ML20133H830

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Application for License,Authorizing U-235,U308,National Bureau of Stds Samples 15g of U Containing 5.16g of U-235, 200 Uci Max
ML20133H830
Person / Time
Site: 07000299
Issue date: 04/06/1960
From: Johari Moore
MALLINCKRODT, INC.
To:
Shared Package
ML20133G976 List: ... further results
References
FOIA-96-343 NUDOCS 9701170306
Download: ML20133H830 (5)
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APPLKATION FOR BYPRODUCT MATERIAL LKENSE

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INSTRUCTIONS.-Complete items 1 through 16 if this is en initial application. If opplication is los renewal of a license, com-plete only items 1 through 7 ond indicoto new enformation or changes in the program os requested in items b throwsh 15. Use supplemental sheets where necessery. ltem 16 must be conipleted en cil applications. Mail tease copies to: U 5. Atomic Energy D. C. Attention: Isotopes Branch, Division of Licensing and Regulation. Upon opproval of this Commission, Washington 25, ll receive on AEC Byproduct Material License. An AEC Byproduct Material License is issued in applictdion, the opplicent wi accordance with ehe general requirements contained in Title 10, Code of Federal Regulations, Port 30 and the Licensee is sub-lect to Title 10, Code of Federal Regulations, Port 20.

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i Mallinckrodt Chemical Works 3600 North Second Street Ste Louis 7, Missouri i

2. DGPAATMENT TO USE SYPeOOUCT MAtletAL 3 PtiviOUS LICIN54 NUmste($k (W fws 4 on appl.co#.an for renewaf ed e f cease. pas.ee sidesse med yve awaber )

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    • "*"""*""'d'i leDr. Perry King, Radiochemist, Optical and other Physical Methods I,aboratory.
3. Mre Joe We Miller l
2. Mr. Dyron De Fielci.

Head of Industrial Hygiene Department Head, Optical and Cther Physical Methods Laboratory.

'e (e) OYPeOOUCf MAff AIAL (Insa.ents

[b) CHEAMCAL AN0/OG PHY54 CAL FOGM AND MAAlMUM NUMMA Of MILUCUttf 5 OF EACH CHEMICAL AN0/OE PH (W se. led sewee(si eine s** n me ei manviern,ry, menisi be,. -6.r.,YOU WILL POS$t$$ AT ANY OP4 DMt.

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U 0, National Bureau of Standards samoles,15 g. of Uranium 235 33 2

uranium containing Se16 g. of U 35, 200 ge maximum.

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Standards for isotopic assay of materials enriched or depleted in U 35 2

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s TR AINING AND EXPEtiENCE OF E ACH INOlVIOUAL NAMED IN ITEM d (U.e swulem.a'al sh..'s af a.****d 8 fvPt of itAINING OUR AriON Oe ON THE JO$

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No Y.s No protect,na b t.dioact vdy meoiv,ement secadardia.

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Yes No Yes No si,wmeats

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9. EXPititNCt WITH RADtAflON (Act,el use et radio soso,es or eqws.ol.ar.sp.<ma<. I 150f0Pt MAtpAUM AMOUNT Whist (IPititNCE WAS GAINED DutAflON Of IIrttafMCI TYPE Of U$t See attached sheet 10, RADIAfiON OfftCTION IN5ftVMENTS.

(Us. supplemental sheets if a.c.ssary )

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AVAILASLE OffECTED (er/hrJ (mg/cm:)

(M.a,s. nag, serverug, sunng)

See attached sheet

11. Mf fMOO. f tEOU4NCV, AND $f ANDARD5 U$tO IN CAUSAAflNG INiitVMENTS U$ftD A40Vt.

Calibration.of Health Physics equipment is done with a Radium source semi-annually for gamma radiation.

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AEC type PF2B film badges with DuPont Dosimeter film #559 are used. Badges are processed and calibrated in our plant using a radium gamma source and aged natural uranium beta source for calibration.

INFORMATION TO BE SUBMITTED ON ADDITIONAL SHEETS I3 #Acutits ANo aOulPM HI.

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$4t@WfCAf!'OP4 Sf M f fHf APPLICANT N AMED IN if tM l. CitfiFY fMAf THIS APPLICATION IS j

Ptf PAttO iN CONFORMiff wifH fifLE 10. C00f fD Al et

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SUPPLEMENTS Aff ACMt0 Pitttfo.15 f aut AN ECT 8 Out K EDGE ANO stLIE8 s

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Mallinckrodt Chemical Works

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t WORM 53 M ALLINCKRODT CHEMICA L WORKS

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April 6, 1960 Application for Byproduct Material License - Supplement 8.

Training and Experience of Each Individual Named in Item h (and 5)

(1) Dr. Perry King:

Dr. King received a B.S. in chemistry from the University of Illinois in 1950. He was employed by the analytical laboratory of the Uranium Division of Mallinckrodt Chemical Works until December of 1953 Twenty-one months experience with chemical warfare agents was obtained at the Chemical and Radiological Laboratory at the Ariqy Chemical Center, Maryland. He received a Ph.D in radiochemistry from Washington University in 1960 He has had formal courses covering a,b,c, and d of Section 8.

In addition fifteen months experience in monitoring, instrument calibration and repair, storage, and waste disposal was obtained during a part-time job under Dr. Arthur C. Wahl at Washington University.

(2) Mr. Byron D. Field: Head, Optical and Other Physical Methods Laboratory

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Mr. Field received the degrees of B.S. and M.S. in chemistry

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years experience with the analysis of fine chemicals at

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Mallinckrodt, including some 10 years on uranium chemicals f

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with the Manhattan District Project and the Atomic Energy 6 /-

Commission. Prior to joining Mallinckrodt, Mr. Field spent Ml) 88 about two years doing spectrographic analysis of high purity y

alkalis and associated products. His present duties include g (A supervision of all radiochemical, spectrographic, infra-red,

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and X-ray analysis in the Department.

j (3) Mr. Joe W. Miller i

Three week formal course at U.S. Public Health Service and I

i five years on-the-job experience at Mallinckrodt Chemical' Works in the prinicples of radiation protection, monitor-ing and radioactivity calculations.

9 Experience with Radiation i

i Maximum Where Experience Duration of Type Isotope Amount Fas Gained Experience of Use 4

88 10 me Wash. Univ.

3 years Tracer (1) Fe Mo '

10 me Wash. Univ.

1 year Tracer 8

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1 me Wash. Univ.

15 months Instrument Calibration i

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-(2) Pa 10 ue Mallinckrodt 1 month Analytical tracer 1

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1 ue Mallinckrodt 3 months Analytical tracer 184 Fe '

1 ue Mallinckrodt 1 month Analytical tracer 8

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' ( 3) Ra 10 me Mallinckrodt 5 years Instrument Calibration ase 4

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g e I ro: M es M ALLINCKRODT CIIEMICAI, WORKS ST. LOUIS.

In addition, all three persons have worked with special nuclear materials under AEC Source Material License No. SNM-276.

10. Radiation Detection Instruments Sensitivity Window Type of Namber Radiation Range Thickness Instruments Available Detected (mr/hr)

(mg/cm) g,,

a llealth Physics Fquipment Measuring PC3A NMC Propor-1

Alpha, tional counter
Beta, w/GeigerMueller Gamma attachment.

0.68 Monitoring Victoreen No. 356 2

Alpha Alpha Survey Meter Victoreen Thyac 2

Beta, Gamma 0-20 30 Monitoring Technical Assoc-2 Beta, Gamma 0-2500 108 Monitoring iates Juno Sur-vey Meter Laboratory Equipment Measuring PC3A NMC Pro-1

Alpha, portional
Beta, counter Gamma Measuring Tracerlab SC-1 18A superscaler with SC-ho Rate-meter and TOC-lh 1

Beta 09 Measuring counter Measuring and P-200 1

Alpha, Scintillation
Beta, detector Gamma

<2 Measuring and TGC-2 mica 1

Alpha, window Geiger Beta tube and TOC-3 Soft X-ray Geiger tube 1
Beta,

<2 Measuring Gamma j

DR-15 NRC flow 1

Alpha, Measuring proportional Beta counter Measuring Baird Atomic 1

Gamma single channel gs::ma-ray spect.mmeter-Model 010 detector Model h32 ratemeter i

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13. Facilities and Equipment Standard laboratory procedures and equipment will be used by the applicants l

in the same analytical laboratory facilities used to handle special nuclear materials under AEC Source Material License No. SNM-276 issued to Mallin-ckrodt Chemical Works.60, Storage will be in a Tracerlab E12B storage container adequate for 125 mc Co lit. Radiation Protection Prograr.

The program involves personnel monitoring with film badges and periodic r

meter surveys for beta and gamma radiation for both exposure levels and contadnation. The Health Physics Department is equipped with standard monitoring equipment and will supervise the health physics aspects so as to be in compliance with 10 CFR Part 20.

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15 Materials will be used as standards and reclaimed. Any wastes will be disposed of in accordance with paragraoh 20 303 of 10 CFR Part 20.

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