ML17158C032

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Rev 4, Solid Radwaste Pcp.
ML17158C032
Person / Time
Site: Susquehanna  Talen Energy icon.png
Issue date: 01/08/1997
From: SEIBERT A C, STEFFENAUER D J
PENNSYLVANIA POWER & LIGHT CO.
To:
Shared Package
ML17158C031 List:
References
NDAP-QA-0646, NDAP-QA-646, NUDOCS 9704030257
Download: ML17158C032 (91)
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Text

APPENDIXBREVISIONSTOSSESSOLIDWASTEPROCESSCONTROLPROGRAM(NDAP-QA-0646)970403025797033iPDRADQCK05000387R

PROCKDURECHANGEAPPROVALFORMPCAFNO.~~I7?PAGEIOFP3.ROCEDURENO.NDAPWA~4.FORMNO..REV.5.PROCEDURETITLESofidRadioactiveNastePmcessControl6.PROCEDURETYPE:QAPROGRAM~YES.,~NOPLANTPROC.YES~NO7.REQUESTEDCHANGEDELETEPCAFsQQNO~YES¹ADDStep4.5.13EnsurethatradwastetanksarepreparedwftbOperationssuppo8.REASONFORCHANGETopreventrecurrenceofCR9&0630.Continued~9.RECOMMENDEDFORTATUS2UUYESNO,EXPIRATIONDATE(60DAYMAXIMUMFORYSTATUS)BIO.IFPLANTPROCED.'ETEITEMSllTHRU15ONPAGE2OF%MSFORM;.':..~:<'.<>>g;>s"<',':~<'..<~gq'-'~ggy'."g~~g>>16.INITIATOR.AfiseC.SefbertDATE:1/3/9717.MANAGEMENTREVIEWa~QADRNOTREQUIREDb.~QADRPERFORMED,NOCOMMITS18.'ARIZAa,4),qg,~/vONRPLANTOCBDURES).~'"'>>.~~~".,".".'<ERVISOR>&<<.-".'-;='.':"-'4:".-DM;~;AGER.DATE19.COMMITTEETYPE:MTG¹GRECOMMENDED:REVISED:NONO20.APPROVAL~(INIIIALS)"'ATE~~&~FORMNDAP~~03-1,Rev.2,DUPLEX,Page1of2>>~>>40lNCtA"-.QkRSA~SOTS.,jcl

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.PROCEDURE.COVERSHEETNUCLEARDEPARTMENTPROCEDURESOLIDRADIOACTIVEWASTEPROCESSCONTROLPROGRAMNDAP-gA-0646Revision4Page1of63c'goEFFECTIVEDATE:PERIODICREVIEWFREQUENCY:PERIODICREVIEWDUEDATE:REVISEDPERIODICREVIEWDUEDATE:PROCEDURETYPE:OAProgram(Q}YES()NOPlantProcedure(j)YES()NOZ'rd/edco~~g'sag&~i~REVIEWMETHOD:()Alternate()Expedited(g)POND()ERDPreparedbyReviewedbyRecommendedSuperctsonaUn'anagerDate3-zz-9'5ApprovedbyPORCCommitteeMeetingNo.ERCCottDateDateFORMNDAP-gA-0002-1,Rev.1,Page1of1IMNSttlmllllHNimmtmMIItillSIIllltlmSlIlllllRttll NDAP-gA-0646Revision4Page2of63PRODURESIONSUMMARSOLIDRADIOACTIVEMASTEPROCESSCONTROLPROGRAMThefollowingchangeswillnotreducetheoverallconformance-ofthesolidifiedwasteproducttoexistingcriteriaforsolidwastes.1)IncorporatedPCAF1-94-1330revisingthePCPimplementingprocedurematrixtoreflectactualproceduresinuseandchangedtherequirementsfordisposalofradioactivewastesamplesafterpackagedradioactivewastehasbeeninitsdesignatedstoragearea.2)AddedSEGNRCapprovedTopicalReportSTD-P-05-011-P-AtoContractedVendorServicestoreflectuseofSEGforwaste'rocessingequipment,methodsandverificationofacceptablewasteformsfordewateringandsolidification.3)AddedActivatedCarbonasanewwaste'typewhichisgeneratedfromprocessingofliquidwastesusingvendorprovideddemineralizationservices.4)AddedtheSolidification/Dewatering/ServicesVendormayperformtestsolidificationanddeterminationofmixingratiosforsolidificationperformedoffsite(vendorfacility)5)AddedRadlok(SEG)typecontainerstoHighIntegrityContainerapprovedforuselist.6)7)AddedSNMinventoryrequirementsduringprocessingperSOOR94-581resolution.AddedNRCTechnicalPositiononConcentrationAveragingandEncapsulationtoRadioactiveMasteAnalysisandClassificationtoensurethatradionuclide/concentrationsareadequatelydistributedoverthevolumeorweightofthewaste.

NDAP-gA-0646Revision4Page3of63SECTION1.0PURPOSE2;0POLICY/DISCUSSION

3.0REFERENCES

TABOFCONTES4.0RESPONSIBILITIES4.1EFFLUENTSMANAGEMENTSUPERVISOR4.2SUPERVISOR-OPERATIONSTECHNOLOGY4.3POMERPRODUCTIONENGINEER-EFFLUENTSMANAGEMENT4.4HEALTHPHYSICIST-EFFLUENTSHANAGEHENT4.5RADMASTESUPERVISOR4.6CHEMISTRYSUPERVISOR4.7HPFOREMAN-EFFLUENTSMANAGEMENT4.8MANAGER-NUCLEARASSESSMENTSERVICES'.9AUXILIARYSYSTEHSOPERATOR4.10SOLIDIFICATION/DEMATERING/SERVICESVENDOR4.11MANAGER-NUCLEARPROCUREMENT4.12MANAGER-NUCLEARSYSTEMSENGINEERING4.13MANAGER-NUCLEARMAINTENANCE4.14LICENSINGSUPERVISOR4.15MANAGER-NUCLEARTRAINING4.16MANAGER-NUCLEARSECURITY5.0DEFINITIONS

NDAP-gA-0646Revision4Page4of63~SECION6.0PROCEDUREABEOFCONTENTSCot'e206.1CONTRACTEDVENDORSERVICES6.2MASTETYPES6.3RADIOACTIVEMASTEANALYSISANDCLASSIFICATION6.4TESTING/TREATHENTOFSOLIDIFIEDRADWASTEFORCOMBUSTIBLEGASES6.5RADIOACTIVEWASTESOLIDIFICATION6.6.RADIOACTIVEWASTEDEWATERING6.7HIGHINTEGRITYCONTAINERS(HIC)6.8IRRADIATEDHARDMAREPROCESSINGANDDEMATERINGII6.9CONTAINERINSPECTIONS6.10WASTECONTAINERSPACEUTILIZATION6.11STORAGEOFPACKAGEDRADIOACTIVEWASTE6.12TRANSPORTATION,SHIPPINGANDDISPOSALREGULATIONS6.13SHIPPINGOFRADIOACTIVEWASTE6.14SHIPHENTCONFIRMATION6.15CHANGESTOTHESOLIDRADIOACTIVEWASTEPROCESSCONTROLPROGRAM6.16EVALUATIONOFPROCESSOR.OPERATIONALCHANGES6.17REPORTINGOFHISHAPSINVOLVINGLOWLEVELMASTEFORHS6.18PCPINPLEHENTINGPROCEDURES7.0RECORDS20212730304051.52 NOAP-gA-0646Revision4Page5of63~](CHANTADACHMNTSSolidificationRecordSheetDewateringRecordSheetSusquehannaGuaranteedSolidified/OewateredMasteVolumeRecordPCPImplementingProcedureMatrixMaterialsnotCompatiblewithPolyethyleneContainers5559.6063 NOAP-gA-0646Revision4Page6of631.0f>URPOSEProvideadministrativecontrol,guidanceandrecordsrtheprocessing,packaging,transportation,anddisposalofradioactivewaste.ThisprocedureistheProcessControlProgramrequiredbySSESTechnical,Specifications.2.0~PL000000100ThisprocedureisapplicabletoLowLevelRadwaste{LLRM)generatedasaresultoftheoperationoftheSusquehannaSteamElectricStation(SSES).ThewastestreamsincludesolidandliquidwasteasdefinedintheFSAR,butdonotincludespentfuelorgreaterthanClassCwaste.EfficientgenerationandprocessingofradioactivewasteisveryimportanttotheoveralloperationofSSES.Animportantobjectivewithrespecttoradioactivewastegenerationistominimize'thevolumeofwastegenerated.Theprocessingoflargevolumesofwastecanresultintheinabilitytodisposeoforstoreallwastepackaged,thesignificantincreasedcostsassociatedwithincreasedwastegeneration,andthe-potentialtoover-burdentheprocessingsystemanddegradeitslongtermreliability.TheProcessControlProgramdescribestheenvelopewithinwhichprocessingandpackagingofradioactivewasteisaccomplishedtoprovidereasonableassuranceofcompliancewithLow-LevelRadwasteregulationsandrequirements.ThisprocedureisapplicabletoSSESinstalledsystems,temporarysystemsandequipmentprovidedbyvendorsforprocessing,packaging,transportation,anddisposalofapplicablewasteforms.3.0~RFRNCES3.13.23.349CFR100-177,Transportation10CFR20,StandardsforProtectionAgainstRadiation10CFR61,LicensingRequirementforLandOisposalofRadioactiveMaste3.43.53.610CFR71,PackagingandTransportationofRadioactiveMaterial40CFR261,IdentificationandListingofHazardousMasteSSESTechnicalSpecificationsSection3/4.11.3,SolidRadwasteSystemi3.7SSESTechnicalSpecificationsSection6.13,ProcessControlProgram(PCP)

NOAP-gA-0646Revision4Page7of633.8NUREG0800,StandardReviewPlan11.4SolidWasteManagement.Systems3.9TechnicalPositiononWasteFormRev.1,19913.10TechnicalPositiononRadioactiveWasteClassification,Rev;0,~19833.11TechnicalPositiononConcentrationAveragingandEncapsulation,Rev.0,19953.12RegulatoryGuide1.21,Measuring,EvaluatingandReportingRadioactiveMaterialinSolidWastesandReleaseofRadioactiveMaterialinLiquidandGaseousEffluentsfromLightMaterCooledNuclearPowerPlants3.13RegulatoryGuide1.143,DesignGuidanceofSolidWasteManagementSystems,3.143.153.163.17RegulatoryGuide7.1,AdministrativeGuideforPackagingandTransportingRadioactiveMaterialANSI/ANS40.35,VolumeReductionofLowLevelRadioactiveWasteANSI/ANS40.37,MobileRadioactiveWasteProcessingSystemsANSI/ANS55.1,SolidRadioactiveWasteProcessingSystemforLightWaterCooledReactorPlant3.18.PacificNuclearDewateringSystemTopicalReportNo.TP-02-P-A,Rev.33.19PacificNuclearSolidificationProcessControlProcedureNo.PT-51-WS,Rev.40-3.20ScientificEcologyGroupMobileIncontainerDewateringandSolidificationSystem(HOSS)TopicalReportNo.STD-R-05-011-P-'A,Rev.23.21DisposalSiteCriteriaforBarnwell,S.C.3.22DHEC-HIC-PL-001SouthCarolinaCertificateofComplianceforCNSIHighIntegrityContainers3.23DHEC-HIC-P0-006,SouthCarolinaCertificateofComplianceforCNSIOverpackHighIntegrityContainers3.24DHEC-HIC-PL-012,SouthCarolinaCertificateofComplianceforVectra'Technologies,Inc.HighIntegerityContainer NOAP-QA-0646Revision4Page8of633.25DHEC-HIC-PL-005,SouthCarolinaCertificateofComplianceforScientificEcologyGroup,Inc.HighIntegrityContainers3.26OHEC-HIC-PL-017,SouthCarolinaCertificateofComplianceforScientificEcologyGroup,Inc,HighIntegrityContainers3.27PLA-1237,ProcessControlProgram,August17,19823.28ReviewofProcessControlProg}amforSusquehanna,Unit1,YoungbloodtoCurtis,September30,19823.29SafetyEvaluationNL-93-008,SolidRadwasteWasteProcessingServicesUtilizingPacificNuclearProcessingSystem3.30IEBulletin79-19,PackagingofLowLevelRadioactiveWasteforTransportationandBurial(')3.31NRCInformationNoticeNo.90-50,MinimizationofMethaneGasGenerationinPlantSystemsandRadwasteShippingContainers(z)3.32GenericLetter91-02,ReportingHishapsInvolvingLLWFormsPreparedforDisposal()3.33SOOR-1-90-148,BarnwellReceivedContainerPressurizedwithFlammableGas()3.34SOOR1-90-172,IncorrectSamplingMethodUsedonResinLiner()3.35SOOR1-91-322,DoseRatesonContainerHigherThanExpected()3.36SOOR94-581,SpentTIPFoundUnexpectedlyinTIPRoom.4.0EEENIBTH4.1EffluentsManagementSupervisorresponsibilities:4.1.14.1.24.1.3Developingandimplementingprogramsandproceduresforradioactivewasteprocessing,packaging,transportationanddisposal.Haintainingtheoverallradwasteprogramtoensurecompliancewithapplicableradiologicalandshippingregulations.Ensuringpersonnelwhoperformsupportactivitiessuchasprocessing,packaging,andtransportationoflowlevelradioactivewasteareavailableandmeetallqualificationsandtrainingrequiredbySSESprocedures.

NDAP-gA-0646Revision4Page9of634.1.4Collecting,maintaining,reviewingandsubmittingaccuratedata/informationrelatedtowastestreamquantityandnuclidecompositionforinclusionintoAnnualRadioactiveEffluentReleaseReportandStateDER-BRPquarterlyReport.4.2Supervisor-OperationsTechnologyresponsibilities:4.2.14.2.24.2.3ProvidingtechnicalassistancetoEffluentsManagementpersonnel.Thisincludesinterpretationsofstate,federal,anddisposalfacilityregulationsregardingnew,imminent,orproposedregulatorychangesgoverningprocessing,packaging,transportation,anddisposal.Naintainingacurrentcopyoflocal,state,federalanddisposalfacilityregulationspertainingtodisposalandtransportationoflowlevelradioactivewaste.CoordinatingthesubmittaloftheAnnualRadioactiveEffluentReleaseReportaspertheSSESTechnicalSpecifications.4.3PowerProductionEngineer-EffluentsManagementresponsibilities:4.3.14.3.24.3.34.3.44.3.5Ensureproceduresareadequatetoprovideforpropersolidificationanddewateringofwaste.Ensuretestdataorrationaleisavailabletojustifyapplicablesolidificationanddewateringfunctionsofeachwastetype,oranycombinations,toaddressdisposalandregulatoryagencies'equirements.Evaluateservicesprovidedbyvariousvendorstoensurecontractedsolidificationanddewateringoperationsareperformedinthemostefficientandeconomicalmethod,asrequiredbytheapplicableregulatoryagencies.PerformthedutiesofRadwasteSupervisorasspecifiedinthisprocedureinhisabsence.Definewastestreamsbasedongenerator,filtrationmediaandmeansofprocessing.

SOAP-gA-0646'evision4page10of634.3.6Cqllecting,reviewing*yndsuhoittingdatarelatedto'hereportingofmishapsandresultsofPCPsurveillancespecimenexaminationstoapplicableregulatoryagen'cies.4;44.4.3HealthPhysicist-EffluentsHanagementresponsibilities:4.4.1Haintainasamplingandana)ysisprogramtoensurelOCFR61compliance.4.4.2Ensureproceduresareadequatetoprovideforproperpackagingandshipmentofwastetoensurecompaiancewithallapplicableregulations.Evaluateservicesprovidedbyvariousvendorstoensurecontractedwastepackaging,processing,and.transportationservicesareperformedinthemostefficientandeconomicalmethod,asrequiredbyapplicableregulatoryagencies.4.4.4PerformthedutiesofHPForeman-EffluentsManagementas'pecifiedinthisprocedureinhisabsence.4.4.5Coordinateradioactivematerialevaluationofproductacceptabilityfordisposalatspecificdisposalfacilities.4.5RadwasteSupervisorresponsibilities:4.5.1EnsureSolidffication/DewateringEquipmentisoperatedinaccordancewithapprovedoperatingprocedure,includingvendorsuppliedequipment.4.5.24.5.34.5.4Ensureappropriatewastesolidificationanddewateringrecordsaregenerated.InterfacewithstationsupportgroupstoensureproperImplementationofprocesscontrolprograms.Providedirectiontocontractorpersonnelinvolvedinsolidwasteprocessingactivitiesincluding:a.Ensuringtestdataisavailableto5ustifyspecificprocessingtechniques.b.Ensuringapplicablevendorproceduresandrevisionsareincorporated.IntoapplicablyplantprocedureandapprovedbyPORC.,

~97-DOCS3oF2,INDAP-QA-0646Revision4Pagellof634.5.54.5.64.5.74.5.84.5.94.5.104.5.ll4.5.124.5.13c..Coordinatingpre-processingandpost-processingtreatmentactivities...d.Evaluatingservicesprovidedtoensureefficientandeconomicalmethodsareused..EnsureSolidificationandDewateringoperationsarecarriedoutinanALARAmanner.InterfacewithHPForeman-EffluentsManagementforlinerandcaskselectionforsolidwasteshippingactivities.Ensurepropermarkingofcontainerspriortofilling.Ensuresolidification/dewateringpersonnelareadequatelytrainedperNTP-gA-42.6..Estimateclassificationofwasteforcontainerselectionandprocessingmethod.EnsurethatwastestreamsloadedintoHighIntegrityContainersaresanipledforradionuclideandevaluatedforchemical,compatibilityapplicabletotheuseofHighIntegrityContainers.EnsureproperinspectionsanddocumentationarecompletepriortouseofaHighIntegrityContainerandensurethatconta1nerisproperlyuseduptothepointoftransfertoHPForeman-EffluentsManagement.CompleteandprocessHighIntegrityContainerUserCertificationStatementtoensurethecontainerisusedproperly.EnsurethatradwastetanksarepreparedwithOperationssupport.4.6ChemistrySupervisorrespons1bilities:4.6.14.6.24.6.34.6.4Performrequiredsamplepreparationandanalysisinaccordancewithapprovedchemistryprocedures.Performtestsolidificationifrequired.Storetestsolidificationbillet1frequired.Providedensityofinitialandfinalwasteform.Providetheisotopicmixandconcentrationofisotopesdetectedinthematerialsampledforsolidificationordewatering.

NDAP-gA-0646Revision4Page12of634.6.64.7.24.6.5CompleteChemistryportionoftheSolidificationandDewateringRecords.EnsurepersonnelareadequatelytrainedperNTP-(A-41.2.4.6.7Providechemicalanalysisand/ortreatmentsupportasnecessaryforuseofHighIntegrityContainersandliners.4.7HPForeman-EffluentsNanag'ementresponsibilities:4.7.1InterfacewithRadwasteSupervisorforlinerandcaskselectionandschedulingforsolidwasteshippingactivities.Complete,process,andfileradioactivewasteshippingdocumentation.4.7.34.7.44.7.54.7.64.7.74.7.84.7.94.7.104.7.11Storageofpackagedradioactivewastewithintheradwastefacilities.Determinewasteclassificationanddescriptionofsolidified,dewatered,andotherpackagedwaste..Finaldispositionofsolidified,dewateredandotherpackagedwaste.EnsuresSSESisaregistereduserofapplicableHighIntegrityContainersatspecificdisposalfacilities..EnsuresHPpersonnelinvolvedwithradioactivewastehandlinghavereceivedRadwasteMorker.trainingperNTP-gA-42.6.Evaluatevendorservicesprovidedtoensureefficientandeconomicalmethodsareused.CompleteandprocessCertificationStatementforDisposalofHighIntegrityContainersasrequiredbyapplicableregulatoryagencies.ProcessandpackageCartr'idgeFilters,DryActiveHaste,solidsealedsourcesandothernonprocesswastes.CollectionofDAMandnon-processwaste(10CFR61)samples.

NDAP-gA-0646Revision4Page13of634.8Manager-NuclearAssessmentServicesresponsibilities:4.8.1~4.8.24.8.3Performperiodicauditofimplementationofthis.programandreviewofradwasteservicevendor'sgAPrograms.InspectionofRadwasteContainersasrequiredbyapplicableprocedures.Ensureprocesscontrolsareadheredtobyinspectionoftestsolidification,wastevolumes,solidificationagentadditions,productacceptabilitychecks,dewateringprocesssequence/acceptancecriteriaandrecordsreview.4.8.4Inspectionofpackaging,storage,andshippingactivities,asrequiredbyapplicableprocedures.4.9AuxiliarySystemsOperatorisresponsibleforoperatingtheplantsolidandliquidradwasteequipmentinaccordancewithapprovedoperatingproceduresasdirectedbytheRadwasteSupervisorandAssistantUnitSupervisor.'.10Solidification/Dewatering/ServicesVendorresponsibilities:4.10.14.10.24.10.34.10.44.10.5Providesolidification,dewateringand/orvolumereductionservicesinaccordancewithavalidcontractforsaidservices.ProvidetestdataormakedataavailableforPPLLreviewduringvendorauditstodemonstratethattheirservicesandequipmentmeet.theapplicableregulatoryanddisposalfacilitylimitationsfortheservicetheyareproviding.Providetrainingdocumentationtodemonstratethatthepersonnelbeingprovided,toconducttheapplicableservice,areinfacttrainedandknowledgeableintheapplicableservices.ProvideproceduresthatareorcanbeplacedintotheSSESprocedureformatfortheservicesbeingprovided.EnsureanapprovedgualityAssuranceProgramexiststhatcoverstheservicesbeingprovided.ThevendorshallworkwithintheSSESgualityAssuranceProgramwhenapplicable.

NDAP-gA-0646Revision4Page14of634.10.64.10.74.10.84.10.9Completeapplicablesectionsof.Solidificationand-DewateringRecordsrequiredforeachcontainerprocessed.Ensurepre-qualificationtestdataforeachwasteformshallbesubmittedtotheNuclearRegulatoryCommission.Provideadescriptionoftheequipment/processthatisusedinprocessingwaste.Obtainwastesamplesfromprocessingequipmentinaccordancewithapprovedoperatingprocedures.4.10.10PerformallpreandposttreatmentactivitiesasdeterminedbyRadwasteSupervisor.4.11Nanager-NuclearProcurementresponsibilities:4.11.1EnsureHighIntegrityContainersarenotexposedtoultravioletlight(sunlight).4.11.24.11.3EnsurepropermaterialcertificationiscompletepriortoissuanceofHighIntegrityContainerstoplantforuse.ReceiptinspectionofHighIntegrityContainersanddocumentreviewtoensureconformance.4.11.4EnsureCertificateofCompliance(CofC)isreceivedwithHighIntegrityContainer.4.12Hanager-NuclearSystemsEngineeringisresponsibleforprovidingengineeringsupportasrequiredforoperationofassignedradwastesystemsandequipment.4.13Manager-NuclearMaintenanceresponsibilities:4.13.1CalibrationandmaintenanceofapplicableplantequipmentinRadwasteProcessingSystems.4.13.2Providemaintenancepersonneltosupportprocessing,packagingandtransportationoflowlevelradioactivewaste.4.14LicensingSupervisorresponsibilities:4.14.1Submittingtransportationcaskuserregistr'ationrequeststoNRCperIOCFRTI.12.

NDAP-gA-0646Revision4Page15of634.14.24.14.3SubmittingtotheNRCtheAnnualRadioactiveEffluentReleaseReport.CoordinatingandsubmittingtotheNRCthereportsrequiredasaresultofConditionReport(CR)events,investigations,andresolutions.4.15Man'ager-NucTearTrainingresponsibilities:4.15.14.15.2Providingtrainingandre-traininginapplicableregulatoryrequitementstopersonneldirectlyinvolvedintransfer,processing,packaging,storage,andtransportofradioactivewaste.Maintainingarecordoftraining,attendees,andsubjectmaterialforallLowLevelRadioactive'Hastetraining.4.16Manager-NuclearSecurityisresponsiblefornotifyingappropriatelawenforcementagenciesintheeventoflostradioactivematerialshipments.TONS3.0KFFI5.1'.25.35.45.55.6APPROYEOCONTAINERS:ApprovedmeansapprovalissuedorrecognizedbytheNRCforuseinshipmentofradioactivematerial.BATCH:Thetotalvolumeofwastecontainedinaliner,isolated-wastemixingtank-spentresintank-concentratestankor-phaseseparatorthathasbeensampledfor,solidification/dewatering.BILLSOFLADING:Shippingpapersormanifestsservingasimilarpurposeandcontainingtheinformationrequiredby49CFR172.202,203,and204.CARRIER:Meansapersonengagedinthetransportationofpassengersorproperty.(10CFR71.4)CERTIFICATEOFCOMPLIANCE:LicenserequirementsestablishedbytheNuclearRegulatoryCoamissionfortheuseofapprovedRadioactiveMaterialShippingContainers.CHELATINGAGENT:Achemicalwhichcombineswithametalsoastoformaringstructureheldbycoordinationbonds.

NDAP-gA-0646Revision4Page16of635.75.85.9CHEMICALFORM:ThechemicalcontentoftheRadioactiveMaterialbeingshipped.CLOSEDTRANSPORTVEHICLE:A.vehicleequippedwithasecurelyattachedexteriorenclosure,whichduringnormaltransport,restrictstheaccessofunauthorizedpersonstothecargospace.(49CFR173-403[C])COMPOSITESAMPLE:Amixtureofsamplescollectedrepresentingconditionsattimeofsampling,fromthesamesamplingpoint,atdifferenttimes.5.10CONSIGNEE:Theindividualororganizationtowhomtheshipmentisconsignedorintended.5.11CURINGTIME:Thetimeallowedforthesolidifiedproducttosetpriortoitsevaluationforproductacceptability.5.125.135.14DECAYHEAT:Theheatproducedbyradioactivedecay,usually'expressedinMattsorBTU/hr,butcanberelatedtoCurieContent.DEMATERED:Theremovaloffreeliquidfromsolidmaterialtoapointwherelessthan1'XforHIC'sandlessthan0.5Xforsteellinersbywastevolumeremainsasrequiredbythedisposalfacilitylicense.EXCLUSIVEUSEVEHICLE(a/k/a:SoleUseorFullLoad):Shipmentfromasingleconsignorhavingtheexclusiveuseofatransportvehicleandforwhichallinitial,intermediate,andfinalloadingandunloadingiscarriedoutby,orunderthedirectionoftheconsignor,consignee,orhisdesignatedagent.(49CFA173.403[i])5.15.FREELIQUID:Liquidwhich-isstillvisibleaftersolidificationordewateringiscomplete,orisdrainablefromthelowpointofapuncturedcontainer.5.16HAZARDOUSMATERIAL-Asubstanceormaterial,includingahazardoussubstancewhichhasbeendeterminedbytheSecretaryofTransportationtobecapableofposingathreattohealth,safety,'ndpropertywhentransportedincommerce,andwhichhasbeensodesignated.Thetermincludeshazardoussubstances,hazardous.wastes,marinepollutants,andelevatedtemperaturematerialsasdefinedin49CFR171.8,materialsdesignatedashazardousunder'theprovisionsof49CFR172.101and172.102,andmaterialsthatmeetthedefiningcriteriaforhazardclassesanddivisionsin49CFR173.

NOAP-QA-0646Revision4Page17of63IHAZARDOUSWASTE:Wastewhichcontainsmateriallistedin40CFR261,SubpartDand/orexhibitsoneormoreofthefour.characteristicscitedin40CFR261,SubpartC,andisnotexcludedfromregulationunder40CFR261,SubpartA.HazmatEmployeemeansapersonwhoisemployedbyaHazmatEmployerwhoduringthecourseofemployment:5.18.1Loads,unloadsorhandleshazardousmaterials.5.18.2Prepareshazardousmaterialsfortransportation.5.18.35.18.4Modifies,marks,orotherwiserepresentscontainers,drums,orpackagingsasqualified.foruseintransportofhazardousmaterials.Isresponsibleforsafetyoftransportinghazardousmaterial.HIGHINTEGRITYCONTAINER(HIC):Adisposalsiteapprovedcontainer.thathasanexpectedlifeof300yearsandprovidesthestructuralstabilitytomeetdisposalrequirements.HIGHWAYROUTECONTROLLEDQUANTITY:Aquantity,theaggregateradioactivityofwhichexceedsthatspecifiedin(49CFR173.403[1]).ISOTOPICANALYSIS:TheidentificationoftheisotopicelementsinvolvedinasampleofRadioactiveMaterial.LABELING:Labelsappliedtoacontainerdenotingthecontentsofthecontaineranddegreeofhazardassociatedwiththecontainers.Thelabelsareidentifiedasthe'WhiteIlabel,theYellowII,andYellowIIIlabel.AlabelstatingRadioactive-LSAcanalsobeappliedtoacontainer.whenappropriate.(49CFR172,SubpartE)LIHITEDQUANTITYOFRADIOACTIVEMATERIAL:Meansaquantityofradioactivematerialnotexceedingthematerialpackagelimitsspecifiedin49CFR172.423,andwhichconforms"withrequirementsspecifiedin49CFR173.421.(49CFR173.403[m])LINER:Steelcontainerinwhichdewateredorsolidificationproductisdeposited.LOWSPECIFICACTIVITY:Naterialinwhichtheactivityisessentiallyuniformlydistributedandinwhichtheestimatedaverageconcentrationpergramofcontentsdoesnotexceedthespecificationasstatedin49CFR173.403(n).

NDAP-gA-0646.Revision4Page18of63.LOMLEVEL-RADIOACTIVEMASTE(LLRM):RadioactivewastegeneratedasaresultofqperationofSSES,excludingspentfuelorbyproductmaterial,isclassifiedbytheNRCaslow-levelradioactivewaste.LLRMdoesnotinclude"greaterthanclassC"waste.jHIXINGRATIO:Theratioofwastetocementandadditives*requiredforsatisfactorysolidification.MIXINGRECIPE:Theamountofwaste,cementandadditivesmixedto'olidifywaste.MIXEDMASTE:Amixtureoflowlevelradioactiveandhazardouswaste.NORHALFORMRADIOACTIVEMATERIALS:MeansradioactivematerialswhichdonotmeettherequirementsofSpecialFormRadioactiveHaterials(49CFR173.403[s]).PLACARDING:AlabelaffixedtoallfoursidesofthetransportvehicledenotingthepresenceandlevelofRadioactivematerialonthevehicle.(49CFR172,SubpartF)'ROCESSCONTROLPROGRAM(PCP):Programwhichcontainsthesampling,analysis,andformulationdeterminationbywhichsolidificationofradioactivewastesfromliquidsystemsisassured.RADIOACTIVEHATERIAL:Forpurposesoftransportationonly,materialinwhichtheactivityisessentiallyuniformlydistributedandtheestimatedspecificactivityexceeds0.002microcuries,pergramofmaterial.(49CFR173.403[y]and[aalu)RAOWASTEMORKER:AHazmatEmployeeinvolvedwiththecollection,packaging,andtransportationofradioactivewaste.SEALEDSOURCES:Anyby-productmaterialthatisencasedinacapsuledesignedtopreventleakageorescapeofby-productmaterial.SOLIDIFICATION:Aconversionofradioactivematerialsfromliquid'ndsolidsystemstoahomogeneous(uniformlydistributed)monolithic,immobilizedsolidwithdefinitevolumeandshape,boundedbyastablesurfaceofdistinctoutlineonallsides(freestanding).

NDAP-gA-0646Revision4Page19of635.375.385.395.405.415.425.435.445.455.465.47SOLIDIFIEDRADWASTE:Wetwastewhichissolid~fied(e.g.evaporatorconcentrates,sludge),meetsthefreeliquidcriteria,andsatisfiesapplicabletransportationanddisposalsiterequirements.Dewateredresinsorfiltersludgesatisfyingthetwolattercriteriashallalsobedefinedassolidifiedradwaste.SPECIALFORMRADIOACTIVEMATERIALS:Radioactivematerialthatiseitherasinglepiece,oriscontainedinasealedcapsule,thatcanbeopenedonlybedestroyingthecapsuleandmeetstheadditionalrequirementsspecifiedin49CFRPart173.403(z).STABLEANDUNSTABLEWASTEFORMS:Shallbedefinedasstatedin10CFRPart61andothersupportingregulatorydocuments.TESTSOLIDIFICATION:Themixingofwaste(s)andsolidificationagentsinthelaboratorytosupportselectionofmixingratiosandprovideinsuranceforfinalproductacceptability.TRANSPORTINDEX(TI):Thedimensionlessnumberplacedonthelabelofapackagetodesignatethedegreeofcontrol,tobeexercisedbythecarrierduringtransportation.Thetransportindexwillbedeterminedinaccordancewith49CFR173.403(bb).TYPE"A"PACKAGING:Packagingwhichisdesignedinaccordancewiththegeneralpackagingrequirementsof49CFR173.24,andwhichisadequatetopreventthelossordispersaloftheradioactivecontents,andtoretaintheefficiencyofitsradiationshieldingpropertiesifthepackageissubjectedtothetestdescribedin49CFR173.465or173.466,asappropriate.{49CFR173.403[gg])TYPE"A"QUANTITYRADIOACTIVEMATERIAL:ThatmaterialwhichmaybetransportedinType"A"packaging.{49CFR173.431[a])TYPE"B"PACKAGING:PackagingwhichmeetsthestandardsforType"A"Packaging,andinaddition,meetsthestandardsforthehypotheticalaccidentconditionssetforthin10CFR71.(49CFR173.403[hh])TYPE"B"QUANTITYRADIOACTIVEMATERIAL:ThatmaterialwhichmaybetransportedinType'B"packaging.(49CFR173.431[b])WASTESTREAM:Aby-productofaprocesssystemorcomponentwithuniquecharacteristicsandmaintainedseparatefromotherwastestreams.IWASTETYPE:Specificcontentsofalinerortankwhichmaycontainoneormultiplewastestreams,thecategoryofwaste.suitableforaparticularmeansofprocessing.

NDAP-qA-0646Revision4page20of635.48MASTEPRE-CONDITIONING:Thephysicalorchemicaladjustmentof'-thewastetobringitwithinanestablishedenvelopetoassuresolidification.6.0JPPocDURE6.1"CONTRACTEDVENDORSERVICES6.1.16.1.26.1.36.1.46.1.56.1.6SolidifiedradwasteprocessingservicesareprovidedbyVectra,Inc.forwastetypesincludedinthisProcessControlProgram.NRCapprovedTopicalReportTP-02-P-A,describesVectraInc.wasteprocessingequipment,methodsandverificationofacceptablewasteformsfordewatering./VectraInc.SolidificationProcessControlProcedurePT-5I-MS,describeswasteprocessingequipment,methodsandverif'icationofacceptablewasteformsforsolidification.ThisproceduredoesnotprovidestabilitypertheBranchTechnicalPositiononMasteForm,Rev.1.Volumereduction,servicesareprovidedbyScientificEcologyGroup(SEG)forwastetypesincludedintheProcessControlProgram.NRCapprovedTopicalReportSTD-P-05-011-P-A,describesScientificEcoplogyGroup(SEG)wasteprocessingequipment,methodsandverificationofacceptablewasteformsfordewateringandsolidification.SelectedsolidifiedwasteformshavebeenapprovedtoprovidestabilitypertheBtanchTechnicalPositiononMasteForm,Rev.l.Othercontractedvendorserviceswhicharerequiredforsolidification,dewateringandvolumereductionservicesshallbeevaluatedtotherequirementsstated'inthisProcessControlProgramonacasebycasebasis NDAP-gA-0646Revision4Page21of"636.2MASTETYPESThefollowingwastetypesshallbeprocessedinaccordancewiththisprocedureorincombinationsasdefined.Thewasteshouldbedewateredwheneverpossibletominimizedisposalvolume.6.2.1EvaporatorConcentratesThefollowingareconcentratedwiththeRadwasteEvaporatorsand.areconsideredEvaporatorConcentrateswastestream:(I)CondensateDemineralizerregenerationeffluent'2)DeconShopdrains(3)ChemistryLaboratorysinkdrains(4)AuxiliaryBoilerblowdowneffluentb.Cid.Theconstituentsofthiswastestreammayincludethefollowing:(1)Tr'i-SodiumPhosphate~(2)SodiumSulfate(3)PhosphoricAcid(4)SulfuricAcid(5)SodiumHydroxide(6)Decontaminationsolutions(7)Negligibleamountsofreagentchemicalsusedforchemi..tryanalysisEvaporatorConcentratesintherangeof0-24weightpercentsodiumsulfate(equivalent)shallbesolidifiedforfinaldisposal.EvaporatorConcentratesshallnotbemixedwithanyotherwastetypeinfinalprocessing.

gDAP-qA-0646Revision4page22of63MixedSolidsaoThefollowingprocesswastestreamsarecollectedeither,in.WasteMixTanks,MasteSludgePhaseSeparatorortransferreddirectlytoaliner/HighIntegrityContainerandareconsideredMixedSolids:(I)LRMFilterMediaanddrainliquid{2)(3)SumpSludgeUltrasonicResin'CleanerMaste(URCMaste)b.d.Theconstituentsofthesewastestreamsmay'ncludethefollowing:{I)DiatomaceousEarth(2)PowderedResins(3)Fibrousmaterial{4)Carbonmaterial(5)Corrosionproducts(6)VarioussolidsanddirtinsmallconcentrationsMixedSolidsmaybesolidifiedordewateredforfinaldisposal.Eachwastestreamshouldbeprocessedseparately.RWCUFilterMediab.TheReactorMaterCleanupSystemandFuelPool'oolingandCleanupSystemfilter/demineralizerwastearecollectedintheRWCUPhaseSeparatorandshouldbeallowedtodecayfor60days.'hiswastestreamisconsideredRWCUFilterMedia.Theconstituentsofthiswastestreammayincludeanionandcationpowderedresin,corrosionandcontaminantsremovedfromtheprimarycoolant.

NDAP-gA-0646Revision4Page23of63C.RWCUFilterMediashallbedewateredinHighIntegrityContainers.Ifthiswastemustbesolidified,TechnicalSpecification3/4.11.3actionstatementmustbeperformed.Condensate/Radwaste/AtmosphericDemineralizerBeadResina~b.C.'IResinsfromtheCondensateOemineralizers,LiquidRadwasteDemineralizerandvendorprovideddemineralizationarecollectedintheSpentResinTankortransferreddirectlytoaliner/HighIntegrityContainer.Thisisconsideredtobe.Condensate/Radwaste/AtmosphericOemineralizerBeadResin.Theconstituentsofthiswastestreammayincludevarioustypesofanion,cation,mixedbeadresinandcorrosionandcontaminatesremovedfromliquidwastestreams.BeadResinmaybeusedtodemineralizeLiquidWasteineithersteellinersorHighIntegrityContainers.d.e.CondensateDemineralizerbeadresinshouldbeultrasonicallycleanedpriortocollectionintheSpentResinTank.BeadResinmaybesolidifiedordewateredforfinaldisposal.BeadResinmayalsobeprocessedbyvolumereductionmethodswhichincludedrying,incineration,compaction,useasfillmaterialsorotherevaluatedmethod(s)onacasebycasebasis.CartridgeFilters'a~CartridgeFilterwastetypeconsistsofthefollowingwastestreamsandconstituents:(I)CRDFilters-CRDorotherfiltersandsmallun-irradiatedprimarysystemequipmentsuchasvalves,CRDliftpumpfilters,RinseTankfiltersandothermetalcomponents.

NOAP-gA-0646..Revision4'Page24of63(2)RNCUSepta-SeptafromRMCUFilte}DemineralizerincludingseptafromFuelPoolCleanupFilterDemineralizer.(3)RadwasteFilters-includingdegasifierfiltersandotherfiberorpaperfiltersotherthanprimarysystem.{4)UnderwaterVacuumFilters-non-processfiltersgeneratedfromwetcleaningactivities.b.CartridgeFiltersmaybeprocessedbythefollowingmethods:{1)Emplacementinacementmatrixinasteeldrum/linerorinaHighIntegrityContainer.(2)Driedtoapointwherenofreeliquidisvisible.Absorbentmaterialmaybeincludedtoabsorbunintentionalandincidentalamountsofliquids.{3)Oewateredifdryingisimpractical.(4)Incinerationorothervolumereductionmethods.c.CartridgeFilterstobesolidifiedforfinaldisposalshallnotbemixedwithanyotherwastetype.d.Eachcartridgefilterwastestreamshouldbepackagedseparatelyunlessanalyzedpriortopackaginginaccordancewiththerequirementsofthisprocedure.IrradiatedHardwarea0Irradiatedhardwareisneutronacti'vatedmetalremovedfromtheinternalareaofthereactorpressurevessel.ThiswastestreamisconsideredIrradiatedHardware.

NDAP-gA-0646Revision4Page25of63Theconstituentsofthiswastestreammayincludecontrolrodblades,LPRHS's,IRK's,TIP'sandcomponentsexpendedduringhardwareprocessingandpackagingactivities.Startupsourcesmayalsobeprocessedaspartofthiswastestream.c.Irradiatedhardwareispackagedinsteellinersfordisposal.d.LiquidshallbedrainedtoensurefreeliquidAcceptanceCriteriaaremet.e.Irradiatedhardwareshallnotbemixedwithanyotherwastetypeinfinalprocessing.DryActiveWaste(DAM)a.DryActiveWasteisawastestream.b.Theconstituentsofthi'swastestreamconsistofcontaminatedpaper,plastic,wood,metalandotherdiscardedmaterial.C.DryActiveMaste,shallbeprocessedbyvolumereductionmethodswhichmayincludeincineration,compaction,decontaminationandmetalmelting.d.Ataminimum,DAMshallbepackagedinstrong-tightcontainersfordisposal.LiquidOilWasteorPetroleumBasedMaterialsTheconstituentsofthiswastestreammayincludeturbinelubricatingoil,EHCfluidandotherpetroleumbasedmaterials.ContaminatedLiquidOilWastegeneratedatthefacilityshouldbeprocessedbyadecontaminationsystem,solidifiedforfinaldisposal,volumereducedbyincineration,orotheracceptablemethods.

NDAP-gA-0646Revision4Page26of63CiLiquidOilMasteatconcentrations1Xandgreatermaybesolidifiedprovidedthefollowingareadheredto:k(1)Anemulsificationagentisaddedatrequiredconcentrations.(2)TheLinerisNOTSHIPPEDtoadisposalfacilitywithoutpriordisposalfacilityapproval.SolidSealedSourcesaob.coSolidSealedSourcesrequiringdisposalshallbepackaged.fordisposalasrequestedbyHealthPhysicsSupervision.MethodofdisposalisdependentonwasteclassoftheSolidSealedSourceanddisposalfacilityrequirements.Acceptablemethodsofdisposalinclude:(1)Placementwithinacontainerconsistingofanotherwastetypeprovided:(a)Thesourcecontainsisotopicsalreadyinthewaste.(b)Thesourceactivityissignificantlylessthanthewasteactivity.(2)ClassBandCsourcesshallbestabilizedwithinanapprovedsolidificationorencapsulationmedia.ActivatedCarbonaob.ActivatedCarbonfromvendorprovidedliquidwastedemineralizationistransferreddirectlytoaliner/HighIntegrityContainer.ThiswastestreamisconsideredActivatedCarbon.Theconstituentsofthiswastestreammayincludevarioustypesofcharcoal,ionspecificcarbonfiltermediaandcorrosionand.contaminantsfromliquidwastestreams.

NDAP-gA-0646Revision4Page27of63C.ActivatedCarbonmaybesolidified,dewatetedorprocessedbyvolumereductionmethodswhichincludedrying,incineration,compaction,useasfillmaterialsorotherevaluatedmethodson'acasebycasebasis.6.2.116.2.126.2.13.AWasteTypethatiscombinedwithaknownamountofhazardouswaste'r"MixedWaste"shallbeprocessed.forfinaldisposalpendingapprovalobtainedfromtheprocessinganddisposalfacilities,EnvironmentalProtectionAgency,U.S.NuclearRegulatoryCommissionandotherregulatoryagenciesasrequired.Wastetypescontainingchelatingagentswithintherangeof0.1to8.0percentbyweightshallbeprocessedtoastablewasteforminaccordancewithandauthorizedbydisposalfacilityrequirementsand.approvals.Variousothermaterialsnotspecificallyidentifiedaswastetypeswillbeevaluatedforsolidification,dewateringvolumereductionorotherprocessingonacasebycasebasis.(")6.3RADIOACTIVEWASTEANALYSISANDCLASSIFICATION6.3.1Radionuclideconcentrationsofradioactivewasteareusedtoclassifywasteforshippinganddisposal.Radionuclideconcentrationsshouldbedeterminedbaseduponisotopicanalysis,volumeandweightoffinalwasteform.6.3.2ThelOCFR61ComplianceProgramestablishesamethodologyforcharacterizingradioactivewastethroughtheuseofcorrelationfactors.Thisprogramshallrequireasaminimumthat:a~SamplesrepresentativeofSusquehanna'swastestreamsarecollecte".andanalyzedsuchthatresultsareobtainedftomadesignatedlaboratoryatleasteverytwoyears(ClassA)fordevelopmentofspecificcorrelationfactors.'WastestreamsknownorsuspectedtobeclassifiedClassBorClassCshouldbeanalyzedonanannualbasis.

NDAP-gA-0646Revision4Page28of63b.Technicalbasisdocumentationandjustificationofcorrelationfactorsaredevelopedforeach.wastestreamandareacceptableforuse.Periodicevaluationsandnecessaryadjustmentstoestablishedratiosareperformedinatimelymanner.c.Correlationfactorsarere-evaluatedfollowingsignificantchanges{greaterthanafactorof10)inplantoperations(suchassignificantchangesinfuelleakage,radwasteoperations,orequipment).Determinationofwasteclassificationshallbeinaccordancewith10CFR61.55,MasteClassification,anditssupplementaryBranchTechnicalPositiononRadioactiveMasteClassificationasfollows:b.C.ClassA-Usuallysegregatedfromotherwasteclassesatthedisposalfacility.Physicalformandcharacteristicsshallmeettheminimumrequirementsspecifiedin10CFR61.56(a).Ifthestabilityrequirementsin10CFR61.56(b)aremet,thewastedoesnothavetobesegregatedfordisposal.ClassS-Physicalformandcharacteristicsshallmeetboththeminimumandstabilityrequirementsspecifiedin10CFR61.56.ClassC-Physicalformandcharacteristicsshallmeetboththeminimumandstabilityrequirementsspecifiedin10CFR61.56.Inaddition,measuresshallbetakenatthedisposalfacilitytoprotectagainstinadvertentintrusion.Isotopicanalysismaybeperformedby:a.Gammaspectrometryofasampleanduseofcorrelationfactors.b.C.d.Directgammaspectrometryofwasteanduseofcorrelationfactors.Completeradionuclideanalysisofwastesample.DosetoCuriecalculations.

NDAP-QA-0646Revision4Page29of63e.Activationanalysis.Volumeandweightoffinalwastemaybedeterminedby:a~Calculationusinganalyticallyderivedsampledensities.b.C~d.Calculationusingstandardwastedensities.Directmeasurementofvolumeandweight.AcceptablemethodsdescribedintheTechnicalPositiononConcentrationAveragingandEncapsulation.Ifsamplesofwasteareusedforclassification,samplingprogramshallinclude:a~b.Samplesshallbeobtainedandanalyzedforeachbatchof.wetwasteifpracticalandALARA.Preferentially,samplesshouldbetakenforanalysisfollowingprocessingintoafinalwasteform.C.Samplestakenpriortofinalprocessingshould.enableresultsofsampleanalysistobedirectlytranslatedtofinalwasteform.d.e.BeadresinandActivatedCarbonusedforchemicaldemineralizationshallbesampledafterhavinghasbeendepletedinprocess.Solidification/DewateringServicesVendororanotherqualifiedindividualshallobtainrequiredsamples.Preparationofwasteforsamplingoranalysisa4b.WetWasteCollectiontanksshallberecirculatedinaccordancewithapprovedoperatingprocedurespriortosamplingoranalysis.Wasteprocessinginsolidificationliners/HighIntegrityContainersshallbemixedinaccordancewithapprovedprocedurespriortosamplingoranalysis.

NDAP-QA-O646Revision4Page30of636.3.81c.Metwastetobeprocessedmayalsobemixed,recirculatedandsampledoranalyzedfrommobileprocessingequipment..Finalwasteformcontainingamixtureofwastetypesorstreamsshallbeindividuallyanalyzedtodetermineradionuclideconcentrations.Thesummationofeachindividualradionuclideconcentrationshallbeusedtocharacterizethefinalwasteformforshippinganddisposal.Wastetypesorstreamsofdifferentwasteclasses(estimatedbyhistoricalprecedentorprojectedanalysis)shallnotbemixed.6.3.9DeviationsfromsamplingandanalysisrequirementsshallbeapprovedbyChemistrySupervisorandEffluentsManagementSupervision.6.4TESTING/TREATMENTOFSOLIDIFIEDRAOMASTEFORCOMBUSTIBLEGASES6.4.1Solidifiedwasteshallbetestedand/ortreatedtoensureitisnotcapableofgeneratingquantitiesofflammableortoxicgases,vaporsorfumeswhichmaybeharmfultopersonstransporting,handling,storingordisposingofthewaste.6.5RADIOACTIVEMASTESOLIDIFICATION6.5.1GeneralRequirementsa.WetMasteTypeswhichmaybesolidifiedinHighIntegrityContainersareEvaporatorConcentrates,MixedSolids,Condensate/RadwasteDemineralizerBeadResin,RMCUFilterMediaandLiquidOilWasteorPetroleumBasedMaterial,CartridgeFilters,SolidSealedSourcesandActivatedCarbon.b.cd.HighIntegrityContainersshallbeusedtomeetthestabilitycriteriainaccordancewithfederalanddisposalfacilityregulations.SolidificationprocessingshallbeconductedbyqualifiedSSESorSolidification/Dewatering/ServicesVendorpersonnel.Thesolidificationprocessshallbeoperatedinaccordancewithapprovedprocedures.Proceduresshallspecifywastestream,amountsofsolidificationagentandadditivesormethodfordetermination.

NDAP-gA-0646Revision4Page31of63MastePreconditioninga~b.Mastepreconditioningrequirementsshallbedeterminedby,chemistryanalysis.Preconditioningofwasteshallbeperformedifrequiredpriortodeterminingmixingratios.c.Mastepreconditioningisrequiredwhenanyofthefollowingconditionsexist:(I)AhighorlowpHcondition,asdeterminedbychemicalanalysis.(2)(3)Liquidcontentofthebatchisoutoftheacceptableenvelopeforsolidification.Solidscontentofthebatchisoutoftheacceptableenvelopefo}solidification.(4)Knownpotentialproblemchemicalsandconstituentswithinwastethatmayadverselyaffectsettingandstabilityofcement-solidifiedwasteform.d.~e.Wastepreconditioningshallbeperformedinaccordancewithapprovedprocedurestoensurewasteiswithintheacceptableenvelopeforsolidification.Uponcompletionofwastepreconditioning,additionalsamples,asrequired,shallbeobtainedinaccordancewithRadioactiveMasteAnalysisandClassificationsectionofthisprocedure.DeterminationofHixingRatiosa.Determinationofmixingratiosshallbeperformedforeachwastebatchtobeprocessed."-b.DeviationfromtherecommendedmixingratiosshallbereviewedbyPlantOperationsReviewCommittee(PORC).c.ChemistryGroupdetermines:(1)Densityofthewastesamples.

NDAP-gA-0646Revision4page32of63d.e.(2)SpecificgravityofSodiumSulfateSolutioninEvaporatorConcentrates.Solidification/Dewatering/ServicesVendordeterminesifthefinalmixingratiosarewithintheacceptableenvelopeforsolidification.Forsolidificationperformedonsite:(2)ChemistryGroupshallperformtestsolidificationofwasteasrequiredbyTestSolidificationsectionofthisprocedure.ChemistryGroupdeterminesmixingratiostoensurepr'opersolidification.Forsolidificationperformedoffsite:(1)Solidification/Dewatering/ServicesVendorshallperformtestsolidificationofwasteasrequiredbyTestSolidificationsectionofthisprocedure.{2)Solidification/Dewatering/ServicesVendor,determinesmixingratiostoensurepropersolidification.TestSolidification'a~Testsolidificationshallbeperformedtosupportwastemixingratiosasfoll'ows:(1)Atleasteverytenth(10th)batchofthesamewastestream.{2)(3)Mhensampleanalysisfalloutsidetheestablishedrangeandcriteriaindicatingachangeinwastecharacteristics.Mhenitisbelievedthatsomeunexpectedorabnormalcontaminantmaybepresent.(4)Mhen'equestedbyRadwasteSupervisor.

NDAP-0A-0646Revision4Page33of63(5)Mixingofmaterialsshallbeaccomplishedinamannerthatduplicates,totheextentpractical,mixingconditionsthatareobtainedwithfull-scalemixingincontainer.b.c~d.e.(6)Curingshallbeperformedunder.conditionssimilartothoseusedinlaboratoryqualificationtestprogram.Uponfailureofatestsolidification,anLCOisentered,additionalsamplesshallbeobtained,'lternativesolidificationparametersaredeterminedandasubsequenttestverifiessolidification.Testsolidificationshallbeperformedoneachsubsequentbatchofthesamewaste'streamuntilatleastthree(3)consecutiveinitialtestsolidificationdemonstrateacceptabilityinaccordancewithTechnicalSpecification3/4.11.3.gualityControlshallverifytestsolidificationacceptabilityandindicatetheacceptabilityonthesurveillancedocumentation.TheacceptabilityrequirementsaredefinedinthePCPSurveillanceSpecimensectionofthisprocedure.Extrasamplevolumeforbackuptestingshallbedisposedofafteracceptablecontainerchecksarecompleted.HighIntegrityContainertestsolidificationbilletsshouldbedisposedafteracceptablecontainerchecksarecompleted.Testsolidificationshouldbeperformedwithsamplesfromwasteobtainedasfollows:(I)InaccordancewithRadioactiveWasteAnalysisandClassificationsectionofthisprocedure.(2)'amplingofthesolidsinthec'ontainerandtheliquidsusedforhydration,thenmixedtotheratiosthatexistinthecontainer.

NDAP-gA"0646Revision4Page34of63g.TestSolidificationProceduresshallbedevelopedforeachspecificwastetypeasrequired.h.Cement,watertypeandadditivestobeusedinactualsolidificationshallbeusedinpreparationoftestsolidification.PCPSurveillanceSpecimensa.HighIntegrityContainertestsolidificationbilletsshallbeexaminedandtestedforacceptabilityafterthespecifiedcuretimefor:(1)Liquidonsurfaceofsolidifiedproductlessthat1.0Xbywastevolume.(2)Visibledefects,suchasctacking,spallin'g,ordisintegration.(3)Strengthbyphysicallypokingthesurfaceofsolidifiedproductwitharigidunyieldingdevice.Nominalsurfacedentingisacceptable.b.IfcementsolidificationinsteellinersisNRCapprovedtoprovidestability,PCPsurveillancespecimenexaminationtestingandreportingisrequiredinaccordancewiththeBranchTechnicalPositiononWasteForm,Rev.l.CuringTimeAminimumof30hoursshallbeallowedforcuringpriortocappingortransportingcontainer.b.cThecontainermaybemovedduringthefirsthour.aftersolidificationbutmustremainundisturbedfortheremaining29hours.DeviationsfromminimumrequiredcuringtimeshallbeapprovedbyRadwasteSupervisor'andjustificationsdocumentedinremarkssectionofSolidificationRecord.

NDAP-gA-0646Revision4Page35of63SolidificationProductequality'a~b.Solidificationproductqualityisassuredbyuseofpredeterminedmixingratiosofwaste,cementandadditive.Liquidtobeusedforsolidificationshouldbedemineralizedwater.Pre-qualificationmixingratiosarebasedonlaboratorytestingusingnon-radioactivewastematerials.c.Mixingratiosarere-enforcedbythefollowing:(I)TestsolidificationperformedperiodicallyasstatedinTestSolidificationsectionofthisprocedure.(2)Visuallyandphysicallycheckingatleasteveryfifth(5th)containerofthesamewastetype.d.Containerchecksshallconsistof:'(I)Avisualcheckofsolidifiedproductforliquidonsurfaceofproductnottoexceed1.0Xbywastevolume.(2)Physicallypokingthesurfaceofsolidifiedproductwitharigidunyieldingdevicepriortocapping(Nominalsurfacedentingmayoccurandisacceptable).e.gualityControlshallverifyacceptabilityofsolidifiedproductwhencontainersarechecked.f.DeviationfromthecontainercheckingrequirementshallbeapprovedbytheRadwasteSupervisor.HandlingofUnacceptableSolidifiedMasteContainers.a0b.Ifasolidifiedwastecontainerdoesnotmeetacceptabilityrequirements,aConditionReport(CR)shallbeissued.Ifthereasonforunacceptabilityisfreeliquid:(I)Thefreeliquidwillberemoved;or NDAP-gA-0646Revision4Page36of63(2)Extracement/additivewillbeaddedtosolidifyfreeliquid.Ifportionsoralloftheproductdidnotsolidifyafterthreedays:k(I)Thewastecontainerwillbecappedaridplacedinastoragelocationandperiodicallycheckeduntil'suchatimeproductisacceptable;or(2)Additionalsolidificationagentsmaybeaddedtoachievesatisfactorysolidification,asdeterminedbytheRadwasteSupervisor.Iftheproductsolidifiesprematurelypriorto.completingtheadditionofrequiredamountofcementandadditive,ascalculatedonthesolidificationcalculationsheetforthespecificprocedureused,thefollowingisrequired:{I)Atestsolidificationshallbeperformedusingtheactualratioofcementandwasteinthecontainer,providedsufficientsamplevolumeremainstocompletethisitem.(2)gualityControlshallchecktheproductforacceptabilityinaccordancewith.ContainerCheckssectionofthisprocedure.(3)Thecontainerisconsideredtomeetacceptablewasteformcriteriaforshippingprovidedthesubsequenttestsolidificationand/orcontainerchecksare.acceptabletogualityControlandconcurrenceoftheRadwasteSupervisoris:obtained.{4)TheaboveapplyonlyiftheEffluentsManagementSupervisordeterminesthattheproductcanbeclassifiedas"ClassAUnstable"orisplacedinaHighIntegrityContainerorstructurethatprovidesstabilityinaccordancewithIOCFR61and~thedisposalfacilitycriteria.

NDAP-QA-0646Revision4Page37of63e.Iftheproductdoesnotsolidifyproperlyinaccordancewiththespecificsolidificationprocedure,thefollowingisrequired:(I)Anevaluationofthelinershallbemadebythefollowingpersonnel:(a)EffluentsManagementSupervision(b)SolidificationVendor-Operations(c)SolidificationVendor-Engineering(3)Disposalfacilitiesshallbecontactedandrequirementsforreceiptofthelinerinquestionshallbedefined.Alternativepackaging/processingshallbeevaluated.(4)Recommendationsfor'finaldispositionshallbemadetothePowerProductionEngineer-EffluentsManagement.(5)FinaldispositionshallbereviewedbyPlantOperationsReviewCommittee(PORC).(6)Recordsshallbekeptanddocumentationsupportiveoffinaldispositionattachedtothesolidificationrecordpackage.'(7)Thelinermaybeshippedafterg.C.reviewofdocumentationiscompleteanddisposalfacilityconcurrenceisreceivedinletterform.9-Specificinstructionsshallbeestablishedforhandlingunacceptablesolidifiedwastecontainer'nacasebycasebasis.gualityControlshallre-verifyacceptabilityofsolidifiedproductbyperformanceofContainerChecks.CappingofSolidifiedWasteContainersa.TherequirementsofSolidificationProductgualitysectionofthisprocedureshallbemetpriortocappingthecontainer.

NDAP-gA-0646Revision4Page38'of63b.Ifthecontainerisnotequippedwithapassiveventanditscontentsarewithinthe.requirementsofLowSpecificActivity(LSA)ensureoneofthefollowing:(1)Thecontainershouldbeshippedwithin(10)tendaysafter.capping;or(2)Ifacontainerhasbeencappedforlongerthan(10)days,itshallbeopened,vented,andre-cappedwithin(10)tendaysofshipment.coIfthecontainerexceedsthelimitsforLowSpecificActivityandcontainswaterand/ororganicsubstanceswhichcouldradiolyticallygeneratecombustiblegases,determinationmustbemadesuchthatthefollowingcriteriaaremetoveraperiodoftimethatistwicetheexpectedshipmenttime:(1)Thehydrogengeneratedshal.lbelimitedtoamolarquantitythatwouldbenomorethan5Xbyvolumeofthecontainergasvold;or(2}Thecontainerandshippingcaskcavitysha11beinertedwithadiluenttoassurethatoxygenislimitedtolessthan5%byvolume.inthoseportionsofthepackagewhichcouldhavehydrogengreaterthan5X.SolidificationAgentControla~b.PortlandCement-.ASTMC-150TypeIshallbeusedforthemobilesolidificationprocess.Othersolidificationagentsmaybeusedonlyafteracceptabletestingoftheagenthasbeencompletedthatdemonstratesacceptablesolidificationanddisposalfacilityapprovalhasbeenobtained.

NDAP-gA-0646Revision4Page39of63C.DocumentedCertificationisnotrequiredfor'aterialsreceivedinbagsprovidedmaterialverificationcanbeobtainedasfollows:(1)CementisacceptableprovidedthebagcontainingthecementindicatesthatcementisPortlandTypeI.'2)SodiumSilicateisacceptableprovidedthebagcontainingtheadditiveindicatesAnhydrousSodiumHetasilicate.(3)Otheradditivesareacceptableprovidedthecontainerisclearlymarkedindicatingthetypeofadditive.d.Otheradditivesmaybeusedforenhancementofsolidificationprocessasspecifiedinthesolidificationprocedureanddocumentedinthesolidificationrecords.RadioactiveMasteSolidificationRecordsASolidificationRecordSheet(FormNOAP-gA-0646-1)shallbecompletedforeachcontainerfilledwithsolidificationproducts.CompletionoftheSolidificationRecordSheetandtherequiredaccompanyingdocumentationshallbeasfollows:a~TheRadwasteSupervisorisresponsibleforinitiatingthisformandcompletingParts1and2.b.C.EffluentsManagementSupervision,ChemistryandSolidification/Oewatering/ServicesVendorpersonnelshallprovideandcheckofftherequireddocumentat~:~.specifiedinPart3.gualityControlshallprovidereviewasrequiredfottheSolidificationRecords.

NOAP-gA-0646Revision4Page40of636.6RADIOACTIVEWASTEDEMATERING6.6.IGeneralRequirementsMasteStreamswhichmaybedewateredineitherHighIntegrityContainersorsteellinersareLRWFilterMedia,.UltrasonicResinCleanerMaste,SumpSludge,RWCUFilteracedia,Condensate/RadwasteDemineralizerBeadResin,CartridgeFiltersandActivatedCarbon.Thetypeofcontainerusedshallbebasedonthewasteclassificationandstabilitycriteriainaccordance'withfederalanddisposalfacilityregulations.b.C.d.e.DewateringofRadioactiveMasteshallbeperformedbyqualifiedSSESorSolidification/DewateringSetvicesVendorpersonnel.DewateringofRadioactiveMasteshallbeperformedinaccordancewithapprovedprocedures.Dewateringproceduresshallbebasedondocumentedtestdatathathasdemonstratedtheabilitytoachievefreeliquidlimitsasspecifiedbydisposalfacilitiesandapplicableregulatoryagencies.Liquidvolumeanddrainagecalculationsandactualdrainageverificationmayalsobeusedtomeetfreeliquidlimits.HighIntegrityContainersshallbeusedfordisposalwhentheconcentrationofradionuclideswithhalf-livesgreaterthan5yearsexceedsIpCi/cc.EachwastestreamwhichmaybedewateredshouldbecharacterizedbytheSolidification/DewateringServicesVendortoensuretheoperatingparametersandeffectivenessof'thedewateringsystemareinaccordancewiththeparametersestablishedintheTopicalReport.I4 NDAP-gA-0646Revision4Page41of63DewateredProductControla.Thefinaldewateredproductshallcontainlessthan1Xnon-corrosivefreeliquidforHighIntegrityContainersand0.5Xforsteelliners.gualityControlchecksshallbeperformedonprocesssteps..b.cIfadewateredwastecontainerdoesnotmeetacceptabilityrequirements,aConditionReport(CR)shallbeissued.Specificinstructionsshallbeestablishedforhandlingunacceptabledewateredwastecontaineronacase-by-casebasis.,d.DeviationfromthecontainercheckingrequirementshallbeapprovedbythePowerProductionEngineer-EffluentsHanagement.-IRadioactiveMasteOewateringRecordsADewatetingRecordSheet(FormNDAP-gA-0646-2)shallbecompletedforeachcontainerfilledwithdewateredwastestreams.Partsoftheformshallbecompletedbythefollowingresponsibleindividualsorgroups:a.TheRadwasteSupervisorisresponsibleforinitiatingthisformandcompletingParts1and2.b.ChemistryGroupshallcompletePart3SamplingandAnalysis.c~EffluentsManagementSupervision,ChemistryandSolidification/Dewatering/ServicesVendorpersonnelshallprovideandcheckofftherequireddocumentationspecifiedinPart4.d.gualityControlshallprovidereviewasrequiredfortheOewateringRecords.

NDAP-gA-0646Revision4Page'42of636.7HIGHINTEGRITYCONTAINERS(HIC)6.7.1StorageofHighIntegrityContainersa~Yectra,RadlokandCNSIHighIntegrityContainers(HIC)storedindirectsunlightorinareaswherethereisastrongsourceofultravioletradiationshaTlbefilledanddisposedofwithinoneyearofmanufacturingdate.6.7.2b.cUsesa~OncefilledaHighIntegrityContainermaybestoredforaperioduntilatotalofone(1)yearofultravioletradiationisreceived.Shortexposures(i.e.,severalhours)tosunlight,suchas'occurringduringshipmentandonsitetransferneednotbecountedwhendeterminingtotalultravioletexposure.ofHighIntegrityContainersHighIntegrityContainersmaybeusedtopackagethefollowingwastematerialsfordisposal:(1)Oewateredbeadresin,powderedresinanddiatomaceousearth.(2)Compressibleandnon-compressiblesolidwastes.(3)Filterelementsandcartridges.(4)Solidifiedresins,sludges,andliquidwastes.(5)Incineratorash,residuals,orequivalentwastewhichhasbeenrenderednon-dispensableinabindingmatrix.(6)Otherdewateredanddrymaterialprovidedconcurrenceisreceivedbycontainervendoranddisposalfacility.

NDAP-gA-0646Revision4Page43of63Priortousinga.HighIntegrityContainerforaspecificwastematerial,proceduresshallbeestablishedtodefinethespecificrequirementthatshallbemetduringuseofthecontainer.Theproceduresshallcontain:Documentationrequirementsthatspecificconditionshavebeenmetsuchasinspectionandexposuretodegradingconditions.Instructionsastohowtohandleandproperlyclosethecontainer.Instructionsforon-sitestorageofloadedcontainersforultimateshipmentfordisposal.Theproceduresshallprovideamethodfordocumentingrequiredinformationrelevanttothecontainerfrominitialreceipttoshippingfordisposal.Requiredinformationshall'bebaseduponthecontainercertificateofcomplianceanddisposalfacilityrequirements.Retentionandutilizationofthedocumentationshallbedefinedintheprocedures.TheproceduresshallestablishspecificgualityControlinspectionrequirements.PriortothefirstshipmentofaspecifictypeofHighIntegrityContainer,authorizationshallberequestedfromtheapplicableregulatoryagencygoverninguseofthecontainerinquestionatthedisposalfacilityofconcern.

NDAP-gA-0646Revision4Page44of63HighIntegrityContainerLimitationsa.HighIntegrityContainersareapprovedforuseprovidedthefollowingphysicallimitationsofthewastearemet:(1)VectraPayloaddensity(2)LoadingtemperatureSl;47gms/ccg170F(3)(4)(5)(6)VectraEL-50N.S.loadedweight:64200lbVectraEL-142N.S.loadedweight:<8250lbVectraEL-142S.loadedweight:611250lbVectraEL-190N.S.loadedweight:gl1950lb(7)VectraEL-190S.loadedweight514800lb(8)VectraEL-210N.S.loadedweight:g13000lb(9)VectraEL-210Sloadedweight{10)CNSISmallloadedweight(ll)CNSIHediumloadedweight(12)CNSILargeloadedweight(13)Radlok179loadedweight(14)Radlok195loadedweight(15)Enduropak105loadedweight5173001b52500lbg2500lbg2500lbgl8500lbgl8500lbgl700lbb.(16)Enduropak205loadedweight:g1900lb{17)Enduropak150loadedweight:g2400'lbThemaximumconcentrationofradionuclideswithhalflivesgreaterthan(5)fiveyearsthatmaybedisposedofinaHighIntegrityContaineris350pCi/[c.Otherwasteformsshallnotexceed1.0X10radsmaximumintegrateddosetothecontainer.

NOAP-QA-0646Revision4Page45of63c.ThepolyethyleneHighIntegrityContainersshallnotcomeintocontactwithmaterialslistedinAttachmentE.d.Apassiveventdesignshallbeincorporatedintothecontainertorelieveinternalcontainer,pressure.ClosureofHighIntegrityContainersa.ClosureofHighIntegrityContainersshallbecompletedinaccordancewithapprovedprocedures.b.C.d.IfthecontainerisnotequippedwithapassiveventanditscontentsarewithinthelimitsofLowSpecificActivityensureoneofthefollowing:(I)Thecontainerisshippedwithin(10)tendaysafterclosing;-or(2)Ifthecontainerhasbeenclosedforlongerthan(10)tendays,itshallbeopened,vented,andre-closedwithinten.(10)daysofshipment.IfthecontainerexceedsthelimitsforLowSpecificActivityorcontainswaterand/ororganicsubstanceswhichcouldradiolyticallygeneratecombustiblegases,determinationmustbemadesuchthatthefollowingcriteriaaremetoveraperiodoftimethatistwicetheexpectedshipmenttime:(I)Thehydrogengeneratedshallbelimitedtoamolarquantitythatwouldbenomorethan5%byvolumeofthecontainergasvoid;or(2)ThecontainerandshippingcaskcavityshallbeinertedwithadiluenttoassurethatoxygenislimitedtogBXbyvolume,inthoseportionsofthepackagewhichcouldhavehydrogengreaterthan5X.Step6.7.4.band6.7.4.cshallalsoapplytodewateredwasteinsteelliners.

NDAP-gA-0646Revision4Page46of63P6.8IRRADIATEDHARDMAREPROCESSINGANDDEMATERING6.8.1GeneralRequirements'.Processingan'ddewater'ingofIrradiatedHardware~..'hallbeperformedby.qualifiedSSESorvendor'ersonnel.b.ProcessinganddewateringofIrradiatedHardwareshallbe.performedinaccordancewithapprovedprocedures.CiIrradiatedHardwareconsistingofnon-fuelSpecialNuclearHaterialshallbeinventoriedduringprocessinginaccordancewithNDAP-QA-'0337.6.8.26.8.3d.Dewateringproceduresshallbebasedonliquid'olumeanddrainagecalculationsandactualdrainageverificatios'fodemonstratethe.ability'..toachievefreeliquidlimitsasspecifiedbydisposal.facilitiesand'applicableregulatoryagencies.0DewateredProductControl'a.Thefinaldewateredproductshallcontainlessthan0.5Xfreeliquidforsteelliners.b.gualityControlchecksshallbeperformedonprocesssteps.IrradiatedHardwareProcessingandDewateringRecords'..Allrecordsgeneratedshallbecompletedandfiledinaccordancewithapprovedimplementingprocedures.6.96.9.2CONTAINERINSPECTIONS6.9.1gualityControlshallinspectcontainerstobeused:fearsolidification,dewatering,andotherpackaging.fordisposal.Thisinspectionshallassurethatpriortouse,the'ontainerstobeusedforsolidification,dewatering,orotherpackagingare.intactandtheirinternalsarefreeof.anyvisualdamagethatwouldpreventthemfrom'.,performingtheirintendedfunction.

IIIf p~gJ-f9',/d>7'HDAP-qA-0646Revision4PQQgX~fN.'age'47of.636.9;3Packagesshallmeet.thegeneralcriter'iafornormaltransportconditionsinaccordancewiththerequirementsof49'CFR.TypeApackagesshallmeettheadditionaldesignrequirementsspecifiedin49CFR.'.10MASTECONTAINERSPACEUTILIZATION6.10.1Mastevolumeshallbemaximizedwithintheguidelinesofspecificprocedurestominimize:'otentialvoidspaceatthetopofwastecontainer.afters'olidificationordewateringis'.complete.6.10.2~6.10.36.10.4~AdcKtionalradioactivematerialshoul'dbeadded'nlyaftertheinitialwastevolumeisinfinalformandsampledandtheaddedwastevolumeisinfinalformandsampled.\b.Theadditionalmaterialmaybedrawnintocontainersabletowithstandhigherexternalpressureswithoutdegredationbycreatinganareaoflowpressurefnsidethecontainer,suchaswithsteelliners.c.torall'thercontainers,theadditional~material.shallbeaddedviamechanital~processesorbyotherconveyancewhichdoesnotexerthigherexteznalpressures.aMastevolumesshallsectorexceed.disposalsitecriteria.Ifwastevolume4slessthandisposalfacility'criteria;requirementfordisposalofthecontainerinquestionshallbedefined'bythedisposalfacility.Specificwastevolumescommittedtobythe.Solidification/Dewatering/ServicesVendorshallbemetorotherwisej'ustifiedastowhywastevolumeswerenot-achieved.SusquehannaGuaranteedSolidified/DewateredMasteVolumeRecord,FormNDAP-gA-0646-3;shallbecompletedbytheSolidification/Dewatering/Servicesvendor'personnel,approvedby.RadwasteSupervisorandshallbeusedtotrack..solidified/dewateredwastevolumes'chieved,ineachindividualcontainer.6.11STORAGEOFPACKAGEDRADIOACTIVEMASTE6.11.16.11.2RadwasteSupervisorshallprovideSolidificationand/orDewateringRecordsheetsthathavebeenreviewedby'gualityControlpersonnelstatingthatprocessedwastehasbeensolidifiedorde-watered'inaccordancewith=theProcessControlProgramandmeetstheapplicableshippinganddisposalcriteria.So'lidificationandDewateringRecordsshall'includetheisotopicmix,isotopicconcentrationofthe',wastethatwaspackaged,thetotalvolumeofthewaste,andtheamountofwater,cementorothersolidificationagentused,asappropriate.

NDAP-gA-0646Revision4.Page48of636.11.36.11.46.11.56.11.6SolidificationandDewateringRecordsshallbepariofthepermanentshippingrecordsandadheretorequirementsoftheProcessControlProgram.Formaterialspackagedinahighintegritycontainer,documentationshallbemaintainedonHIC,storageandpre-shipmentchecklistinformation.-PackagedradioactivewasteshallbestoredinareasdesignatedbyHPForemanEffluentsManagement.StorageofpackagedradioactivewasteintheLowLevelRadwasteHoldingFacility(LLRWHF)shallbeinaccordancewithapprovedprocedures.Aninventoryof.stored,packagedwasteshallbemaintainedinaccordancewithapprovedprocedures.6.12TRANSPORTATION,SHIPPINGANDDISPOSALREGULATIONS6.12.1Specificregulatorydocuments'shallbemaintainedonsiteinastatusthatiscurrent.Specificregulationsthatshallbemaintainedincludebutarenotlimitedtothefollowing:a.10CFR71PackagingofRadioactiveMaterialfortransportandtransportationofradioactivematerialundercertainconditions.b.c~d.e.949CFR100-199Transportation.Chem-NuclearSystemsInc.BarnwellS.C.disposalsiteoperatinglicensenumber097Stateof.SouthCarolina,asrequired.Chem-NuclearSystemInc.NRCMaterialLicense12-13536-01,asrequired.Chem-NuclearSystemInc.Barnwell-S.C.disposalsiteoperatingproceduresandsitecriteria,as.required.ScientificEcologyGroupLicensesR-73008-E94,R-01052-A91.CaskManualsforcasksofwhichPPKLisanauthorizeduser.h.AcopyofthelicenseforeachfacilitytowhichRadioactiveMaterialissent:

NDAP-gA-0646Revision4Page49of636.12.26.12.3i.10CFR61LicensingrequirementsforlanddisposalofRadioactiveWaste.Proceduresapplicabletotransportation,shippinganddisposalshallbedeveloped.a.Proceduresshallbeestablishedandmaintainedtoprovidedirectionsandassureregulatory'omplianceformanifesting,whichincludeapplicablefederal,state,anddisposalfacility'egulations,andNRCguidance.b.Proceduresshallcontaincheckofflistswhere'ndwhenapplicabletoassurespecificattentionispaidtothecriticalfunctionbeingcontrolled.c.ProceduresshallcontaingualityControlnotificationsorholdpoints.IIComputersoftwareusedtoimplementapplicableportionsoftheProcessControlProgramshallbeinaccordancewithNDAP-gA-0801.6.13SHIPPINGOFRADIOACTIVEWASTE6.13.16.13.26.13.36.13.4AllradioactivewasteshallbeshippedbyEffluentsManagement.AllradioactivewasteshippedfromSSESshallonlybetofacilitieslicensedtoreceivethewasteandinaccordancewith10CFR20,10CFR71and49CFR100-199.DryActiveWaste{DAW)shouldnormallybeshippedasTypeAquantitiesandthereforedonotrequirespecificlicensedcontainers.WastecontainersshallbeplacedinaUSNRCapproved1'icensedshippingcontainerifit:ExceedsTypeAquantitiesb.cExceeds1000mr/hroncontactExceeds1000dpm/100cmloosesurfacecontaminationontheexteriorofthecontainer.

gmp-qA-0646Revision4Page50of.63ThespecificconditionsoftheCertificateofComplianceforeachapprovedshippingcaskshallbestrictlyadheredto.Packagedwastemaybeshippedunshieldedif:a.-Contactdoseratesarelessthan200mrem/hr.anddoseratesat6feetarelessthan10mrem/hr.b.CuriecontentofthepackageshallbeaTypeAquantity.c.Containershallbeaminimumofastrongtightcontainer..Priortotheshipmentofapackageofradioactivewaste,theHPForemanEffluentsHanagementshallassurethecontainerissurveyedforcontactdoseratesandsurfacecontamination.Decontamination,ifrequired,shallbedoneunderthedirectionoftheHP'oremanEffluentsmanagement.Decontaminationmaybewaivedbaseduponradiologicalconditions.Allvehiclesusedtotransportradioactivewasterequiringthevehicletobeplacardedshallbecheckedforadequateoperationandsafetyconditions.AllRadwasteshipmentsfromSSESshallnormallybevia"ExclusiveUse"vehicles.Specificinstructionsgiventothedriverinclude:a.Expectedrouteoftraveltohisfinaldestination.b.CiMaintaining"ExclusiveUse"status.Specificactionstobetakenintheeventofanaccident.NovehiclecarryingradioactivewastethatisoverweightshallleaveSSESwithoutaPennsylvaniaoverweightpermit.a.ADAWshipmentorothershipmentcapableofhavingitsweightadjusted,shallnotbeallowedtoleaveSSESoverloaded.b.Anoverloadedconditionforanyvehicleisbasedontotalweightandweightperaxle.

NOAP-gA-0646Revision4,Page51of636.13.11In'theeventaccessisdeniedtoSSESatalloperatingdisposalfacilities,PALwillprovidecarrierwithaletterstatingthatSSESwillmeetallapplicablefederal,state,andcompactrequirementsforreceiptbackoftheradioactivewaste/materialincarrier'spossession.6.14SHIPMENTCONFIRMATIONIfdisposalsiteshipmentacknowledgementisnotreceivedwithin18daysfromdeparturefromSSES,EffluentsManagementSupervisionshallconductatraceinvestigationforshipmentlocation.Ifthedisposalfacilityshipmentreceiptcannotbeconfirmedwithin20days,aConditionReport(CR)shallbegenerated.6.15CHANGESTOTHESOLIDRADIOACTIVENSTEPROCESSCONTROLPROGRAM6.15.1AnychangesasdescribedintheTechnicalSpecifications,totheSolidRadioactiveMasteProcessControlProgramshallbeprovidedintheAnnualRadioactiveEffluentReleaseReportfiledwiththeNRC.6.15.2AnychangestotheSolidRadioactiveHasteProcessControlProgramshallbeapprovedbyPlantOperationsReviewCommittee(PORC)priortoimplementation.(")6.16EVALUATIONOFPROCESSOROPERATIONALCHANGES6.16.16.16.2Changesinradioactivewasteprocessingoroperationalchangesshallbeevaluatedtodetermineanyimpactsonwastecharacteristicsand/orform.Evaluationshouldincludeasaminimum:a.Operationalevaluationofprocessingimpacts.b.Chemistryevaluationofchangestosamplingand.analysismethodology.-Cid.EffluentsManagementevaluationofpackagingand/orshippingimpacts.EffluentsManagementevaluationfor10CFR61compliance.

8 NDAP-gA-0646Revision4Page52of63e.Solidification/DewateringServicesVendorwastestreamcharacteristicevaluationofthedewatering/solidificationsystemoperatingparametersandeffectiveness.()6.17REPORTINGOFNISHAPSINVOLVINGLOWLEVELMASTEFORMS6.17.110CFR61establishestheminimumandstabilityrequirementsforLowLevelMaste(LLM)forms.10CFR20requirescertificationthattheprocessedwastesatisfiestherequirementsof10CFR61.MishapswhichmayimpactthefinalwasteformshallbereportedtotheNRC.6.17.2Typesofmishapswhichshouldbereportedinclude:'a~b.C.Failureofhigh-integritycontainersusedtoensureastablewasteform.Containerfailurecanbeevidencedbychangedcontainerdimensions,cracking,ordamageresultingfrommishand'ting(e.g.,droppingorimpactingagainstanotherobject).Misuseofhigh-integritycontainers,evidencedbyaquantityoffreeliquidgreaterthan1percentofcontainervolume,orbyanexcessive(>1M)voidspacewithinthecontainer.ProductionofacementsolidifiedClassBorCwasteformthathasanyofthe-followingcharacteristics:(1)Containsfreeliquidinquantitiesexceeding0.5percentofthevolumeofthewaste.(2)Containswastewithradionuclidesinconcentrationsexceedingthoseconsideredduringwasteformqualificationtestingacceptedbytheregulatoryagency,whichcouldleadtoerrorsinassessmentof-wasteclass.(3)Containsasignificantlydifferentwasteloadingthanthatusedinqualificationtestingacceptedbytheregulatoryagency.

NDAP-gA-0646Revision4Page53of63d.(4)Containschemicalingredientsnotpresentinqualificationtestingacceptedbytheregulatoryagency,and.thosequantitiesaresufficienttounacceptablydegradethewasteproduct.(5)Showsinstabilityevidencedbycrumbling,cracking,spalling,voids,softening,disintegration,non-homogeneity,ordimensionalchanges.(6)Evidenceofprocessingphenomenathatexceedthelimitingprocessingconditionsidentifiedinapplicabletopicalreportsorprocesscontrolplans,e.g.,foaming,temperatureextremes,prematureorslowhardening,andproductionofvolatilematerial.IFailuretoadheretohighintegritycontainerlimitationsasrequiredbycontainercertificateofcompliance.6.17.36.17.4e.Notificationofviolationbydisposalfacilityregulatoryauthoritiesattimeofcontainer.receiptfordisposal.'ailureofcement-solidifiedstablewasteformlongtermPCPsurveillancespecimensduetoevidenceofsignificantcracking,spalling,orbulkdisintegration,compressionorpenetrometerstrengthandi@versiontestresults.Requirementsforreportingofmishapsshallapplyonlytoprocessinglinersandhighintegritycontainerscontainingradioactivewasteinitsfinalproductform.AConditionReport(CR)shallbegeneratedifoneofthemishapsmentionedoccurs.6.18PCPIHPLEHENTINGPROCEDURESProceduresrequiredforimplementationoftheProcessControlProgramareshowninAttachmentD.*

NDAP-gA-0646Revssion4Page54of637.0~RECODS7.1TheSolidificationRecordsorDewateringRecordsandtheattacheddocumentsshallbeforwardedtofffluentsManagementSupervisionforretentionuntilsuchtimeasthecontaineridentifiedonRecordisshippedforfinaldisposition.7.2WhentheidentifiedcontainerisshippedtheSolidificationRecordsorDewateringRecordsandotherdocumentsconcerningthe.ShipmentshallbefiledwiththeshippingdocumentationandforwardedtoDCSforretention.7.3DocumentationofRadioactiveWasteShipmentsshallberetainedasrequiredbySSESTechnic'alSpecifications.7.4Radioactivewasteshippingdocumentationshallconsistof,butnotlimitedto,thefollowingrecords:7.4;17.4.27.4.37.4.47.4.57.4.67.4.7RadioactiveMaterialShippingNanifestEvaluationofisotopicmixandconcentrationRadiologicalsurveysof:a.Vehicleuponarrivalb.Packagetobeshippedc.LoadedvehiclepriortoshipmentVehicleSafetyinspectionCheck-offsheetforloadingprocedureDocumentationofadherencetoProcessControlProgram(ifapplicable)Specialinstructionstodriver

SOLIDIFICATIONRECORDSHEETPARTI:ContaineridentificationInformationdAttachmentANDAP-gA-0646Revision.4'age55of631.PPSLLinerNumberNumber'.ContainerVendorSerial{RWCUFilterMedia.cannotbeentered)(circleone)3.WasteStreamTestSolidificationrequired7YESNOPART2:ContainerSelection(RefertoMH-PS-100)3.ExpectedMasteClassification/Stabilityl.EstimatedLinerContactDoseRatesmR/hrt.P'dt/tttt~tt/d4.ContainerTypetobeUsed6.ExpectedCaskTypetobeUsedPART3:DocumentationChecklist5.EmptyReightofContainet'hal.2.3~FormNDAP-gA-0646-1(original)WasteFormDocumentationWH-RP-Forms(original)SC-068-%2Forms(copy)MasteForm:STABLEUNSTABLE{circleone)~85%LinerVolumeUtilized:YESNO(circleone)QasteActivityDocumentationCH-RC-.Forms(copy)Isotop>cAnalysis(copy)Compostadded/LogentrymadeonCH-TP-055-14,PART4:HealthPhysicsDataLinerRadiologicalSurvey(original)ActualFilledContainerWeightREMARKS:lb.(IfavailableALARA}FORMNDAP-(A-0646-1,Rev.2,Page1of1(FileR69-1)

TNGCOSAttachmentBNDAP-gA-0646Revision4Page56.of63PARTI:ContainerIdentificationInformation1.PPKLLinerNumber2.ContainerVendorSerialNumber3.Maste'treamPART2:ContainerSelection(RefertoRR-PS-100)1.EstimatedLinerContactDoseRates'R/hr'I2.PtdCiCtt'li/g3.ExpectedMasteClassification/Stability4.LinerTypetobeUsed6.ExpectedCaskTypetobeUsed5.EmptyMeightofContainerawasteupervlsorate>meFORMNDAP-(A-0646-2,Rev.3,(DUPLEX),Page1of3(FileR69-1)

~PRT3:SamplingandAnalysis1.Tank/Containersampled2..SampleNumber3.WasteStream4.IsotopicAnalysisattachedATINGCODS'ttachmentBNDAP-gA-0646Revision4Page57of635.SpecificactivityofDewateredSamplepCi/gm6.a.DewateredVolumeb.DewateredWeightc.Sampledensitymlgmgm/ccx62.43lb/ft7.Compositeadded/LogentrymadeonCH-TP-055-1Theabovetank/containercontainingsolidshasbeenanalyzedinaccordancewithCH-RC-075andfoundtocontaintheisotopesandspecificactivitiesasindicatedontheattacheddatasheets.em>stryupervsssonae>meFORMNDAP-(A-0646-2,Rev.3,(DVPLEX)Page2of3(FileR69-I)

ATERNGCODS+gT4:ContainerShipmentInformationSummaryAttachment8NDAP-gA-0646Revision4Page58of633.4.PPELLinerNumberFormNDAP-gA-0646-2(original)MasteFormDocumentation2.MasteVolumeMM-RP-Forms(original)t~CalculatedMasteMeightlb/ft3xftlbPart~ActualFilledContainerWeightlb.(ifavailableALARA))00x(DewateredWasteVolume)fts~fts>85%ContainerVolumeUtilizedYES/NO(Circleone)WasteForm:STABLEUNSTABLE(Circleone)MasteActivityDocumentationCH-RC-Forms(Copy)IsotopicAnalysis(Copy)PART5:REMARKS:awasteupvateeview~ateoremanI~acFORMNDAP-gA-0646-2,Rev.3,(DUPLEX),Page3of3(FileR69-I)

SUUHANNAGU0SOFEOEWTAttachmentCNDAP-gA-0646Revision4Page59of63STVoU001.DateLinernumber2..WasteType3.4.ContainerTypeBurialVolumeUseableContainerVolume7.8.GuaranteedMinimumWasteVolumeWasteVolumeAttainedinchesxWasteVolumeContainerUsageftsft>/inch.100x(WasteVol.ft>~GuaranteedWin.WasteVol.ft3)-100DeadbandAssessmentVolumeGuaranteedMin.WasteVol.ftk{0.01XGuaranteedMin.WasteVol.ftMinimum{-).fttoMaximum(+)ft10.'PerformanceAssessmentVolumeDeadbandAssessmentVol.ftWasteVol.ftft11.Remarks:12.Signatureos1>cationenorepresentatsve13.Signatureawasteuperv~sorFORMNDAP-(A-0646-3,Rev.2,Page1of1(FileR69-1)

MSTPOCSSNGCPPMNGOCDURAttachmentDNDAP-qA-0646Revision4Page60of63vaoratorConcentrates-SolidifiedPacificNuclearPT-51-WS'acificNuclearOM-114-NSPacificNuclearOM-104MixedSolids-SolidifiedPacificNuclearPT-51-MSPacificNuclearON-104PacificNuclearOH-114-NSLRWFilterMediaURCWastWCUFtered'aSSude-DewateredPacificNuclearOH-43-WSMM-RP-107CondensateRadwasteDeminera'readesi-SoidifiedPacificNuclearPT-51-MSPacificNuclearON-114PacificNuclearOH-104CondensateRadwasteDemineral'rBeadResin-DewateredPacificNuclearOH-43-MSWM-RP-106CartrideFiltersCNSIFO-OP-019(Overpack)WM-PS-230PacificNuclearOH-16-NSMM-RP-)05SEGSTD-P-22-002(ResinExpress)WH-RP-104SEGSTD-P-03-051MH-RP-108.Page1of3 CPIMPMNGOCUAttachmentDNDAP-gA-0646Revision4Page61of63rad'atedHardware-DewateredSte'rNoneDrctiveWasteDAW-PackaWM-PS-210'idOilWaste-SolidifedNone'idOilWaste-DecontaminationNoneSolidSealedSourcesNoneWASTFANALYSISANDCLASSIFICATION-OCFR6PacificNuclearOM-45NSWM-RP-008CH-RC-075CH-RC-076CH-TP-055WM-PS-155WM-PS-160WM-PS-170TSTINGTREATMENTCOMBUSTIBGASSWM-RP-009WM-RP-3010CTVWASTSOFICTON-PacificNuclearOM-114-.NSSC-068-002(TestSolidification)CMNTPage2of3 PCPIPLMENTNGPROCDUAttachmentDNDAP-qA-0646Revision4,Page62of63RADIOACIVEWASTEDEWATERING-GENERALPacificNuclearOH-60-MSWM-RP-010HIGHINGRITYCONTAINRSPacificNuclearOM-16-NSPacificNuclearH-18-NSWH-RP-012ISPOSAFACILITYREUIEMENTSMH-PS-180~AC@GINGMH-RP-Ol1WH-PS-401(LLRMHF)WN-PS-310WN-PS-311WH-PS-315MN-PS-345WH-PS-351WM-PS-352WH-PS-356(HN-'142)(LN-142)(SEG3-82)(CNSI14-195)(CNSI21.;300)(CNSI8-120A)MH-PS-354(CNSI14-215)WM-PS-316(SEG14-215)WH-PS-318(WestinghouseTCT)TRANSPORTATION-49CFOCF7WN-PS-100WH-PS-120MH-PS-140WM-PS-180MH-PS-240WN-PS-250Page3of3

ATEISNOTCOMPABEWPOAttachmentENDAP-gA-0646Revision4Page63of63YNCOINERSAliphatichydrocarbons(hexane,octahe,bexene,octane,etc.)AcetoneAmylAcetateAmylChlorideAnilineAquaRegiaBenzeneBromineliquidButaneCamphorOilCarbonDisulphideCarbonTetrachlorideChlorineliquidChlorobenzeneChloroformChlorosulfonicacidChromic/sulfuricacidCyclohexanoneDibutylphtalateDimethylamineDieselfuelEthylacetateEthylbutyrateEthylchlorideEthyletherEthylenechlorideEthylenechlorohydrinEthylenedichlorideFluorineFurfuralFurfurylalcoholFuelOilGasolineIodineMethylbromideMethylChlorideMethylethylketone(MEK)NethyleneChlorideMoistChlorinegasNitricAcid(50Kweightconcentration)OrganPeroxidesOctylcresolOleicacidOleumPentanePetroleumetherPhenolPropanePropylenedichlorideSulfricacid(60Kweightconcentration)TetrahydrofuranceTitaniumtetrachlorideTouleneTrichloroethyleneTurpentineTetralinXylenePageIofI

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