ML16231A028: Difference between revisions

From kanterella
Jump to navigation Jump to search
(Created page by program invented by StriderTol)
(Created page by program invented by StriderTol)
Line 16: Line 16:


=Text=
=Text=
{{#Wiki_filter:From: Silko, Thomas B. [mailto:tsilko@entergy.com] Sent: Thursday, August 11, 2016 11:26 AM To: Parrott, Jack <Jack.Parrott@nrc.gov>  
{{#Wiki_filter:From: Silko, Thomas B. [mailto:tsilko@entergy.com]
Sent: Thursday, August 11, 2016 11:26 AM To: Parrott, Jack <Jack.Parrott@nrc.gov>


==Subject:==
==Subject:==
  [External_Sender] Response to NRC Questions dated 7-28-16  Jack, Based upon our conversation on Wednesday 8/3/16, VY agreed to provide a copy of the Part 61 analysis which was used to identify the radionuclide concentrations on the Torus water. Accordingly, please find attached a copy of the Part 61 report from GEL Laboratories, dated April 26, 2016.
  [External_Sender] Response to NRC Questions dated 7 16  Jack, Based upon our conversation on Wednesday 8/3/16, VY agreed to provide a copy of the Part 61 analysis which was used to identify the radionuclide concentrations on the Torus water. Accordingly, please find attached a copy of the Part 61 report from GEL Laboratories, dated April 26, 2016.
In response to the Staffs second question, VY and the NRC discussed the process for sampling of material prior to making radioactive shipments. VY procedure V-EN-RW-102, Shipment of Radioactive Material, requires an isotopic be performed to ensure the material is appropriately classified per 10 CFR 61.55 requirements. The isotopic is performed on a sample of the material (in this case a water sample) prior to completing the shipment manifest. As such, VY is committed to sampling water prior to shipment to satisfy the requirements of 10CFR61.55.
 
In addition, Vermont Yankee commits to the following: Vermont Yankee will perform a representative sample prior to each shipment of water and will confirm that the radionuclide concentrations result in doses that are equal to or less than, the doses delineated within the Summary of Project Alternative Disposal Dose Results, in our June 28, 2016 letter (BVY 16-021; ADAMS Accession No. ML16182A035).
In response to the Staffs second question, VY and the NRC discussed the process for sampling of material prior to making radioactive shipments.
For example, the above could be satisfied in the following manner: A representative sample is taken prior to a shipment and the radionuclide concentrations are verified to be equal to or less than those concentrations shown on the Data Input Worksheet, of our June 28, 2016 letter. An alternative method to be used, such as when a radionuclide is identified as being slightly above the concentrations (while others may be lower), then sample radionuclide concentrations would be input into the Site Specific Dose Assessment Methodology (SSDA) used in our June 28, 2016 letter and the dose consequences verified to be equal to or less than that delineated within the Summary of Project Alternative Disposal Dose Results.
VY procedure V
Please let me know if there are any further questions. Thank You. Tom Silko (802) 451-3166     
-EN-RW-102, Shipment of Radioactive Material, requires an isotopic be performed to ensure the material is appropriately classified per 10 CFR 61.55 requirements.
The isotopic is performed on a sample of the material (in this case a water sample) prior to completing the shipment manifest.
As such, VY is committed to sampling water prior to shipment to satisfy the requirements of 10CFR61.55.
 
In addition, Vermont Yankee commits to the following:
Vermont Yankee will perform a representative sample prior to each shipment of water and will confirm that the radionuclide concentrations result in doses that are equal to or less than, the doses delineated within the Summary of Project Alternative Disposal Dose Results, in our June 28, 2016 letter (BVY 16
-021; ADAMS Accession No. ML16182A035).  
 
For example, the above could be satisfied in the following manner:
A representative sample is taken prior to a shipment and the radionuclide concentrations are verified to be equal to or less than those concentrations shown on the Data Input Worksheet, of our June 28, 2016 letter.
An alternative method to be used, such as when a radionuclide is identified as being slightly above the concentrations (while others may be lower), then sample radionuclide concentrations would be input into the Site Specific Dose Assessment Methodology (SSDA) used in our June 28, 2016 letter and the dose consequences verified to be equal to or less than that delineated within the Summary of Project Alternative Disposal Dose Results.
 
Please let me know if there are any further questions.
Thank You.
Tom Silko (802) 451
-3166     


April 26, 2016  
April 26, 2016  
Line 35: Line 51:
GEL Laboratories, LLC GEL appreciates the opportunity to provide the enclosed analytical results for the samples we received on April 21, 2016. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures.
GEL Laboratories, LLC GEL appreciates the opportunity to provide the enclosed analytical results for the samples we received on April 21, 2016. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at 843 556-8171, ext. 4504.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at 843 556-8171, ext. 4504.
Sincerely,PM_SIGN_HEREErin TrentProject ManagerPurchase Order: 10287833 Enclosures Table of ContentsCase Narrative......................................................................................1Chain of Custody..................................................................................3 Laboratory Certifications......................................................................7 Radiological Analysis...........................................................................9Case Narrative............................................................................10 Sample Data Summary...............................................................33 Quality Control Summary..........................................................37 Case NarrativePage 1 of 49 Case Narrative for Vermont Yankee, Entergy Nuclear Operations Inc. SDG: 395827 April 26, 2016 Laboratory Identification:  
Sincerely, PM_SIGN_HERE Erin Trent Project Manager Purchase Order: 10287833 Enclosures Table of Contents Case Narrative......................................................................................1 Chain of Custody..................................................................................3
 
Laboratory Certifications......................................................................7
 
Radiological Analysis...........................................................................9 Case Narrative............................................................................10
 
Sample Data Summary...............................................................33
 
Quality Control Summary..........................................................37 Case Narrative Page 1 of 49 Case Narrative for Vermont Yankee, Entergy Nuclear Operations Inc.
SDG: 395827 April 26, 2016 Laboratory Identification:  
 
GEL Laboratories LLC
 
2040 Savage Road
 
Charleston, South Carolina 29407
 
843 556-8171 Summary Sample Receipt The sample arrived at GEL Laboratories LLC, Charleston, South Carolina on April 21, 2016 for analysis. Chain of Custody form did not contain a relinquished signature. All sample containers arrived without
 
any visible signs of tampering or breakage. There are no additional comments concerning sample receipt.
Sample Identification The laboratory received the following sample:
Laboratory IDClient ID395827001 Torus Water #2 Case Narrative Sample analyses were conducted using methodology as outlined in GEL Laboratories, LLC GEL Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and
 
reduction are contained in the analytical case narratives in the enclosed data package.
Data Package The enclosed data package contains the following sections: General Narrative, Chain of Custody and Supporting Documentation, and data from the following fractions: Radiochemistry.
 
PM_SIGN_HERE Erin Trent
 
Project Manager Page 2 of 49 Chain of Custody Page 3 of 49 Page 4 of 49 Page 5 of 49 Page 6 of 49 Laboratory Certifications Page 7 of 49 StateCertification AlaskaArkansasCLIACalifornia ColoradoConnecticut DelawareDoD ELAP/ ISO17025 A2LA Florida NELAP Foreign Soils Permit GeorgiaGeorgia SDWA HawaiiIdaho Chemistry Idaho Radiochemistry Illinois NELAP IndianaKansas NELAP Kentucky SDWA Kentucky Wastewater Louisiana NELAP Louisiana SDWA MarylandMassachusetts MichiganMississippi NebraskaNevadaNew Hampshire NELAP New Jersey NELAP New Mexico New York NELAP North Carolina North Carolina SDWA North Dakota OklahomaPennsylvania NELAP S.Carolina Radchem South Carolina Chemistry Tennessee Texas NELAP Utah NELAP VermontVirginia NELAP Washington West Virginia UST-011088-065142D0904046 2940 SC00012PH-0169SC000122567.01E87156P330-15-00283, P330-15-00253 SC00012967SC00012SC00012SC00012200029C-SC-01E-10332901299012903046 (AI33904)
LA160006270M-SC0129976SC00012NE-OS-26-13 SC000122016-1 205415SC002SC000121150123345709R-158990468-004851012000210120001TN 02934T104704235-16-11 SC000122016-20 VT87156460202C780997404List of current GEL Certifications as of 26 April 2016 Page 8 of 49 Radiological Analysis Page 9 of 49 Case Narrative Page 10 of 49 Radiochemistry Technical Case Narrative Vermont Yankee, Entergy Nuclear Operations Inc. NTRG SDG #: 395827
 
Method/Analysis Information Product:
Alphaspec Pu242, Liquid Analytical Method:
DOE EML HASL-300, Pu-11-RC Modified Analytical Batch Number:
1562629Sample ID Client ID 395827001 Torus Water #2 1203535939 Method Blank MB 1203535941 Laboratory Control Sample LCS 1203535940 395827001Torus Water #2 Sample Duplicate DUP
 
The samples in this SDG were analyzed on an "as received" basis.
 
SOP Reference
 
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
 
Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with
 
GL-RAD-A-011 REV# 26.
Calibration Information:
 
Calibration Information
 
All initial and continuing calibration requirements have been met.
 
Standards Information
 
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
 
before the expiration dates.
 
Sample Geometry
 
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control QC Information:
 
Blank Information
 
The blank volume is representative of the sample volume in this batch.
 
QC Information
 
All of the QC samples met the required acceptance limits.
 
Designated QC
 
The following sample was used for QC: 395827001 Torus Water #2.
Page 11 of 49 Technical Information:
Holding Time
 
All sample procedures for this sample set were performed within the required holding time.
 
Sample Re-prep/Re-analysis
 
None of the samples in this sample set required reprep or reanalysis.
 
Recounts Sample 395827001 Torus Water #2 was recounted due to a suspected false positive. The recount is reported.
Miscellaneous Information:
 
Data Exception DER Documentation
 
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
 
SOP or contractual documents. A data exception report DER was not generated for this SDG.
 
Manual Integration
 
No manual integrations were performed on data in this batch.
 
Sample-Specific MDA/MDC


GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 843 556-8171 Summary Sample Receipt The sample arrived at GEL Laboratories LLC, Charleston, South Carolina on April 21, 2016 foranalysis. Chain of Custody form did not contain a relinquished signature. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification The laboratory received the following sample: Laboratory IDClient ID395827001Torus Water #2Case Narrative  Sample analyses were conducted using methodology as outlined in GEL Laboratories, LLC GELStandard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. Data Package  The enclosed data package contains the following sections: General Narrative, Chain of Custody andSupporting Documentation, and data from the following fractions: Radiochemistry.  
The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.  


PM_SIGN_HEREErin Trent Project ManagerPage 2 of 49 Chain of CustodyPage 3 of 49 Page 4 of 49 Page 5 of 49 Page 6 of 49 LaboratoryCertificationsPage 7 of 49 StateCertificationAlaskaArkansasCLIACalifornia ColoradoConnecticutDelawareDoD ELAP/ ISO17025 A2LAFlorida NELAPForeign Soils PermitGeorgiaGeorgia SDWAHawaiiIdaho ChemistryIdaho RadiochemistryIllinois NELAPIndianaKansas NELAPKentucky SDWAKentucky WastewaterLouisiana NELAPLouisiana SDWAMarylandMassachusettsMichiganMississippiNebraskaNevadaNew Hampshire NELAPNew Jersey NELAPNew MexicoNew York NELAPNorth CarolinaNorth Carolina SDWANorth DakotaOklahomaPennsylvania NELAPS.Carolina RadchemSouth Carolina ChemistryTennesseeTexas NELAPUtah NELAPVermontVirginia NELAPWashingtonWest VirginiaUST-011088-065142D09040462940 SC00012PH-0169SC000122567.01E87156P330-15-00283, P330-15-00253SC00012967SC00012SC00012SC00012200029C-SC-01E-10332901299012903046 (AI33904)LA160006270M-SC0129976SC00012NE-OS-26-13SC000122016-1205415SC002SC000121150123345709R-158990468-004851012000210120001TN 02934T104704235-16-11SC000122016-20VT87156460202C780997404List of current GEL Certifications as of 26 April 2016Page 8 of 49 Radiological AnalysisPage 9 of 49 Case NarrativePage 10 of 49 Radiochemistry Technical Case Narrative Vermont Yankee, Entergy Nuclear Operations Inc. NTRG SDG #: 395827 Method/Analysis Information Product: Alphaspec Pu242, LiquidAnalytical Method: DOE EML HASL-300, Pu-11-RC ModifiedAnalytical Batch Number: 1562629Sample IDClient ID395827001 Torus Water #21203535939Method Blank MB1203535941Laboratory Control Sample LCS1203535940395827001Torus Water #2 Sample Duplicate DUP The samples in this SDG were analyzed on an "as received" basis.
Additional Comments


SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-011 REV# 26. Calibration Information:
Additional comments were not required for this sample set.
Calibration Information All initial and continuing calibration requirements have been met.
Qualifier Information


Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.  
Manual qualifiers were not required.  


Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control QC Information:
Method/Analysis Information Product:
Blank Information The blank volume is representative of the sample volume in this batch.
Alphaspec Am241, Cm, Liquid Analytical Method:
DOE EML HASL-300, Am-05-RC Modified Analytical Batch Number:
1562630Sample ID Client ID 395827001 Torus Water #2 1203535946 Method Blank MB 1203535948 Laboratory Control Sample LCS 1203535947 395827001Torus Water #2 Sample Duplicate DUP


QC Information All of the QC samples met the required acceptance limits.  
The samples in this SDG were analyzed on an "as received" basis.  


Designated QC The following sample was used for QC: 395827001 Torus Water #2. Page 11 of 49 Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time.
SOP Reference


Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as


Recounts Sample 395827001 Torus Water #2 was recounted due to a suspected false positive. The recount is reported. Miscellaneous Information:
Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with Page 12 of 49 GL-RAD-A-011 REV# 26.
Data Exception DER Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report DER was not generated for this SDG.
Calibration Information:
Calibration Information


Manual Integration No manual integrations were performed on data in this batch.  
All initial and continuing calibration requirements have been met.  


Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.
Standards Information


Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required.
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used


Method/Analysis Information Product: Alphaspec Am241, Cm, LiquidAnalytical Method: DOE EML HASL-300, Am-05-RC ModifiedAnalytical Batch Number: 1562630Sample IDClient ID395827001 Torus Water #21203535946Method Blank MB1203535948Laboratory Control Sample LCS1203535947395827001Torus Water #2 Sample Duplicate DUP The samples in this SDG were analyzed on an "as received" basis.  
before the expiration dates.  


SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance withPage 12 of 49 GL-RAD-A-011 REV# 26. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met.
Sample Geometry


Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.  
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control QC Information:


Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control QC Information:
Blank Information
Blank Information The blank volume is representative of the sample volume in this batch.


QC Information All of the QC samples met the required acceptance limits.  
The blank volume is representative of the sample volume in this batch.  


Designated QC The following sample was used for QC: 395827001 Torus Water #2. Technical Information:
QC Information
Holding Time All sample procedures for this sample set were performed within the required holding time.


Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.  
All of the QC samples met the required acceptance limits.  


Recounts None of the samples in this sample set were recounted. Miscellaneous Information:
Designated QC
Data Exception DER Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report DER was not generated for this SDG.


Manual Integration No manual integrations were performed on data in this batch.  
The following sample was used for QC: 395827001 Torus Water #2.
Technical Information:


Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.
Holding Time


Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required.
All sample procedures for this sample set were performed within the required holding time.  
Page 13 of 49 Method/Analysis Information Product: Alphaspec Np, LiquidAnalytical Method: ASTM C 1476-00 ModifiedAnalytical Batch Number: 1562631Sample IDClient ID395827001 Torus Water #21203535949Method Blank MB1203535951Laboratory Control Sample LCS1203535950395827001Torus Water #2 Sample Duplicate DUP The samples in this SDG were analyzed on an "as received" basis.  


SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-032 REV# 20. Calibration Information:
Sample Re-prep/Re-analysis
Calibration Information All initial and continuing calibration requirements have been met.


Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.  
None of the samples in this sample set required reprep or reanalysis.  


Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control QC Information:
Recounts None of the samples in this sample set were recounted.
Blank Information The blank volume is representative of the sample volume in this batch.  
Miscellaneous Information:


QC Information All of the QC samples met the required acceptance limits.
Data Exception DER Documentation


Designated QC The following sample was used for QC: 395827001 Torus Water #2. Technical Information:
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
Holding Time All sample procedures for this sample set were performed within the required holding time.


Sample Re-prep/Re-analysis Page 14 of 49 None of the samples in this sample set required reprep or reanalysis.
SOP or contractual documents. A data exception report DER was not generated for this SDG.  
Recounts None of the samples in this sample set were recounted. Miscellaneous Information:
Data Exception DER Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report DER was not generated for this SDG.  


Manual Integration No manual integrations were performed on data in this batch.
Manual Integration


Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.  
No manual integrations were performed on data in this batch.  


Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required.
Sample-Specific MDA/MDC


Method/Analysis Information Product: Gammaspec, Gamma, Liquid Standard ListAnalytical Method: EPA 901.1Analytical Batch Number: 1561698Sample IDClient ID395827001 Torus Water #21203533384Method Blank MB1203533386Laboratory Control Sample LCS1203533385395827001Torus Water #2 Sample Duplicate DUP The samples in this SDG were analyzed on an "as received" basis.  
The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.  


SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-013 REV# 25. Calibration Information:
Additional Comments
Calibration Information All initial and continuing calibration requirements have been met. Page 15 of 49 Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.


Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control QC Information:
Additional comments were not required for this sample set.
Blank Information The blank volume is representative of the sample volume in this batch.
Qualifier Information


QC Information All of the QC samples meet the required acceptance limits with the following exceptions: Refer to Data Exception Report DER.  
Manual qualifiers were not required.  


Designated QC The following sample was used for QC: 395827001 Torus Water #2. Technical Information:
Page 13 of 49 Method/Analysis Information Product:
Holding Time All sample procedures for this sample set were performed within the required holding time.
Alphaspec Np, Liquid Analytical Method:
ASTM C 1476-00 Modified Analytical Batch Number:
1562631Sample ID Client ID 395827001 Torus Water #2 1203535949 Method Blank MB 1203535951 Laboratory Control Sample LCS 1203535950 395827001Torus Water #2 Sample Duplicate DUP


Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.  
The samples in this SDG were analyzed on an "as received" basis.  


Recounts None of the samples in this sample set were recounted. Miscellaneous Information:
SOP Reference
Data Exception DER Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. The following DER was generated for this SDG: DER 1513408 was generated due to RDL less than MDA. The following RDLs in sample 395827001 were not achieved: Cs-134, Fe-59, Nb-95 and Zr-95. The following RDLs in DUP 1203533385 were not achieved: Cs-134, Fe-59, Nb-95 and Zr-95. Samples did not meet the required detection limit due to high sample activity. Reporting results.


Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as


Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required.
Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with


Method/Analysis Information Page 16 of 49 Product: Gamma I129, LiquidAnalytical Method: DOE EML HASL-300,I-01 ModifiedAnalytical Batch Number: 1562602Sample IDClient ID395827001 Torus Water #21203535843Method Blank MB1203535846Laboratory Control Sample LCS1203535844395827001Torus Water #2 Sample Duplicate DUP1203535845395827001Torus Water #2 Matrix Spike MSThe samples in this SDG were analyzed on an "as received" basis.  
GL-RAD-A-032 REV# 20.
Calibration Information:


SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-006 REV# 21. Calibration Information:
Calibration Information
Calibration Information All initial and continuing calibration requirements have been met.


Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.  
All initial and continuing calibration requirements have been met.  


Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control QC Information:
Standards Information
Blank Information The blank volume is representative of the sample volume in this batch.


QC Information All of the QC samples met the required acceptance limits.
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used


Designated QC The following sample was used for QC: 395827001 Torus Water #2. Technical Information:
before the expiration dates.  
Holding Time All sample procedures for this sample set were performed within the required holding time.  


Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
Sample Geometry


Recounts None of the samples in this sample set were recounted. Page 17 of 49 Miscellaneous Information: Data Exception DER Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report DER was not generated for this SDG.
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control QC Information:


Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.
Blank Information


Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required.  
The blank volume is representative of the sample volume in this batch.  


Method/Analysis Information Product: Gamma Ni59, LiquidAnalytical Method: DOE RESL Ni-1Analytical Batch Number: 1562693Sample IDClient ID395827001 Torus Water #21203536149Method Blank MB1203536151Laboratory Control Sample LCS1203536150395827001Torus Water #2 Sample Duplicate DUP The samples in this SDG were analyzed on an "as received" basis.
QC Information


SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 17. Calibration Information:
All of the QC samples met the required acceptance limits.  
Calibration Information All initial and continuing calibration requirements have been met.  


Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.
Designated QC


Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Page 18 of 49 Quality Control QC Information: Blank Information The blank volume is representative of the sample volume in this batch.
The following sample was used for QC: 395827001 Torus Water #2.
Technical Information:


QC Information All of the QC samples met the required acceptance limits.
Holding Time


Designated QC The following sample was used for QC: 395827001 Torus Water #2. Technical Information:
All sample procedures for this sample set were performed within the required holding time.  
Holding Time All sample procedures for this sample set were performed within the required holding time.  


Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.  
Sample Re-prep/Re-analysis Page 14 of 49 None of the samples in this sample set required reprep or reanalysis.  


Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.  
Recounts None of the samples in this sample set were recounted.
Miscellaneous Information:


Recounts None of the samples in this sample set were recounted. Miscellaneous Information:
Data Exception DER Documentation
Data Exception DER Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report DER was not generated for this SDG.


Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.
Data exception reports are generated to document any procedural anomalies that may deviate from referenced


Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required.  
SOP or contractual documents. A data exception report DER was not generated for this SDG.  


Method/Analysis Information Product: GFPC, Sr89&Sr90, LiquidAnalytical Method: EPA 905.0 Modified/DOE RP501 Rev. 1 ModifiedAnalytical Batch Number: 1562716Sample IDClient IDPage 19 of 49 395827001 Torus Water #21203536197Method Blank MB1203536199Laboratory Control Sample LCS1203536198395827001Torus Water #2 Sample Duplicate DUPThe samples in this SDG were analyzed on an "as received" basis.
Manual Integration


SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 17. Calibration Information:
No manual integrations were performed on data in this batch.  
Calibration Information All initial and continuing calibration requirements have been met.  


Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.
Sample-Specific MDA/MDC


Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control QC Information:
The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.  
Blank Information The blank volume is representative of the sample volume in this batch.  


QC Information All of the QC samples met the required acceptance limits.
Additional Comments


Designated QC The following sample was used for QC: 395827001 Torus Water #2. Technical Information:
Additional comments were not required for this sample set.
Holding Time All sample procedures for this sample set were performed within the required holding time.  
Qualifier Information


Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.  
Manual qualifiers were not required.  


Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.  
Method/Analysis Information Product:
Gammaspec, Gamma, Liquid Standard List Analytical Method:
EPA 901.1 Analytical Batch Number:
1561698Sample ID Client ID 395827001 Torus Water #2 1203533384 Method Blank MB 1203533386 Laboratory Control Sample LCS 1203533385 395827001Torus Water #2 Sample Duplicate DUP


Recounts Sample 1203536198 Torus Water #2DUP was recounted due to a suspected total strontium false positive. The recount is reported. Miscellaneous Information:
The samples in this SDG were analyzed on an "as received" basis.  
Data Exception DER Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report DER was not generated for this SDG. Page 20 of 49


Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.
SOP Reference


Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required.
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as


Method/Analysis Information Product: Liquid Scint Pu241, LiquidAnalytical Method: DOE EML HASL-300, Pu-11-RC ModifiedAnalytical Batch Number: 1562632Sample IDClient ID395827001 Torus Water #21203535952Method Blank MB1203535954Laboratory Control Sample LCS1203535953395827001Torus Water #2 Sample Duplicate DUP The samples in this SDG were analyzed on an "as received" basis.
Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with


SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-035 REV# 16. Calibration Information:
GL-RAD-A-013 REV# 25.
Calibration Information All initial and continuing calibration requirements have been met.
Calibration Information:


Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.  
Calibration Information
 
All initial and continuing calibration requirements have been met.
Page 15 of 49 Standards Information
 
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
 
before the expiration dates.
 
Sample Geometry
 
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control QC Information:
 
Blank Information
 
The blank volume is representative of the sample volume in this batch.
 
QC Information
 
All of the QC samples meet the required acceptance limits with the following exceptions: Refer to Data
 
Exception Report DER.
 
Designated QC
 
The following sample was used for QC: 395827001 Torus Water #2.
Technical Information:
 
Holding Time
 
All sample procedures for this sample set were performed within the required holding time.
 
Sample Re-prep/Re-analysis
 
None of the samples in this sample set required reprep or reanalysis.
 
Recounts None of the samples in this sample set were recounted.
Miscellaneous Information:
 
Data Exception DER Documentation
 
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
 
SOP or contractual documents. The following DER was generated for this SDG: DER 1513408 was generated
 
due to RDL less than MDA. The following RDLs in sample 395827001 were not achieved: Cs-134, Fe-59,
 
Nb-95 and Zr-95. The following RDLs in DUP 1203533385 were not achieved: Cs-134, Fe-59, Nb-95 and
 
Zr-95. Samples did not meet the required detection limit due to high sample activity. Reporting results.
 
Sample-Specific MDA/MDC
 
The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.
 
Additional Comments
 
Additional comments were not required for this sample set.
Qualifier Information
 
Manual qualifiers were not required.
 
Method/Analysis Information Page 16 of 49 Product:
Gamma I129, Liquid Analytical Method:
DOE EML HASL-300,I-01 Modified Analytical Batch Number:
1562602Sample ID Client ID 395827001 Torus Water #2 1203535843 Method Blank MB 1203535846 Laboratory Control Sample LCS 1203535844 395827001Torus Water #2 Sample Duplicate DUP 1203535845 395827001Torus Water #2 Matrix Spike MS The samples in this SDG were analyzed on an "as received" basis.
 
SOP Reference
 
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
 
Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with
 
GL-RAD-A-006 REV# 21.
Calibration Information:
 
Calibration Information
 
All initial and continuing calibration requirements have been met.
 
Standards Information
 
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
 
before the expiration dates.
 
Sample Geometry
 
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control QC Information:
 
Blank Information
 
The blank volume is representative of the sample volume in this batch.
 
QC Information
 
All of the QC samples met the required acceptance limits.
 
Designated QC
 
The following sample was used for QC: 395827001 Torus Water #2.
Technical Information:
 
Holding Time
 
All sample procedures for this sample set were performed within the required holding time.
 
Sample Re-prep/Re-analysis
 
None of the samples in this sample set required reprep or reanalysis.
 
Recounts None of the samples in this sample set were recounted.
Page 17 of 49 Miscellaneous Information:
Data Exception DER Documentation
 
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
 
SOP or contractual documents. A data exception report DER was not generated for this SDG.
 
Sample-Specific MDA/MDC
 
The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.
 
Additional Comments
 
Additional comments were not required for this sample set.
Qualifier Information
 
Manual qualifiers were not required.
 
Method/Analysis Information Product:
Gamma Ni59, Liquid Analytical Method:
DOE RESL Ni-1 Analytical Batch Number:
1562693Sample ID Client ID 395827001 Torus Water #2 1203536149 Method Blank MB 1203536151 Laboratory Control Sample LCS 1203536150 395827001Torus Water #2 Sample Duplicate DUP
 
The samples in this SDG were analyzed on an "as received" basis.
 
SOP Reference
 
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
 
Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with
 
GL-RAD-A-022 REV# 17.
Calibration Information:
 
Calibration Information
 
All initial and continuing calibration requirements have been met.
 
Standards Information
 
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
 
before the expiration dates.
 
Sample Geometry
 
All counting sources were prepared in the same geometry as the calibration standards.
Page 18 of 49 Quality Control QC Information:
Blank Information
 
The blank volume is representative of the sample volume in this batch.
 
QC Information
 
All of the QC samples met the required acceptance limits.
 
Designated QC
 
The following sample was used for QC: 395827001 Torus Water #2.
Technical Information:
 
Holding Time
 
All sample procedures for this sample set were performed within the required holding time.
 
Sample Re-prep/Re-analysis
 
None of the samples in this sample set required reprep or reanalysis.
 
Chemical Recoveries
 
All chemical recoveries meet the required acceptance limits for this sample set.
 
Recounts None of the samples in this sample set were recounted.
Miscellaneous Information:
 
Data Exception DER Documentation
 
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
 
SOP or contractual documents. A data exception report DER was not generated for this SDG.
 
Sample-Specific MDA/MDC
 
The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.
 
Additional Comments
 
Additional comments were not required for this sample set.
Qualifier Information
 
Manual qualifiers were not required.
 
Method/Analysis Information Product:
GFPC, Sr89&Sr90, Liquid Analytical Method:
EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Analytical Batch Number:
1562716Sample ID Client ID Page 19 of 49 395827001 Torus Water #2 1203536197 Method Blank MB 1203536199 Laboratory Control Sample LCS 1203536198 395827001Torus Water #2 Sample Duplicate DUP The samples in this SDG were analyzed on an "as received" basis.
 
SOP Reference
 
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
 
Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with
 
GL-RAD-A-004 REV# 17.
Calibration Information:
 
Calibration Information
 
All initial and continuing calibration requirements have been met.
 
Standards Information
 
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
 
before the expiration dates.
 
Sample Geometry
 
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control QC Information:
 
Blank Information
 
The blank volume is representative of the sample volume in this batch.
 
QC Information
 
All of the QC samples met the required acceptance limits.
 
Designated QC
 
The following sample was used for QC: 395827001 Torus Water #2.
Technical Information:
 
Holding Time
 
All sample procedures for this sample set were performed within the required holding time.
 
Sample Re-prep/Re-analysis
 
None of the samples in this sample set required reprep or reanalysis.
 
Chemical Recoveries
 
All chemical recoveries meet the required acceptance limits for this sample set.
 
Recounts Sample 1203536198 Torus Water #2DUP was recounted due to a suspected total strontium false positive. The
 
recount is reported.
Miscellaneous Information:
 
Data Exception DER Documentation
 
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
 
SOP or contractual documents. A data exception report DER was not generated for this SDG.
Page 20 of 49
 
Sample-Specific MDA/MDC
 
The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.
 
Additional Comments
 
Additional comments were not required for this sample set.
Qualifier Information
 
Manual qualifiers were not required.
 
Method/Analysis Information Product:
Liquid Scint Pu241, Liquid Analytical Method:
DOE EML HASL-300, Pu-11-RC Modified Analytical Batch Number:
1562632Sample ID Client ID 395827001 Torus Water #2 1203535952 Method Blank MB 1203535954 Laboratory Control Sample LCS 1203535953 395827001Torus Water #2 Sample Duplicate DUP
 
The samples in this SDG were analyzed on an "as received" basis.
 
SOP Reference
 
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
 
Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with
 
GL-RAD-A-035 REV# 16.
Calibration Information:
 
Calibration Information
 
All initial and continuing calibration requirements have been met.
 
Standards Information
 
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
 
before the expiration dates.
 
Sample Geometry
 
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control QC Information:
 
Blank Information
 
The blank volume is representative of the sample volume in this batch.  


Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control QC Information:
Blank Information The blank volume is representative of the sample volume in this batch.
Page 21 of 49 QC Information All of the QC samples met the required acceptance limits.  
Page 21 of 49 QC Information All of the QC samples met the required acceptance limits.  


Designated QC The following sample was used for QC: 395827001 Torus Water #2. Technical Information:
Designated QC
Holding Time All sample procedures for this sample set were performed within the required holding time.  
 
The following sample was used for QC: 395827001 Torus Water #2.
Technical Information:
 
Holding Time
 
All sample procedures for this sample set were performed within the required holding time.
 
Sample Re-prep/Re-analysis
 
None of the samples in this sample set required reprep or reanalysis.
 
Recounts Samples 1203535952 MB, 1203535953 Torus Water #2DUP and 395827001 Torus Water #2 were
 
recounted due to high MDCs. The recounts are reported.
Miscellaneous Information:
 
Data Exception DER Documentation
 
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
 
SOP or contractual documents. A data exception report DER was not generated for this SDG.
 
Manual Integration
 
No manual integrations were performed on data in this batch.
 
Sample-Specific MDA/MDC
 
The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.
 
Additional Comments
 
Additional comments were not required for this sample set.
Qualifier Information
 
Manual qualifiers were not required.
 
Method/Analysis Information Product:
Liquid Scint Fe55, Liquid Analytical Method:
DOE RESL Fe-1, Modified Analytical Batch Number:
1562672Sample ID Client ID 395827001 Torus Water #2 1203536076 Method Blank MB 1203536078 Laboratory Control Sample LCS 1203536077 395827001Torus Water #2 Sample Duplicate DUP Page 22 of 49 The samples in this SDG were analyzed on an "as received" basis.
 
SOP Reference
 
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
 
Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with
 
GL-RAD-A-040 REV# 12.
Calibration Information:
 
Calibration Information
 
All initial and continuing calibration requirements have been met.
 
Standards Information
 
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
 
before the expiration dates.
 
Sample Geometry
 
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control QC Information:
 
Blank Information
 
The blank volume is representative of the sample volume in this batch.
 
QC Information
 
All of the QC samples met the required acceptance limits.  


Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
Designated QC


Recounts Samples 1203535952 MB, 1203535953 Torus Water #2DUP and 395827001 Torus Water #2 were recounted due to high MDCs. The recounts are reported. Miscellaneous Information:
The following sample was used for QC: 395827001 Torus Water #2.
Data Exception DER Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report DER was not generated for this SDG.
Technical Information:


Manual Integration No manual integrations were performed on data in this batch.
Holding Time


Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.  
All sample procedures for this sample set were performed within the required holding time.  


Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required.
Sample Re-prep/Re-analysis


Method/Analysis Information Product: Liquid Scint Fe55, LiquidAnalytical Method: DOE RESL Fe-1, ModifiedAnalytical Batch Number: 1562672Sample IDClient ID395827001 Torus Water #21203536076Method Blank MB1203536078Laboratory Control Sample LCS1203536077395827001Torus Water #2 Sample Duplicate DUPPage 22 of 49 The samples in this SDG were analyzed on an "as received" basis.  
None of the samples in this sample set required reprep or reanalysis.  


SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-040 REV# 12. Calibration Information:
Recounts None of the samples in this sample set were recounted.
Calibration Information All initial and continuing calibration requirements have been met.
Miscellaneous Information:


Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.
Data Exception DER Documentation


Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control QC Information:
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
Blank Information The blank volume is representative of the sample volume in this batch.


QC Information All of the QC samples met the required acceptance limits.  
SOP or contractual documents. A data exception report DER was not generated for this SDG.  


Designated QC The following sample was used for QC: 395827001 Torus Water #2. Technical Information:
Sample-Specific MDA/MDC
Holding Time All sample procedures for this sample set were performed within the required holding time.


Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.  
The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.  


Recounts None of the samples in this sample set were recounted. Miscellaneous Information:
Additional Comments
Data Exception DER Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report DER was not generated for this SDG.


Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.  
Additional comments were not required for this sample set.
Page 23 of 49 Qualifier Information Manual qualifiers were not required.  


Additional Comments Additional comments were not required for this sample set. Page 23 of 49 Qualifier Information Manual qualifiers were not required.
Method/Analysis Information Product:
Liquid Scint Ni63, Liquid Analytical Method:
DOE RESL Ni-1, Modified Analytical Batch Number:
1562678Sample ID Client ID 395827001 Torus Water #2 1203536092 Method Blank MB 1203536094 Laboratory Control Sample LCS 1203536093 395827001Torus Water #2 Sample Duplicate DUP


Method/Analysis Information Product: Liquid Scint Ni63, LiquidAnalytical Method: DOE RESL Ni-1, ModifiedAnalytical Batch Number: 1562678Sample IDClient ID395827001 Torus Water #21203536092Method Blank MB1203536094Laboratory Control Sample LCS1203536093395827001Torus Water #2 Sample Duplicate DUP The samples in this SDG were analyzed on an "as received" basis.  
The samples in this SDG were analyzed on an "as received" basis.  


SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 17. Calibration Information:
SOP Reference
Calibration Information All initial and continuing calibration requirements have been met.


Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as


Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control QC Information:
Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with
Blank Information The blank volume is representative of the sample volume in this batch.


QC Information All of the QC samples met the required acceptance limits.
GL-RAD-A-022 REV# 17.
Calibration Information:


Designated QC The following sample was used for QC: 395827001 Torus Water #2. Page 24 of 49 Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time.
Calibration Information


Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.  
All initial and continuing calibration requirements have been met.  


Recounts None of the samples in this sample set were recounted. Miscellaneous Information:
Standards Information
Data Exception DER Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report DER was not generated for this SDG.


Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used


Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required.  
before the expiration dates.  


Method/Analysis Information Product: Liquid Scint Tc99, LiquidAnalytical Method: DOE EML HASL-300, Tc-02-RC ModifiedAnalytical Batch Number: 1562683Sample IDClient ID395827001 Torus Water #21203536111Method Blank MB1203536113Laboratory Control Sample LCS1203536112395827001Torus Water #2 Sample Duplicate DUP The samples in this SDG were analyzed on an "as received" basis.
Sample Geometry


SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-059 REV# 4. Page 25 of 49 Calibration Information: Calibration Information All initial and continuing calibration requirements have been met.
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control QC Information:


Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.
Blank Information


Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control QC Information:
The blank volume is representative of the sample volume in this batch.  
Blank Information The blank volume is representative of the sample volume in this batch.  


QC Information All of the QC samples meet the required acceptance limits with the following exceptions: Refer to Data Exception Report DER.
QC Information


Designated QC The following sample was used for QC: 395827001 Torus Water #2. Technical Information:
All of the QC samples met the required acceptance limits.  
Holding Time All sample procedures for this sample set were performed within the required holding time.  


Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.  
Designated QC
 
The following sample was used for QC: 395827001 Torus Water #2.
Page 24 of 49 Technical Information:
Holding Time
 
All sample procedures for this sample set were performed within the required holding time.
 
Sample Re-prep/Re-analysis
 
None of the samples in this sample set required reprep or reanalysis.
 
Recounts None of the samples in this sample set were recounted.
Miscellaneous Information:
 
Data Exception DER Documentation
 
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
 
SOP or contractual documents. A data exception report DER was not generated for this SDG.
 
Sample-Specific MDA/MDC
 
The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.
 
Additional Comments
 
Additional comments were not required for this sample set.
Qualifier Information
 
Manual qualifiers were not required.
 
Method/Analysis Information Product:
Liquid Scint Tc99, Liquid Analytical Method:
DOE EML HASL-300, Tc-02-RC Modified Analytical Batch Number:
1562683Sample ID Client ID 395827001 Torus Water #2 1203536111 Method Blank MB 1203536113 Laboratory Control Sample LCS 1203536112 395827001Torus Water #2 Sample Duplicate DUP
 
The samples in this SDG were analyzed on an "as received" basis.
 
SOP Reference
 
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
 
Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with
 
GL-RAD-A-059 REV# 4.
Page 25 of 49 Calibration Information:
Calibration Information
 
All initial and continuing calibration requirements have been met.
 
Standards Information
 
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
 
before the expiration dates.
 
Sample Geometry
 
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control QC Information:
 
Blank Information
 
The blank volume is representative of the sample volume in this batch.
 
QC Information
 
All of the QC samples meet the required acceptance limits with the following exceptions: Refer to Data
 
Exception Report DER.
 
Designated QC
 
The following sample was used for QC: 395827001 Torus Water #2.
Technical Information:
 
Holding Time
 
All sample procedures for this sample set were performed within the required holding time.
 
Sample Re-prep/Re-analysis
 
None of the samples in this sample set required reprep or reanalysis.
 
Recounts Samples were recounted due to high relative percent difference/relative error ratio. The recount results are
 
similar to the original results. Original results are reported.
Miscellaneous Information:
 
Data Exception DER Documentation
 
A data exception report DER 1517546 was generated for samples in this SDG/batch. DER 1517546 was
 
generated due to Failed RPD for DUP. 1. Sample 395827001 and duplicate 1203536112 do not meet the relative
 
percent difference requirement or the relative error ratio requirement due to the matrix of the sample. 1.


Recounts Samples were recounted due to high relative percent difference/relative error ratio. The recount results are similar to the original results. Original results are reported. Miscellaneous Information:
Data Exception DER Documentation A data exception report DER 1517546 was generated for samples in this SDG/batch. DER 1517546 was generated due to Failed RPD for DUP. 1. Sample 395827001 and duplicate 1203536112 do not meet the relative percent difference requirement or the relative error ratio requirement due to the matrix of the sample. 1.
Reporting results.  
Reporting results.  


Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.  
Sample-Specific MDA/MDC
 
The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.
 
Additional Comments
 
Additional comments were not required for this sample set.
Qualifier Information
 
Manual qualifiers were not required.
 
Page 26 of 49 Method/Analysis Information Product:
LSC, Tritium Dist, Liquid Analytical Method:
EPA 906.0 Modified Analytical Batch Number:
1562687Sample ID Client ID 395827001 Torus Water #2 1203536126 Method Blank MB 1203536129 Laboratory Control Sample LCS 1203536127 395827001Torus Water #2 Sample Duplicate DUP 1203536128 395827001Torus Water #2 Matrix Spike MS The samples in this SDG were analyzed on an "as received" basis.
 
SOP Reference
 
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
 
Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with
 
GL-RAD-A-002 REV# 21.
Calibration Information:
 
Calibration Information
 
All initial and continuing calibration requirements have been met.
 
Standards Information
 
Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
 
before the expiration dates.
 
Sample Geometry
 
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control QC Information:
 
Blank Information
 
The blank volume is representative of the sample volume in this batch.  


Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required.
QC Information


Page 26 of 49 Method/Analysis Information Product: LSC, Tritium Dist, LiquidAnalytical Method: EPA 906.0 ModifiedAnalytical Batch Number: 1562687Sample IDClient ID395827001 Torus Water #21203536126Method Blank MB1203536129Laboratory Control Sample LCS1203536127395827001Torus Water #2 Sample Duplicate DUP1203536128395827001Torus Water #2 Matrix Spike MSThe samples in this SDG were analyzed on an "as received" basis.
All of the QC samples meet the required acceptance limits with the following exceptions: The Matrix Spike


SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-002 REV# 21. Calibration Information:
1203536128 Torus Water #2MS did not meet recovery requirements due to the sample activity being greater
Calibration Information All initial and continuing calibration requirements have been met.


Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.  
than five times the spiked nominal concentration.  


Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control QC Information:
Designated QC
Blank Information The blank volume is representative of the sample volume in this batch.


QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The Matrix Spike 1203536128 Torus Water #2MS did not meet recovery requirements due to the sample activity being greater than five times the spiked nominal concentration.  
The following sample was used for QC: 395827001 Torus Water #2.
Technical Information:
 
Holding Time
 
All sample procedures for this sample set were performed within the required holding time.  


Designated QC The following sample was used for QC: 395827001 Torus Water #2. Technical Information:
Holding Time All sample procedures for this sample set were performed within the required holding time.
Page 27 of 49 Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.  
Page 27 of 49 Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.  


Recounts Sample 1203536129 LCS was recounted due to low recovery. The recount is reported. Miscellaneous Information:
Recounts Sample 1203536129 LCS was recounted due to low recovery. The recount is reported.
Data Exception DER Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report DER was not generated for this SDG.  
Miscellaneous Information:
 
Data Exception DER Documentation
 
Data exception reports are generated to document any procedural anomalies that may deviate from referenced
 
SOP or contractual documents. A data exception report DER was not generated for this SDG.  
 
Sample-Specific MDA/MDC
 
The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.
 
Additional Comments
 
The matrix spike, 1203536128 Torus Water #2MS, aliquot was reduced to conserve sample volume.
Qualifier Information
 
Manual qualifiers were not required.
 
Method/Analysis Information Product:
Liquid Scint C14, Liquid Analytical Method:
EPA EERF C-01 Modified Analytical Batch Number:
1562691Sample ID Client ID 395827001 Torus Water #2 1203536141 Method Blank MB 1203536144 Laboratory Control Sample LCS 1203536142 395827001Torus Water #2 Sample Duplicate DUP 1203536143 395827001Torus Water #2 Matrix Spike MS
 
The samples in this SDG were analyzed on an "as received" basis.
 
SOP Reference
 
Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as
 
Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with
 
GL-RAD-A-003 REV# 15.
Calibration Information:
 
Calibration Information
 
All initial and continuing calibration requirements have been met.
 
Page 28 of 49 Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used
 
before the expiration dates.
 
Sample Geometry
 
All counting sources were prepared in the same geometry as the calibration standards.
Quality Control QC Information:
 
Blank Information
 
The blank volume is representative of the sample volume in this batch.
 
QC Information
 
All of the QC samples met the required acceptance limits.
 
Designated QC
 
The following sample was used for QC: 395827001 Torus Water #2.
Technical Information:
 
Holding Time
 
All sample procedures for this sample set were performed within the required holding time.
 
Sample Re-prep/Re-analysis
 
None of the samples in this sample set required reprep or reanalysis.
 
Recounts None of the samples in this sample set were recounted.
Miscellaneous Information:
 
Data Exception DER Documentation
 
Data exception reports are generated to document any procedural anomalies that may deviate from referenced


Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.  
SOP or contractual documents. A data exception report DER was not generated for this SDG.  


Additional Comments The matrix spike, 1203536128 Torus Water #2MS, aliquot was reduced to conserve sample volume. Qualifier Information Manual qualifiers were not required.
Manual Integration


Method/Analysis Information Product: Liquid Scint C14, LiquidAnalytical Method: EPA EERF C-01 ModifiedAnalytical Batch Number: 1562691Sample IDClient ID395827001 Torus Water #21203536141Method Blank MB1203536144Laboratory Control Sample LCS1203536142395827001Torus Water #2 Sample Duplicate DUP1203536143395827001Torus Water #2 Matrix Spike MS The samples in this SDG were analyzed on an "as received" basis.  
No manual integrations were performed on data in this batch.  


SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-003 REV# 15. Calibration Information:
Sample-Specific MDA/MDC
Calibration Information All initial and continuing calibration requirements have been met.
Page 28 of 49 Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.


Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control QC Information:
The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.  
Blank Information The blank volume is representative of the sample volume in this batch.  


QC Information All of the QC samples met the required acceptance limits.
Additional Comments


Designated QC The following sample was used for QC: 395827001 Torus Water #2. Technical Information:
Additional comments were not required for this sample set.
Holding Time All sample procedures for this sample set were performed within the required holding time.  
Qualifier Information


Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.  
Manual qualifiers were not required.  


Recounts None of the samples in this sample set were recounted. Miscellaneous Information:
Certification Statement
Data Exception DER Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report DER was not generated for this SDG.


Manual Integration No manual integrations were performed on data in this batch.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the


Sample-Specific MDA/MDC The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.  
requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
Page 29 of 49 GEL LABORATORIES LLC 2040 Savage Road  Charleston SC 29407 - (843) 556-8171 - www.gel.com VERM001 Vermont Yankee, Entergy Nuclear Operations Inc.
Client SDG: 395827  GEL Work Order: 395827 Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Erin Trent.
Reviewed by Sample(s) Contained within this report:
395827001Lab Sample IDClient Sample ID Sample Description Torus Water #2 N/ACollected 04/11/2016 09:10 Signature:
Name:Date:Title:05 MAY 2016 Theresa Austin Group Leader Page 30 of 49 1513408DER Report No.:
1Revision No.:
Spencer Collins Originator's Name:
22-APR-16 Shenise Gerideau


Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required.  
Data Validator/Group Leader:
22-APR-16 Instrument Type:
Client Code:
Quality Criteria:
GAMMA SPECTROMETER Specifications VERMType:ProcessDivision:
Radiochemistry Mo.Day Yr.


Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. Page 29 of 49 GEL LABORATORIES LLC2040 Savage Road  Charleston SC 29407 - (843) 556-8171 - www.gel.comVERM001 Vermont Yankee, Entergy Nuclear Operations Inc.Client SDG: 395827  GEL Work Order: 395827Where the analytical method has been performed under NELAP certification, the analysis has met all of therequirements of the NELAC standard unless qualified on the Certificate of Analysis.This data report has been prepared and reviewed in accordance with GEL Laboratories LLCstandard operating procedures. Please direct any questions to your Project Manager, Erin Trent.Reviewed by Sample(s) Contained within this report:395827001Lab Sample IDClient Sample IDSample DescriptionTorus Water #2N/ACollected04/11/2016 09:10Signature:Name:Date:Title:05 MAY 2016Theresa AustinGroup LeaderPage 30 of 49 1513408DER Report No.:1Revision No.:Spencer CollinsOriginator's Name:22-APR-16Shenise Gerideau Data Validator/Group Leader:22-APR-16Instrument Type:Client Code:Quality Criteria:GAMMA SPECTROMETERSpecificationsVERMType:ProcessDivision:RadiochemistryMo.Day Yr.
22-APR-16 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT DER Disposition:
22-APR-16GEL Laboratories LLCForm GEL-DERDATA EXCEPTION REPORT   DER Disposition:Samples did not meet the required detection limit due to high sample activity. Reporting results. Specification and Requirements Exception
Samples did not meet the required detection limit due to high sample
 
activity. Reporting results.
Specification and Requirements
 
Exception


== Description:==
== Description:==
The following RDLs in sample 395827001 were not achieved: Cs-134, Fe-59, Nb-95 and Zr-95.
 
The following RDLs in DUP 1203533385 were not achieved: Cs-134, Fe-59, Nb-95 and Zr-95. Application Issues:RDL less than MDABatch ID:1561698Test / Method:
The following RDLs in sample 395827001 were not achieved: Cs-134,
EPA 901.1LiquidMatrix Type:See Below Sample Numbers:Potentially affected work order(s)(SDG):395827Page 31 of 49 1517546DER Report No.:2Revision No.:Elizabeth KrouseOriginator's Name:05-MAY-16Lyndsey Pace Data Validator/Group Leader:05-MAY-16Instrument Type:Client Code:Quality Criteria:LSCSpecificationsVERMType:ProcessDivision:RadiochemistryMo.Day Yr.
 
05-MAY-16GEL Laboratories LLCForm GEL-DERDATA EXCEPTION REPORT   DER Disposition:1. Reporting results. Specification and Requirements Exception
Fe-59, Nb-95 and Zr-95.
 
The following RDLs in DUP 1203533385 were not achieved: Cs-134,
 
Fe-59, Nb-95 and Zr-95.
Application Issues:
RDL less than MDA Batch ID:
1561698Test / Method:
 
EPA 901.1 LiquidMatrix Type:
See Below
 
Sample Numbers:Potentially affected work order(s)(SDG):395827 Page 31 of 49 1517546DER Report No.:
2Revision No.:
Elizabeth Krouse Originator's Name:
05-MAY-16 Lyndsey Pace
 
Data Validator/Group Leader:
05-MAY-16 Instrument Type:
Client Code:
Quality Criteria:
LSCSpecifications VERMType:ProcessDivision:
Radiochemistry Mo.Day Yr.
 
05-MAY-16 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT DER Disposition:
: 1. Reporting results.
Specification and Requirements
 
Exception


== Description:==
== Description:==
: 1. Sample 395827001 and duplicate 1203536112 do not meet the relative percent difference requirement or the relative error ratio requirement due to the matrix of the sample.Application Issues:Failed RPD for DUPBatch ID:1562683Test / Method:
: 1. Sample 395827001 and duplicate 1203536112 do not meet the relative
DOE EML HASL-300, Tc-02-RCModifiedLiquidMatrix Type:See Below Sample Numbers:Potentially affected work order(s)(SDG):395827Page 32 of 49 Sample Data SummaryPage 33 of 49 GEL LABORATORIES LLC2040 Savage Road  Charleston SC 29407 - (843) 556-8171 - www.gel.com Note(s):1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
 
: 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigmauncertainty)   U    Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.10 CFR Part 50/61 Certificate of AnalysisGEL Sample ID:Matrix:Geometry Received:Client:Collect Date:Receive Date:Client Sample ID:395827001WaterVermont Yankee, Entergy Nuclear OperatioApril     11, 2016April     21, 2016Torus Water #2Report Date:May      05, 2016AnalyteRun DateActivityMDAQualifier2 SigmaUncertaintyRL Alpha SpecGamma SpecH-3C-14Fe-55Ni-63Sr-89Sr-90Tc-99Pu-241Np-237Pu-238Pu-239/240Pu-242Am-241Cm-242Cm-243/244Be-7Na-22K-40Cr-51Mn-54Fe-59Co-56Co-57 Co-58Co-60Ni-59Zn-65Y-88Zr-95Nb-94Nb-95Ru-106Ag-110mSn-11304/29/1605/03/1604/28/1604/29/1605/02/1605/02/1605/03/1605/04/1604/30/1605/02/1605/02/1605/02/1604/30/1604/30/1604/30/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/16 04/21/1604/21/1604/28/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/16  1.70E+06 1.49E+01 9.53E+01 7.94E+02 1.08E+00 3.31E-01 3.89E+03 7.38E+00 -1.66E-01 1.96E-02 4.85E-02 1.91E-01 4.31E-02 0.00E+00 -5.11E-03 3.92E+01 6.07E+00 1.14E+01 3.07E+01 4.71E+02 2.87E+01 7.28E+00 3.24E+00 9.00E+01 2.07E+04 5.85E+00 1.95E+03 -1.32E+00 2.37E+01 -7.62E+00 6.97E+00 3.19E+01 -4.46E+00 9.02E+00 3.33E+04 2.41E+01 6.05E+01 7.12E+01 1.29E+00 9.80E-01 9.37E+01 1.13E+01 3.14E-01 2.14E-01 2.13E-01 2.99E-01 7.39E-02 4.66E-02 4.41E-02 9.40E+01 7.93E+00 5.16E+01 9.82E+01 2.43E+01 3.55E+01 1.52E+01 7.66E+00 2.06E+01 7.10E+01 6.40E+00 6.85E+01 5.08E+00 2.40E+01 1.13E+01 1.34E+01 1.04E+02 2.14E+01 1.28E+01 1.75E+03 4.08E+01 8.07E+01 7.04E+01 2.18E+00 2.66E+00 4.26E+01 1.91E+01 9.68E-01 4.50E-01 3.86E-01 4.10E-01 6.47E-02 6.93E-02 1.02E-01 1.59E+02 1.35E+01 8.56E+01 1.69E+02 2.38E+01 6.01E+01 2.61E+01 1.28E+01 2.46E+01 1.26E+01 1.01E+01 5.59E+01 8.67E+00 4.17E+01 1.84E+01 2.31E+01 1.72E+02 3.65E+01 2.19E+01 2.00E+03 5.00E+01 1.10E+02 5.30E+02 2.30E+01 3.50E+00 5.00E+01 2.50E+01 1.50E+01 1.50E+01 1.50E+01 1.50E+01 1.50E+01 1.50E+01 1.50E+01 1.50E+01 3.00E+01 1.50E+01 1.50E+01 2.00E+01 3.00E+01 3.00E+01 1.50E+013U33U U3UUUUUUUUUUUU3UUU33U3U UUUUUU12pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/L pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LUnitsPage 34 of 49 GEL LABORATORIES LLC2040 Savage Road  Charleston SC 29407 - (843) 556-8171 - www.gel.com Note(s):1. Calculated MDAs are a-posteriori values at the 95% confidence level.2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
percent difference requirement or the relative error ratio requirement due
: 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigmauncertainty)   U    Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.10 CFR Part 50/61 Certificate of AnalysisGEL Sample ID:Matrix:Geometry Received:Client:Collect Date:Receive Date:Client Sample ID:395827001WaterVermont Yankee, Entergy Nuclear OperatioApril     11, 2016April     21, 2016Torus Water #2Report Date:May      05, 2016AnalyteRun DateActivityMDAQualifier2 SigmaUncertaintyRLSb-124Sb-125I-129Cs-134Cs-136Cs-137Ba-133Ba-140Ce-139Ce-141Ce-144Nd-147Pm-144Pm-146Eu-152Eu-154Eu-155Ir-192Hg-203Tl-208Pb-210Pb-212Pb-214 Bi-212Bi-214Ra-228Ac-228Th-234U-235U-238Np-239Am-24104/21/1604/21/1604/27/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/16 04/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/16 -3.65E+00 8.30E+00 -3.73E-02 -1.30E+01 5.93E+00 1.13E+03 -7.26E+00
 
  -1.12E+01 -8.99E+00 -9.12E+00 3.42E+01 -8.63E+01 1.21E+00 4.46E+00 1.35E+01 1.78E+01 1.43E+01 -2.79E+00 8.62E+00 8.75E+00 9.04E+02 -1.47E+00
to the matrix of the sample.
Application Issues:
Failed RPD for DUP Batch ID:
1562683Test / Method:
 
DOE EML HASL-300, Tc-02-RC ModifiedLiquidMatrix Type:
See Below
 
Sample Numbers:Potentially affected work order(s)(SDG):395827 Page 32 of 49 Sample Data Summary Page 33 of 49 GEL LABORATORIES LLC 2040 Savage Road  Charleston SC 29407 - (843) 556-8171 - www.gel.com Note(s):1. Calculated MDAs are a-posteriori values at the 95% confidence level.
: 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the
 
sample collect date.
: 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U    Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:Geometry Received:
Client:Collect Date:
Receive Date:
Client Sample ID:
395827001 WaterVermont Yankee, Entergy Nuclear Operatio April     11, 2016 April     21, 2016 Torus Water #2 Report Date:
May      05, 2016AnalyteRun Date ActivityMDAQualifier 2 SigmaUncertainty RL Alpha Spec Gamma Spec H-3C-14Fe-55Ni-63Sr-89Sr-90Tc-99Pu-241Np-237Pu-238Pu-239/240 Pu-242Am-241Cm-242Cm-243/244 Be-7Na-22K-40Cr-51Mn-54Fe-59Co-56Co-57 Co-58Co-60Ni-59Zn-65Y-88Zr-95Nb-94Nb-95Ru-106Ag-110mSn-11304/29/1605/03/1604/28/1604/29/1605/02/1605/02/1605/03/1605/04/1604/30/1605/02/1605/02/1605/02/1604/30/1604/30/1604/30/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/16 04/21/1604/21/1604/28/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/16  1.70E+06 1.49E+01 9.53E+01 7.94E+02 1.08E+00 3.31E-01 3.89E+03 7.38E+00
-1.66E-01 1.96E-02
 
4.85E-02 1.91E-01 4.31E-02 0.00E+00
-5.11E-03 3.92E+01
 
6.07E+00 1.14E+01 3.07E+01 4.71E+02 2.87E+01 7.28E+00 3.24E+00
 
9.00E+01 2.07E+04 5.85E+00 1.95E+03
-1.32E+00 2.37E+01
-7.62E+00 6.97E+00 3.19E+01
-4.46E+00 9.02E+00 3.33E+04 2.41E+01 6.05E+01 7.12E+01 1.29E+00 9.80E-01 9.37E+01 1.13E+01 3.14E-01 2.14E-01 2.13E-01 2.99E-01 7.39E-02 4.66E-02 4.41E-02 9.40E+01 7.93E+00 5.16E+01 9.82E+01 2.43E+01 3.55E+01 1.52E+01 7.66E+00
 
2.06E+01 7.10E+01 6.40E+00 6.85E+01 5.08E+00 2.40E+01 1.13E+01 1.34E+01 1.04E+02 2.14E+01 1.28E+01 1.75E+03 4.08E+01 8.07E+01 7.04E+01 2.18E+00 2.66E+00 4.26E+01 1.91E+01 9.68E-01 4.50E-01 3.86E-01 4.10E-01 6.47E-02 6.93E-02 1.02E-01 1.59E+02 1.35E+01 8.56E+01 1.69E+02 2.38E+01 6.01E+01 2.61E+01 1.28E+01
 
2.46E+01 1.26E+01 1.01E+01 5.59E+01 8.67E+00 4.17E+01 1.84E+01 2.31E+01 1.72E+02 3.65E+01 2.19E+01 2.00E+03 5.00E+01 1.10E+02 5.30E+02 2.30E+01 3.50E+00 5.00E+01 2.50E+01 1.50E+01 1.50E+01 1.50E+01 1.50E+01 1.50E+01 1.50E+01 1.50E+01 1.50E+01 3.00E+01 1.50E+01 1.50E+01 2.00E+01 3.00E+01 3.00E+01
 
1.50E+01 3U33U U3UUUUUUUUUUUU3UUU33U3U UUUUUU12pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/L pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LUnitsPage 34 of 49 GEL LABORATORIES LLC 2040 Savage Road  Charleston SC 29407 - (843) 556-8171 - www.gel.com Note(s):1. Calculated MDAs are a-posteriori values at the 95% confidence level.
: 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the
 
sample collect date.
: 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U    Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:Geometry Received:
Client:Collect Date:
Receive Date:
Client Sample ID:
395827001 WaterVermont Yankee, Entergy Nuclear Operatio April     11, 2016 April     21, 2016 Torus Water #2 Report Date:
May      05, 2016AnalyteRun Date ActivityMDAQualifier 2 SigmaUncertainty RLSb-124Sb-125I-129Cs-134Cs-136Cs-137Ba-133Ba-140Ce-139Ce-141Ce-144Nd-147Pm-144Pm-146Eu-152Eu-154Eu-155Ir-192Hg-203Tl-208Pb-210Pb-212Pb-214 Bi-212Bi-214Ra-228Ac-228Th-234U-235U-238Np-239Am-24104/21/1604/21/1604/27/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/16 04/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/16 -3.65E+00 8.30E+00
-3.73E-02
-1.30E+01 5.93E+00
 
1.13E+03
-7.26E+00
 
  -1.12E+01
-8.99E+00
-9.12E+00 3.42E+01
-8.63E+01 1.21E+00
 
4.46E+00 1.35E+01 1.78E+01 1.43E+01
-2.79E+00 8.62E+00 8.75E+00 9.04E+02
-1.47E+00
 
  -6.77E+00
  -6.77E+00
  -6.90E+01 -1.64E+00 4.22E+01 4.22E+01 3.77E+02 -3.80E+01 3.77E+02 7.01E+01 -2.43E+01 1.09E+01 2.74E+01 8.59E-01 1.47E+01 3.45E+01 2.43E+01 1.32E+01 6.57E+01 8.66E+00 1.67E+01 5.98E+01 1.33E+02 1.14E+01 1.29E+01 2.86E+01 2.25E+01 3.04E+01 9.96E+00 1.07E+01 1.20E+01 1.07E+03 1.92E+01 2.15E+01 1.77E+02 2.21E+01 6.30E+01 6.30E+01 3.56E+02 5.95E+01 3.56E+02 7.43E+01 4.16E+01 1.88E+01 4.64E+01 1.51E+00 2.52E+01 5.84E+01 2.06E+01 2.09E+01 1.10E+02 1.42E+01 2.77E+01 9.96E+01 2.22E+02 1.88E+01 2.19E+01 4.91E+01 3.83E+01 5.10E+01 1.71E+01 1.86E+01 1.91E+01 1.84E+03 3.09E+01 3.65E+01 2.89E+02 3.64E+01 1.08E+02 1.08E+02 5.78E+02 9.77E+01 5.78E+02 1.32E+02 7.09E+01 2.00E+00 1.50E+01 1.80E+01UUUUU3UUUUUUUUUUUUUUUUU UUUU3,UU3,UUU12pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/L pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LUnitsPage 35 of 49 GEL LABORATORIES, LLC2040 Savage Road  Charleston SC 29407 - (843) 556-8171 - www.gel.com 10 CFR Part 50/61 Isotope Abundance ReportGEL Sample ID:Matrix:Client:Collect Date:Receive Date:Client Sample ID:395827001WaterVermont Yankee, Entergy Nuclear Operations Inc.April    11, 2016April     21, 2016Torus Water #2AnalyteActivity Alpha SpecGamma SpecNi-63Tc-99 H-3Cs-137Co-60Mn-54Zn-65  7.94E+02 3.89E+03 1.70E+06 1.13E+03 2.07E+04 4.71E+02 1.95E+03pCi/LpCi/L pCi/LpCi/LpCi/LpCi/LpCi/LUnits% Abundance 000.05 000.22 098.31 000.07 001.20 000.03 000.11Total Activity:  1.73E+06Total % Abundance: 100.00Page 36 of 49 Quality ControlSummaryPage 37 of 49 QC SummaryGEL LABORATORIES LLC2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.comRad Alpha Spec15626291562630Batch BatchPlutonium-238Plutonium-239/240 Plutonium-242Plutonium-238Plutonium-239/240 Plutonium-242Plutonium-238Plutonium-239/240 Plutonium-242Americium-241Curium-242Curium-243/244Americium-241Curium-242 Curium-243/244Americium-241Curium-242ParmnameMr. Mark VandaleContact:Entergy Nuclear Operations, Inc., VY530 Governor Hunt RoadVernon, Vermont May 5, 2016Report Date:Units  pCi/LpCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LAnlstDateTimeMXS2MXS204/30/16 11:0304/30/16 11:0304/30/16 11:0504/30/16 11:0504/30/16 11:0804/30/16 11:05QC0.1320.08240.07630.04755.710.05450.0605-0.01350.02150.07650.000.02525.270.01446.220.0246-0.00542NOMSample0.01960.04850.1910.04310.00-0.00511RangeN/A N/A N/A(75%-125%)N/AN/AN/A(75%-125%)(75%-125%)QualUU UUUUU UUUU UUQC1203535940    395827001QC1203535941    QC1203535939     QC1203535947    395827001QC1203535948    QC1203535946     N/AN/AN/A16.6N/AN/AREC%11610794.14.94 4.936.61DUPLCSMBDUPLCS MB395827Workorder:PO Box 250UUUUU U+/-0.214
 
+/-0.213+/-0.299+/-0.0739+/-0.0466
  -6.90E+01
+/-0.0441+/-0.142
-1.64E+00 4.22E+01
 
4.22E+01 3.77E+02
-3.80E+01 3.77E+02 7.01E+01
-2.43E+01 1.09E+01
 
2.74E+01 8.59E-01 1.47E+01 3.45E+01 2.43E+01 1.32E+01 6.57E+01 8.66E+00 1.67E+01 5.98E+01 1.33E+02 1.14E+01 1.29E+01 2.86E+01 2.25E+01 3.04E+01 9.96E+00 1.07E+01 1.20E+01 1.07E+03 1.92E+01 2.15E+01
 
1.77E+02 2.21E+01 6.30E+01 6.30E+01 3.56E+02 5.95E+01 3.56E+02 7.43E+01 4.16E+01 1.88E+01 4.64E+01 1.51E+00 2.52E+01 5.84E+01 2.06E+01 2.09E+01 1.10E+02 1.42E+01 2.77E+01 9.96E+01 2.22E+02 1.88E+01 2.19E+01 4.91E+01 3.83E+01 5.10E+01 1.71E+01 1.86E+01 1.91E+01 1.84E+03 3.09E+01 3.65E+01
 
2.89E+02 3.64E+01 1.08E+02 1.08E+02 5.78E+02 9.77E+01 5.78E+02 1.32E+02 7.09E+01 2.00E+00 1.50E+01 1.80E+01 UUUUU3UUUUUUUUUUUUUUUUU UUUU3,UU3,UUU12pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/L pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LUnitsPage 35 of 49 GEL LABORATORIES, LLC 2040 Savage Road  Charleston SC 29407 - (843) 556-8171 - www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:Client:Collect Date:
Receive Date:
Client Sample ID:
395827001 WaterVermont Yankee, Entergy Nuclear Operations Inc.
April    11, 2016 April     21, 2016 Torus Water #2 AnalyteActivity Alpha Spec Gamma Spec Ni-63Tc-99 H-3Cs-137Co-60Mn-54Zn-65  7.94E+02 3.89E+03
 
1.70E+06 1.13E+03 2.07E+04 4.71E+02 1.95E+03 pCi/LpCi/L pCi/LpCi/LpCi/LpCi/LpCi/LUnits% Abundance 000.05 000.22 098.31 000.07 001.20 000.03 000.11Total Activity:  1.73E+06Total % Abundance: 100.00 Page 36 of 49 Quality Control SummaryPage 37 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Alpha Spec 15626291562630Batch BatchPlutonium-238 Plutonium-239/240
 
Plutonium-242 Plutonium-238 Plutonium-239/240
 
Plutonium-242 Plutonium-238 Plutonium-239/240
 
Plutonium-242 Americium-241 Curium-242 Curium-243/244 Americium-241 Curium-242
 
Curium-243/244 Americium-241 Curium-242 ParmnameMr. Mark Vandale Contact:Entergy Nuclear Operations, Inc., VY 530 Governor Hunt Road Vernon, Vermont May 5, 2016 Report Date:
Units  pCi/LpCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LAnlstDateTimeMXS2MXS204/30/16 11:03 04/30/16 11:03 04/30/16 11:05 04/30/16 11:05 04/30/16 11:08 04/30/16 11:05 QC0.1320.08240.07630.04755.710.05450.0605-0.01350.02150.07650.000.02525.270.01446.220.0246-0.00542NOMSample0.01960.04850.1910.04310.00-0.00511RangeN/A N/A N/A(75%-125%)
N/AN/AN/A(75%-125%)
(75%-125%)
QualUU UUUUU UUUU UUQC1203535940    395827001 QC1203535941 QC1203535939 QC1203535947    395827001 QC1203535948 QC1203535946 N/AN/AN/A16.6N/AN/AREC%11610794.14.94 4.936.61DUPLCSMBDUPLCS MB395827Workorder:
PO Box 250 UUUUU U+/-0.214
+/-0.213+/-0.299+/-0.0739
+/-0.0466
 
+/-0.0441
+/-0.142
+/-0.113+/-0.113+/-0.107+/-0.770
+/-0.113+/-0.113+/-0.107+/-0.770
+/-0.108+/-0.0977
+/-0.108+/-0.0977
+/-0.0611+/-0.0828+/-0.101+/-0.055+/-0.0707+/-0.623+/-0.0539+/-0.671+/-0.0949
 
+/-0.0468RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page  1 of  12Page 38 of 49 QC SummaryGEL LABORATORIES LLC2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.comRad Alpha SpecRad Gamma Spec1562630156263115626321561698BatchBatchBatchBatchCurium-243/244Neptunium-237Neptunium-237 Neptunium-237Plutonium-241Plutonium-241Plutonium-241Actinium-228Americium-241Antimony-124 Antimony-125 Barium-133 Barium-140Beryllium-7Bismuth-212 Bismuth-214 Cerium-139ParmnameUnits pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LAnlstDateTimeMXS2MXS2MJH104/30/16 10:5704/30/16 10:59 04/30/16 10:5705/04/16 15:2505/03/16 14:1905/04/16 13:5404/22/16 06:34QC0.006290.22591.80.0941-1.65216-1.4-83.9-30.21.84-5.76-11.255.051.4 27.2 1.581.86NOMSample-0.1667.3842.2-24.3-3.658.30-7.26
+/-0.0611
-11.239.2-69-1.64-8.99RangeN/A(75%-125%)N/A(75%-125%)N/A N/AN/A N/A N/A N/AN/AN/A N/A N/AQualUUUUUUUUU U
+/-0.0828
+/-0.101+/-0.055+/-0.0707
+/-0.623+/-0.0539
+/-0.671+/-0.0949
 
+/-0.0468 RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty  
 
Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty  
 
Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page  1 of  12 Page 38 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Alpha Spec Rad Gamma Spec 1562630156263115626321561698BatchBatchBatchBatchCurium-243/244 Neptunium-237 Neptunium-237
 
Neptunium-237 Plutonium-241 Plutonium-241 Plutonium-241 Actinium-228 Americium-241 Antimony-124
 
Antimony-125
 
Barium-133
 
Barium-140 Beryllium-7 Bismuth-212
 
Bismuth-214
 
Cerium-139 ParmnameUnits pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LAnlstDateTimeMXS2MXS2MJH104/30/16 10:57 04/30/16 10:59
 
04/30/16 10:57 05/04/16 15:25 05/03/16 14:19 05/04/16 13:54 04/22/16 06:34 QC0.006290.22591.80.0941-1.65216-1.4-83.9-30.21.84-5.76-11.255.051.4 27.2 1.581.86NOMSample-0.1667.3842.2-24.3-3.658.30-7.26
-11.239.2-69-1.64-8.99RangeN/A(75%-125%)
N/A(75%-125%)
N/A N/AN/A N/A N/A N/AN/AN/A N/A N/AQualUUUUUUUUU U
U U
U U
UUUQC1203535950    395827001QC1203535951 QC1203535949     QC1203535953    395827001QC1203535954    QC1203535952     QC1203533385    395827001N/AN/AN/AN/A N/A N/A N/AN/AN/A N/A N/A N/AREC%10311189.3194DUPLCSMBDUPLCSMBDUP395827Workorder:UUUU U
UUUQC1203535950    395827001 QC1203535951   
 
QC1203535949 QC1203535953    395827001 QC1203535954 QC1203535952 QC1203533385    395827001 N/AN/AN/AN/A N/A N/A N/AN/AN/A N/A N/A N/AREC%10311189.3194DUPLCSMBDUPLCSMBDUP395827Workorder:
UUUU U
U UUU U
U UUU U
U U+/-0.314+/-11.3+/-63.0+/-41.6
U U+/-0.314+/-11.3+/-63.0+/-41.6
Line 384: Line 1,258:
+/-27.4
+/-27.4
+/-13.2+/-65.7+/-94.0+/-177+/-22.1
+/-13.2+/-65.7+/-94.0+/-177+/-22.1
+/-8.66+/-0.0657+/-0.654+/-6.94+/-0.422+/-7.13+/-27.4
+/-8.66+/-0.0657
+/-0.654+/-6.94+/-0.422+/-7.13+/-27.4
+/-7.62+/-95.8+/-50.5
+/-7.62+/-95.8+/-50.5
+/-15.8
+/-15.8
Line 391: Line 1,266:
+/-144
+/-144
+/-257+/-34.0
+/-257+/-34.0
+/-12.7RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page  2 of  12Page 39 of 49 QC SummaryGEL LABORATORIES LLC2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.comRad Gamma Spec1561698BatchCerium-141Cerium-144Cesium-134Cesium-136 Cesium-137 Chromium-51 Cobalt-56Cobalt-57Cobalt-58 Cobalt-60 Europium-152 Europium-154Europium-155Iridium-192 Iron-59 Lead-210 Lead-212Lead-214Manganese-54 Mercury-203 Neodymium-147 Neptunium-239ParmnameUnits pCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/LAnlstDateTimeMJH104/22/16 06:34QC-1216.8-8.32
+/-12.7RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Page  2 of  12 Page 39 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1561698BatchCerium-141 Cerium-144 Cesium-134 Cesium-136
 
Cesium-137
 
Chromium-51
 
Cobalt-56 Cobalt-57 Cobalt-58
 
Cobalt-60
 
Europium-152
 
Europium-154 Europium-155 Iridium-192
 
Iron-59 Lead-210 Lead-212Lead-214Manganese-54
 
Mercury-203
 
Neodymium-147
 
Neptunium-239 ParmnameUnits pCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/LAnlstDateTimeMJH104/22/16 06:34 QC-1216.8-8.32
-39.411503.78 5.84 6.90 89.120400-7.8117.7 20.9-2.06-55.9-4140.3657.394810.957-52.1-65.9NOMSample-9.1234.2-135.93113030.7 7.28 3.24 90.02070013.5 17.8 14.3-2.7928.7904-1.47
-39.411503.78 5.84 6.90 89.120400-7.8117.7 20.9-2.06-55.9-4140.3657.394810.957-52.1-65.9NOMSample-9.1234.2-135.93113030.7 7.28 3.24 90.02070013.5 17.8 14.3-2.7928.7904-1.47
-6.774718.62-86.370.1RangeN/A N/AN/AN/A(0%-20%)N/A N/AN/A(0% - 100%)(0%-20%)N/AN/AN/AN/A N/A N/A N/AN/A(0%-20%)N/AN/A N/AQualU U
-6.774718.62-86.370.1RangeN/A N/AN/AN/A(0%-20%)N/A N/AN/A(0% - 100%)
(0%-20%)N/AN/AN/AN/A N/A N/A N/AN/A(0%-20%)N/AN/A N/AQualU U
UUUU UUU UUU U
UUUU UUU UUU U
U UUU UN/AN/AN/A N/A2.28N/AN/AN/A0.9821.55N/AN/AN/A N/A N/A N/AN/AN/A1.95N/A N/AN/AREC%395827Workorder:U UU UUUUUUU U
U UUU UN/AN/AN/A N/A2.28N/AN/AN/A0.9821.55N/AN/AN/A N/A N/A N/AN/AN/A1.95N/A N/AN/AREC%395827Workorder:
U UU UUUUUUU U
U UUUUUU+/-16.7
U UUUUUU+/-16.7
+/-59.8+/-14.7
+/-59.8+/-14.7
Line 417: Line 1,328:
+/-32.0
+/-32.0
+/-36.4
+/-36.4
+/-15.9+/-208+/-115RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page  3 of  12Page 40 of 49 QC SummaryGEL LABORATORIES LLC2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.comRad Gamma Spec1561698BatchNiobium-94Niobium-95Potassium-40Promethium-144 Promethium-146 Radium-228 Ruthenium-106Silver-110mSodium-22 Thallium-208 Thorium-234 Tin-113Uranium-235Uranium-238 Yttrium-88 Zinc-65 Zirconium-95Actinium-228Americium-241 Antimony-124 Antimony-125 Barium-133ParmnameUnits pCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/LAnlstDateTimeMJH104/22/16 06:3404/22/16 06:39QC14.9 22.9 16.1 1.11-18.9
+/-15.9+/-208+/-115RPD%Uncertainty Uncertainty  
-83.913640.9 6.22-15.11550.62216.4155-5.551870-5.381223970015.9-15727.6NOMSample-7.626.97 11.4 1.214.4642.2 31.9-4.466.078.753779.02-38377-1.32195023.7RangeN/AN/AN/AN/A N/A N/A N/AN/AN/A N/A N/A N/AN/AN/A N/A(0%-20%)N/A(75%-125%)QualU U
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty Page  3 of  12 Page 40 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1561698BatchNiobium-94 Niobium-95 Potassium-40 Promethium-144
 
Promethium-146
 
Radium-228
 
Ruthenium-106 Silver-110m Sodium-22
 
Thallium-208
 
Thorium-234
 
Tin-113Uranium-235 Uranium-238
 
Yttrium-88
 
Zinc-65 Zirconium-95 Actinium-228 Americium-241
 
Antimony-124
 
Antimony-125
 
Barium-133 ParmnameUnits pCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/LAnlstDateTimeMJH104/22/16 06:34 04/22/16 06:39 QC14.9 22.9 16.1 1.11-18.9
-83.913640.9 6.22-15.11550.62216.4155-5.551870-5.381223970015.9-15727.6NOMSample-7.626.97 11.4 1.214.4642.2 31.9-4.466.078.753779.02-38377-1.32195023.7RangeN/AN/AN/AN/A N/A N/A N/AN/AN/A N/A N/A N/AN/AN/A N/A(0%-20%)N/A(75%-125%)
QualU U
UUU U
UUU U
U UUU U
U UUU U
U UUUUUUU UQC1203533386     N/AN/AN/A N/A N/A N/AN/AN/A N/A N/A N/AN/AN/A N/A N/A3.98N/AREC%11534400LCS395827Workorder:UUU U
U UUUUUUU UQC1203533386 N/AN/AN/A N/A N/A N/AN/AN/A N/A N/A N/AN/AN/A N/A N/A3.98N/AREC%11534400LCS395827Workorder:
UUU U
U UUU U
U UUU U
U UUU U
U UUU U
Line 439: Line 1,398:
+/-19.0+/-425+/-19.4
+/-19.0+/-425+/-19.4
+/-85.7+/-425+/-7.20
+/-85.7+/-425+/-7.20
+/-96.7+/-36.8+/-399+/-1740+/-46.1+/-241RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page  4 of  12Page 41 of 49 QC SummaryGEL LABORATORIES LLC2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.comRad Gamma Spec1561698BatchBarium-140Beryllium-7Bismuth-212 Bismuth-214 Cerium-139 Cerium-141Cerium-144Cesium-134 Cesium-136 Cesium-137 Chromium-51Cobalt-56Cobalt-57 Cobalt-58 Cobalt-60 Europium-152Europium-154Europium-155 Iridium-192 Iron-59 Lead-210ParmnameUnits  pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/LAnlstDateTimeMJH104/22/16 06:39QC153-119540-68.543.7-75.7-26823.7-66.413700-19981.9267-46.914200-10143.314657.9 45.34.51E+05NOMSampleRange(75%-125%)(75%-125%)QualUUUU U
+/-96.7+/-36.8+/-399+/-1740+/-46.1+/-241RPD%Uncertainty Uncertainty  
U UUUUUUUUUU UREC%10210313500 13800395827Workorder:+/-103+/-282+/-768+/-1080+/-142+/-66.4+/-112
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Page  4 of  12 Page 41 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1561698BatchBarium-140 Beryllium-7 Bismuth-212
 
Bismuth-214
 
Cerium-139
 
Cerium-141 Cerium-144 Cesium-134
 
Cesium-136
 
Cesium-137
 
Chromium-51 Cobalt-56 Cobalt-57
 
Cobalt-58
 
Cobalt-60
 
Europium-152 Europium-154 Europium-155
 
Iridium-192
 
Iron-59 Lead-210ParmnameUnits  pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/LAnlstDateTimeMJH104/22/16 06:39 QC153-119540-68.543.7-75.7-26823.7-66.413700-19981.9267-46.914200-10143.314657.9 45.34.51E+05NOMSampleRange(75%-125%)
(75%-125%)
QualUUUU U
U UUUUUUUUUU UREC%10210313500 13800395827Workorder:
+/-103+/-282+/-768+/-1080+/-142+/-66.4+/-112
+/-478+/-94.4+/-158
+/-478+/-94.4+/-158
+/-354+/-630+/-88.7+/-108+/-87.5+/-408
+/-354+/-630+/-88.7+/-108+/-87.5+/-408
+/-237+/-136
+/-237+/-136
+/-300+/-74.3+/-199+/-50700RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page  5 of  12Page 42 of 49 QC SummaryGEL LABORATORIES LLC2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.comRad Gamma Spec1561698BatchLead-212Lead-214Manganese-54Mercury-203 Neodymium-147 Neptunium-239 Niobium-94Niobium-95Potassium-40 Promethium-144 Promethium-146 Radium-228Ruthenium-106Silver-110m Sodium-22 Thallium-208 Thorium-234Tin-113Uranium-235 Uranium-238 Yttrium-88 Zinc-65ParmnameUnits  pCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/LAnlstDateTimeMJH104/22/16 06:39QC-41.7
+/-300+/-74.3+/-199+/-50700RPD%Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty Page  5 of  12 Page 42 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1561698BatchLead-212Lead-214Manganese-54 Mercury-203
 
Neodymium-147
 
Neptunium-239
 
Niobium-94 Niobium-95 Potassium-40
 
Promethium-144
 
Promethium-146
 
Radium-228 Ruthenium-106 Silver-110m
 
Sodium-22
 
Thallium-208
 
Thorium-234 Tin-113Uranium-235
 
Uranium-238
 
Yttrium-88
 
Zinc-65ParmnameUnits  pCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/LAnlstDateTimeMJH104/22/16 06:39 QC-41.7
-66.522.0-25.5-2593569.74 28.1-26.76.91-31.7122 16678.214.5-13.8-1950-66.5147-1950-3.091030NOMSampleRangeQualUU UUU U
-66.522.0-25.5-2593569.74 28.1-26.76.91-31.7122 16678.214.5-13.8-1950-66.5147-1950-3.091030NOMSampleRangeQualUU UUU U
U UUU U
U UUU U
U UUU U
U UUU U
U UUU UREC%395827Workorder:+/-143+/-183+/-87.1+/-77.1+/-538
U UUU UREC%395827Workorder:
+/-143+/-183+/-87.1+/-77.1+/-538
+/-781+/-68.8
+/-781+/-68.8
+/-77.3+/-253+/-68.5+/-124+/-399+/-727
+/-77.3+/-253+/-68.5+/-124+/-399+/-727
+/-140+/-47.5
+/-140+/-47.5
+/-73.8+/-5510+/-108
+/-73.8+/-5510+/-108
+/-479+/-5510+/-28.7+/-363RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page  6 of  12Page 43 of 49 QC SummaryGEL LABORATORIES LLC2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.comRad Gamma Spec1561698BatchZirconium-95Actinium-228Americium-241Antimony-124 Antimony-125 Barium-133 Barium-140Beryllium-7Bismuth-212 Bismuth-214 Cerium-139 Cerium-141Cerium-144Cesium-134 Cesium-136 Cesium-137 Chromium-51Cobalt-56Cobalt-57 Cobalt-58 Cobalt-60 Europium-152ParmnameUnits pCi/LpCi/LpCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/LAnlstDateTimeMJH104/22/16 06:34QC31.9-7.16
+/-479+/-5510+/-28.7+/-363RPD%Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty Page  6 of  12 Page 43 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1561698BatchZirconium-95 Actinium-228 Americium-241 Antimony-124
 
Antimony-125
 
Barium-133
 
Barium-140 Beryllium-7 Bismuth-212
 
Bismuth-214
 
Cerium-139
 
Cerium-141 Cerium-144 Cesium-134
 
Cesium-136
 
Cesium-137
 
Chromium-51 Cobalt-56 Cobalt-57
 
Cobalt-58
 
Cobalt-60
 
Europium-152 ParmnameUnits pCi/LpCi/LpCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/LAnlstDateTimeMJH104/22/16 06:34 QC31.9-7.16
-1.73-0.03870.9600.347-0.895-8.8614.21.92-0.5332.38 5.240.137-1.240.1341.840.706-0.1720.6801.03 1.98NOMSampleRangeQualUUUUU U
-1.73-0.03870.9600.347-0.895-8.8614.21.92-0.5332.38 5.240.137-1.240.1341.840.706-0.1720.6801.03 1.98NOMSampleRangeQualUUUUU U
U U
U U
UUU U
UUU U
U UUU U
U UUU U
U UUU UQC1203533384     REC%MB395827Workorder:+/-141+/-8.38
U UUU UQC1203533384 REC%MB395827Workorder:
+/-141+/-8.38
+/-9.55
+/-9.55
+/-2.87
+/-2.87
Line 471: Line 1,577:
+/-1.53
+/-1.53
+/-1.64
+/-1.64
+/-1.93RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page  7 of  12Page 44 of 49 QC SummaryGEL LABORATORIES LLC2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.comRad Gamma Spec1561698BatchEuropium-154Europium-155Iridium-192 Iron-59 Lead-210 Lead-212Lead-214Manganese-54 Mercury-203 Neodymium-147 Neptunium-239Niobium-94Niobium-95 Potassium-40 Promethium-144 Promethium-146Radium-228Ruthenium-106 Silver-110m Sodium-22 Thallium-208ParmnameUnits pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/LAnlstDateTimeMJH104/22/16 06:34QC-0.771-2.76-0.3172.12-1321.26 1.93-0.121.53-3.95-0.573
+/-1.93RPD%Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Page  7 of  12 Page 44 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1561698BatchEuropium-154 Europium-155 Iridium-192
 
Iron-59 Lead-210 Lead-212Lead-214Manganese-54
 
Mercury-203
 
Neodymium-147
 
Neptunium-239 Niobium-94 Niobium-95
 
Potassium-40
 
Promethium-144
 
Promethium-146 Radium-228 Ruthenium-106
 
Silver-110m
 
Sodium-22
 
Thallium-208 ParmnameUnits pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/LAnlstDateTimeMJH104/22/16 06:34 QC-0.771-2.76-0.3172.12-1321.26 1.93-0.121.53-3.95-0.573
-0.765-0.074314.30.643 0.158-7.16
-0.765-0.074314.30.643 0.158-7.16
-15.7-0.238
-15.7-0.238
Line 478: Line 1,628:
U UUU U
U UUU U
U UUU U
U UUU U
UREC%395827Workorder:+/-4.87+/-4.66+/-6.43
UREC%395827Workorder:
+/-4.87+/-4.66+/-6.43
+/-1.62
+/-1.62
+/-2.97+/-275+/-4.97
+/-2.97+/-275+/-4.97
Line 490: Line 1,641:
+/-18.9
+/-18.9
+/-1.98
+/-1.98
+/-1.62+/-2.16RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page  8 of  12Page 45 of 49 QC SummaryGEL LABORATORIES LLC2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.comRad Gamma SpecRad Gas Flow1561698156260215626931562716BatchBatchBatchBatchThorium-234Tin-113Uranium-235Uranium-238 Yttrium-88 Zinc-65 Zirconium-95Iodine-129Iodine-129Iodine-129 Iodine-129Nickel-59Nickel-59 Nickel-59Strontium-89Strontium-90Strontium-89ParmnameUnits pCi/LpCi/L pCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/LpCi/LAnlstDateTimeMJH1MJH1CXS7KSD104/22/16 06:34 04/27/16 09:2004/27/16 11:0404/27/16 09:19 04/27/16 09:2004/28/16 15:3604/29/16 06:45 04/28/16 15:3605/02/16 16:2405/02/16 16:24QC60.30.153-0.38860.3-0.7980.806-1.70.38850.2-0.1757.53.143722.87-1.39-0.222550NOMSample-0.0373-0.03735.851.080.331RangeN/A(75%-125%)(75%-125%)N/A(75%-125%)N/AN/A(75%-125%)QualU U
+/-1.62+/-2.16RPD%Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty Page  8 of  12 Page 45 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec Rad Gas Flow 1561698156260215626931562716BatchBatchBatchBatchThorium-234 Tin-113Uranium-235 Uranium-238
 
Yttrium-88
 
Zinc-65 Zirconium-95 Iodine-129 Iodine-129 Iodine-129
 
Iodine-129 Nickel-59 Nickel-59
 
Nickel-59 Strontium-89 Strontium-90 Strontium-89 ParmnameUnits pCi/LpCi/L pCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/LpCi/LAnlstDateTimeMJH1MJH1CXS7KSD104/22/16 06:34
 
04/27/16 09:20 04/27/16 11:04 04/27/16 09:19
 
04/27/16 09:20 04/28/16 15:36 04/29/16 06:45
 
04/28/16 15:36 05/02/16 16:24 05/02/16 16:24 QC60.30.153-0.38860.3-0.7980.806-1.70.38850.2-0.1757.53.143722.87-1.39-0.222550NOMSample-0.0373-0.03735.851.080.331RangeN/A(75%-125%)
(75%-125%)
N/A(75%-125%)
N/AN/A(75%-125%)
QualU U
UUU U
UUU U
UUUUUUUQC1203535844    395827001QC1203535846    QC1203535843     QC1203535845    395827001QC1203536150   395827001QC1203536151 QC1203536149     QC1203536198    395827001QC1203536199    N/AN/AN/AN/AREC%96.411188.810552.052.0419522DUPLCSMBMSDUPLCSMBDUPLCS395827Workorder:UUUUU+/-0.859+/-0.859+/-6.40+/-1.29+/-0.980+/-140+/-2.10+/-13.5+/-140+/-1.85
UUUUUUUQC1203535844    395827001 QC1203535846 QC1203535843 QC1203535845    395827001 QC1203536150   395827001 QC1203536151   
 
QC1203536149 QC1203536198    395827001 QC1203536199 N/AN/AN/AN/AREC%96.411188.810552.052.0419522DUPLCSMBMSDUPLCSMBDUPLCS395827Workorder:
UUUUU+/-0.859+/-0.859+/-6.40+/-1.29+/-0.980+/-140+/-2.10+/-13.5+/-140+/-1.85
+/-3.61+/-2.56+/-1.13+/-6.44+/-0.835+/-6.83+/-2.49+/-26.7
+/-3.61+/-2.56+/-1.13+/-6.44+/-0.835+/-6.83+/-2.49+/-26.7
+/-5.02+/-1.93+/-1.22RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page  9 of  12Page 46 of 49 QC SummaryGEL LABORATORIES LLC2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.comRad Gas FlowRad Liquid Scintillation1562716156267215626781562683 1562687BatchBatchBatchBatch BatchStrontium-90Strontium-89Strontium-90Iron-55Iron-55 Iron-55Nickel-63Nickel-63 Nickel-63Technetium-99Technetium-99 Technetium-99TritiumTritiumParmnameUnits pCi/L pCi/LpCi/LpCi/LpCi/L pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LAnlstDateTimeKSD1CXS7CXS7MYM1GXR105/02/16 16:2405/02/16 16:2704/28/16 23:2604/29/16 00:13 04/28/16 22:3904/29/16 14:5304/29/16 15:09 04/29/16 14:3705/03/16 15:1205/03/16 15:28 05/03/16 14:5504/29/16 23:1104/30/16 11:54QC445-1.50.11691.21440-42.58402090-6.46254841-11.41.72E+062410NOMSample95.379438901.70E+06Range(75%-125%)(0% - 100%)(75%-125%)(0%-20%)(75%-125%)(0%-20%)(75%-125%)(0%-20%)(75%-125%)QualUUUU UQC1203536197     QC1203536077    395827001QC1203536078 QC1203536076     QC1203536093    395827001QC1203536094 QC1203536092     QC1203536112    395827001QC1203536113 QC1203536111     QC1203536127    395827001QC1203536129    4.425.651751.36REC%8386.812497.71025361660 16908612350MBDUPLCSMBDUPLCS MBDUPLCS MBDUPLCS395827Workorder:+/-60.5+/-71.2
+/-5.02+/-1.93+/-1.22RPD%Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty  
 
Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty Uncertainty Uncertainty Page  9 of  12 Page 46 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gas Flow Rad Liquid Scintillation 1562716156267215626781562683 1562687BatchBatchBatchBatch BatchStrontium-90 Strontium-89 Strontium-90 Iron-55Iron-55 Iron-55Nickel-63 Nickel-63
 
Nickel-63 Technetium-99 Technetium-99
 
Technetium-99 TritiumTritiumParmnameUnits pCi/L pCi/LpCi/LpCi/LpCi/L pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LAnlstDateTimeKSD1CXS7CXS7MYM1GXR105/02/16 16:24 05/02/16 16:27 04/28/16 23:26 04/29/16 00:13
 
04/28/16 22:39 04/29/16 14:53 04/29/16 15:09
 
04/29/16 14:37 05/03/16 15:12 05/03/16 15:28
 
05/03/16 14:55 04/29/16 23:11 04/30/16 11:54 QC445-1.50.11691.21440-42.58402090-6.46254841-11.41.72E+062410NOMSample95.379438901.70E+06Range(75%-125%)
(0% - 100%)
(75%-125%)
(0%-20%)(75%-125%)
(0%-20%)(75%-125%)
(0%-20%)(75%-125%)
QualUUUU UQC1203536197 QC1203536077    395827001 QC1203536078   
 
QC1203536076 QC1203536093    395827001 QC1203536094   
 
QC1203536092 QC1203536112    395827001 QC1203536113   
 
QC1203536111 QC1203536127    395827001 QC1203536129 4.425.651751.36REC%8386.812497.71025361660 16908612350MBDUPLCSMBDUPLCS MBDUPLCS MBDUPLCS395827Workorder:
+/-60.5+/-71.2
+/-93.7+/-33300+/-13.0+/-10.4+/-1.18+/-1.00+/-58.8+/-86.2
+/-93.7+/-33300+/-13.0+/-10.4+/-1.18+/-1.00+/-58.8+/-86.2
+/-58.1+/-71.1+/-101+/-37.6
+/-58.1+/-71.1+/-101+/-37.6
+/-33.3+/-48.9
+/-33.3+/-48.9
+/-24.1+/-33700+/-461*RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page  10 of  12Page 47 of 49 QC SummaryGEL LABORATORIES LLC2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.comRad Liquid Scintillation15626871562691Batch BatchTritiumTritiumCarbon-14Carbon-14 Carbon-14 Carbon-14ParmnameUnits pCi/LpCi/LpCi/LpCi/LpCi/L pCi/LAnlstDateTimeGXR1TXJ104/29/16 22:55 04/29/16 23:1305/03/16 17:2305/03/16 18:26 05/03/16 16:51 05/03/16 17:54QC1361.62E+0628.01310-4.591400NOMSample1.70E+0614.914.9Range(75%-125%)N/A(75%-125%)(75%-125%)QualUUUQC1203536126     QC1203536128    395827001QC1203536142   395827001QC1203536144 QC1203536141 QC1203536143    395827001The Qualifiers in this report are defined as follows:N/AREC%N/A103111471012601260MBMSDUPLCSMBMS395827Workorder:**<
+/-24.1+/-33700+/-461*RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty Uncertainty Uncertainty  
 
Uncertainty Uncertainty Uncertainty Page  10 of  12 Page 47 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Liquid Scintillation 15626871562691Batch BatchTritiumTritiumCarbon-14 Carbon-14
 
Carbon-14
 
Carbon-14 ParmnameUnits pCi/LpCi/LpCi/LpCi/LpCi/L pCi/LAnlstDateTimeGXR1TXJ104/29/16 22:55
 
04/29/16 23:13 05/03/16 17:23 05/03/16 18:26
 
05/03/16 16:51
 
05/03/16 17:54 QC1361.62E+0628.01310-4.591400NOMSample1.70E+0614.914.9Range(75%-125%)
N/A(75%-125%)
(75%-125%)
QualUUUQC1203536126 QC1203536128    395827001 QC1203536142   395827001 QC1203536144   
 
QC1203536141    
 
QC1203536143    395827001 The Qualifiers in this report are defined as follows:
N/AREC%N/A103111471012601260MBMSDUPLCSMBMS395827Workorder:
**<
>
>
BDFAH J
BDFAH J
KLM MN/AN1 ND NJQR UAnalyte is a Tracer compound Result is less than value reported Result is greater than value reportedResults are either below the MDC or tracer recovery is lowFailed analysis.
KLM MN/AN1 ND NJQR UAnalyte is a Tracer compound
Analytical holding time was exceeded Value is estimatedAnalyte present. Reported value may be biased high. Actual value is expected to be lower.Analyte present. Reported value may be biased low. Actual value is expected to be higher.
 
M if above MDC and less than LLD REMP Result > MDC/CL and < RDLRPD or %Recovery limits do not apply.See case narrative Analyte concentration is not detected above the detection limitConsult Case Narrative, Data Summary package, or Project Manager concerning this qualifierOne or more quality control criteria have not been met. Refer to the applicable narrative or DER.
Result is less than value reported
Sample results are rejected Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.UU+/-33300+/-24.1+/-24.1+/-301+/-31600+/-24.9+/-47.0
 
Result is greater than value reported Results are either below the MDC or tracer recovery is low Failed analysis.
 
Analytical holding time was exceeded
 
Value is estimated Analyte present. Reported value may be biased high. Actual value is expected to be lower.
Analyte present. Reported value may be biased low. Actual value is expected to be higher.
 
M if above MDC and less than LLD
 
REMP Result > MDC/CL and < RDL RPD or %Recovery limits do not apply.
See case narrative
 
Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
 
Sample results are rejected
 
Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
UU+/-33300+/-24.1+/-24.1+/-301+/-31600+/-24.9+/-47.0
+/-23.6
+/-23.6
+/-49.8RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Notes:Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).Page  11 of  12Page 48 of 49 QC SummaryGEL LABORATORIES LLC2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.comParmnamePage 12 of  12Units AnlstDateTimeQCNOMSampleRangeQualREC%395827Workorder:UIUJUL X
+/-49.8RPD%Uncertainty  
 
Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Notes:Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
Page  11 of  12 Page 48 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road  Charleston, SC 29407 - (843) 556-8171 - www.gel.com ParmnamePage 12 of  12 Units AnlstDateTimeQCNOMSampleRangeQualREC%395827Workorder:
UIUJUL X
Y^hGamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
Y^hGamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifierOther specific qualifiers were required to properly define the results. Consult case narrative.RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
 
Preparation or preservation holding time was exceededN/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable.^ The Relative Percent Difference (RPD) obtained from the sample duplicate  (DUP) is evaluated against the acceptance criteria when the sample is greater thanfive times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- theRL is used to evaluate the DUP result.
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Other specific qualifiers were required to properly define the results. Consult case narrative.
RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
 
Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable.
^ The Relative Percent Difference (RPD) obtained from the sample duplicate  (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.
* Indicates that a Quality Control parameter was not within specifications.
* Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.Where the analytical method has been performed under NELAP certification, the analysis has met all of therequirements of the NELAC standard unless qualified on the QC Summary.RPD%Page 49 of 49}}
 
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.
RPD%Page 49 of 49}}

Revision as of 03:54, 30 June 2018

Response to NRC Questions Related to Request for 20.2002 Disposal of Contaminated Water
ML16231A028
Person / Time
Site: Vermont Yankee File:NorthStar Vermont Yankee icon.png
Issue date: 08/11/2016
From: Silko T B
Entergy Corp
To: Jack Parrott
Reactor Decommissioning Branch
PARROTJ , 415-6634, T-8E47
References
SDG: 395827
Download: ML16231A028 (52)
v • d • e


Text

From: Silko, Thomas B. [1]

Sent: Thursday, August 11, 2016 11:26 AM To: Parrott, Jack <Jack.Parrott@nrc.gov>

Subject:

[External_Sender] Response to NRC Questions dated 7 16 Jack, Based upon our conversation on Wednesday 8/3/16, VY agreed to provide a copy of the Part 61 analysis which was used to identify the radionuclide concentrations on the Torus water. Accordingly, please find attached a copy of the Part 61 report from GEL Laboratories, dated April 26, 2016.

In response to the Staffs second question, VY and the NRC discussed the process for sampling of material prior to making radioactive shipments.

VY procedure V

-EN-RW-102, Shipment of Radioactive Material, requires an isotopic be performed to ensure the material is appropriately classified per 10 CFR 61.55 requirements.

The isotopic is performed on a sample of the material (in this case a water sample) prior to completing the shipment manifest.

As such, VY is committed to sampling water prior to shipment to satisfy the requirements of 10CFR61.55.

In addition, Vermont Yankee commits to the following:

Vermont Yankee will perform a representative sample prior to each shipment of water and will confirm that the radionuclide concentrations result in doses that are equal to or less than, the doses delineated within the Summary of Project Alternative Disposal Dose Results, in our June 28, 2016 letter (BVY 16

-021; ADAMS Accession No. ML16182A035).

For example, the above could be satisfied in the following manner:

A representative sample is taken prior to a shipment and the radionuclide concentrations are verified to be equal to or less than those concentrations shown on the Data Input Worksheet, of our June 28, 2016 letter.

An alternative method to be used, such as when a radionuclide is identified as being slightly above the concentrations (while others may be lower), then sample radionuclide concentrations would be input into the Site Specific Dose Assessment Methodology (SSDA) used in our June 28, 2016 letter and the dose consequences verified to be equal to or less than that delineated within the Summary of Project Alternative Disposal Dose Results.

Please let me know if there are any further questions.

Thank You.

Tom Silko (802) 451

-3166

April 26, 2016

Mr. Mark Vandale Entergy Nuclear Operations, Inc., VY 530 Governor Hunt Road PO Box 250 Vernon, Vermont 05354

Re: Vermont Yankee Part 61 Work Order: 395827

Dear Mr. Vandale:

GEL Laboratories, LLC GEL appreciates the opportunity to provide the enclosed analytical results for the samples we received on April 21, 2016. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures.

Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at 843 556-8171, ext. 4504.

Sincerely, PM_SIGN_HERE Erin Trent Project Manager Purchase Order: 10287833 Enclosures Table of Contents Case Narrative......................................................................................1 Chain of Custody..................................................................................3

Laboratory Certifications......................................................................7

Radiological Analysis...........................................................................9 Case Narrative............................................................................10

Sample Data Summary...............................................................33

Quality Control Summary..........................................................37 Case Narrative Page 1 of 49 Case Narrative for Vermont Yankee, Entergy Nuclear Operations Inc.

SDG: 395827 April 26, 2016 Laboratory Identification:

GEL Laboratories LLC

2040 Savage Road

Charleston, South Carolina 29407

843 556-8171 Summary Sample Receipt The sample arrived at GEL Laboratories LLC, Charleston, South Carolina on April 21, 2016 for analysis. Chain of Custody form did not contain a relinquished signature. All sample containers arrived without

any visible signs of tampering or breakage. There are no additional comments concerning sample receipt.

Sample Identification The laboratory received the following sample:

Laboratory IDClient ID395827001 Torus Water #2 Case Narrative Sample analyses were conducted using methodology as outlined in GEL Laboratories, LLC GEL Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and

reduction are contained in the analytical case narratives in the enclosed data package.

Data Package The enclosed data package contains the following sections: General Narrative, Chain of Custody and Supporting Documentation, and data from the following fractions: Radiochemistry.

PM_SIGN_HERE Erin Trent

Project Manager Page 2 of 49 Chain of Custody Page 3 of 49 Page 4 of 49 Page 5 of 49 Page 6 of 49 Laboratory Certifications Page 7 of 49 StateCertification AlaskaArkansasCLIACalifornia ColoradoConnecticut DelawareDoD ELAP/ ISO17025 A2LA Florida NELAP Foreign Soils Permit GeorgiaGeorgia SDWA HawaiiIdaho Chemistry Idaho Radiochemistry Illinois NELAP IndianaKansas NELAP Kentucky SDWA Kentucky Wastewater Louisiana NELAP Louisiana SDWA MarylandMassachusetts MichiganMississippi NebraskaNevadaNew Hampshire NELAP New Jersey NELAP New Mexico New York NELAP North Carolina North Carolina SDWA North Dakota OklahomaPennsylvania NELAP S.Carolina Radchem South Carolina Chemistry Tennessee Texas NELAP Utah NELAP VermontVirginia NELAP Washington West Virginia UST-011088-065142D0904046 2940 SC00012PH-0169SC000122567.01E87156P330-15-00283, P330-15-00253 SC00012967SC00012SC00012SC00012200029C-SC-01E-10332901299012903046 (AI33904)

LA160006270M-SC0129976SC00012NE-OS-26-13 SC000122016-1 205415SC002SC000121150123345709R-158990468-004851012000210120001TN 02934T104704235-16-11 SC000122016-20 VT87156460202C780997404List of current GEL Certifications as of 26 April 2016 Page 8 of 49 Radiological Analysis Page 9 of 49 Case Narrative Page 10 of 49 Radiochemistry Technical Case Narrative Vermont Yankee, Entergy Nuclear Operations Inc. NTRG SDG #: 395827

Method/Analysis Information Product:

Alphaspec Pu242, Liquid Analytical Method:

DOE EML HASL-300, Pu-11-RC Modified Analytical Batch Number:

1562629Sample ID Client ID 395827001 Torus Water #2 1203535939 Method Blank MB 1203535941 Laboratory Control Sample LCS 1203535940 395827001Torus Water #2 Sample Duplicate DUP

The samples in this SDG were analyzed on an "as received" basis.

SOP Reference

Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as

Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with

GL-RAD-A-011 REV# 26.

Calibration Information:

Calibration Information

All initial and continuing calibration requirements have been met.

Standards Information

Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used

before the expiration dates.

Sample Geometry

All counting sources were prepared in the same geometry as the calibration standards.

Quality Control QC Information:

Blank Information

The blank volume is representative of the sample volume in this batch.

QC Information

All of the QC samples met the required acceptance limits.

Designated QC

The following sample was used for QC: 395827001 Torus Water #2.

Page 11 of 49 Technical Information:

Holding Time

All sample procedures for this sample set were performed within the required holding time.

Sample Re-prep/Re-analysis

None of the samples in this sample set required reprep or reanalysis.

Recounts Sample 395827001 Torus Water #2 was recounted due to a suspected false positive. The recount is reported.

Miscellaneous Information:

Data Exception DER Documentation

Data exception reports are generated to document any procedural anomalies that may deviate from referenced

SOP or contractual documents. A data exception report DER was not generated for this SDG.

Manual Integration

No manual integrations were performed on data in this batch.

Sample-Specific MDA/MDC

The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Additional Comments

Additional comments were not required for this sample set.

Qualifier Information

Manual qualifiers were not required.

Method/Analysis Information Product:

Alphaspec Am241, Cm, Liquid Analytical Method:

DOE EML HASL-300, Am-05-RC Modified Analytical Batch Number:

1562630Sample ID Client ID 395827001 Torus Water #2 1203535946 Method Blank MB 1203535948 Laboratory Control Sample LCS 1203535947 395827001Torus Water #2 Sample Duplicate DUP

The samples in this SDG were analyzed on an "as received" basis.

SOP Reference

Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as

Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with Page 12 of 49 GL-RAD-A-011 REV# 26.

Calibration Information:

Calibration Information

All initial and continuing calibration requirements have been met.

Standards Information

Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used

before the expiration dates.

Sample Geometry

All counting sources were prepared in the same geometry as the calibration standards.

Quality Control QC Information:

Blank Information

The blank volume is representative of the sample volume in this batch.

QC Information

All of the QC samples met the required acceptance limits.

Designated QC

The following sample was used for QC: 395827001 Torus Water #2.

Technical Information:

Holding Time

All sample procedures for this sample set were performed within the required holding time.

Sample Re-prep/Re-analysis

None of the samples in this sample set required reprep or reanalysis.

Recounts None of the samples in this sample set were recounted.

Miscellaneous Information:

Data Exception DER Documentation

Data exception reports are generated to document any procedural anomalies that may deviate from referenced

SOP or contractual documents. A data exception report DER was not generated for this SDG.

Manual Integration

No manual integrations were performed on data in this batch.

Sample-Specific MDA/MDC

The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Additional Comments

Additional comments were not required for this sample set.

Qualifier Information

Manual qualifiers were not required.

Page 13 of 49 Method/Analysis Information Product:

Alphaspec Np, Liquid Analytical Method:

ASTM C 1476-00 Modified Analytical Batch Number:

1562631Sample ID Client ID 395827001 Torus Water #2 1203535949 Method Blank MB 1203535951 Laboratory Control Sample LCS 1203535950 395827001Torus Water #2 Sample Duplicate DUP

The samples in this SDG were analyzed on an "as received" basis.

SOP Reference

Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as

Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with

GL-RAD-A-032 REV# 20.

Calibration Information:

Calibration Information

All initial and continuing calibration requirements have been met.

Standards Information

Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used

before the expiration dates.

Sample Geometry

All counting sources were prepared in the same geometry as the calibration standards.

Quality Control QC Information:

Blank Information

The blank volume is representative of the sample volume in this batch.

QC Information

All of the QC samples met the required acceptance limits.

Designated QC

The following sample was used for QC: 395827001 Torus Water #2.

Technical Information:

Holding Time

All sample procedures for this sample set were performed within the required holding time.

Sample Re-prep/Re-analysis Page 14 of 49 None of the samples in this sample set required reprep or reanalysis.

Recounts None of the samples in this sample set were recounted.

Miscellaneous Information:

Data Exception DER Documentation

Data exception reports are generated to document any procedural anomalies that may deviate from referenced

SOP or contractual documents. A data exception report DER was not generated for this SDG.

Manual Integration

No manual integrations were performed on data in this batch.

Sample-Specific MDA/MDC

The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Additional Comments

Additional comments were not required for this sample set.

Qualifier Information

Manual qualifiers were not required.

Method/Analysis Information Product:

Gammaspec, Gamma, Liquid Standard List Analytical Method:

EPA 901.1 Analytical Batch Number:

1561698Sample ID Client ID 395827001 Torus Water #2 1203533384 Method Blank MB 1203533386 Laboratory Control Sample LCS 1203533385 395827001Torus Water #2 Sample Duplicate DUP

The samples in this SDG were analyzed on an "as received" basis.

SOP Reference

Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as

Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with

GL-RAD-A-013 REV# 25.

Calibration Information:

Calibration Information

All initial and continuing calibration requirements have been met.

Page 15 of 49 Standards Information

Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used

before the expiration dates.

Sample Geometry

All counting sources were prepared in the same geometry as the calibration standards.

Quality Control QC Information:

Blank Information

The blank volume is representative of the sample volume in this batch.

QC Information

All of the QC samples meet the required acceptance limits with the following exceptions: Refer to Data

Exception Report DER.

Designated QC

The following sample was used for QC: 395827001 Torus Water #2.

Technical Information:

Holding Time

All sample procedures for this sample set were performed within the required holding time.

Sample Re-prep/Re-analysis

None of the samples in this sample set required reprep or reanalysis.

Recounts None of the samples in this sample set were recounted.

Miscellaneous Information:

Data Exception DER Documentation

Data exception reports are generated to document any procedural anomalies that may deviate from referenced

SOP or contractual documents. The following DER was generated for this SDG: DER 1513408 was generated

due to RDL less than MDA. The following RDLs in sample 395827001 were not achieved: Cs-134, Fe-59,

Nb-95 and Zr-95. The following RDLs in DUP 1203533385 were not achieved: Cs-134, Fe-59, Nb-95 and

Zr-95. Samples did not meet the required detection limit due to high sample activity. Reporting results.

Sample-Specific MDA/MDC

The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Additional Comments

Additional comments were not required for this sample set.

Qualifier Information

Manual qualifiers were not required.

Method/Analysis Information Page 16 of 49 Product:

Gamma I129, Liquid Analytical Method:

DOE EML HASL-300,I-01 Modified Analytical Batch Number:

1562602Sample ID Client ID 395827001 Torus Water #2 1203535843 Method Blank MB 1203535846 Laboratory Control Sample LCS 1203535844 395827001Torus Water #2 Sample Duplicate DUP 1203535845 395827001Torus Water #2 Matrix Spike MS The samples in this SDG were analyzed on an "as received" basis.

SOP Reference

Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as

Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with

GL-RAD-A-006 REV# 21.

Calibration Information:

Calibration Information

All initial and continuing calibration requirements have been met.

Standards Information

Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used

before the expiration dates.

Sample Geometry

All counting sources were prepared in the same geometry as the calibration standards.

Quality Control QC Information:

Blank Information

The blank volume is representative of the sample volume in this batch.

QC Information

All of the QC samples met the required acceptance limits.

Designated QC

The following sample was used for QC: 395827001 Torus Water #2.

Technical Information:

Holding Time

All sample procedures for this sample set were performed within the required holding time.

Sample Re-prep/Re-analysis

None of the samples in this sample set required reprep or reanalysis.

Recounts None of the samples in this sample set were recounted.

Page 17 of 49 Miscellaneous Information:

Data Exception DER Documentation

Data exception reports are generated to document any procedural anomalies that may deviate from referenced

SOP or contractual documents. A data exception report DER was not generated for this SDG.

Sample-Specific MDA/MDC

The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Additional Comments

Additional comments were not required for this sample set.

Qualifier Information

Manual qualifiers were not required.

Method/Analysis Information Product:

Gamma Ni59, Liquid Analytical Method:

DOE RESL Ni-1 Analytical Batch Number:

1562693Sample ID Client ID 395827001 Torus Water #2 1203536149 Method Blank MB 1203536151 Laboratory Control Sample LCS 1203536150 395827001Torus Water #2 Sample Duplicate DUP

The samples in this SDG were analyzed on an "as received" basis.

SOP Reference

Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as

Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with

GL-RAD-A-022 REV# 17.

Calibration Information:

Calibration Information

All initial and continuing calibration requirements have been met.

Standards Information

Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used

before the expiration dates.

Sample Geometry

All counting sources were prepared in the same geometry as the calibration standards.

Page 18 of 49 Quality Control QC Information:

Blank Information

The blank volume is representative of the sample volume in this batch.

QC Information

All of the QC samples met the required acceptance limits.

Designated QC

The following sample was used for QC: 395827001 Torus Water #2.

Technical Information:

Holding Time

All sample procedures for this sample set were performed within the required holding time.

Sample Re-prep/Re-analysis

None of the samples in this sample set required reprep or reanalysis.

Chemical Recoveries

All chemical recoveries meet the required acceptance limits for this sample set.

Recounts None of the samples in this sample set were recounted.

Miscellaneous Information:

Data Exception DER Documentation

Data exception reports are generated to document any procedural anomalies that may deviate from referenced

SOP or contractual documents. A data exception report DER was not generated for this SDG.

Sample-Specific MDA/MDC

The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Additional Comments

Additional comments were not required for this sample set.

Qualifier Information

Manual qualifiers were not required.

Method/Analysis Information Product:

GFPC, Sr89&Sr90, Liquid Analytical Method:

EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Analytical Batch Number:

1562716Sample ID Client ID Page 19 of 49 395827001 Torus Water #2 1203536197 Method Blank MB 1203536199 Laboratory Control Sample LCS 1203536198 395827001Torus Water #2 Sample Duplicate DUP The samples in this SDG were analyzed on an "as received" basis.

SOP Reference

Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as

Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with

GL-RAD-A-004 REV# 17.

Calibration Information:

Calibration Information

All initial and continuing calibration requirements have been met.

Standards Information

Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used

before the expiration dates.

Sample Geometry

All counting sources were prepared in the same geometry as the calibration standards.

Quality Control QC Information:

Blank Information

The blank volume is representative of the sample volume in this batch.

QC Information

All of the QC samples met the required acceptance limits.

Designated QC

The following sample was used for QC: 395827001 Torus Water #2.

Technical Information:

Holding Time

All sample procedures for this sample set were performed within the required holding time.

Sample Re-prep/Re-analysis

None of the samples in this sample set required reprep or reanalysis.

Chemical Recoveries

All chemical recoveries meet the required acceptance limits for this sample set.

Recounts Sample 1203536198 Torus Water #2DUP was recounted due to a suspected total strontium false positive. The

recount is reported.

Miscellaneous Information:

Data Exception DER Documentation

Data exception reports are generated to document any procedural anomalies that may deviate from referenced

SOP or contractual documents. A data exception report DER was not generated for this SDG.

Page 20 of 49

Sample-Specific MDA/MDC

The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Additional Comments

Additional comments were not required for this sample set.

Qualifier Information

Manual qualifiers were not required.

Method/Analysis Information Product:

Liquid Scint Pu241, Liquid Analytical Method:

DOE EML HASL-300, Pu-11-RC Modified Analytical Batch Number:

1562632Sample ID Client ID 395827001 Torus Water #2 1203535952 Method Blank MB 1203535954 Laboratory Control Sample LCS 1203535953 395827001Torus Water #2 Sample Duplicate DUP

The samples in this SDG were analyzed on an "as received" basis.

SOP Reference

Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as

Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with

GL-RAD-A-035 REV# 16.

Calibration Information:

Calibration Information

All initial and continuing calibration requirements have been met.

Standards Information

Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used

before the expiration dates.

Sample Geometry

All counting sources were prepared in the same geometry as the calibration standards.

Quality Control QC Information:

Blank Information

The blank volume is representative of the sample volume in this batch.

Page 21 of 49 QC Information All of the QC samples met the required acceptance limits.

Designated QC

The following sample was used for QC: 395827001 Torus Water #2.

Technical Information:

Holding Time

All sample procedures for this sample set were performed within the required holding time.

Sample Re-prep/Re-analysis

None of the samples in this sample set required reprep or reanalysis.

Recounts Samples 1203535952 MB, 1203535953 Torus Water #2DUP and 395827001 Torus Water #2 were

recounted due to high MDCs. The recounts are reported.

Miscellaneous Information:

Data Exception DER Documentation

Data exception reports are generated to document any procedural anomalies that may deviate from referenced

SOP or contractual documents. A data exception report DER was not generated for this SDG.

Manual Integration

No manual integrations were performed on data in this batch.

Sample-Specific MDA/MDC

The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Additional Comments

Additional comments were not required for this sample set.

Qualifier Information

Manual qualifiers were not required.

Method/Analysis Information Product:

Liquid Scint Fe55, Liquid Analytical Method:

DOE RESL Fe-1, Modified Analytical Batch Number:

1562672Sample ID Client ID 395827001 Torus Water #2 1203536076 Method Blank MB 1203536078 Laboratory Control Sample LCS 1203536077 395827001Torus Water #2 Sample Duplicate DUP Page 22 of 49 The samples in this SDG were analyzed on an "as received" basis.

SOP Reference

Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as

Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with

GL-RAD-A-040 REV# 12.

Calibration Information:

Calibration Information

All initial and continuing calibration requirements have been met.

Standards Information

Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used

before the expiration dates.

Sample Geometry

All counting sources were prepared in the same geometry as the calibration standards.

Quality Control QC Information:

Blank Information

The blank volume is representative of the sample volume in this batch.

QC Information

All of the QC samples met the required acceptance limits.

Designated QC

The following sample was used for QC: 395827001 Torus Water #2.

Technical Information:

Holding Time

All sample procedures for this sample set were performed within the required holding time.

Sample Re-prep/Re-analysis

None of the samples in this sample set required reprep or reanalysis.

Recounts None of the samples in this sample set were recounted.

Miscellaneous Information:

Data Exception DER Documentation

Data exception reports are generated to document any procedural anomalies that may deviate from referenced

SOP or contractual documents. A data exception report DER was not generated for this SDG.

Sample-Specific MDA/MDC

The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Additional Comments

Additional comments were not required for this sample set.

Page 23 of 49 Qualifier Information Manual qualifiers were not required.

Method/Analysis Information Product:

Liquid Scint Ni63, Liquid Analytical Method:

DOE RESL Ni-1, Modified Analytical Batch Number:

1562678Sample ID Client ID 395827001 Torus Water #2 1203536092 Method Blank MB 1203536094 Laboratory Control Sample LCS 1203536093 395827001Torus Water #2 Sample Duplicate DUP

The samples in this SDG were analyzed on an "as received" basis.

SOP Reference

Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as

Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with

GL-RAD-A-022 REV# 17.

Calibration Information:

Calibration Information

All initial and continuing calibration requirements have been met.

Standards Information

Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used

before the expiration dates.

Sample Geometry

All counting sources were prepared in the same geometry as the calibration standards.

Quality Control QC Information:

Blank Information

The blank volume is representative of the sample volume in this batch.

QC Information

All of the QC samples met the required acceptance limits.

Designated QC

The following sample was used for QC: 395827001 Torus Water #2.

Page 24 of 49 Technical Information:

Holding Time

All sample procedures for this sample set were performed within the required holding time.

Sample Re-prep/Re-analysis

None of the samples in this sample set required reprep or reanalysis.

Recounts None of the samples in this sample set were recounted.

Miscellaneous Information:

Data Exception DER Documentation

Data exception reports are generated to document any procedural anomalies that may deviate from referenced

SOP or contractual documents. A data exception report DER was not generated for this SDG.

Sample-Specific MDA/MDC

The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Additional Comments

Additional comments were not required for this sample set.

Qualifier Information

Manual qualifiers were not required.

Method/Analysis Information Product:

Liquid Scint Tc99, Liquid Analytical Method:

DOE EML HASL-300, Tc-02-RC Modified Analytical Batch Number:

1562683Sample ID Client ID 395827001 Torus Water #2 1203536111 Method Blank MB 1203536113 Laboratory Control Sample LCS 1203536112 395827001Torus Water #2 Sample Duplicate DUP

The samples in this SDG were analyzed on an "as received" basis.

SOP Reference

Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as

Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with

GL-RAD-A-059 REV# 4.

Page 25 of 49 Calibration Information:

Calibration Information

All initial and continuing calibration requirements have been met.

Standards Information

Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used

before the expiration dates.

Sample Geometry

All counting sources were prepared in the same geometry as the calibration standards.

Quality Control QC Information:

Blank Information

The blank volume is representative of the sample volume in this batch.

QC Information

All of the QC samples meet the required acceptance limits with the following exceptions: Refer to Data

Exception Report DER.

Designated QC

The following sample was used for QC: 395827001 Torus Water #2.

Technical Information:

Holding Time

All sample procedures for this sample set were performed within the required holding time.

Sample Re-prep/Re-analysis

None of the samples in this sample set required reprep or reanalysis.

Recounts Samples were recounted due to high relative percent difference/relative error ratio. The recount results are

similar to the original results. Original results are reported.

Miscellaneous Information:

Data Exception DER Documentation

A data exception report DER 1517546 was generated for samples in this SDG/batch. DER 1517546 was

generated due to Failed RPD for DUP. 1. Sample 395827001 and duplicate 1203536112 do not meet the relative

percent difference requirement or the relative error ratio requirement due to the matrix of the sample. 1.

Reporting results.

Sample-Specific MDA/MDC

The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Additional Comments

Additional comments were not required for this sample set.

Qualifier Information

Manual qualifiers were not required.

Page 26 of 49 Method/Analysis Information Product:

LSC, Tritium Dist, Liquid Analytical Method:

EPA 906.0 Modified Analytical Batch Number:

1562687Sample ID Client ID 395827001 Torus Water #2 1203536126 Method Blank MB 1203536129 Laboratory Control Sample LCS 1203536127 395827001Torus Water #2 Sample Duplicate DUP 1203536128 395827001Torus Water #2 Matrix Spike MS The samples in this SDG were analyzed on an "as received" basis.

SOP Reference

Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as

Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with

GL-RAD-A-002 REV# 21.

Calibration Information:

Calibration Information

All initial and continuing calibration requirements have been met.

Standards Information

Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used

before the expiration dates.

Sample Geometry

All counting sources were prepared in the same geometry as the calibration standards.

Quality Control QC Information:

Blank Information

The blank volume is representative of the sample volume in this batch.

QC Information

All of the QC samples meet the required acceptance limits with the following exceptions: The Matrix Spike

1203536128 Torus Water #2MS did not meet recovery requirements due to the sample activity being greater

than five times the spiked nominal concentration.

Designated QC

The following sample was used for QC: 395827001 Torus Water #2.

Technical Information:

Holding Time

All sample procedures for this sample set were performed within the required holding time.

Page 27 of 49 Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Recounts Sample 1203536129 LCS was recounted due to low recovery. The recount is reported.

Miscellaneous Information:

Data Exception DER Documentation

Data exception reports are generated to document any procedural anomalies that may deviate from referenced

SOP or contractual documents. A data exception report DER was not generated for this SDG.

Sample-Specific MDA/MDC

The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Additional Comments

The matrix spike, 1203536128 Torus Water #2MS, aliquot was reduced to conserve sample volume.

Qualifier Information

Manual qualifiers were not required.

Method/Analysis Information Product:

Liquid Scint C14, Liquid Analytical Method:

EPA EERF C-01 Modified Analytical Batch Number:

1562691Sample ID Client ID 395827001 Torus Water #2 1203536141 Method Blank MB 1203536144 Laboratory Control Sample LCS 1203536142 395827001Torus Water #2 Sample Duplicate DUP 1203536143 395827001Torus Water #2 Matrix Spike MS

The samples in this SDG were analyzed on an "as received" basis.

SOP Reference

Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as

Standard Operating Procedure SOP. The data discussed in this narrative has been analyzed in accordance with

GL-RAD-A-003 REV# 15.

Calibration Information:

Calibration Information

All initial and continuing calibration requirements have been met.

Page 28 of 49 Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used

before the expiration dates.

Sample Geometry

All counting sources were prepared in the same geometry as the calibration standards.

Quality Control QC Information:

Blank Information

The blank volume is representative of the sample volume in this batch.

QC Information

All of the QC samples met the required acceptance limits.

Designated QC

The following sample was used for QC: 395827001 Torus Water #2.

Technical Information:

Holding Time

All sample procedures for this sample set were performed within the required holding time.

Sample Re-prep/Re-analysis

None of the samples in this sample set required reprep or reanalysis.

Recounts None of the samples in this sample set were recounted.

Miscellaneous Information:

Data Exception DER Documentation

Data exception reports are generated to document any procedural anomalies that may deviate from referenced

SOP or contractual documents. A data exception report DER was not generated for this SDG.

Manual Integration

No manual integrations were performed on data in this batch.

Sample-Specific MDA/MDC

The MDA/MDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Additional Comments

Additional comments were not required for this sample set.

Qualifier Information

Manual qualifiers were not required.

Certification Statement

Where the analytical method has been performed under NELAP certification, the analysis has met all of the

requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Page 29 of 49 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com VERM001 Vermont Yankee, Entergy Nuclear Operations Inc.

Client SDG: 395827 GEL Work Order: 395827 Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Erin Trent.

Reviewed by Sample(s) Contained within this report:

395827001Lab Sample IDClient Sample ID Sample Description Torus Water #2 N/ACollected 04/11/2016 09:10 Signature:

Name:Date:Title:05 MAY 2016 Theresa Austin Group Leader Page 30 of 49 1513408DER Report No.:

1Revision No.:

Spencer Collins Originator's Name:

22-APR-16 Shenise Gerideau

Data Validator/Group Leader:

22-APR-16 Instrument Type:

Client Code:

Quality Criteria:

GAMMA SPECTROMETER Specifications VERMType:ProcessDivision:

Radiochemistry Mo.Day Yr.

22-APR-16 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT DER Disposition:

Samples did not meet the required detection limit due to high sample

activity. Reporting results.

Specification and Requirements

Exception

Description:

The following RDLs in sample 395827001 were not achieved: Cs-134,

Fe-59, Nb-95 and Zr-95.

The following RDLs in DUP 1203533385 were not achieved: Cs-134,

Fe-59, Nb-95 and Zr-95.

Application Issues:

RDL less than MDA Batch ID:

1561698Test / Method:

EPA 901.1 LiquidMatrix Type:

See Below

Sample Numbers:Potentially affected work order(s)(SDG):395827 Page 31 of 49 1517546DER Report No.:

2Revision No.:

Elizabeth Krouse Originator's Name:

05-MAY-16 Lyndsey Pace

Data Validator/Group Leader:

05-MAY-16 Instrument Type:

Client Code:

Quality Criteria:

LSCSpecifications VERMType:ProcessDivision:

Radiochemistry Mo.Day Yr.

05-MAY-16 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT DER Disposition:

1. Reporting results.

Specification and Requirements

Exception

Description:

1. Sample 395827001 and duplicate 1203536112 do not meet the relative

percent difference requirement or the relative error ratio requirement due

to the matrix of the sample.

Application Issues:

Failed RPD for DUP Batch ID:

1562683Test / Method:

DOE EML HASL-300, Tc-02-RC ModifiedLiquidMatrix Type:

See Below

Sample Numbers:Potentially affected work order(s)(SDG):395827 Page 32 of 49 Sample Data Summary Page 33 of 49 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Note(s):1. Calculated MDAs are a-posteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the

sample collect date.

3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.

10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:

Matrix:Geometry Received:

Client:Collect Date:

Receive Date:

Client Sample ID:

395827001 WaterVermont Yankee, Entergy Nuclear Operatio April 11, 2016 April 21, 2016 Torus Water #2 Report Date:

May 05, 2016AnalyteRun Date ActivityMDAQualifier 2 SigmaUncertainty RL Alpha Spec Gamma Spec H-3C-14Fe-55Ni-63Sr-89Sr-90Tc-99Pu-241Np-237Pu-238Pu-239/240 Pu-242Am-241Cm-242Cm-243/244 Be-7Na-22K-40Cr-51Mn-54Fe-59Co-56Co-57 Co-58Co-60Ni-59Zn-65Y-88Zr-95Nb-94Nb-95Ru-106Ag-110mSn-11304/29/1605/03/1604/28/1604/29/1605/02/1605/02/1605/03/1605/04/1604/30/1605/02/1605/02/1605/02/1604/30/1604/30/1604/30/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/16 04/21/1604/21/1604/28/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/16 1.70E+06 1.49E+01 9.53E+01 7.94E+02 1.08E+00 3.31E-01 3.89E+03 7.38E+00

-1.66E-01 1.96E-02

4.85E-02 1.91E-01 4.31E-02 0.00E+00

-5.11E-03 3.92E+01

6.07E+00 1.14E+01 3.07E+01 4.71E+02 2.87E+01 7.28E+00 3.24E+00

9.00E+01 2.07E+04 5.85E+00 1.95E+03

-1.32E+00 2.37E+01

-7.62E+00 6.97E+00 3.19E+01

-4.46E+00 9.02E+00 3.33E+04 2.41E+01 6.05E+01 7.12E+01 1.29E+00 9.80E-01 9.37E+01 1.13E+01 3.14E-01 2.14E-01 2.13E-01 2.99E-01 7.39E-02 4.66E-02 4.41E-02 9.40E+01 7.93E+00 5.16E+01 9.82E+01 2.43E+01 3.55E+01 1.52E+01 7.66E+00

2.06E+01 7.10E+01 6.40E+00 6.85E+01 5.08E+00 2.40E+01 1.13E+01 1.34E+01 1.04E+02 2.14E+01 1.28E+01 1.75E+03 4.08E+01 8.07E+01 7.04E+01 2.18E+00 2.66E+00 4.26E+01 1.91E+01 9.68E-01 4.50E-01 3.86E-01 4.10E-01 6.47E-02 6.93E-02 1.02E-01 1.59E+02 1.35E+01 8.56E+01 1.69E+02 2.38E+01 6.01E+01 2.61E+01 1.28E+01

2.46E+01 1.26E+01 1.01E+01 5.59E+01 8.67E+00 4.17E+01 1.84E+01 2.31E+01 1.72E+02 3.65E+01 2.19E+01 2.00E+03 5.00E+01 1.10E+02 5.30E+02 2.30E+01 3.50E+00 5.00E+01 2.50E+01 1.50E+01 1.50E+01 1.50E+01 1.50E+01 1.50E+01 1.50E+01 1.50E+01 1.50E+01 3.00E+01 1.50E+01 1.50E+01 2.00E+01 3.00E+01 3.00E+01

1.50E+01 3U33U U3UUUUUUUUUUUU3UUU33U3U UUUUUU12pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/L pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LUnitsPage 34 of 49 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Note(s):1. Calculated MDAs are a-posteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the

sample collect date.

3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.

10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:

Matrix:Geometry Received:

Client:Collect Date:

Receive Date:

Client Sample ID:

395827001 WaterVermont Yankee, Entergy Nuclear Operatio April 11, 2016 April 21, 2016 Torus Water #2 Report Date:

May 05, 2016AnalyteRun Date ActivityMDAQualifier 2 SigmaUncertainty RLSb-124Sb-125I-129Cs-134Cs-136Cs-137Ba-133Ba-140Ce-139Ce-141Ce-144Nd-147Pm-144Pm-146Eu-152Eu-154Eu-155Ir-192Hg-203Tl-208Pb-210Pb-212Pb-214 Bi-212Bi-214Ra-228Ac-228Th-234U-235U-238Np-239Am-24104/21/1604/21/1604/27/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/16 04/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/1604/21/16 -3.65E+00 8.30E+00

-3.73E-02

-1.30E+01 5.93E+00

1.13E+03

-7.26E+00

-1.12E+01

-8.99E+00

-9.12E+00 3.42E+01

-8.63E+01 1.21E+00

4.46E+00 1.35E+01 1.78E+01 1.43E+01

-2.79E+00 8.62E+00 8.75E+00 9.04E+02

-1.47E+00

-6.77E+00

-6.90E+01

-1.64E+00 4.22E+01

4.22E+01 3.77E+02

-3.80E+01 3.77E+02 7.01E+01

-2.43E+01 1.09E+01

2.74E+01 8.59E-01 1.47E+01 3.45E+01 2.43E+01 1.32E+01 6.57E+01 8.66E+00 1.67E+01 5.98E+01 1.33E+02 1.14E+01 1.29E+01 2.86E+01 2.25E+01 3.04E+01 9.96E+00 1.07E+01 1.20E+01 1.07E+03 1.92E+01 2.15E+01

1.77E+02 2.21E+01 6.30E+01 6.30E+01 3.56E+02 5.95E+01 3.56E+02 7.43E+01 4.16E+01 1.88E+01 4.64E+01 1.51E+00 2.52E+01 5.84E+01 2.06E+01 2.09E+01 1.10E+02 1.42E+01 2.77E+01 9.96E+01 2.22E+02 1.88E+01 2.19E+01 4.91E+01 3.83E+01 5.10E+01 1.71E+01 1.86E+01 1.91E+01 1.84E+03 3.09E+01 3.65E+01

2.89E+02 3.64E+01 1.08E+02 1.08E+02 5.78E+02 9.77E+01 5.78E+02 1.32E+02 7.09E+01 2.00E+00 1.50E+01 1.80E+01 UUUUU3UUUUUUUUUUUUUUUUU UUUU3,UU3,UUU12pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/L pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LUnitsPage 35 of 49 GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:

Matrix:Client:Collect Date:

Receive Date:

Client Sample ID:

395827001 WaterVermont Yankee, Entergy Nuclear Operations Inc.

April 11, 2016 April 21, 2016 Torus Water #2 AnalyteActivity Alpha Spec Gamma Spec Ni-63Tc-99 H-3Cs-137Co-60Mn-54Zn-65 7.94E+02 3.89E+03

1.70E+06 1.13E+03 2.07E+04 4.71E+02 1.95E+03 pCi/LpCi/L pCi/LpCi/LpCi/LpCi/LpCi/LUnits% Abundance 000.05 000.22 098.31 000.07 001.20 000.03 000.11Total Activity: 1.73E+06Total % Abundance: 100.00 Page 36 of 49 Quality Control SummaryPage 37 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Alpha Spec 15626291562630Batch BatchPlutonium-238 Plutonium-239/240

Plutonium-242 Plutonium-238 Plutonium-239/240

Plutonium-242 Plutonium-238 Plutonium-239/240

Plutonium-242 Americium-241 Curium-242 Curium-243/244 Americium-241 Curium-242

Curium-243/244 Americium-241 Curium-242 ParmnameMr. Mark Vandale Contact:Entergy Nuclear Operations, Inc., VY 530 Governor Hunt Road Vernon, Vermont May 5, 2016 Report Date:

Units pCi/LpCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LAnlstDateTimeMXS2MXS204/30/16 11:03 04/30/16 11:03 04/30/16 11:05 04/30/16 11:05 04/30/16 11:08 04/30/16 11:05 QC0.1320.08240.07630.04755.710.05450.0605-0.01350.02150.07650.000.02525.270.01446.220.0246-0.00542NOMSample0.01960.04850.1910.04310.00-0.00511RangeN/A N/A N/A(75%-125%)

N/AN/AN/A(75%-125%)

(75%-125%)

QualUU UUUUU UUUU UUQC1203535940 395827001 QC1203535941 QC1203535939 QC1203535947 395827001 QC1203535948 QC1203535946 N/AN/AN/A16.6N/AN/AREC%11610794.14.94 4.936.61DUPLCSMBDUPLCS MB395827Workorder:

PO Box 250 UUUUU U+/-0.214

+/-0.213+/-0.299+/-0.0739

+/-0.0466

+/-0.0441

+/-0.142

+/-0.113+/-0.113+/-0.107+/-0.770

+/-0.108+/-0.0977

+/-0.0611

+/-0.0828

+/-0.101+/-0.055+/-0.0707

+/-0.623+/-0.0539

+/-0.671+/-0.0949

+/-0.0468 RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty

Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty

Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page 1 of 12 Page 38 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Alpha Spec Rad Gamma Spec 1562630156263115626321561698BatchBatchBatchBatchCurium-243/244 Neptunium-237 Neptunium-237

Neptunium-237 Plutonium-241 Plutonium-241 Plutonium-241 Actinium-228 Americium-241 Antimony-124

Antimony-125

Barium-133

Barium-140 Beryllium-7 Bismuth-212

Bismuth-214

Cerium-139 ParmnameUnits pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LAnlstDateTimeMXS2MXS2MJH104/30/16 10:57 04/30/16 10:59

04/30/16 10:57 05/04/16 15:25 05/03/16 14:19 05/04/16 13:54 04/22/16 06:34 QC0.006290.22591.80.0941-1.65216-1.4-83.9-30.21.84-5.76-11.255.051.4 27.2 1.581.86NOMSample-0.1667.3842.2-24.3-3.658.30-7.26

-11.239.2-69-1.64-8.99RangeN/A(75%-125%)

N/A(75%-125%)

N/A N/AN/A N/A N/A N/AN/AN/A N/A N/AQualUUUUUUUUU U

U U

UUUQC1203535950 395827001 QC1203535951

QC1203535949 QC1203535953 395827001 QC1203535954 QC1203535952 QC1203533385 395827001 N/AN/AN/AN/A N/A N/A N/AN/AN/A N/A N/A N/AREC%10311189.3194DUPLCSMBDUPLCSMBDUP395827Workorder:

UUUU U

U UUU U

U U+/-0.314+/-11.3+/-63.0+/-41.6

+/-10.9

+/-27.4

+/-13.2+/-65.7+/-94.0+/-177+/-22.1

+/-8.66+/-0.0657

+/-0.654+/-6.94+/-0.422+/-7.13+/-27.4

+/-7.62+/-95.8+/-50.5

+/-15.8

+/-41.9

+/-20.8+/-103

+/-144

+/-257+/-34.0

+/-12.7RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Page 2 of 12 Page 39 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1561698BatchCerium-141 Cerium-144 Cesium-134 Cesium-136

Cesium-137

Chromium-51

Cobalt-56 Cobalt-57 Cobalt-58

Cobalt-60

Europium-152

Europium-154 Europium-155 Iridium-192

Iron-59 Lead-210 Lead-212Lead-214Manganese-54

Mercury-203

Neodymium-147

Neptunium-239 ParmnameUnits pCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/LAnlstDateTimeMJH104/22/16 06:34 QC-1216.8-8.32

-39.411503.78 5.84 6.90 89.120400-7.8117.7 20.9-2.06-55.9-4140.3657.394810.957-52.1-65.9NOMSample-9.1234.2-135.93113030.7 7.28 3.24 90.02070013.5 17.8 14.3-2.7928.7904-1.47

-6.774718.62-86.370.1RangeN/A N/AN/AN/A(0%-20%)N/A N/AN/A(0% - 100%)

(0%-20%)N/AN/AN/AN/A N/A N/A N/AN/A(0%-20%)N/AN/A N/AQualU U

UUUU UUU UUU U

U UUU UN/AN/AN/A N/A2.28N/AN/AN/A0.9821.55N/AN/AN/A N/A N/A N/AN/AN/A1.95N/A N/AN/AREC%395827Workorder:

U UU UUUUUUU U

U UUUUUU+/-16.7

+/-59.8+/-14.7

+/-34.5

+/-24.3

+/-98.2+/-15.2+/-7.66

+/-20.6

+/-71.0

+/-28.6+/-22.5+/-30.4

+/-9.96

+/-35.5+/-1070+/-19.2

+/-21.5

+/-24.3

+/-10.7+/-133+/-74.3+/-24.6+/-87.5+/-22.6

+/-53.9

+/-36.7+/-147+/-23.3

+/-12.0

+/-28.7+/-103+/-42.7+/-31.6+/-44.2

+/-15.4

+/-53.1+/-1020+/-26.2

+/-32.0

+/-36.4

+/-15.9+/-208+/-115RPD%Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty Page 3 of 12 Page 40 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1561698BatchNiobium-94 Niobium-95 Potassium-40 Promethium-144

Promethium-146

Radium-228

Ruthenium-106 Silver-110m Sodium-22

Thallium-208

Thorium-234

Tin-113Uranium-235 Uranium-238

Yttrium-88

Zinc-65 Zirconium-95 Actinium-228 Americium-241

Antimony-124

Antimony-125

Barium-133 ParmnameUnits pCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/LAnlstDateTimeMJH104/22/16 06:34 04/22/16 06:39 QC14.9 22.9 16.1 1.11-18.9

-83.913640.9 6.22-15.11550.62216.4155-5.551870-5.381223970015.9-15727.6NOMSample-7.626.97 11.4 1.214.4642.2 31.9-4.466.078.753779.02-38377-1.32195023.7RangeN/AN/AN/AN/A N/A N/A N/AN/AN/A N/A N/A N/AN/AN/A N/A(0%-20%)N/A(75%-125%)

QualU U

UUU U

U UUU U

U UUUUUUU UQC1203533386 N/AN/AN/A N/A N/A N/AN/AN/A N/A N/A N/AN/AN/A N/A N/A3.98N/AREC%11534400LCS395827Workorder:

UUU U

U UUU U

U UUU U

UU+/-11.3+/-13.4+/-51.6

+/-11.4

+/-12.9

+/-63.0+/-104+/-21.4

+/-7.93

+/-12.0+/-356+/-12.8

+/-59.5+/-356+/-5.08

+/-68.5+/-24.0+/-16.4

+/-23.5+/-69.1

+/-16.5

+/-19.7

+/-95.8+/-159+/-33.1

+/-11.1

+/-19.0+/-425+/-19.4

+/-85.7+/-425+/-7.20

+/-96.7+/-36.8+/-399+/-1740+/-46.1+/-241RPD%Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty Uncertainty Page 4 of 12 Page 41 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1561698BatchBarium-140 Beryllium-7 Bismuth-212

Bismuth-214

Cerium-139

Cerium-141 Cerium-144 Cesium-134

Cesium-136

Cesium-137

Chromium-51 Cobalt-56 Cobalt-57

Cobalt-58

Cobalt-60

Europium-152 Europium-154 Europium-155

Iridium-192

Iron-59 Lead-210ParmnameUnits pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/LAnlstDateTimeMJH104/22/16 06:39 QC153-119540-68.543.7-75.7-26823.7-66.413700-19981.9267-46.914200-10143.314657.9 45.34.51E+05NOMSampleRange(75%-125%)

(75%-125%)

QualUUUU U

U UUUUUUUUUU UREC%10210313500 13800395827Workorder:

+/-103+/-282+/-768+/-1080+/-142+/-66.4+/-112

+/-478+/-94.4+/-158

+/-354+/-630+/-88.7+/-108+/-87.5+/-408

+/-237+/-136

+/-300+/-74.3+/-199+/-50700RPD%Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty Page 5 of 12 Page 42 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1561698BatchLead-212Lead-214Manganese-54 Mercury-203

Neodymium-147

Neptunium-239

Niobium-94 Niobium-95 Potassium-40

Promethium-144

Promethium-146

Radium-228 Ruthenium-106 Silver-110m

Sodium-22

Thallium-208

Thorium-234 Tin-113Uranium-235

Uranium-238

Yttrium-88

Zinc-65ParmnameUnits pCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/LAnlstDateTimeMJH104/22/16 06:39 QC-41.7

-66.522.0-25.5-2593569.74 28.1-26.76.91-31.7122 16678.214.5-13.8-1950-66.5147-1950-3.091030NOMSampleRangeQualUU UUU U

U UUU U

U UUU U

U UUU UREC%395827Workorder:

+/-143+/-183+/-87.1+/-77.1+/-538

+/-781+/-68.8

+/-77.3+/-253+/-68.5+/-124+/-399+/-727

+/-140+/-47.5

+/-73.8+/-5510+/-108

+/-479+/-5510+/-28.7+/-363RPD%Uncertainty

Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty Page 6 of 12 Page 43 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1561698BatchZirconium-95 Actinium-228 Americium-241 Antimony-124

Antimony-125

Barium-133

Barium-140 Beryllium-7 Bismuth-212

Bismuth-214

Cerium-139

Cerium-141 Cerium-144 Cesium-134

Cesium-136

Cesium-137

Chromium-51 Cobalt-56 Cobalt-57

Cobalt-58

Cobalt-60

Europium-152 ParmnameUnits pCi/LpCi/LpCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/LAnlstDateTimeMJH104/22/16 06:34 QC31.9-7.16

-1.73-0.03870.9600.347-0.895-8.8614.21.92-0.5332.38 5.240.137-1.240.1341.840.706-0.1720.6801.03 1.98NOMSampleRangeQualUUUUU U

U U

UUU U

U UUU U

U UUU UQC1203533384 REC%MB395827Workorder:

+/-141+/-8.38

+/-9.55

+/-2.87

+/-4.35

+/-2.37+/-6.51+/-12.3

+/-25.1

+/-4.84

+/-1.59+/-2.53+/-10.6

+/-1.84

+/-2.06

+/-1.80+/-13.4+/-1.49

+/-1.53

+/-1.64

+/-1.93RPD%Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Page 7 of 12 Page 44 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1561698BatchEuropium-154 Europium-155 Iridium-192

Iron-59 Lead-210 Lead-212Lead-214Manganese-54

Mercury-203

Neodymium-147

Neptunium-239 Niobium-94 Niobium-95

Potassium-40

Promethium-144

Promethium-146 Radium-228 Ruthenium-106

Silver-110m

Sodium-22

Thallium-208 ParmnameUnits pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/L pCi/L pCi/LpCi/LpCi/L pCi/LAnlstDateTimeMJH104/22/16 06:34 QC-0.771-2.76-0.3172.12-1321.26 1.93-0.121.53-3.95-0.573

-0.765-0.074314.30.643 0.158-7.16

-15.7-0.238

-0.342-2.26NOMSampleRangeQualU UUU U

U UUU U

U UUU U

U UUU U

UREC%395827Workorder:

+/-4.87+/-4.66+/-6.43

+/-1.62

+/-2.97+/-275+/-4.97

+/-5.83

+/-1.62

+/-1.59

+/-11.0+/-14.9+/-1.67

+/-1.40

+/-24.8

+/-1.79+/-2.18+/-8.38

+/-18.9

+/-1.98

+/-1.62+/-2.16RPD%Uncertainty Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty Page 8 of 12 Page 45 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec Rad Gas Flow 1561698156260215626931562716BatchBatchBatchBatchThorium-234 Tin-113Uranium-235 Uranium-238

Yttrium-88

Zinc-65 Zirconium-95 Iodine-129 Iodine-129 Iodine-129

Iodine-129 Nickel-59 Nickel-59

Nickel-59 Strontium-89 Strontium-90 Strontium-89 ParmnameUnits pCi/LpCi/L pCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/L pCi/L pCi/LpCi/LpCi/L pCi/LpCi/LpCi/LpCi/LAnlstDateTimeMJH1MJH1CXS7KSD104/22/16 06:34

04/27/16 09:20 04/27/16 11:04 04/27/16 09:19

04/27/16 09:20 04/28/16 15:36 04/29/16 06:45

04/28/16 15:36 05/02/16 16:24 05/02/16 16:24 QC60.30.153-0.38860.3-0.7980.806-1.70.38850.2-0.1757.53.143722.87-1.39-0.222550NOMSample-0.0373-0.03735.851.080.331RangeN/A(75%-125%)

(75%-125%)

N/A(75%-125%)

N/AN/A(75%-125%)

QualU U

UUU U

UUUUUUUQC1203535844 395827001 QC1203535846 QC1203535843 QC1203535845 395827001 QC1203536150 395827001 QC1203536151

QC1203536149 QC1203536198 395827001 QC1203536199 N/AN/AN/AN/AREC%96.411188.810552.052.0419522DUPLCSMBMSDUPLCSMBDUPLCS395827Workorder:

UUUUU+/-0.859+/-0.859+/-6.40+/-1.29+/-0.980+/-140+/-2.10+/-13.5+/-140+/-1.85

+/-3.61+/-2.56+/-1.13+/-6.44+/-0.835+/-6.83+/-2.49+/-26.7

+/-5.02+/-1.93+/-1.22RPD%Uncertainty

Uncertainty

Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty

Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty Uncertainty Uncertainty Page 9 of 12 Page 46 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gas Flow Rad Liquid Scintillation 1562716156267215626781562683 1562687BatchBatchBatchBatch BatchStrontium-90 Strontium-89 Strontium-90 Iron-55Iron-55 Iron-55Nickel-63 Nickel-63

Nickel-63 Technetium-99 Technetium-99

Technetium-99 TritiumTritiumParmnameUnits pCi/L pCi/LpCi/LpCi/LpCi/L pCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LpCi/LAnlstDateTimeKSD1CXS7CXS7MYM1GXR105/02/16 16:24 05/02/16 16:27 04/28/16 23:26 04/29/16 00:13

04/28/16 22:39 04/29/16 14:53 04/29/16 15:09

04/29/16 14:37 05/03/16 15:12 05/03/16 15:28

05/03/16 14:55 04/29/16 23:11 04/30/16 11:54 QC445-1.50.11691.21440-42.58402090-6.46254841-11.41.72E+062410NOMSample95.379438901.70E+06Range(75%-125%)

(0% - 100%)

(75%-125%)

(0%-20%)(75%-125%)

(0%-20%)(75%-125%)

(0%-20%)(75%-125%)

QualUUUU UQC1203536197 QC1203536077 395827001 QC1203536078

QC1203536076 QC1203536093 395827001 QC1203536094

QC1203536092 QC1203536112 395827001 QC1203536113

QC1203536111 QC1203536127 395827001 QC1203536129 4.425.651751.36REC%8386.812497.71025361660 16908612350MBDUPLCSMBDUPLCS MBDUPLCS MBDUPLCS395827Workorder:

+/-60.5+/-71.2

+/-93.7+/-33300+/-13.0+/-10.4+/-1.18+/-1.00+/-58.8+/-86.2

+/-58.1+/-71.1+/-101+/-37.6

+/-33.3+/-48.9

+/-24.1+/-33700+/-461*RPD%Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty Uncertainty Uncertainty

Uncertainty Uncertainty Uncertainty Page 10 of 12 Page 47 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Liquid Scintillation 15626871562691Batch BatchTritiumTritiumCarbon-14 Carbon-14

Carbon-14

Carbon-14 ParmnameUnits pCi/LpCi/LpCi/LpCi/LpCi/L pCi/LAnlstDateTimeGXR1TXJ104/29/16 22:55

04/29/16 23:13 05/03/16 17:23 05/03/16 18:26

05/03/16 16:51

05/03/16 17:54 QC1361.62E+0628.01310-4.591400NOMSample1.70E+0614.914.9Range(75%-125%)

N/A(75%-125%)

(75%-125%)

QualUUUQC1203536126 QC1203536128 395827001 QC1203536142 395827001 QC1203536144

QC1203536141

QC1203536143 395827001 The Qualifiers in this report are defined as follows:

N/AREC%N/A103111471012601260MBMSDUPLCSMBMS395827Workorder:

    • <

>

BDFAH J

KLM MN/AN1 ND NJQR UAnalyte is a Tracer compound

Result is less than value reported

Result is greater than value reported Results are either below the MDC or tracer recovery is low Failed analysis.

Analytical holding time was exceeded

Value is estimated Analyte present. Reported value may be biased high. Actual value is expected to be lower.

Analyte present. Reported value may be biased low. Actual value is expected to be higher.

M if above MDC and less than LLD

REMP Result > MDC/CL and < RDL RPD or %Recovery limits do not apply.

See case narrative

Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER.

Sample results are rejected

Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.

UU+/-33300+/-24.1+/-24.1+/-301+/-31600+/-24.9+/-47.0

+/-23.6

+/-49.8RPD%Uncertainty

Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Notes:Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).

Page 11 of 12 Page 48 of 49 QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com ParmnamePage 12 of 12 Units AnlstDateTimeQCNOMSampleRangeQualREC%395827Workorder:

UIUJUL X

Y^hGamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.

Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Other specific qualifiers were required to properly define the results. Consult case narrative.

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.

Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable.

^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.

  • Indicates that a Quality Control parameter was not within specifications.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

RPD%Page 49 of 49

Retrieved from "https://kanterella.com/w/index.php?title=ML16231A028&oldid=762540"