1.68E-021.97E-021.97E-023.18E-02UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified5.89E+007.05E-017.67E-014.46E-01pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Lead-212LANL ER-130 Modified5.13E-015.35E-025.96E-028.50E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Lead-214LANL ER-130 Modified4.53E-011.30E-011.32E-016.76E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.20E-016.85E-027.04E-023.88E-02pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/18/2018 3:23 PMPage 5 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S ampleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i on Solutions101 Shiloh Blvd17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified3.10E-011.38E-011.39E-012.87E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified2.90E-018.05E-028.19E-021.08E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-1.08E-024.50E-024.50E-025.74E-02UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified7.65E-031.58E-021.58E-024.69E-02UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified3.28E-016.71E-026.92E-028.42E-02pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified9.77E+001.40E+001.49E+006.37E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.17E-015.43E-025.66E-029.23E-02pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.38E-017.09E-027.30E-021.13E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.08E-011.13E-011.14E-011.65E-01pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.28E-018.53E-028.80E-021.50E-01pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.40E-017.01E-027.22E-029.44E-02pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.84E-022.40E-022.40E-023.33E-02UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-2.32E-022.89E-022.89E-023.14E-02UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified2.81E-022.43E-022.43E-023.95E-02UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified7.18E+008.97E-019.70E-015.24E-01pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Lead-212LANL ER-130 Modified5.13E-017.92E-028.35E-026.71E-02pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.46E-015.95E-026.21E-027.38E-02pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.96E-018.55E-028.78E-021.12E-01pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.89E-011.08E-011.09E-011.71E-01pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.18E-018.65E-028.91E-027.83E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified6.19E-032.06E-022.06E-022.63E-02UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified6.73E-031.17E-021.17E-022.91E-02UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.84E-022.08E-022.11E-023.89E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified7.14E+009.28E-019.97E-014.26E-01pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.24E-011.13E-011.15E-019.05E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.61E-011.29E-011.30E-015.38E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.52E-017.63E-027.74E-021.17E-01pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/18/2018 3:23 PMPage 6 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S ampleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i on Solutions101 Shiloh Blvd17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Actinium-228LANL ER-130 Modified2.73E-019.62E-029.72E-021.03E-01pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Bismuth-214LANL ER-130 Modified2.99E-016.02E-026.21E-026.14E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Cobalt-60LANL ER-130 Modified2.51E-021.55E-021.56E-022.24E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Cesium-134LANL ER-130 Modified-5.07E-039.42E-039.43E-032.76E-02UpCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Cesium-137LANL ER-130 Modified3.38E-014.02E-024.38E-023.33E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Potassium-40LANL ER-130 Modified6.77E+008.72E-019.39E-013.88E-01pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Lead-212LANL ER-130 Modified3.17E-011.10E-011.11E-016.70E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Lead-214LANL ER-130 Modified2.31E-018.83E-028.91E-025.75E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Thallium-208LANL ER-130 Modified3.12E-017.53E-027.70E-025.09E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Actinium-228LANL ER-130 Modified3.28E-015.75E-025.99E-021.19E-01pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Bismuth-214LANL ER-130 Modified2.77E-015.55E-025.72E-027.49E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Cobalt-60LANL ER-130 Modified2.22E-031.65E-021.65E-022.20E-02UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Cesium-134LANL ER-130 Modified2.87E-036.84E-036.84E-031.89E-02UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Cesium-137LANL ER-130 Modified2.03E-021.30E-021.30E-022.04E-02UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Potassium-40LANL ER-130 Modified6.22E+006.92E-017.62E-012.36E-01pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Lead-212LANL ER-130 Modified2.87E-014.16E-024.42E-024.20E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Lead-214LANL ER-130 Modified2.66E-014.22E-024.44E-024.27E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Thallium-208LANL ER-130 Modified2.87E-015.58E-025.77E-024.54E-02pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Actinium-228LANL ER-130 Modified3.84E-011.09E-011.11E-012.05E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Bismuth-214LANL ER-130 Modified2.85E-019.70E-029.81E-021.05E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Cobalt-60LANL ER-130 Modified8.55E-033.20E-023.20E-025.09E-02UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Cesium-134LANL ER-130 Modified1.76E-031.48E-021.48E-024.53E-02UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Cesium-137LANL ER-130 Modified3.37E-016.23E-026.46E-027.54E-02pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Potassium-40LANL ER-130 Modified6.05E+008.31E-018.87E-015.71E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Lead-212LANL ER-130 Modified4.33E-015.83E-026.23E-028.32E-02pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Lead-214LANL ER-130 Modified3.29E-011.49E-011.50E-011.23E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Thallium-208LANL ER-130 Modified2.56E-018.59E-028.69E-021.05E-01pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect