Text

Westinghouse Hematite Decommissioning Project - Final Status Survey Final Report Volume 3, Chapter 16, Survey Area Release Record for Land Survey Area 05, Survey Units 01, 02, 03 and 04, Revision 1, J3571-1 Uds Level 2 Report Final Report
	ML18019A680
Person / Time
Site:	07000036
Issue date:	01/09/2018
From:	; Westinghouse
To:	; Office of Nuclear Material Safety and Safeguards
Shared Package
ML18019A532	List: ML18019A541; ML18019A556; ML18019A584; ML18019A585; ML18019A611; ML18019A613; ML18019A628; ML18019A643; ML18019A645; ML18019A658; ML18019A660; ML18019A666; ML18019A669; ML18019A671; ML18019A673; ML18019A676; ML18019A677; ML18019A680; ML18019A682; ML18019A683; ML18019A685; ML18019A687; ML18019A689; ML18019A695; ML18019A696; ML18019A697; ML18019A702; ML18019A704; ML18019A705; ML18019A706; ML18019A707; ML18019A708; ML18019A709; ML18019A710; ML18019A711; ML18019A712; ML18019A713; ML18019A722; ML18019A723; ML18019A724; ML18019A725; ML18019A726; ML18019A728; ML18019A730; ML18019A733; ML18019A735; ML18019A736; ML18019A737; ML18019A738; ML18019A739; ... further results
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ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-3571-1 Client Project/Site: RFP-CBA-022 (7 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Martin Swanson Authorized for release by:

9/8/2013 11:04:17 AM Ivan Vania, Project Manager I ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

TestAmerica Job ID: 160-3571-1 Page 2 of 45 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

6 Receipt Checklists.........................................

9 Definitions/Glossary.......................................

10 Method Summary.........................................

11 Sample Summary.........................................

12 Client Sample Results......................................

13 QC Sample Results........................................

34 QC Association Summary...................................

40 Tracer Carrier Summary....................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3571-1 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-3571-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: RFP-CBA-022 (7 DAY TAT)

Report Number: 160-3571-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 08/29/2013; the samples arrived in good condition, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 20.0º C and 20.0º C.

TECHNETIUM-99 (ICPMS)

Samples L050119TSQ00 (160-3571-1), L050119TSS00 (160-3571-2), L050120TRS00 (160-3571-3), L050121TSS00 (160-3571-4),

L050122TRS00 (160-3571-5), L050125TRS00 (160-3571-6), L050127TRS00 (160-3571-7), L050128TES00 (160-3571-8),

L050131TRS00 (160-3571-9), L050132TES00 (160-3571-10), L050133TRS00 (160-3571-11), L050139TES00 (160-3571-12),

L050140TRS00 (160-3571-13), L050148TRS00 (160-3571-14), L050154TRS00 (160-3571-15), L050155TES00 (160-3571-16),

L050156TRS00 (160-3571-17), L050157TES00 (160-3571-18), L050162TRQ00 (160-3571-19), L050162TRS00 (160-3571-20),

L050163TES00 (160-3571-21), L050164TRS00 (160-3571-22), L050165TEQ00 (160-3571-23), L050165TES00 (160-3571-24),

L050169TSS00 (160-3571-25), L050170TRS00 (160-3571-26), L050171TRS00 (160-3571-27) and L050172TES00 (160-3571-28) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 08/30/2013 and 09/03/2013 and analyzed on 09/03/2013 and 09/04/2013.

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3571-1 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-3571-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

Preparation Batches 70096 & 69983; Analytical Batches 70530 & 70531:

The following sample(s) was diluted due to matrix interference indicated by internal standard failure in the undiluted sample:

L050154TRS00 (160-3571-15). Elevated reporting limits (RLs) are provided.

Sample L050154TRS00 (160-3571-15)[2X] required dilution prior to analysis. The reporting limits have been adjusted accordingly.

No difficulties were encountered during the Tc-99 analysis. All quality control parameters were within the acceptance limits.

PERCENT SOLIDS Samples L050119TSQ00 (160-3571-1), L050119TSS00 (160-3571-2), L050120TRS00 (160-3571-3), L050121TSS00 (160-3571-4),

L050122TRS00 (160-3571-5), L050125TRS00 (160-3571-6), L050127TRS00 (160-3571-7), L050128TES00 (160-3571-8),

L050131TRS00 (160-3571-9), L050132TES00 (160-3571-10), L050133TRS00 (160-3571-11), L050139TES00 (160-3571-12),

L050140TRS00 (160-3571-13), L050148TRS00 (160-3571-14), L050154TRS00 (160-3571-15), L050155TES00 (160-3571-16),

L050156TRS00 (160-3571-17), L050157TES00 (160-3571-18), L050162TRQ00 (160-3571-19), L050162TRS00 (160-3571-20),

L050163TES00 (160-3571-21), L050164TRS00 (160-3571-22), L050165TEQ00 (160-3571-23), L050165TES00 (160-3571-24),

L050169TSS00 (160-3571-25), L050170TRS00 (160-3571-26), L050171TRS00 (160-3571-27) and L050172TES00 (160-3571-28) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 09/03/2013.

No difficulties were encountered during the % solids analysis. All quality control parameters were within the acceptance limits.

CESIUM-137 & OTHER GAMMA EMITTERS (GS)

Samples L050119TSQ00 (160-3571-1), L050119TSS00 (160-3571-2), L050120TRS00 (160-3571-3), L050121TSS00 (160-3571-4),

L050122TRS00 (160-3571-5), L050125TRS00 (160-3571-6), L050127TRS00 (160-3571-7), L050128TES00 (160-3571-8),

L050131TRS00 (160-3571-9), L050132TES00 (160-3571-10), L050133TRS00 (160-3571-11), L050139TES00 (160-3571-12),

L050140TRS00 (160-3571-13), L050148TRS00 (160-3571-14), L050154TRS00 (160-3571-15), L050155TES00 (160-3571-16),

L050156TRS00 (160-3571-17), L050157TES00 (160-3571-18), L050162TRQ00 (160-3571-19), L050162TRS00 (160-3571-20),

L050163TES00 (160-3571-21), L050164TRS00 (160-3571-22), L050165TEQ00 (160-3571-23), L050165TES00 (160-3571-24),

L050169TSS00 (160-3571-25), L050170TRS00 (160-3571-26), L050171TRS00 (160-3571-27) and L050172TES00 (160-3571-28) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 08/30/2013, prepared on 09/04/2013 and analyzed on 09/04/2013 and 09/05/2013.

Preparation Batch 70600:

Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of Bismuth-214.

Because the samples have not had a 21-day ingrowth, the activity for Radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between Radium-226 and Bismuth-214 by the loss of Radon-222 during sample preparation. (160-3570-8 DU), (LCS 160-70600/2-A), (MB 160-70600/1-A), L050117TUB00 (160-3570-8), L050163TES00 (160-3571-21), L050164TRS00 (160-3571-22), L050165TEQ00 (160-3571-23), L050165TES00 (160-3571-24), L050169TSS00 (160-3571-25), L050170TRS00 (160-3571-26), L050171TRS00 (160-3571-27), L050172TES00 (160-3571-28)

The reporting limit for thorium-234 was not met due to insufficient sample weight available for analysis. Analytical results are reported with the MDC achieved. L050165TEQ00 (160-3571-23), L050171TRS00 (160-3571-27)

Preparation Batch 70555:

Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of Bismuth-214.

Because the samples have not had a 21-day ingrowth, the activity for Radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between Radium-226 and Bismuth-214 by the loss of Radon-222 during sample preparation. (160-3571-20 DU), (LCS 160-70555/2-A), (MB 160-70555/1-A), L050119TSQ00 (160-3571-1), L050119TSS00 (160-3571-2), L050120TRS00 (160-3571-3), L050121TSS00 (160-3571-4), L050122TRS00 (160-3571-5), L050125TRS00 (160-3571-6),

L050127TRS00 (160-3571-7), L050128TES00 (160-3571-8), L050131TRS00 (160-3571-9), L050132TES00 (160-3571-10),

L050133TRS00 (160-3571-11), L050139TES00 (160-3571-12), L050140TRS00 (160-3571-13), L050148TRS00 (160-3571-14),

L050154TRS00 (160-3571-15), L050155TES00 (160-3571-16), L050156TRS00 (160-3571-17), L050157TES00 (160-3571-18),

L050162TRQ00 (160-3571-19), L050162TRS00 (160-3571-20)

The reporting limit for thorium-234 was not met due to insufficient sample weight available for analysis. Analytical results are reported with the MDC achieved. L050122TRS00 (160-3571-5), L050125TRS00 (160-3571-6), L050162TRQ00 (160-3571-19)

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-3571-1 Project/Site: RFP-CBA-022 (7 DAY TAT)

Job ID: 160-3571-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

No other difficulties were encountered during the Gamma spec analysis. All other quality control parameters were within the acceptance limits.

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Procedw:e HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project !Revision: 3 I

Page.I of l j Westinghouse Non"Proprieta,y Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cntody ID No. I F-082913-02 Page 1/3 Project Name:

Westinghouse Electric Company Contact Person:

Geralq. Rood Phone Number:

314-810-3382 Sampler Name Scott Jenkins Sample ID L050119TSQOO IL050119TSS00 L050120TRS00 L050121TSSOO IL050122TRS00 L050l25TRS00 L050l27TRS00

.L050128TES00 L05013 l TRSOO

'L050132TES00 L050l33TRS00 L050l39TES00 Company Name:

Received by:

Company Name:

Relinquished by:

Company Name:

Date Time 8/28/2013 8:50 8/28/2013 8:50 8/28/2013 10:15 8/28/2013 8:40 8/28/2013 9:15

,8/28/2013 10:10 8/28/2013 8:33 8/28/2013 8:45 8/28/2013 10:35 8/28/2013 10:40 8/28/2013 8/28/2013

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Date/Time Matrix s

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TA-MO Laboratory Address:

13715 Rider Trail North Phone No.

314-298-8566 Laboratory Contact Person:

Joe Walker Phone No.

708-870-8453 Rush TlllJl Around Time (7 days)

Remarks 1 I L-.5 F\\

v os-o Cooler Temperature:

Comments: Please re-analyze samples after 21 day ingrowth period.

Verified By:

U\\l V,

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!Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project !Revision: 3 I

Page I of 11 Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAlN OF CUSTODY

,J.nstructions: Each time the container is transferred to another organization, a person from eaeh organization should sign the CoC. The Laboratozy/End User must verify that the. sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cutody ID No. l F-082913-02 Page 2/3 Project Name; Westinghouse Electric Company Contact Person:

Gerald Rood Phone Number:

0 314-810"3382 Sampler Name Scott Jenkins n

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Sample ID iL050 l 40TRSOO L050148TRSOO L050154TRSOO L050155TESOO L0501S6TRSOO LOS01S7TESOO LOS0162TRQOO LOSO I 62TRSOO

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Company Name: w Received by:

Company Name:

Reljnquished by:

Company Name:

!Date Time 8/28/2013 8:35 8/28/2013 16:25 8/28/2013 13:05 8/28/2013 13:10 8/28/2013 13:15 8/28/2013 13:40 8/28/2013 11:10 8/28/2013 11:10 8/28/2013 14:00 8/28/2013 10:55 8/28/2013 11:05 8/28/2013 Date/Time Matrix s

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Laboratory Name:

,TA-MO Laboratory Address:

13715 Rider Trail North Phone No.

314-298-8566 Laboratory Contact Person:

Joe Walker Phone No.

708-870-8453 Turn Al"_ou11d T_ime Rush (7 days)

Remarks Li L

Cooler Temperature:

Shipper and Number:

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Comments: Please re-analyz:isamples after 21 day ingrowth period.

Verified By:

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10 11 12 Procedure HDP-PR-QA-006, Chain of Custody Page l ofl Hematite Decommissioning Project !Revision: 3 I

I WestinghoUse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organizatiQn, a person from each organization should sign the CoC. The Laboratory/End User must verify lhat the sample is correctly identified

'before the sample is releasei;l. for use or analysis and send the completed CoC to HDP.

Chain of Cutod ID No, F-082913-02 Pa e 3/3

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Company Nam\\_,o t,L-Received by:

Company Name:

Relinquished bv:

Company Name:

Date/fiine Date/fiine ct. ()0 e?..,1.,,

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Date/Time I' r I i'-*.> "l'~I'->

Comp?IlY Name:

t<._S_~, c,,,

(&':j.fj Coo I er Temperature:

Cooler ID: I Shio.oer and Number:

Comments: Pleas~re-analyze samples after 21 day ingrowth period.

Verified By:

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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-3571-1 Login Number: 3571 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

N/A Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

False Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Qualifiers Metals Qualifier Description J

Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier Rad Qualifier Description U

Indicates the analyte was analyzed for but not detected.

Qualifier X

Carrier exceeds control limit Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 11 of 45 1

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Sample Summary TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID Client Sample ID Received Collected Matrix 160-3571-1 L050119TSQ00 Solid 08/28/13 08:50 08/29/13 18:38 160-3571-2 L050119TSS00 Solid 08/28/13 08:50 08/29/13 18:38 160-3571-3 L050120TRS00 Solid 08/28/13 10:15 08/29/13 18:38 160-3571-4 L050121TSS00 Solid 08/28/13 08:40 08/29/13 18:38 160-3571-5 L050122TRS00 Solid 08/28/13 09:15 08/29/13 18:38 160-3571-6 L050125TRS00 Solid 08/28/13 10:10 08/29/13 18:38 160-3571-7 L050127TRS00 Solid 08/28/13 08:33 08/29/13 18:38 160-3571-8 L050128TES00 Solid 08/28/13 08:45 08/29/13 18:38 160-3571-9 L050131TRS00 Solid 08/28/13 10:35 08/29/13 18:38 160-3571-10 L050132TES00 Solid 08/28/13 10:40 08/29/13 18:38 160-3571-11 L050133TRS00 Solid 08/28/13 09:20 08/29/13 18:38 160-3571-12 L050139TES00 Solid 08/28/13 10:20 08/29/13 18:38 160-3571-13 L050140TRS00 Solid 08/28/13 08:35 08/29/13 18:38 160-3571-14 L050148TRS00 Solid 08/28/13 16:25 08/29/13 18:38 160-3571-15 L050154TRS00 Solid 08/28/13 13:05 08/29/13 18:38 160-3571-16 L050155TES00 Solid 08/28/13 13:10 08/29/13 18:38 160-3571-17 L050156TRS00 Solid 08/28/13 13:15 08/29/13 18:38 160-3571-18 L050157TES00 Solid 08/28/13 13:40 08/29/13 18:38 160-3571-19 L050162TRQ00 Solid 08/28/13 11:10 08/29/13 18:38 160-3571-20 L050162TRS00 Solid 08/28/13 11:10 08/29/13 18:38 160-3571-21 L050163TES00 Solid 08/28/13 14:00 08/29/13 18:38 160-3571-22 L050164TRS00 Solid 08/28/13 10:55 08/29/13 18:38 160-3571-23 L050165TEQ00 Solid 08/28/13 11:05 08/29/13 18:38 160-3571-24 L050165TES00 Solid 08/28/13 11:05 08/29/13 18:38 160-3571-25 L050169TSS00 Solid 08/28/13 13:10 08/29/13 18:38 160-3571-26 L050170TRS00 Solid 08/28/13 13:30 08/29/13 18:38 160-3571-27 L050171TRS00 Solid 08/28/13 11:00 08/29/13 18:38 160-3571-28 L050172TES00 Solid 08/28/13 11:15 08/29/13 18:38 TestAmerica St. Louis Page 12 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-1 Client Sample ID: L050119TSQ00 Matrix: Solid Date Collected: 08/28/13 08:50 Percent Solids: 89.8 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000018 J

0.00060 0.000018 mg/Kg

09/03/13 07:18 09/03/13 17:41 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.300 (2+/-)

0.0542 (2+/-)

1 09/03/13 17:41 09/03/13 07:18 pCi/g 0.204 1.19 RL MDC 0.0426 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 17:41 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 94 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.747 (2+/-)

0.160 (2+/-)

1 09/04/13 19:17 09/04/13 10:53 pCi/g 0.103 RL MDC 0.141 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.0931 0.0569 0.0567 U

0.0498 Americium 241 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.262 0.312 0.296 0.963 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.0658 0.112 0.0885 0.667 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.0741 0.122 0.0689 0.775 Lead 212 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.0714 0.112 0.0836 0.711 Lead 214 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.367 1.95 1.05 16.0 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.969 0.247 0.243 U

0.414 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.0658 1.00 0.112 0.0885 0.667 Radium 226 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.860 1.00 0.733 0.714 1.57 Thorium 234 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.215 0.133 0.133 U

0.150 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 19:17 1

4.95 1.97 1.96 U

1.27 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.103 0.160 0.141 0.747 Thorium 232 Tl-208 0.278 0.0484 0.0564 0.0381 pCi/g 09/04/13 10:53 09/04/13 19:17 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-2 Client Sample ID: L050119TSS00 Matrix: Solid Date Collected: 08/28/13 08:50 Percent Solids: 90.8 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000025 J

0.00060 0.000018 mg/Kg

09/03/13 07:18 09/03/13 17:53 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.423 (2+/-)

0.113 (2+/-)

1 09/03/13 17:53 09/03/13 07:18 pCi/g 0.207 1.21 RL MDC 0.0951 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 17:53 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 91 TestAmerica St. Louis Page 13 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-2 Client Sample ID: L050119TSS00 Matrix: Solid Date Collected: 08/28/13 08:50 Date Received: 08/29/13 18:38 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.12 (2+/-)

0.185 (2+/-)

1 09/04/13 19:17 09/04/13 10:53 pCi/g 0.144 RL MDC 0.146 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.102 0.285 0.285 U

-0.00521 Americium 241 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.573 0.400 0.392 0.734 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.0827 0.140 0.116 0.764 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.0581 0.151 0.0778 1.00 Lead 212 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.0807 0.123 0.0904 0.802 Lead 214 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.404 2.26 1.33 17.8 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 19:17 1

1.22 0.162 0.160 U

0.228 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.0827 1.00 0.140 0.116 0.764 Radium 226 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.882 1.00 0.723 0.697 1.82 Thorium 234 pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.197 0.121 0.119 U

0.177 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 19:17 1

5.88 2.12 2.12 U

0.537 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 19:17 1

0.144 0.185 0.146 1.12 Thorium 232 Tl-208 0.270 0.0490 0.0565 0.0406 pCi/g 09/04/13 10:53 09/04/13 19:17 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-3 Client Sample ID: L050120TRS00 Matrix: Solid Date Collected: 08/28/13 10:15 Percent Solids: 92.6 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000018 J

0.00059 0.000018 mg/Kg

09/03/13 07:18 09/03/13 17:57 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.302 (2+/-)

0.0999 (2+/-)

1 09/03/13 17:57 09/03/13 07:18 pCi/g 0.202 1.18 RL MDC 0.0869 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 17:57 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 91 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.904 (2+/-)

0.165 (2+/-)

1 09/04/13 19:18 09/04/13 10:53 pCi/g 0.141 RL MDC 0.137 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 19:18 1

0.101 0.0602 0.0601 U

0.0198 Americium 241 pCi/g 09/04/13 10:53 09/04/13 19:18 1

0.369 0.351 0.343 0.691 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 19:18 1

0.0679 0.126 0.0990 0.743 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 19:18 1

0.0677 0.128 0.0729 0.813 Lead 212 pCi/g 09/04/13 10:53 09/04/13 19:18 1

0.0616 0.118 0.0860 0.780 Lead 214 pCi/g 09/04/13 10:53 09/04/13 19:18 1

0.279 2.18 1.27 17.4 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 19:18 1

1.31 0.803 0.799 U

-0.728 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 19:18 1

0.0679 1.00 0.126 0.0990 0.743 Radium 226 TestAmerica St. Louis Page 14 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-3 Client Sample ID: L050120TRS00 Matrix: Solid Date Collected: 08/28/13 10:15 Date Received: 08/29/13 18:38 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 1.54 (2+/-)

0.667 (2+/-)

1 09/04/13 19:18 09/04/13 10:53 pCi/g 0.827 1.00 RL MDC 0.647 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 19:18 1

0.245 0.141 0.140 U

0.136 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 19:18 1

4.42 2.35 2.35 U

0.0323 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 19:18 1

0.141 0.165 0.137 0.904 Thorium 232 Tl-208 0.274 0.0495 0.0571 0.0400 pCi/g 09/04/13 10:53 09/04/13 19:18 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-4 Client Sample ID: L050121TSS00 Matrix: Solid Date Collected: 08/28/13 08:40 Percent Solids: 90.8 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00018 J

0.00062 0.000019 mg/Kg

09/03/13 07:18 09/03/13 18:00 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 3.11 (2+/-)

0.468 (2+/-)

1 09/03/13 18:00 09/03/13 07:18 pCi/g 0.213 1.24 RL MDC 0.306 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 18:00 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 89 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.782 (2+/-)

0.142 (2+/-)

1 09/04/13 19:19 09/04/13 10:53 pCi/g 0.0570 RL MDC 0.118 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.0889 0.0528 0.0528 U

-0.0118 Americium 241 pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.222 0.322 0.302 1.06 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.0537 0.104 0.0817 0.622 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.0503 0.106 0.0591 0.684 Lead 212 pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.0654 0.102 0.0739 0.681 Lead 214 pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.303 1.39 0.879 10.5 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.944 0.156 0.154 U

0.216 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.0537 1.00 0.104 0.0817 0.622 Radium 226 pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.790 1.00 0.310 0.301 U

0.718 Thorium 234 pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.197 0.122 0.121 U

0.156 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 19:19 1

4.19 2.41 2.41 U

1.30 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.0570 0.142 0.118 0.782 Thorium 232 Tl-208 0.224 0.0404 0.0466 0.0320 pCi/g 09/04/13 10:53 09/04/13 19:19 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-5 Client Sample ID: L050122TRS00 Matrix: Solid Date Collected: 08/28/13 09:15 Percent Solids: 83.0 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000023 J

0.00067 0.000020 mg/Kg

09/03/13 07:18 09/03/13 18:04 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.402 (2+/-)

0.0741 (2+/-)

1 09/03/13 18:04 09/03/13 07:18 pCi/g 0.228 1.33 RL MDC 0.0564 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 18:04 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 91 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.13 (2+/-)

0.215 (2+/-)

1 09/04/13 19:51 09/04/13 10:53 pCi/g 0.164 RL MDC 0.182 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 19:51 1

0.116 0.0681 0.0681 U

0.00232 Americium 241 pCi/g 09/04/13 10:53 09/04/13 19:51 1

0.363 0.440 0.420 1.26 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 19:51 1

0.0767 0.162 0.128 0.947 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 19:51 1

0.0755 0.164 0.0906 1.06 Lead 212 pCi/g 09/04/13 10:53 09/04/13 19:51 1

0.0927 0.134 0.101 0.841 Lead 214 pCi/g 09/04/13 10:53 09/04/13 19:51 1

0.227 2.26 1.44 17.0 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 19:51 1

1.23 0.329 0.325 U

0.490 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 19:51 1

0.0767 1.00 0.162 0.128 0.947 Radium 226 pCi/g 09/04/13 10:53 09/04/13 19:51 1

1.01 1.00 0.395 0.378 1.12 Thorium 234 pCi/g 09/04/13 10:53 09/04/13 19:51 1

0.241 0.0851 0.0850 U

0.0276 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 19:51 1

7.65 3.46 3.43 U

4.38 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 19:51 1

0.164 0.215 0.182 1.13 Thorium 232 Tl-208 0.309 0.0516 0.0607 0.0367 pCi/g 09/04/13 10:53 09/04/13 19:51 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-6 Client Sample ID: L050125TRS00 Matrix: Solid Date Collected: 08/28/13 10:10 Percent Solids: 70.6 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00017 J

0.00081 0.000024 mg/Kg

09/03/13 07:18 09/03/13 18:08 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 2.97 (2+/-)

0.471 (2+/-)

1 09/03/13 18:08 09/03/13 07:18 pCi/g 0.278 1.62 RL MDC 0.307 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 18:08 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 87 TestAmerica St. Louis Page 16 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-6 Client Sample ID: L050125TRS00 Matrix: Solid Date Collected: 08/28/13 10:10 Date Received: 08/29/13 18:38 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.779 (2+/-)

0.214 (2+/-)

1 09/04/13 19:19 09/04/13 10:53 pCi/g 0.101 RL MDC 0.198 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.249 0.173 0.173 U

0.0895 Americium 241 pCi/g 09/04/13 10:53 09/04/13 19:19 1

1.14 0.681 0.679 U

0.458 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.176 0.211 0.193 0.805 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.143 0.210 0.128 0.769 Lead 212 pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.177 0.206 0.161 0.969 Lead 214 pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.933 1.93 1.57 11.0 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 19:19 1

2.06 0.401 0.400 U

0.177 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.176 1.00 0.211 0.193 0.805 Radium 226 pCi/g 09/04/13 10:53 09/04/13 19:19 1

2.26 1.00 0.696 0.691 U

0.834 Thorium 234 pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.531 0.292 0.291 U

0.207 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 19:19 1

10.3 6.23 6.23 U

2.60 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 19:19 1

0.101 0.214 0.198 0.779 Thorium 232 Tl-208 0.219 0.0636 0.0675 0.0657 pCi/g 09/04/13 10:53 09/04/13 19:19 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-7 Client Sample ID: L050127TRS00 Matrix: Solid Date Collected: 08/28/13 08:33 Percent Solids: 82.5 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000022 J

0.00064 0.000019 mg/Kg

09/03/13 07:18 09/03/13 18:20 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.380 (2+/-)

0.0415 (2+/-)

1 09/03/13 18:20 09/03/13 07:18 pCi/g 0.221 1.29 RL MDC 0.0167 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 18:20 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 93 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.11 (2+/-)

0.154 (2+/-)

1 09/04/13 19:55 09/04/13 10:53 pCi/g 0.0882 RL MDC 0.104 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.102 0.0607 0.0607 U

0.00965 Americium 241 pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.317 0.397 0.374 1.29 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.0551 0.120 0.0853 0.807 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.0583 0.158 0.0713 1.09 Lead 212 pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.0639 0.117 0.0739 0.871 Lead 214 pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.372 2.16 1.10 18.1 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 19:55 1

1.10 0.218 0.214 U

0.405 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.0551 1.00 0.120 0.0853 0.807 Radium 226 TestAmerica St. Louis Page 17 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-7 Client Sample ID: L050127TRS00 Matrix: Solid Date Collected: 08/28/13 08:33 Date Received: 08/29/13 18:38 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 1.57 (2+/-)

0.616 (2+/-)

1 09/04/13 19:55 09/04/13 10:53 pCi/g 0.775 1.00 RL MDC 0.593 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.164 0.134 0.132 0.212 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 19:55 1

3.36 3.33 3.26 6.51 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.0882 0.154 0.104 1.11 Thorium 232 Tl-208 0.359 0.0447 0.0582 0.0314 pCi/g 09/04/13 10:53 09/04/13 19:55 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-8 Client Sample ID: L050128TES00 Matrix: Solid Date Collected: 08/28/13 08:45 Percent Solids: 82.5 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00065 0.000020 mg/Kg

09/03/13 07:18 09/03/13 18:24 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.278 (2+/-)

0.0416 (2+/-)

1 09/03/13 18:24 09/03/13 07:18 pCi/g 0.223 1.30 RL MDC 0.0291 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 18:24 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 93 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.16 (2+/-)

0.174 (2+/-)

1 09/04/13 19:54 09/04/13 10:53 pCi/g 0.115 RL MDC 0.128 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.0814 0.0605 0.0602 U

0.0521 Americium 241 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.321 0.376 0.354 1.23 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.0727 0.134 0.0995 0.866 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.0868 0.156 0.0819 1.02 Lead 212 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.0769 0.125 0.0868 0.862 Lead 214 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.353 2.46 1.23 20.9 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.844 0.503 0.502 U

0.271 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.0727 1.00 0.134 0.0995 0.866 Radium 226 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.864 1.00 0.706 0.687 1.55 Thorium 234 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.258 0.163 0.163 U

0.101 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 19:54 1

4.63 2.42 2.41 U

2.00 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.115 0.174 0.128 1.16 Thorium 232 Tl-208 0.365 0.0514 0.0638 0.0381 pCi/g 09/04/13 10:53 09/04/13 19:54 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-9 Client Sample ID: L050131TRS00 Matrix: Solid Date Collected: 08/28/13 10:35 Percent Solids: 94.6 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000089 J

0.00057 0.000017 mg/Kg

09/03/13 07:18 09/03/13 18:28 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.52 (2+/-)

0.188 (2+/-)

1 09/03/13 18:28 09/03/13 07:18 pCi/g 0.195 1.14 RL MDC 0.107 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 18:28 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 94 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.420 (2+/-)

0.101 (2+/-)

1 09/04/13 19:55 09/04/13 10:53 pCi/g 0.0693 RL MDC 0.0910 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.0618 0.0364 0.0364 U

0.00766 Americium 241 pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.128 0.211 0.198 0.699 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.0455 0.0865 0.0678 0.517 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.0397 0.0624 0.0405 0.367 Lead 212 pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.0458 0.0798 0.0567 0.540 Lead 214 pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.187 1.25 0.762 9.74 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.806 0.203 0.202 U

0.184 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.0455 1.00 0.0865 0.0678 0.517 Radium 226 pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.505 1.00 0.394 0.384 0.857 Thorium 234 pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.145 0.0934 0.0933 U

0.0459 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 19:55 1

3.73 2.25 2.24 U

1.55 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 19:55 1

0.0693 0.101 0.0910 0.420 Thorium 232 Tl-208 0.117 0.0244 0.0272 0.0218 pCi/g 09/04/13 10:53 09/04/13 19:55 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-10 Client Sample ID: L050132TES00 Matrix: Solid Date Collected: 08/28/13 10:40 Percent Solids: 95.6 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00015 J

0.00055 0.000017 mg/Kg

09/03/13 07:18 09/03/13 18:31 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 2.50 (2+/-)

0.255 (2+/-)

1 09/03/13 18:31 09/03/13 07:18 pCi/g 0.189 1.10 RL MDC 0.0783 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 18:31 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 95 TestAmerica St. Louis Page 19 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-10 Client Sample ID: L050132TES00 Matrix: Solid Date Collected: 08/28/13 10:40 Date Received: 08/29/13 18:38 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.441 (2+/-)

0.0898 (2+/-)

1 09/04/13 19:56 09/04/13 10:53 pCi/g 0.0537 RL MDC 0.0777 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 19:56 1

0.0728 0.0432 0.0432 U

-0.00865 Americium 241 pCi/g 09/04/13 10:53 09/04/13 19:56 1

0.359 0.217 0.217 U

0.160 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 19:56 1

0.0542 0.0929 0.0761 0.514 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 19:56 1

0.0431 0.0660 0.0441 0.380 Lead 212 pCi/g 09/04/13 10:53 09/04/13 19:56 1

0.0575 0.0952 0.0729 0.588 Lead 214 pCi/g 09/04/13 10:53 09/04/13 19:56 1

0.213 1.27 0.818 9.45 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 19:56 1

0.856 0.516 0.515 U

-0.344 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 19:56 1

0.0542 1.00 0.0929 0.0761 0.514 Radium 226 pCi/g 09/04/13 10:53 09/04/13 19:56 1

0.580 1.00 0.233 0.224 0.608 Thorium 234 pCi/g 09/04/13 10:53 09/04/13 19:56 1

0.167 0.0937 0.0930 U

0.107 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 19:56 1

4.15 2.35 2.35 U

0.649 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 19:56 1

0.0537 0.0898 0.0777 0.441 Thorium 232 Tl-208 0.124 0.0311 0.0337 0.0267 pCi/g 09/04/13 10:53 09/04/13 19:56 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-11 Client Sample ID: L050133TRS00 Matrix: Solid Date Collected: 08/28/13 09:20 Percent Solids: 93.6 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00017 J

0.00059 0.000018 mg/Kg

09/03/13 07:18 09/03/13 18:35 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 2.94 (2+/-)

0.332 (2+/-)

1 09/03/13 18:35 09/03/13 07:18 pCi/g 0.200 1.17 RL MDC 0.139 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 18:35 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.583 (2+/-)

0.103 (2+/-)

1 09/04/13 19:54 09/04/13 10:53 pCi/g 0.0747 RL MDC 0.0838 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.0863 0.0509 0.0509 U

0.000244 Americium 241 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.256 0.329 0.315 0.911 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.0584 0.103 0.0841 0.569 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.0446 0.106 0.0562 0.692 Lead 212 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.0552 0.0854 0.0589 0.595 Lead 214 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.285 1.68 0.953 13.5 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.901 0.178 0.174 U

0.327 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.0584 1.00 0.103 0.0841 0.569 Radium 226 TestAmerica St. Louis Page 20 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-11 Client Sample ID: L050133TRS00 Matrix: Solid Date Collected: 08/28/13 09:20 Date Received: 08/29/13 18:38 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 1.07 (2+/-)

0.532 (2+/-)

1 09/04/13 19:54 09/04/13 10:53 pCi/g 0.693 1.00 RL MDC 0.520 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.195 0.118 0.117 U

0.0829 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 19:54 1

4.58 3.95 3.95 U

-1.71 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 19:54 1

0.0747 0.103 0.0838 0.583 Thorium 232 Tl-208 0.211 0.0357 0.0419 0.0286 pCi/g 09/04/13 10:53 09/04/13 19:54 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-12 Client Sample ID: L050139TES00 Matrix: Solid Date Collected: 08/28/13 10:20 Percent Solids: 94.3 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00067 0.00057 0.000017 mg/Kg

09/03/13 07:18 09/03/13 18:39 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 11.5 (2+/-)

1.72 (2+/-)

1 09/03/13 18:39 09/03/13 07:18 pCi/g 0.194 1.13 RL MDC 1.23 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 18:39 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 94 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.444 (2+/-)

0.107 (2+/-)

1 09/04/13 20:28 09/04/13 10:53 pCi/g 0.0930 RL MDC 0.0968 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 20:28 1

0.0795 0.0466 0.0466 U

-0.000285 Americium 241 pCi/g 09/04/13 10:53 09/04/13 20:28 1

0.369 0.254 0.252 U

0.366 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 20:28 1

0.0491 0.116 0.0933 0.667 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 20:28 1

0.0480 0.0658 0.0477 0.350 Lead 212 pCi/g 09/04/13 10:53 09/04/13 20:28 1

0.0541 0.106 0.0800 0.666 Lead 214 pCi/g 09/04/13 10:53 09/04/13 20:28 1

0.168 1.27 0.895 8.80 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 20:28 1

0.730 0.243 0.241 U

0.206 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 20:28 1

0.0491 1.00 0.116 0.0933 0.667 Radium 226 pCi/g 09/04/13 10:53 09/04/13 20:28 1

0.676 1.00 0.313 0.284 1.26 Thorium 234 pCi/g 09/04/13 10:53 09/04/13 20:28 1

0.190 0.131 0.130 0.199 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 20:28 1

5.80 3.29 3.29 U

0.831 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 20:28 1

0.0930 0.107 0.0968 0.444 Thorium 232 Tl-208 0.129 0.0413 0.0434 0.0364 pCi/g 09/04/13 10:53 09/04/13 20:28 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-13 Client Sample ID: L050140TRS00 Matrix: Solid Date Collected: 08/28/13 08:35 Percent Solids: 92.5 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00011 J

0.00057 0.000017 mg/Kg

09/03/13 07:18 09/03/13 18:43 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.86 (2+/-)

0.223 (2+/-)

1 09/03/13 18:43 09/03/13 07:18 pCi/g 0.197 1.15 RL MDC 0.125 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 18:43 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 95 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.465 (2+/-)

0.0907 (2+/-)

1 09/04/13 20:32 09/04/13 10:53 pCi/g 0.0682 RL MDC 0.0773 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0709 0.0424 0.0424 U

0.0184 Americium 241 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.310 0.230 0.225 0.478 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0505 0.0932 0.0710 0.581 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0436 0.0732 0.0459 0.440 Lead 212 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0520 0.0879 0.0591 0.625 Lead 214 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.310 1.19 0.751 8.97 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.756 0.185 0.181 U

0.342 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0505 1.00 0.0932 0.0710 0.581 Radium 226 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.562 1.00 0.419 0.410 0.834 Thorium 234 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.173 0.109 0.109 U

0.0997 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 20:32 1

3.80 2.03 2.03 U

0.112 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0682 0.0907 0.0773 0.465 Thorium 232 Tl-208 0.164 0.0283 0.0330 0.0203 pCi/g 09/04/13 10:53 09/04/13 20:32 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-14 Client Sample ID: L050148TRS00 Matrix: Solid Date Collected: 08/28/13 16:25 Percent Solids: 79.1 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.0030 0.00065 0.000019 mg/Kg

09/03/13 07:18 09/03/13 18:47 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 51.4 (2+/-)

5.19 (2+/-)

1 09/03/13 18:47 09/03/13 07:18 pCi/g 0.221 1.29 RL MDC 1.73 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 18:47 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 97 TestAmerica St. Louis Page 22 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-14 Client Sample ID: L050148TRS00 Matrix: Solid Date Collected: 08/28/13 16:25 Date Received: 08/29/13 18:38 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.195 (2+/-)

0.0512 (2+/-)

1 09/04/13 20:34 09/04/13 10:53 pCi/g 0.0213 RL MDC 0.0472 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 20:34 1

0.0624 0.0368 0.0368 U

0.000918 Americium 241 pCi/g 09/04/13 10:53 09/04/13 20:34 1

0.223 0.132 0.132 U

0.0804 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 20:34 1

0.0404 0.0886 0.0648 0.582 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 20:34 1

0.0393 0.0330 0.0289 0.124 Lead 212 pCi/g 09/04/13 10:53 09/04/13 20:34 1

0.0441 0.0920 0.0580 0.687 Lead 214 pCi/g 09/04/13 10:53 09/04/13 20:34 1

0.189 0.436 0.352 2.51 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 20:34 1

0.459 0.103 0.102 U

0.0926 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 20:34 1

0.0404 1.00 0.0886 0.0648 0.582 Radium 226 pCi/g 09/04/13 10:53 09/04/13 20:34 1

0.536 1.00 0.497 0.469 1.57 Thorium 234 pCi/g 09/04/13 10:53 09/04/13 20:34 1

0.126 0.0804 0.0781 0.189 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 20:34 1

2.71 1.58 1.58 U

0.782 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 20:34 1

0.0213 0.0512 0.0472 0.195 Thorium 232 Tl-208 0.0673 0.0221 0.0232 0.0207 pCi/g 09/04/13 10:53 09/04/13 20:34 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-15 Client Sample ID: L050154TRS00 Matrix: Solid Date Collected: 08/28/13 13:05 Percent Solids: 95.3 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.0039 0.0010 0.000031 mg/Kg

09/03/13 07:18 09/04/13 07:49 2

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 67.5 (2+/-)

6.71 (2+/-)

2 09/04/13 07:49 09/03/13 07:18 pCi/g 0.356 2.08 RL MDC 2.79 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/04/13 07:49 2

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 101 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.0444 U

(2+/-)

0.0512 (2+/-)

1 09/04/13 20:32 09/04/13 10:53 pCi/g 0.0909 RL MDC 0.0510 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0580 0.0345 0.0344 U

0.0144 Americium 241 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.287 0.173 0.173 U

0.125 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0370 0.113 0.0757 0.806 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0366 0.0293 0.0265 0.0961 Lead 212 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0409 0.112 0.0638 0.889 Lead 214 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.185 0.328 0.294 1.41 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.545 0.0806 0.0803 U

0.0685 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0370 1.00 0.113 0.0757 0.806 Radium 226 TestAmerica St. Louis Page 23 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-15 Client Sample ID: L050154TRS00 Matrix: Solid Date Collected: 08/28/13 13:05 Date Received: 08/29/13 18:38 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 1.97 (2+/-)

0.526 (2+/-)

1 09/04/13 20:32 09/04/13 10:53 pCi/g 0.548 1.00 RL MDC 0.484 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.119 0.105 0.100 0.301 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 20:32 1

1.54 2.03 1.96 5.13 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0909 0.0512 0.0510 U

0.0444 Thorium 232 Tl-208 0.0504 0.0181 0.0189 0.0180 pCi/g 09/04/13 10:53 09/04/13 20:32 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-16 Client Sample ID: L050155TES00 Matrix: Solid Date Collected: 08/28/13 13:10 Percent Solids: 92.4 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.0048 0.00058 0.000018 mg/Kg

09/03/13 07:18 09/03/13 18:55 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 82.5 (2+/-)

8.67 (2+/-)

1 09/03/13 18:55 09/03/13 07:18 pCi/g 0.200 1.17 RL MDC 2.76 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 18:55 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 93 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.0982 (2+/-)

0.0557 (2+/-)

1 09/04/13 20:32 09/04/13 10:53 pCi/g 0.0892 RL MDC 0.0548 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0700 0.0411 0.0411 U

0.0000572 Americium 241 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.334 0.188 0.188 U

0.0536 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0358 0.112 0.0793 0.762 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0335 0.0288 0.0260 0.0956 Lead 212 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0476 0.104 0.0638 0.787 Lead 214 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.220 0.333 0.308 1.23 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.668 0.0753 0.0750 U

0.0624 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0358 1.00 0.112 0.0793 0.762 Radium 226 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.610 1.00 0.332 0.295 1.45 Thorium 234 pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.120 0.107 0.101 0.342 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 20:32 1

4.10 1.85 1.82 U

3.32 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 20:32 1

0.0892 0.0557 0.0548 0.0982 Thorium 232 Tl-208 0.0609 0.0191 0.0201 0.0173 pCi/g 09/04/13 10:53 09/04/13 20:32 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-17 Client Sample ID: L050156TRS00 Matrix: Solid Date Collected: 08/28/13 13:15 Percent Solids: 93.4 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00016 J

0.00054 0.000016 mg/Kg

09/03/13 07:18 09/03/13 19:06 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 2.75 (2+/-)

0.270 (2+/-)

1 09/03/13 19:06 09/03/13 07:18 pCi/g 0.184 1.08 RL MDC 0.0950 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 19:06 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 100 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.390 (2+/-)

0.0870 (2+/-)

1 09/04/13 20:35 09/04/13 10:53 pCi/g 0.0638 RL MDC 0.0774 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 20:35 1

0.0660 0.0388 0.0388 U

-0.000846 Americium 241 pCi/g 09/04/13 10:53 09/04/13 20:35 1

0.246 0.244 0.240 0.440 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 20:35 1

0.0325 0.0719 0.0551 0.444 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 20:35 1

0.0372 0.0591 0.0385 0.346 Lead 212 pCi/g 09/04/13 10:53 09/04/13 20:35 1

0.0415 0.0742 0.0499 0.528 Lead 214 pCi/g 09/04/13 10:53 09/04/13 20:35 1

0.171 1.04 0.653 7.97 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 20:35 1

0.619 0.187 0.186 U

0.136 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 20:35 1

0.0325 1.00 0.0719 0.0551 0.444 Radium 226 pCi/g 09/04/13 10:53 09/04/13 20:35 1

0.495 1.00 0.365 0.358 0.671 Thorium 234 pCi/g 09/04/13 10:53 09/04/13 20:35 1

0.142 0.0897 0.0894 U

0.0736 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 20:35 1

4.21 11.5 11.5 U

-0.287 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 20:35 1

0.0638 0.0870 0.0774 0.390 Thorium 232 Tl-208 0.131 0.0244 0.0279 0.0192 pCi/g 09/04/13 10:53 09/04/13 20:35 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-18 Client Sample ID: L050157TES00 Matrix: Solid Date Collected: 08/28/13 13:40 Percent Solids: 90.8 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000038 J

0.00058 0.000017 mg/Kg

09/03/13 07:18 09/03/13 19:10 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.657 (2+/-)

0.206 (2+/-)

1 09/03/13 19:10 09/03/13 07:18 pCi/g 0.199 1.16 RL MDC 0.187 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 19:10 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 95 TestAmerica St. Louis Page 25 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-18 Client Sample ID: L050157TES00 Matrix: Solid Date Collected: 08/28/13 13:40 Date Received: 08/29/13 18:38 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.419 (2+/-)

0.120 (2+/-)

1 09/04/13 21:23 09/04/13 10:53 pCi/g 0.0911 RL MDC 0.112 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 21:23 1

0.0743 0.0440 0.0439 U

0.0101 Americium 241 pCi/g 09/04/13 10:53 09/04/13 21:23 1

0.400 0.258 0.256 U

0.296 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 21:23 1

0.0337 0.0856 0.0675 0.506 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 21:23 1

0.0558 0.0711 0.0511 0.382 Lead 212 pCi/g 09/04/13 10:53 09/04/13 21:23 1

0.0615 0.0961 0.0777 0.543 Lead 214 pCi/g 09/04/13 10:53 09/04/13 21:23 1

0.251 1.13 0.805 7.73 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 21:23 1

0.784 0.123 0.122 U

0.129 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 21:23 1

0.0337 1.00 0.0856 0.0675 0.506 Radium 226 pCi/g 09/04/13 10:53 09/04/13 21:23 1

0.641 1.00 0.517 0.510 0.817 Thorium 234 pCi/g 09/04/13 10:53 09/04/13 21:23 1

0.177 0.106 0.106 U

0.0360 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 21:23 1

4.65 2.76 2.74 U

3.25 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 21:23 1

0.0911 0.120 0.112 0.419 Thorium 232 Tl-208 0.148 0.0341 0.0374 0.0297 pCi/g 09/04/13 10:53 09/04/13 21:23 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-19 Client Sample ID: L050162TRQ00 Matrix: Solid Date Collected: 08/28/13 11:10 Percent Solids: 83.7 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00010 J

0.00064 0.000019 mg/Kg

09/03/13 07:18 09/03/13 19:14 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.75 (2+/-)

0.174 (2+/-)

1 09/03/13 19:14 09/03/13 07:18 pCi/g 0.219 1.28 RL MDC 0.0165 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 19:14 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 93 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.996 (2+/-)

0.199 (2+/-)

1 09/04/13 22:00 09/04/13 10:53 pCi/g 0.111 RL MDC 0.171 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 22:00 1

0.132 0.0789 0.0788 U

-0.0326 Americium 241 pCi/g 09/04/13 10:53 09/04/13 22:00 1

0.657 0.447 0.441 0.718 Bismuth 212 pCi/g 09/04/13 10:53 09/04/13 22:00 1

0.0792 0.156 0.126 0.898 Bismuth 214 pCi/g 09/04/13 10:53 09/04/13 22:00 1

0.0721 0.172 0.0905 1.13 Lead 212 pCi/g 09/04/13 10:53 09/04/13 22:00 1

0.0836 0.139 0.0981 0.943 Lead 214 pCi/g 09/04/13 10:53 09/04/13 22:00 1

0.216 2.73 1.59 21.6 Potassium 40 pCi/g 09/04/13 10:53 09/04/13 22:00 1

1.43 0.443 0.435 U

0.803 Protactinium 231 pCi/g 09/04/13 10:53 09/04/13 22:00 1

0.0792 1.00 0.156 0.126 0.898 Radium 226 TestAmerica St. Louis Page 26 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-19 Client Sample ID: L050162TRQ00 Matrix: Solid Date Collected: 08/28/13 11:10 Date Received: 08/29/13 18:38 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 1.77 (2+/-)

0.873 (2+/-)

1 09/04/13 22:00 09/04/13 10:53 pCi/g 1.08 1.00 RL MDC 0.853 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/04/13 22:00 1

0.279 0.183 0.181 U

0.219 Uranium 235 pCi/g 09/04/13 10:53 09/04/13 22:00 1

7.05 4.11 4.11 U

1.95 Protactinium 234m pCi/g 09/04/13 10:53 09/04/13 22:00 1

0.111 0.199 0.171 0.996 Thorium 232 Tl-208 0.406 0.0678 0.0798 0.0504 pCi/g 09/04/13 10:53 09/04/13 22:00 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-20 Client Sample ID: L050162TRS00 Matrix: Solid Date Collected: 08/28/13 11:10 Percent Solids: 82.5 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000088 J

0.00066 0.000020 mg/Kg

09/03/13 07:18 09/03/13 19:18 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.50 (2+/-)

0.261 (2+/-)

1 09/03/13 19:18 09/03/13 07:18 pCi/g 0.224 1.31 RL MDC 0.195 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 09/03/13 07:18 09/03/13 19:18 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.27 (2+/-)

0.202 (2+/-)

1 09/05/13 08:40 09/04/13 10:53 pCi/g 0.112 RL MDC 0.155 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 10:53 09/05/13 08:40 1

0.114 0.0687 0.0687 U

0.0260 Americium 241 pCi/g 09/04/13 10:53 09/05/13 08:40 1

0.477 0.577 0.551 1.64 Bismuth 212 pCi/g 09/04/13 10:53 09/05/13 08:40 1

0.0703 0.140 0.101 0.939 Bismuth 214 pCi/g 09/04/13 10:53 09/05/13 08:40 1

0.0869 0.155 0.0797 1.02 Lead 212 pCi/g 09/04/13 10:53 09/05/13 08:40 1

0.0820 0.149 0.101 1.05 Lead 214 pCi/g 09/04/13 10:53 09/05/13 08:40 1

0.418 2.40 1.19 20.4 Potassium 40 pCi/g 09/04/13 10:53 09/05/13 08:40 1

1.09 0.384 0.381 U

0.466 Protactinium 231 pCi/g 09/04/13 10:53 09/05/13 08:40 1

0.0703 1.00 0.140 0.101 0.939 Radium 226 pCi/g 09/04/13 10:53 09/05/13 08:40 1

0.955 1.00 0.811 0.792 1.66 Thorium 234 pCi/g 09/04/13 10:53 09/05/13 08:40 1

0.190 0.132 0.128 0.296 Uranium 235 pCi/g 09/04/13 10:53 09/05/13 08:40 1

5.08 2.92 2.92 U

0.711 Protactinium 234m pCi/g 09/04/13 10:53 09/05/13 08:40 1

0.112 0.202 0.155 1.27 Thorium 232 Tl-208 0.353 0.0446 0.0578 0.0325 pCi/g 09/04/13 10:53 09/05/13 08:40 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 27 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-21 Client Sample ID: L050163TES00 Matrix: Solid Date Collected: 08/28/13 14:00 Percent Solids: 83.0 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000025 J

0.00063 0.000019 mg/Kg

08/30/13 10:44 09/03/13 19:29 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.435 (2+/-)

0.0905 (2+/-)

1 09/03/13 19:29 08/30/13 10:44 pCi/g 0.217 1.27 RL MDC 0.0752 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/30/13 10:44 09/03/13 19:29 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 94 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.03 (2+/-)

0.183 (2+/-)

1 09/04/13 21:58 09/04/13 13:12 pCi/g 0.126 RL MDC 0.150 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 13:12 09/04/13 21:58 1

0.118 0.0695 0.0695 U

0.00255 Americium 241 pCi/g 09/04/13 13:12 09/04/13 21:58 1

0.597 0.430 0.421 0.864 Bismuth 212 pCi/g 09/04/13 13:12 09/04/13 21:58 1

0.0604 0.135 0.105 0.809 Bismuth 214 pCi/g 09/04/13 13:12 09/04/13 21:58 1

0.0735 0.157 0.0849 1.02 Lead 212 pCi/g 09/04/13 13:12 09/04/13 21:58 1

0.0816 0.116 0.0879 0.731 Lead 214 pCi/g 09/04/13 13:12 09/04/13 21:58 1

0.460 2.43 1.46 19.0 Potassium 40 pCi/g 09/04/13 13:12 09/04/13 21:58 1

1.40 0.261 0.258 U

0.367 Protactinium 231 pCi/g 09/04/13 13:12 09/04/13 21:58 1

0.0604 1.00 0.135 0.105 0.809 Radium 226 pCi/g 09/04/13 13:12 09/04/13 21:58 1

0.885 1.00 0.378 0.369 U

0.791 Thorium 234 pCi/g 09/04/13 13:12 09/04/13 21:58 1

0.261 0.135 0.134 U

0.0918 Uranium 235 pCi/g 09/04/13 13:12 09/04/13 21:58 1

6.20 2.43 2.42 U

1.23 Protactinium 234m pCi/g 09/04/13 13:12 09/04/13 21:58 1

0.126 0.183 0.150 1.03 Thorium 232 Tl-208 0.304 0.0600 0.0677 0.0496 pCi/g 09/04/13 13:12 09/04/13 21:58 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-22 Client Sample ID: L050164TRS00 Matrix: Solid Date Collected: 08/28/13 10:55 Percent Solids: 83.4 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000029 J

0.00069 0.000021 mg/Kg

08/30/13 10:44 09/03/13 19:41 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.503 (2+/-)

0.0629 (2+/-)

1 09/03/13 19:41 08/30/13 10:44 pCi/g 0.235 1.37 RL MDC 0.0295 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/30/13 10:44 09/03/13 19:41 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 87 TestAmerica St. Louis Page 28 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-22 Client Sample ID: L050164TRS00 Matrix: Solid Date Collected: 08/28/13 10:55 Date Received: 08/29/13 18:38 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.973 (2+/-)

0.178 (2+/-)

1 09/04/13 22:01 09/04/13 13:12 pCi/g 0.0944 RL MDC 0.148 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 13:12 09/04/13 22:01 1

0.0953 0.0569 0.0569 U

0.0179 Americium 241 pCi/g 09/04/13 13:12 09/04/13 22:01 1

0.330 0.410 0.383 1.39 Bismuth 212 pCi/g 09/04/13 13:12 09/04/13 22:01 1

0.0746 0.123 0.0969 0.733 Bismuth 214 pCi/g 09/04/13 13:12 09/04/13 22:01 1

0.0580 0.154 0.0705 1.06 Lead 212 pCi/g 09/04/13 13:12 09/04/13 22:01 1

0.0656 0.119 0.0863 0.788 Lead 214 pCi/g 09/04/13 13:12 09/04/13 22:01 1

0.381 2.30 1.16 19.4 Potassium 40 pCi/g 09/04/13 13:12 09/04/13 22:01 1

1.04 0.641 0.638 U

-0.593 Protactinium 231 pCi/g 09/04/13 13:12 09/04/13 22:01 1

0.0746 1.00 0.123 0.0969 0.733 Radium 226 pCi/g 09/04/13 13:12 09/04/13 22:01 1

0.815 1.00 0.656 0.635 1.56 Thorium 234 pCi/g 09/04/13 13:12 09/04/13 22:01 1

0.210 0.129 0.128 U

0.0894 Uranium 235 pCi/g 09/04/13 13:12 09/04/13 22:01 1

5.36 9.06 9.06 U

-0.683 Protactinium 234m pCi/g 09/04/13 13:12 09/04/13 22:01 1

0.0944 0.178 0.148 0.973 Thorium 232 Tl-208 0.311 0.0435 0.0541 0.0344 pCi/g 09/04/13 13:12 09/04/13 22:01 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-23 Client Sample ID: L050165TEQ00 Matrix: Solid Date Collected: 08/28/13 11:05 Percent Solids: 80.0 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00068 0.000021 mg/Kg

08/30/13 10:44 09/03/13 19:53 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.200 U

(2+/-)

0.0678 (2+/-)

1 09/03/13 19:53 08/30/13 10:44 pCi/g 0.234 1.37 RL MDC 0.0595 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/30/13 10:44 09/03/13 19:53 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 92 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.13 (2+/-)

0.199 (2+/-)

1 09/04/13 22:35 09/04/13 13:12 pCi/g 0.128 RL MDC 0.163 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 13:12 09/04/13 22:35 1

0.102 0.0611 0.0611 U

-0.0296 Americium 241 pCi/g 09/04/13 13:12 09/04/13 22:35 1

0.554 0.685 0.663 1.65 Bismuth 212 pCi/g 09/04/13 13:12 09/04/13 22:35 1

0.0847 0.148 0.123 0.797 Bismuth 214 pCi/g 09/04/13 13:12 09/04/13 22:35 1

0.0729 0.165 0.0898 1.07 Lead 212 pCi/g 09/04/13 13:12 09/04/13 22:35 1

0.0826 0.134 0.0970 0.885 Lead 214 pCi/g 09/04/13 13:12 09/04/13 22:35 1

0.438 2.34 1.51 17.5 Potassium 40 pCi/g 09/04/13 13:12 09/04/13 22:35 1

1.56 0.256 0.252 U

0.400 Protactinium 231 pCi/g 09/04/13 13:12 09/04/13 22:35 1

0.0847 1.00 0.148 0.123 0.797 Radium 226 TestAmerica St. Louis Page 29 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-23 Client Sample ID: L050165TEQ00 Matrix: Solid Date Collected: 08/28/13 11:05 Date Received: 08/29/13 18:38 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 1.01 U

(2+/-)

0.379 (2+/-)

1 09/04/13 22:35 09/04/13 13:12 pCi/g 1.04 1.00 RL MDC 0.364 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 13:12 09/04/13 22:35 1

0.261 0.156 0.156 U

0.0821 Uranium 235 pCi/g 09/04/13 13:12 09/04/13 22:35 1

7.38 4.21 4.20 U

1.31 Protactinium 234m pCi/g 09/04/13 13:12 09/04/13 22:35 1

0.128 0.199 0.163 1.13 Thorium 232 Tl-208 0.354 0.0560 0.0669 0.0375 pCi/g 09/04/13 13:12 09/04/13 22:35 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-24 Client Sample ID: L050165TES00 Matrix: Solid Date Collected: 08/28/13 11:05 Percent Solids: 81.2 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00065 0.000020 mg/Kg

08/30/13 10:44 09/03/13 19:57 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.163 U

(2+/-)

0.0769 (2+/-)

1 09/03/13 19:57 08/30/13 10:44 pCi/g 0.223 1.31 RL MDC 0.0708 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/30/13 10:44 09/03/13 19:57 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 94 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.18 (2+/-)

0.201 (2+/-)

1 09/04/13 22:36 09/04/13 13:12 pCi/g 0.135 RL MDC 0.162 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 13:12 09/04/13 22:36 1

0.109 0.0651 0.0651 U

0.0178 Americium 241 pCi/g 09/04/13 13:12 09/04/13 22:36 1

0.505 0.393 0.377 1.08 Bismuth 212 pCi/g 09/04/13 13:12 09/04/13 22:36 1

0.0645 0.119 0.0919 0.726 Bismuth 214 pCi/g 09/04/13 13:12 09/04/13 22:36 1

0.0575 0.166 0.0770 1.14 Lead 212 pCi/g 09/04/13 13:12 09/04/13 22:36 1

0.0682 0.125 0.0904 0.835 Lead 214 pCi/g 09/04/13 13:12 09/04/13 22:36 1

0.403 2.37 1.24 19.8 Potassium 40 pCi/g 09/04/13 13:12 09/04/13 22:36 1

1.20 0.309 0.298 U

0.750 Protactinium 231 pCi/g 09/04/13 13:12 09/04/13 22:36 1

0.0645 1.00 0.119 0.0919 0.726 Radium 226 pCi/g 09/04/13 13:12 09/04/13 22:36 1

0.866 1.00 0.660 0.647 1.23 Thorium 234 pCi/g 09/04/13 13:12 09/04/13 22:36 1

0.262 0.151 0.151 U

0.120 Uranium 235 pCi/g 09/04/13 13:12 09/04/13 22:36 1

6.07 2.52 2.48 U

4.78 Protactinium 234m pCi/g 09/04/13 13:12 09/04/13 22:36 1

0.135 0.201 0.162 1.18 Thorium 232 Tl-208 0.336 0.0468 0.0584 0.0363 pCi/g 09/04/13 13:12 09/04/13 22:36 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 30 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-25 Client Sample ID: L050169TSS00 Matrix: Solid Date Collected: 08/28/13 13:10 Percent Solids: 97.8 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00057 0.000017 mg/Kg

08/30/13 10:44 09/03/13 20:00 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.131 U

(2+/-)

0.0336 (2+/-)

1 09/03/13 20:00 08/30/13 10:44 pCi/g 0.195 1.14 RL MDC 0.0277 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/30/13 10:44 09/03/13 20:00 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.159 (2+/-)

0.0581 (2+/-)

1 09/04/13 22:37 09/04/13 13:12 pCi/g 0.0708 RL MDC 0.0558 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 13:12 09/04/13 22:37 1

0.0455 0.0270 0.0270 U

-0.00987 Americium 241 pCi/g 09/04/13 13:12 09/04/13 22:37 1

0.206 0.130 0.129 U

0.127 Bismuth 212 pCi/g 09/04/13 13:12 09/04/13 22:37 1

0.0383 0.0504 0.0447 0.225 Bismuth 214 pCi/g 09/04/13 13:12 09/04/13 22:37 1

0.0325 0.0349 0.0296 0.143 Lead 212 pCi/g 09/04/13 13:12 09/04/13 22:37 1

0.0323 0.0450 0.0380 0.232 Lead 214 pCi/g 09/04/13 13:12 09/04/13 22:37 1

0.165 0.791 0.502 5.97 Potassium 40 pCi/g 09/04/13 13:12 09/04/13 22:37 1

0.536 0.0319 0.0317 U

0.0331 Protactinium 231 pCi/g 09/04/13 13:12 09/04/13 22:37 1

0.0383 1.00 0.0504 0.0447 0.225 Radium 226 pCi/g 09/04/13 13:12 09/04/13 22:37 1

0.466 1.00 0.148 0.147 U

0.156 Thorium 234 pCi/g 09/04/13 13:12 09/04/13 22:37 1

0.0916 0.0459 0.0457 U

0.0302 Uranium 235 pCi/g 09/04/13 13:12 09/04/13 22:37 1

2.42 1.32 1.32 U

-0.0205 Protactinium 234m pCi/g 09/04/13 13:12 09/04/13 22:37 1

0.0708 0.0581 0.0558 0.159 Thorium 232 Tl-208 0.0555 0.0170 0.0180 0.0150 pCi/g 09/04/13 13:12 09/04/13 22:37 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-26 Client Sample ID: L050170TRS00 Matrix: Solid Date Collected: 08/28/13 13:30 Percent Solids: 96.4 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.25 0.0074 mg/Kg

08/30/13 10:44 09/03/13 20:04 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 40.5 U

(2+/-)

2720000 (2+/-)

1 09/03/13 20:04 08/30/13 10:44 pCi/g 84.1 491 RL MDC 5740 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier X

08/30/13 10:44 09/03/13 20:04 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 0.2 TestAmerica St. Louis Page 31 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-26 Client Sample ID: L050170TRS00 Matrix: Solid Date Collected: 08/28/13 13:30 Date Received: 08/29/13 18:38 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.229 (2+/-)

0.0641 (2+/-)

1 09/04/13 22:40 09/04/13 13:12 pCi/g 0.0468 RL MDC 0.0597 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 13:12 09/04/13 22:40 1

0.0439 0.0254 0.0254 U

0.00363 Americium 241 pCi/g 09/04/13 13:12 09/04/13 22:40 1

0.268 0.151 0.151 U

0.0428 Bismuth 212 pCi/g 09/04/13 13:12 09/04/13 22:40 1

0.0546 0.0475 0.0439 0.176 Bismuth 214 pCi/g 09/04/13 13:12 09/04/13 22:40 1

0.0291 0.0341 0.0282 0.149 Lead 212 pCi/g 09/04/13 13:12 09/04/13 22:40 1

0.0344 0.0476 0.0379 0.276 Lead 214 pCi/g 09/04/13 13:12 09/04/13 22:40 1

0.183 0.838 0.586 5.85 Potassium 40 pCi/g 09/04/13 13:12 09/04/13 22:40 1

0.530 0.110 0.109 U

0.0702 Protactinium 231 pCi/g 09/04/13 13:12 09/04/13 22:40 1

0.0546 1.00 0.0475 0.0439 0.176 Radium 226 pCi/g 09/04/13 13:12 09/04/13 22:40 1

0.467 1.00 0.161 0.159 U

0.222 Thorium 234 pCi/g 09/04/13 13:12 09/04/13 22:40 1

0.102 0.0636 0.0634 U

0.0473 Uranium 235 pCi/g 09/04/13 13:12 09/04/13 22:40 1

2.29 1.23 1.23 U

0.254 Protactinium 234m pCi/g 09/04/13 13:12 09/04/13 22:40 1

0.0468 0.0641 0.0597 0.229 Thorium 232 Tl-208 0.0719 0.0185 0.0199 0.0160 pCi/g 09/04/13 13:12 09/04/13 22:40 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-27 Client Sample ID: L050171TRS00 Matrix: Solid Date Collected: 08/28/13 11:00 Percent Solids: 83.3 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00066 0.000020 mg/Kg

08/30/13 10:44 09/03/13 20:08 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.153 U

(2+/-)

0.0551 (2+/-)

1 09/03/13 20:08 08/30/13 10:44 pCi/g 0.227 1.33 RL MDC 0.0477 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/30/13 10:44 09/03/13 20:08 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 90 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.26 (2+/-)

0.217 (2+/-)

1 09/04/13 22:39 09/04/13 13:12 pCi/g 0.159 RL MDC 0.174 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 13:12 09/04/13 22:39 1

0.131 0.0787 0.0786 U

-0.0416 Americium 241 pCi/g 09/04/13 13:12 09/04/13 22:39 1

0.278 0.544 0.493 2.23 Bismuth 212 pCi/g 09/04/13 13:12 09/04/13 22:39 1

0.0929 0.139 0.115 0.742 Bismuth 214 pCi/g 09/04/13 13:12 09/04/13 22:39 1

0.0833 0.170 0.0927 1.10 Lead 212 pCi/g 09/04/13 13:12 09/04/13 22:39 1

0.0834 0.157 0.119 0.977 Lead 214 pCi/g 09/04/13 13:12 09/04/13 22:39 1

0.620 2.56 1.59 19.6 Potassium 40 pCi/g 09/04/13 13:12 09/04/13 22:39 1

1.50 0.247 0.242 U

0.439 Protactinium 231 pCi/g 09/04/13 13:12 09/04/13 22:39 1

0.0929 1.00 0.139 0.115 0.742 Radium 226 TestAmerica St. Louis Page 32 of 45 1

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Client Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-3571-27 Client Sample ID: L050171TRS00 Matrix: Solid Date Collected: 08/28/13 11:00 Date Received: 08/29/13 18:38 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 1.43 (2+/-)

0.840 (2+/-)

1 09/04/13 22:39 09/04/13 13:12 pCi/g 1.05 1.00 RL MDC 0.827 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 13:12 09/04/13 22:39 1

0.244 0.171 0.171 U

0.126 Uranium 235 pCi/g 09/04/13 13:12 09/04/13 22:39 1

7.06 3.94 3.94 U

-0.577 Protactinium 234m pCi/g 09/04/13 13:12 09/04/13 22:39 1

0.159 0.217 0.174 1.26 Thorium 232 Tl-208 0.416 0.0761 0.0875 0.0597 pCi/g 09/04/13 13:12 09/04/13 22:39 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-3571-28 Client Sample ID: L050172TES00 Matrix: Solid Date Collected: 08/28/13 11:15 Percent Solids: 85.1 Date Received: 08/29/13 18:38 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.00065 0.000020 mg/Kg

08/30/13 10:44 09/03/13 20:12 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.203 U

(2+/-)

0.0293 (2+/-)

1 09/03/13 20:12 08/30/13 10:44 pCi/g 0.223 1.30 RL MDC 0.0184 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 08/30/13 10:44 09/03/13 20:12 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 89 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.12 (2+/-)

0.194 (2+/-)

1 09/04/13 23:14 09/04/13 13:12 pCi/g 0.148 RL MDC 0.157 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 09/04/13 13:12 09/04/13 23:14 1

0.0994 0.0591 0.0591 U

0.0223 Americium 241 pCi/g 09/04/13 13:12 09/04/13 23:14 1

0.649 0.447 0.441 0.746 Bismuth 212 pCi/g 09/04/13 13:12 09/04/13 23:14 1

0.0747 0.160 0.127 0.950 Bismuth 214 pCi/g 09/04/13 13:12 09/04/13 23:14 1

0.0775 0.166 0.0910 1.08 Lead 212 pCi/g 09/04/13 13:12 09/04/13 23:14 1

0.110 0.167 0.134 0.956 Lead 214 pCi/g 09/04/13 13:12 09/04/13 23:14 1

0.221 2.62 1.57 20.5 Potassium 40 pCi/g 09/04/13 13:12 09/04/13 23:14 1

1.23 0.484 0.470 U

1.06 Protactinium 231 pCi/g 09/04/13 13:12 09/04/13 23:14 1

0.0747 1.00 0.160 0.127 0.950 Radium 226 pCi/g 09/04/13 13:12 09/04/13 23:14 1

0.936 1.00 0.687 0.671 1.41 Thorium 234 pCi/g 09/04/13 13:12 09/04/13 23:14 1

0.293 0.109 0.108 U

0.0652 Uranium 235 pCi/g 09/04/13 13:12 09/04/13 23:14 1

7.18 3.26 3.22 U

5.20 Protactinium 234m pCi/g 09/04/13 13:12 09/04/13 23:14 1

0.148 0.194 0.157 1.12 Thorium 232 Tl-208 0.390 0.0615 0.0736 0.0475 pCi/g 09/04/13 13:12 09/04/13 23:14 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 33 of 45 1

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QC Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-69983/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70530 Prep Batch: 69983 RL MDL Technetium 99 ND 0.00050 0.000015 mg/Kg 08/30/13 10:44 09/03/13 19:22 1

MB MB Analyte Dil Fac Analyzed Prepared D

Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-69983/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70530 Prep Batch: 69983 Technetium 99 0.00237 0.00248 mg/Kg 104 80 - 120 Analyte LCS LCS D

Unit Result Qualifier

%Rec Spike Added

%Rec.

Limits Client Sample ID: L050163TES00 Lab Sample ID: 160-3571-21 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 70530 Prep Batch: 69983 Technetium 99 0.000025 J

0.00316 0.00298 mg/Kg 93 75 - 125

Analyte MS MS D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Client Sample ID: L050163TES00 Lab Sample ID: 160-3571-21 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 70530 Prep Batch: 69983 Technetium 99 0.000025 J

0.00311 0.00292 mg/Kg 93 75 - 125 2

30

Analyte MSD MSD D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Limit RPD RPD Client Sample ID: Method Blank Lab Sample ID: MB 160-70096/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70530 Prep Batch: 70096 RL MDL Technetium 99 ND 0.00052 0.000016 mg/Kg 09/03/13 07:18 09/03/13 17:33 1

MB MB Analyte Dil Fac Analyzed Prepared D

Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-70096/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70530 Prep Batch: 70096 Technetium 99 0.00234 0.00241 mg/Kg 103 80 - 120 Analyte LCS LCS D

Unit Result Qualifier

%Rec Spike Added

%Rec.

Limits Client Sample ID: L050119TSQ00 Lab Sample ID: 160-3571-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 70530 Prep Batch: 70096 Technetium 99 0.000018 J

0.00295 0.00268 mg/Kg 91 75 - 125

Analyte MS MS D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Client Sample ID: L050119TSQ00 Lab Sample ID: 160-3571-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 70530 Prep Batch: 70096 Technetium 99 0.000018 J

0.00289 0.00268 mg/Kg 93 75 - 125 0

30

Analyte MSD MSD D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Limit RPD RPD TestAmerica St. Louis Page 34 of 45 1

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QC Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-69983/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70531 Prep Batch: 69983 Technetium 99 Analyte U

1 09/03/13 19:22 08/30/13 10:44 pCi/g 0.170 MDC 0.991 RL 0.0456 0.0449 (2+/-)

(2+/-)

MB 0.1284 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Carrier Re 30 - 110 08/30/13 10:44 09/03/13 19:22 1

Dil Fac Prepared Analyzed Qualifier Limits

%Yield 102 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-69983/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70531 Prep Batch: 69983 Technetium 99 Analyte 120 80 104 42.40 40.7 3.96 1.02 0.174 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 LCS Qualifier Limits

%Yield 99 LCS Client Sample ID: L050163TES00 Lab Sample ID: 160-3571-21 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 70531 Prep Batch: 69983 Technetium 99 Analyte 125 75 93 50.98 54.1 0.435 5.57 1.35 0.231 RL MDC (2+/-)

MS MS pCi/g Unit Result Qual

%Rec Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 MS Qualifier Limits

%Yield 90 MS Client Sample ID: L050163TES00 Lab Sample ID: 160-3571-21 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 70531 Prep Batch: 69983 Technetium 99 Analyte 1

0.09 125 75 93 49.98 53.3 0.435 5.13 1.33 0.228 RL MDC (2+/-)

MSD MSD pCi/g Unit Result Qual

%Rec Limit Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits

%Yield 90 MSD Client Sample ID: Method Blank Lab Sample ID: MB 160-70096/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70531 Prep Batch: 70096 Technetium 99 Analyte U

1 09/03/13 17:33 09/03/13 07:18 pCi/g 0.178 MDC 1.04 RL 0.0395 0.0374 (2+/-)

(2+/-)

MB 0.08381 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total TestAmerica St. Louis Page 35 of 45 1

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QC Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)

Client Sample ID: Method Blank Lab Sample ID: MB 160-70096/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70531 Prep Batch: 70096 Carrier Re 30 - 110 09/03/13 07:18 09/03/13 17:33 1

Dil Fac Prepared Analyzed Qualifier Limits

%Yield 97 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-70096/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70531 Prep Batch: 70096 Technetium 99 Analyte 120 80 103 41.32 40.1 3.99 1.00 0.172 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 LCS Qualifier Limits

%Yield 100 LCS Client Sample ID: L050119TSQ00 Lab Sample ID: 160-3571-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 70531 Prep Batch: 70096 Technetium 99 Analyte 125 75 90 45.86 50.4 0.300 5.26 1.26 0.216 RL MDC (2+/-)

MS MS pCi/g Unit Result Qual

%Rec Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 MS Qualifier Limits

%Yield 89 MS Client Sample ID: L050119TSQ00 Lab Sample ID: 160-3571-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 70531 Prep Batch: 70096 Technetium 99 Analyte 1

0 125 75 92 45.88 49.6 0.300 5.14 1.24 0.212 RL MDC (2+/-)

MSD MSD pCi/g Unit Result Qual

%Rec Limit Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits

%Yield 90 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-70555/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70404 Prep Batch: 70555 Actinium 228 Analyte U

1 09/04/13 19:10 09/04/13 10:53 pCi/g 0.0414 MDC RL 0.0112 0.0112 (2+/-)

(2+/-)

MB 0.001613 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

09/04/13 19:10 09/04/13 10:53 pCi/g 0.0189 0.0114 0.0114 U

0.008326 Americium 241 1

09/04/13 19:10 09/04/13 10:53 pCi/g 0.207 0.0979 0.0979 U

0.003871 Bismuth 212 1

09/04/13 19:10 09/04/13 10:53 pCi/g 0.0391 0.0215 0.0215 U

0.007521 Bismuth 214 TestAmerica St. Louis Page 36 of 45 1

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QC Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: Method Blank Lab Sample ID: MB 160-70555/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70404 Prep Batch: 70555 Lead 212 Analyte U

1 09/04/13 19:10 09/04/13 10:53 pCi/g 0.0297 MDC RL 0.0242 0.0242 (2+/-)

(2+/-)

MB

-0.002086 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

09/04/13 19:10 09/04/13 10:53 pCi/g 0.0316 0.0145 0.0145 U

0.0006809 Lead 214 1

09/04/13 19:10 09/04/13 10:53 pCi/g 0.174 0.141 0.140 U

0.1609 Potassium 40 1

09/04/13 19:10 09/04/13 10:53 pCi/g 0.440 0.246 0.245 U

-0.07701 Protactinium 231 1

09/04/13 19:10 09/04/13 10:53 pCi/g 0.0391 1.00 0.0215 0.0215 U

0.007521 Radium 226 1

09/04/13 19:10 09/04/13 10:53 pCi/g 0.271 1.00 0.126 0.125 U

0.03321 Thorium 234 1

09/04/13 19:10 09/04/13 10:53 pCi/g 0.0617 0.0335 0.0335 U

-0.006296 Uranium 235 1

09/04/13 19:10 09/04/13 10:53 pCi/g 3.73 0.600 0.600 U

0.0000 Protactinium 234m 1

09/04/13 19:10 09/04/13 10:53 pCi/g 0.0414 0.0112 0.0112 U

0.001613 Thorium 232 Other Detected Radionuclide None MB (2+/-)

(2+/-)

MDC RL pCi/g 09/04/13 10:53 09/04/13 19:10 1

MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-70555/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70571 Prep Batch: 70555 Americium 241 Analyte 116 87 93 90.94 97.7 9.46 0.494 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 31.6 30.32 3.17 0.200 0.108 pCi/g 96 87 - 120 Cobalt 60 24.7 23.15 2.34 0.0565 pCi/g 94 87 - 115 Client Sample ID: L050162TRS00 Lab Sample ID: 160-3571-20 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 70839 Prep Batch: 70555 Actinium 228 Analyte 1

0.04 1.251 1.27 0.204 0.133 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Americium 241 0.0260 U

0.06001 U

0.0583 0.0831 pCi/g 0.27 1

Bismuth 212 1.64 1.657 0.466 0.324 pCi/g 0.01 1

Bismuth 214 0.939 0.8695 0.150 0.0867 pCi/g 0.24 1

Lead 212 1.02 1.202 0.176 0.0643 pCi/g 0.54 1

Lead 214 1.05 0.9296 0.130 0.0749 pCi/g 0.44 1

Potassium 40 20.4 20.59 2.50 0.359 pCi/g 0.04 1

Protactinium 231 0.466 U

-0.6526 U

0.791 1.30 pCi/g 0.95 1

Radium 226 0.939 0.8695 0.150 1.00 0.0867 pCi/g 0.24 1

Thorium 234 1.66 1.924 0.769 1.00 0.920 pCi/g 0.17 1

Uranium 235 0.296 0.1022 U

0.139 0.265 pCi/g 0.71 1

Protactinium 234m 0.711 U

1.687 U

3.61 6.16 pCi/g 0.15 1

Thorium 232 1.27 1.251 0.204 0.133 pCi/g 0.04 1

TestAmerica St. Louis Page 37 of 45 1

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QC Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: Method Blank Lab Sample ID: MB 160-70600/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70572 Prep Batch: 70600 Actinium 228 Analyte U

1 09/04/13 21:58 09/04/13 13:12 pCi/g 0.0465 MDC RL 0.0191 0.0191 (2+/-)

(2+/-)

MB 0.008675 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

09/04/13 21:58 09/04/13 13:12 pCi/g 0.0189 0.0114 0.0114 U

0.008474 Americium 241 1

09/04/13 21:58 09/04/13 13:12 pCi/g 0.122 0.0575 0.0575 U

0.001267 Bismuth 212 1

09/04/13 21:58 09/04/13 13:12 pCi/g 0.0396 0.0879 0.0879 U

-0.01059 Bismuth 214 1

09/04/13 21:58 09/04/13 13:12 pCi/g 0.0188 0.00978 0.00975 U

0.006140 Lead 212 1

09/04/13 21:58 09/04/13 13:12 pCi/g 0.0346 0.470 0.470 U

-0.01411 Lead 214 1

09/04/13 21:58 09/04/13 13:12 pCi/g 0.239 0.180 0.180 U

-0.03629 Potassium 40 1

09/04/13 21:58 09/04/13 13:12 pCi/g 0.299 0.159 0.159 U

-0.0007753 Protactinium 231 1

09/04/13 21:58 09/04/13 13:12 pCi/g 0.0396 1.00 0.0879 0.0879 U

-0.01059 Radium 226 1

09/04/13 21:58 09/04/13 13:12 pCi/g 0.224 1.00 0.107 0.107 U

0.01706 Thorium 234 1

09/04/13 21:58 09/04/13 13:12 pCi/g 0.0675 0.000412 0.000412 U

0.0001144 Uranium 235 1

09/04/13 21:58 09/04/13 13:12 pCi/g 2.00 0.923 0.923 U

0.1530 Protactinium 234m 1

09/04/13 21:58 09/04/13 13:12 pCi/g 0.0465 0.0191 0.0191 U

0.008675 Thorium 232 Other Detected Radionuclide None MB (2+/-)

(2+/-)

MDC RL pCi/g 09/04/13 13:12 09/04/13 21:58 1

MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-70600/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 70581 Prep Batch: 70600 Americium 241 Analyte 116 87 95 92.66 97.7 9.64 0.473 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 31.6 30.45 3.19 0.200 0.151 pCi/g 96 87 - 120 Cobalt 60 24.7 23.85 2.41 0.0926 pCi/g 97 87 - 115 Client Sample ID: Duplicate Lab Sample ID: 160-3570-A-8-E DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 70581 Prep Batch: 70600 Actinium 228 Analyte 1

0.07 0.7632 0.746 0.131 0.0839 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Americium 241 0.00169 U

-0.00281 7

U 0.133 0.0903 pCi/g 0.02 1

Bismuth 212 1.07 1.003 0.418 0.377 pCi/g 0.09 1

Bismuth 214 0.632 0.6603 0.114 0.0643 pCi/g 0.13 1

Lead 212 0.714 0.6978 0.109 0.0519 pCi/g 0.07 1

Lead 214 0.746 0.6657 0.0985 0.0592 pCi/g 0.39 1

Potassium 40 14.5 13.92 1.77 0.247 pCi/g 0.15 1

Protactinium 231 0.383 U

0.1268 U

0.117 1.06 pCi/g 0.70 1

Radium 226 0.632 0.6603 0.114 1.00 0.0643 pCi/g 0.13 1

Thorium 234 2.02 1.647 0.373 1.00 0.779 pCi/g 0.36 1

Uranium 235 0.403 0.4261 0.169 0.189 pCi/g 0.08 1

TestAmerica St. Louis Page 38 of 45 1

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QC Sample Results TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: Duplicate Lab Sample ID: 160-3570-A-8-E DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 70581 Prep Batch: 70600 Protactinium 234m Analyte 1

0.26 U

3.462 1.97 U

2.95 4.55 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Thorium 232 0.746 0.7632 0.131 0.0839 pCi/g 0.07 1

TestAmerica St. Louis Page 39 of 45 1

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QC Association Summary TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Metals Prep Batch: 69983 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3571-21 L050163TES00 Total/NA Solid None 160-3571-21 MS L050163TES00 Total/NA Solid None 160-3571-21 MSD L050163TES00 Total/NA Solid None 160-3571-22 L050164TRS00 Total/NA Solid None 160-3571-23 L050165TEQ00 Total/NA Solid None 160-3571-24 L050165TES00 Total/NA Solid None 160-3571-25 L050169TSS00 Total/NA Solid None 160-3571-26 L050170TRS00 Total/NA Solid None 160-3571-27 L050171TRS00 Total/NA Solid None 160-3571-28 L050172TES00 Total/NA Solid None LCS 160-69983/2-A Lab Control Sample Total/NA Solid None MB 160-69983/1-A Method Blank Total/NA Prep Batch: 70096 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3571-1 L050119TSQ00 Total/NA Solid None 160-3571-1 MS L050119TSQ00 Total/NA Solid None 160-3571-1 MSD L050119TSQ00 Total/NA Solid None 160-3571-2 L050119TSS00 Total/NA Solid None 160-3571-3 L050120TRS00 Total/NA Solid None 160-3571-4 L050121TSS00 Total/NA Solid None 160-3571-5 L050122TRS00 Total/NA Solid None 160-3571-6 L050125TRS00 Total/NA Solid None 160-3571-7 L050127TRS00 Total/NA Solid None 160-3571-8 L050128TES00 Total/NA Solid None 160-3571-9 L050131TRS00 Total/NA Solid None 160-3571-10 L050132TES00 Total/NA Solid None 160-3571-11 L050133TRS00 Total/NA Solid None 160-3571-12 L050139TES00 Total/NA Solid None 160-3571-13 L050140TRS00 Total/NA Solid None 160-3571-14 L050148TRS00 Total/NA Solid None 160-3571-15 L050154TRS00 Total/NA Solid None 160-3571-16 L050155TES00 Total/NA Solid None 160-3571-17 L050156TRS00 Total/NA Solid None 160-3571-18 L050157TES00 Total/NA Solid None 160-3571-19 L050162TRQ00 Total/NA Solid None 160-3571-20 L050162TRS00 Total/NA Solid None LCS 160-70096/2-A Lab Control Sample Total/NA Solid None MB 160-70096/1-A Method Blank Total/NA Analysis Batch: 70530 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 70096 160-3571-1 L050119TSQ00 Total/NA Solid 6020A 70096 160-3571-1 MS L050119TSQ00 Total/NA Solid 6020A 70096 160-3571-1 MSD L050119TSQ00 Total/NA Solid 6020A 70096 160-3571-2 L050119TSS00 Total/NA Solid 6020A 70096 160-3571-3 L050120TRS00 Total/NA Solid 6020A 70096 160-3571-4 L050121TSS00 Total/NA Solid 6020A 70096 160-3571-5 L050122TRS00 Total/NA Solid 6020A 70096 160-3571-6 L050125TRS00 Total/NA Solid 6020A 70096 160-3571-7 L050127TRS00 Total/NA TestAmerica St. Louis Page 40 of 45 1

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QC Association Summary TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Metals (Continued)

Analysis Batch: 70530 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 70096 160-3571-8 L050128TES00 Total/NA Solid 6020A 70096 160-3571-9 L050131TRS00 Total/NA Solid 6020A 70096 160-3571-10 L050132TES00 Total/NA Solid 6020A 70096 160-3571-11 L050133TRS00 Total/NA Solid 6020A 70096 160-3571-12 L050139TES00 Total/NA Solid 6020A 70096 160-3571-13 L050140TRS00 Total/NA Solid 6020A 70096 160-3571-14 L050148TRS00 Total/NA Solid 6020A 70096 160-3571-15 L050154TRS00 Total/NA Solid 6020A 70096 160-3571-16 L050155TES00 Total/NA Solid 6020A 70096 160-3571-17 L050156TRS00 Total/NA Solid 6020A 70096 160-3571-18 L050157TES00 Total/NA Solid 6020A 70096 160-3571-19 L050162TRQ00 Total/NA Solid 6020A 70096 160-3571-20 L050162TRS00 Total/NA Solid 6020A 69983 160-3571-21 L050163TES00 Total/NA Solid 6020A 69983 160-3571-21 MS L050163TES00 Total/NA Solid 6020A 69983 160-3571-21 MSD L050163TES00 Total/NA Solid 6020A 69983 160-3571-22 L050164TRS00 Total/NA Solid 6020A 69983 160-3571-23 L050165TEQ00 Total/NA Solid 6020A 69983 160-3571-24 L050165TES00 Total/NA Solid 6020A 69983 160-3571-25 L050169TSS00 Total/NA Solid 6020A 69983 160-3571-26 L050170TRS00 Total/NA Solid 6020A 69983 160-3571-27 L050171TRS00 Total/NA Solid 6020A 69983 160-3571-28 L050172TES00 Total/NA Solid 6020A 69983 LCS 160-69983/2-A Lab Control Sample Total/NA Solid 6020A 70096 LCS 160-70096/2-A Lab Control Sample Total/NA Solid 6020A 69983 MB 160-69983/1-A Method Blank Total/NA Solid 6020A 70096 MB 160-70096/1-A Method Blank Total/NA General Chemistry Analysis Batch: 70086 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-3571-1 L050119TSQ00 Total/NA Solid Moisture 160-3571-2 L050119TSS00 Total/NA Solid Moisture 160-3571-3 L050120TRS00 Total/NA Solid Moisture 160-3571-4 L050121TSS00 Total/NA Solid Moisture 160-3571-5 L050122TRS00 Total/NA Solid Moisture 160-3571-6 L050125TRS00 Total/NA Solid Moisture 160-3571-7 L050127TRS00 Total/NA Solid Moisture 160-3571-8 L050128TES00 Total/NA Solid Moisture 160-3571-9 L050131TRS00 Total/NA Solid Moisture 160-3571-10 L050132TES00 Total/NA Solid Moisture 160-3571-11 L050133TRS00 Total/NA Solid Moisture 160-3571-12 L050139TES00 Total/NA Solid Moisture 160-3571-13 L050140TRS00 Total/NA Solid Moisture 160-3571-14 L050148TRS00 Total/NA Solid Moisture 160-3571-15 L050154TRS00 Total/NA Solid Moisture 160-3571-16 L050155TES00 Total/NA Solid Moisture 160-3571-17 L050156TRS00 Total/NA Solid Moisture 160-3571-18 L050157TES00 Total/NA TestAmerica St. Louis Page 41 of 45 1

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General Chemistry (Continued)

Analysis Batch: 70086 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-3571-19 L050162TRQ00 Total/NA Solid Moisture 160-3571-20 L050162TRS00 Total/NA Solid Moisture 160-3571-21 L050163TES00 Total/NA Solid Moisture 160-3571-22 L050164TRS00 Total/NA Solid Moisture 160-3571-23 L050165TEQ00 Total/NA Solid Moisture 160-3571-24 L050165TES00 Total/NA Solid Moisture 160-3571-25 L050169TSS00 Total/NA Solid Moisture 160-3571-26 L050170TRS00 Total/NA Solid Moisture 160-3571-27 L050171TRS00 Total/NA Solid Moisture 160-3571-28 L050172TES00 Total/NA Solid Moisture 160-3571-28 DU L050172TES00 Total/NA Rad Leach Batch: 69978 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3570-A-8-E DU Duplicate Total/NA Prep Batch: 69983 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3571-21 L050163TES00 Total/NA Solid None 160-3571-21 MS L050163TES00 Total/NA Solid None 160-3571-21 MSD L050163TES00 Total/NA Solid None 160-3571-22 L050164TRS00 Total/NA Solid None 160-3571-23 L050165TEQ00 Total/NA Solid None 160-3571-24 L050165TES00 Total/NA Solid None 160-3571-25 L050169TSS00 Total/NA Solid None 160-3571-26 L050170TRS00 Total/NA Solid None 160-3571-27 L050171TRS00 Total/NA Solid None 160-3571-28 L050172TES00 Total/NA Solid None LCS 160-69983/2-A Lab Control Sample Total/NA Solid None MB 160-69983/1-A Method Blank Total/NA Leach Batch: 69988 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3571-1 L050119TSQ00 Total/NA Solid Dry and Grind 160-3571-2 L050119TSS00 Total/NA Solid Dry and Grind 160-3571-3 L050120TRS00 Total/NA Solid Dry and Grind 160-3571-4 L050121TSS00 Total/NA Solid Dry and Grind 160-3571-5 L050122TRS00 Total/NA Solid Dry and Grind 160-3571-6 L050125TRS00 Total/NA Solid Dry and Grind 160-3571-7 L050127TRS00 Total/NA Solid Dry and Grind 160-3571-8 L050128TES00 Total/NA Solid Dry and Grind 160-3571-9 L050131TRS00 Total/NA Solid Dry and Grind 160-3571-10 L050132TES00 Total/NA Solid Dry and Grind 160-3571-11 L050133TRS00 Total/NA Solid Dry and Grind 160-3571-12 L050139TES00 Total/NA Solid Dry and Grind 160-3571-13 L050140TRS00 Total/NA Solid Dry and Grind 160-3571-14 L050148TRS00 Total/NA Solid Dry and Grind 160-3571-15 L050154TRS00 Total/NA TestAmerica St. Louis Page 42 of 45 1

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QC Association Summary TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Rad (Continued)

Leach Batch: 69988 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-3571-16 L050155TES00 Total/NA Solid Dry and Grind 160-3571-17 L050156TRS00 Total/NA Solid Dry and Grind 160-3571-18 L050157TES00 Total/NA Solid Dry and Grind 160-3571-19 L050162TRQ00 Total/NA Solid Dry and Grind 160-3571-20 L050162TRS00 Total/NA Solid Dry and Grind 160-3571-20 DU L050162TRS00 Total/NA Solid Dry and Grind 160-3571-21 L050163TES00 Total/NA Solid Dry and Grind 160-3571-22 L050164TRS00 Total/NA Solid Dry and Grind 160-3571-23 L050165TEQ00 Total/NA Solid Dry and Grind 160-3571-24 L050165TES00 Total/NA Solid Dry and Grind 160-3571-25 L050169TSS00 Total/NA Solid Dry and Grind 160-3571-26 L050170TRS00 Total/NA Solid Dry and Grind 160-3571-27 L050171TRS00 Total/NA Solid Dry and Grind 160-3571-28 L050172TES00 Total/NA Prep Batch: 70096 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-3571-1 L050119TSQ00 Total/NA Solid None 160-3571-1 MS L050119TSQ00 Total/NA Solid None 160-3571-1 MSD L050119TSQ00 Total/NA Solid None 160-3571-2 L050119TSS00 Total/NA Solid None 160-3571-3 L050120TRS00 Total/NA Solid None 160-3571-4 L050121TSS00 Total/NA Solid None 160-3571-5 L050122TRS00 Total/NA Solid None 160-3571-6 L050125TRS00 Total/NA Solid None 160-3571-7 L050127TRS00 Total/NA Solid None 160-3571-8 L050128TES00 Total/NA Solid None 160-3571-9 L050131TRS00 Total/NA Solid None 160-3571-10 L050132TES00 Total/NA Solid None 160-3571-11 L050133TRS00 Total/NA Solid None 160-3571-12 L050139TES00 Total/NA Solid None 160-3571-13 L050140TRS00 Total/NA Solid None 160-3571-14 L050148TRS00 Total/NA Solid None 160-3571-15 L050154TRS00 Total/NA Solid None 160-3571-16 L050155TES00 Total/NA Solid None 160-3571-17 L050156TRS00 Total/NA Solid None 160-3571-18 L050157TES00 Total/NA Solid None 160-3571-19 L050162TRQ00 Total/NA Solid None 160-3571-20 L050162TRS00 Total/NA Solid None LCS 160-70096/2-A Lab Control Sample Total/NA Solid None MB 160-70096/1-A Method Blank Total/NA Prep Batch: 70555 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 69988 160-3571-1 L050119TSQ00 Total/NA Solid Fill_Geo-0 69988 160-3571-2 L050119TSS00 Total/NA Solid Fill_Geo-0 69988 160-3571-3 L050120TRS00 Total/NA Solid Fill_Geo-0 69988 160-3571-4 L050121TSS00 Total/NA Solid Fill_Geo-0 69988 160-3571-5 L050122TRS00 Total/NA Solid Fill_Geo-0 69988 160-3571-6 L050125TRS00 Total/NA Solid Fill_Geo-0 69988 160-3571-7 L050127TRS00 Total/NA TestAmerica St. Louis Page 43 of 45 1

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Rad (Continued)

Prep Batch: 70555 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 69988 160-3571-8 L050128TES00 Total/NA Solid Fill_Geo-0 69988 160-3571-9 L050131TRS00 Total/NA Solid Fill_Geo-0 69988 160-3571-10 L050132TES00 Total/NA Solid Fill_Geo-0 69988 160-3571-11 L050133TRS00 Total/NA Solid Fill_Geo-0 69988 160-3571-12 L050139TES00 Total/NA Solid Fill_Geo-0 69988 160-3571-13 L050140TRS00 Total/NA Solid Fill_Geo-0 69988 160-3571-14 L050148TRS00 Total/NA Solid Fill_Geo-0 69988 160-3571-15 L050154TRS00 Total/NA Solid Fill_Geo-0 69988 160-3571-16 L050155TES00 Total/NA Solid Fill_Geo-0 69988 160-3571-17 L050156TRS00 Total/NA Solid Fill_Geo-0 69988 160-3571-18 L050157TES00 Total/NA Solid Fill_Geo-0 69988 160-3571-19 L050162TRQ00 Total/NA Solid Fill_Geo-0 69988 160-3571-20 L050162TRS00 Total/NA Solid Fill_Geo-0 69988 160-3571-20 DU L050162TRS00 Total/NA Solid Fill_Geo-0 LCS 160-70555/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-70555/1-A Method Blank Total/NA Prep Batch: 70600 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 69978 160-3570-A-8-E DU Duplicate Total/NA Solid Fill_Geo-0 69988 160-3571-21 L050163TES00 Total/NA Solid Fill_Geo-0 69988 160-3571-22 L050164TRS00 Total/NA Solid Fill_Geo-0 69988 160-3571-23 L050165TEQ00 Total/NA Solid Fill_Geo-0 69988 160-3571-24 L050165TES00 Total/NA Solid Fill_Geo-0 69988 160-3571-25 L050169TSS00 Total/NA Solid Fill_Geo-0 69988 160-3571-26 L050170TRS00 Total/NA Solid Fill_Geo-0 69988 160-3571-27 L050171TRS00 Total/NA Solid Fill_Geo-0 69988 160-3571-28 L050172TES00 Total/NA Solid Fill_Geo-0 LCS 160-70600/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-70600/1-A Method Blank Total/NA TestAmerica St. Louis Page 44 of 45 1

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Tracer/Carrier Summary TestAmerica Job ID: 160-3571-1 Client: Westinghouse Electric Company LLC Project/Site: RFP-CBA-022 (7 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)

Re 94 160-3571-1 Percent Yield (Acceptance Limits)

L050119TSQ00 89 160-3571-1 MS L050119TSQ00 90 160-3571-1 MSD L050119TSQ00 91 160-3571-2 L050119TSS00 91 160-3571-3 L050120TRS00 89 160-3571-4 L050121TSS00 91 160-3571-5 L050122TRS00 87 160-3571-6 L050125TRS00 93 160-3571-7 L050127TRS00 93 160-3571-8 L050128TES00 94 160-3571-9 L050131TRS00 95 160-3571-10 L050132TES00 92 160-3571-11 L050133TRS00 94 160-3571-12 L050139TES00 95 160-3571-13 L050140TRS00 97 160-3571-14 L050148TRS00 101 160-3571-15 L050154TRS00 93 160-3571-16 L050155TES00 100 160-3571-17 L050156TRS00 95 160-3571-18 L050157TES00 93 160-3571-19 L050162TRQ00 92 160-3571-20 L050162TRS00 94 160-3571-21 L050163TES00 90 160-3571-21 MS L050163TES00 90 160-3571-21 MSD L050163TES00 87 160-3571-22 L050164TRS00 92 160-3571-23 L050165TEQ00 94 160-3571-24 L050165TES00 90 160-3571-25 L050169TSS00 0.2 X 160-3571-26 L050170TRS00 90 160-3571-27 L050171TRS00 89 160-3571-28 L050172TES00 99 LCS 160-69983/2-A Lab Control Sample 100 LCS 160-70096/2-A Lab Control Sample 102 MB 160-69983/1-A Method Blank 97 MB 160-70096/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 45 of 45 1

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