ML24214A069
| ML24214A069 | |
| Person / Time | |
|---|---|
| Site: | Oyster Creek |
| Issue date: | 08/01/2024 |
| From: | Erickson M Holtec Decommissioning International, Westinghouse |
| To: | Office of Nuclear Reactor Regulation |
| Shared Package | |
| ML24214A209 | List: |
| References | |
| HDI-OC-24-018 24-01-12-2888, Rev 0 | |
| Download: ML24214A069 (1) | |
Text
Technical Basis Document No. 24- 01-12-2888 R0
Dose Contribution from Insignificant Radionuclides in the Oyster Creek Site-Specific Suite of Radiological Nuclides
Revision 1
Prepared by:
Westinghouse - Radiological Engineering Group 141 Longwater Drive Suite 113 Norwell, MA 02061 Technical Basis Document No. 24-01-12-2888 R0 Dose Contribution from Insignificant Radionuclides in the Oyster Creek Site-Specific Suite of Radiological Nuclides
Revision Record Revision Record 0 1/18/2024 1 2/14/2024
Summary of Changes:
Rev 0 - Initial Issue Rev 1 - DCGL Value Updates
Page 2 Technical Basis Document No. 24-01-12-2888 R0 Dose Contribution from Insignificant Radionuclides in the Oyster Creek Site-Specific Suite of Radiological Nuclides
Author:
Martin C. Erickson Date
Reviewer:
Joseph Bisson Date
Reviewer:
William Parish Date
Approved:
Christopher C. Messier Date
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Technical Basis Document No. 24-01-12-2888 R0 Dose Contribution from Insignificant Radionuclides in the Oyster Creek Site-Specific Suite of Radiological Nuclides
CONTENTS EXECUTIVE
SUMMARY
..................................................................................................... 5
1.0 INTRODUCTION
....................................................................................................... 6 2.0 TECHNICAL BASES................................................................................................. 6 3.0 METHODOLOGY...................................................................................................... 6 4.0 CALCULATIONS....................................................................................................... 8
5.0 CONCLUSION
............................................................................................................ 8 6.0 RECOMMENDATIONS............................................................................................. 8
Table 2-1: MDC Values for HTD Radionuclides.......................................................................... 7 Table 4-1: Calculation of Aggregate HTD Dose........................................................................... 8
Attachment A: Off-Site Results.................................................................................................... 10
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Technical Basis Document No. 24-01-12-2888 R0 Dose Contribution from Insignificant Radionuclides in the Oyster Creek Site-Specific Suite of Radiological Nuclides
EXECUTIVE
SUMMARY
The Oyster Creek Nuclear Generating Station (OCNGS) site-specific suite of radionuclides consists of 21 radionuclides of which 14 are hard-to-detect (HTD) beta-emitting and alpha-emitting radionuclides. Site characterization data have shown that the HTD nuclides are consistently below or slightly above the minimum detectable concentration (MDC) in laboratory results, which supports classifying them as insignificant nuclides. Dose assessment showing the HTD nuclides collectively contribute less than 10% of the dose criterion provides confirmation for the insignificant classification. Some gamma-emitting radionuclides were also identified as potentially insignificant based on analytical data; however, since they will all be analyzed for in every FSS sample, they are excluded in this technical basis document.
Five soil samples from the OCNGS Radiologically Controlled Area (RCA), the area where the residual plant radioactivity was greatest during the Phase 1 site characterization, were collected and sent off-site for analysis of HTD nuclides. Except for Sr-90, the analytical results showed that the concentrations of all other HTD nuclides were below their respective MDC values in all samples. Sr-90 was detected at a concentration greater than MDC for the analysis in only 1 of the 5 samples.
The HTD nuclide values were set at the maximum of the MDC values, except for Sr-90, which was set at the identified analysis value, and then compared to the OCNGS Industrial Use (IU)
DCGLs discussed in the OCNGS LTP Chapter 6.
The results of the assessment confirmed that the HTDs contribute less than 10% of the site closure dose criteria (i.e., 25 mrem/y) and can be deemed insignificant. The HTD radionuclides will not be required to undergo further assessment, however, the potential dose contribution of 0.075 mrem/y will be added to each survey unit total dose. Survey unit QC samples will still include an assessment of the HTDs to verify their insignificant status. Should the QC sample results indicate the presence of HTD Radionuclides the potential dose contribution will be evaluated and adjusted, as appropriate.
This effort resulted in the following four recommendations:
- QC sample analyses should include the analysis of insignificant radionuclides.
- A dose contribution of 0.075 mrem/y from soil should be added to the FSS survey unit total dose.
- If additional information regarding the presence of insignificant radionuclides become available during remediation activities or FSS, the potential dose contribution/analysis frequency will be reevaluated and adjusted, as appropriate.
- The approach used for determining the insignificant status of HTD nuclides in soil should be applied to other volumetric site media, such as concrete in basement remaining below grade and buried pipe.
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Technical Basis Document No. 24-01-12-2888 R0 Dose Contribution from Insignificant Radionuclides in the Oyster Creek Site-Specific Suite of Radiological Nuclides
1.0 INTRODUCTION
Derivation of a site-specific suite of radionuclides present at Oyster Creek Nuclear Generating Station (OCNGS) is discussed in Chapter 6, Compliance with the Radiological Criteria for License Termination, of the OCNGS License Termination Plan (LTP). This suite of potential radionuclides contains a total of 21 radionuclides. This Technical Basis is centered on the hard-to-detect (HTD) radionuclides since all easy-to-detect radionuclides will be analyzed for in every Final Status Survey (FSS) sample.
OCNGS submitted 5 soil samples from the Radiologically Controlled Area (RCA) to an off-site laboratory for analysis of 14 HTD radionuclides. The analyses positively identified only 1 HTD radionuclide, Sr-90, in 1 sample at a concentration above the MDC.
2.0 TECHNICAL BASES The guidance contained in NUREG-1757, Vol. 2, Section 3.3, states:
it is reasonable to eliminate radionuclides or pathways that are insignificant contributors to dose from further detailed consideration.
The guidance further states, NRC staff considers radionuclides and exposure pathways that contribute no greater than 10 percent of the dose criteria, considering uncertainty, to be insignificant contributors to dose. Because the dose criteria are performance criteria, this 10 percent limit is an aggregate limitation only.
That is, the sum of the dose contributions from all radionuclides and pathways is necessary considered insignificant should be no more than 10 percent of the dose criteria. No limitation on either single radionuclides or individual pathways is necessary.
Once a licensee has demonstrated that radionuclides or exposure pathways are insignificant, then (1) the dose from the insignificant radionuclides and pathways must be accounted for in demonstrating compliance, but (2) the insignificant radionuclides and pathways may be eliminated from further detailed evaluations.
Therefore, it is necessary to calculate potential dose from HTD radionuclides and compare the aggregate potential dose to ensure that it does not exceed 10% of the dose limit (i.e.,
2.5 mrem/y TEDE).
3.0 METHODOLOGY Five sample locations were chosen based on a review of all the soil data collected during the Phase I Characterization effort. These locations were all within the RCA and represented the highest Co-60 and Cs-137 activity concentrations. Once identified, GPS was used to stake out the original sample location. An area representing approximately 1m2 around each location was scanned and a soil sample collected at the highest direct measurement location. Transfer of the sample to the off-site laboratory was controlled by chain of custody procedure and documented by a COC form. Detection sensitivities for
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Technical Basis Document No. 24-01-12-2888 R0 Dose Contribution from Insignificant Radionuclides in the Oyster Creek Site-Specific Suite of Radiological Nuclides
analysis of the HTD radionuclides were established at the lowest levels achievable by the off-site laboratory to ensure detection of very low activity concentrations.
The OCNGS Phase 1 Characterization soil samples sent for HTD analysis consistently indicate the activities and subsequent dose, contribute, in aggregate, less than 10% of the of the 25 mrem/y release criteria for unrestricted use. Therefore, it is appropriate to deem these radionuclides as insignificant dose contributors. The potential dose contribution and pathways for these radionuclides must be determined and included in the final dose evaluation for site release.
Except for Sr-90, the estimated dose for HTDs is based on the maximum MDC values.
The estimated dose for Sr-90 was based on an activity concentration of 0.0697 pCi/g which corresponds to the activity concentration of the sample result (see soil sample RCS-SOIL-16-B in Table 3-1 below.) The MDC values for the HTD radionuclide are presented in in Table 4-1. The HTD nuclide values were set at the maximum of the MDC values, except for Sr-90, which was set at the identified analysis value, and then compared to the OCNGS Industrial Use (IU) DCGLs discussed in the OCNGS LTP Chapter 6. Industrial Use DCGLs include direct exposure, indirect ingestion of soil, inhalation, and ingestion of aquatic foods.
Table 3-1: MDC Values for HTD Radionuclides
Am-241 Pu - 238 Sr - 90 Tc-99 MDC Values MDC Va l ues MDC Va l ues MDC Values Sam p l e ID (pCi/g) Sam p l e ID ( p Ci/g ) Sam p l e ID ( p Ci/g ) Sam pl e ID ( p Ci/g)
RCA -SOI L- 04-B 0.0622 RCA -SO IL-04-B 0.01 25 RCA-SOIL-04-B 0.0167 RCA-SOIL-04-B 1.46 RCA -SOI L-10-B 0.0298 RCA-SOIL-10-B 0.019 RCA-SOIL-10-B 0.0176 RCA-SOIL-10-B 1. 08 RCA -SOI L-15-B 0.152 RCA -SOI L-15-B 0.0198 RCA-SOIL-15-B 0.0 171 RCA-SOIL-15-B 0.921 RCA -SOI L-16-B 0.05 1 RCA -SO IL-16-B 0.0184 RCA-SOIL-16-B* 0.0697 RCA-SOIL-16-B 0. 703 RCA -SOI L-19-B 0.104 RCA -SO IL-19-B 0.0192 RCA-SOIL-19-B 0.0176 RCA-SOIL-19-B 0.814 Maximum 0.152 Maximum 0.0198 Maximum 0.0697 Max imum 1.46
Cm-243/244 Pu - 239/240 H-3 Fe-55 MDC Va l ues MDC Va l ues MDC Va l ues MDC Va l ues Sam p l e ID (pCi/ g ) Sam p l e ID ( p Ci/g ) Sam p l e ID ( p Ci/g ) Sam pl e ID ( p Ci/g)
RCA -SOI L- 04-B 0.0497 RCA -SO IL-04-B 0.0274 RCA-SOIL-04-B 4.51 RCA-SOIL-04-B 75.1 RCA -SOI L-10-B 0.0339 RCA -SOI L-10-B 0.0241 RCA -SOI L-10-B 4.54 RCA -SOI L-10-B 88.9 RCA -SOI L-15-B 0.253 RCA -SOI L-15-B 0.0347 RCA-SOIL-15-B 4.47 RCA-SOIL-15-B 90.6 RCA -SOI L-16-B 0.0411 RCA-SOIL-16-B 0.0184 RCA -SOI L B 4.38 RCA-SOI L B 87. 5 RCA -SOI L-19-B 0.10 2 RCA -SOIL-19-B 0.0244 RCA -SOI L-19-B 4.55 RCA-SOIL-19-B 79. 5 Maximum 0.253 Maximum 0.034 7 Maximum 4.55 Max imum 90.6
N p-237 Pu - 241 C-14 Ni -63 MDC Va l ues MDC Va l ues MDC Va l ues MDC Va l ues Sam p l e ID (p Ci/g ) Sam p l e ID ( p Ci/g ) Sam p l e ID ( p Ci/g) Sam pl e I D ( p Ci/g)
RCA -SOI L- 04-B 0.0083 RCA -SOI L- 04-B 7.49 RCA -SOI L-04-B 0.62 RCA -SOI L-04-B 5.5 1 RCA -SOI L-10-B 0.0066 RCA -SOI L-10-B 7.65 RCA -SOI L-10-B 0.618 RCA-SOIL-10-B 5. 26 RCA -SOI L-15-B 0.0107 RCA -SOIL-15-B 6.97 RCA -SO I L-15-B 0. 634 RCA-SOI L-15-B 5.03 RCA -SOI L-16-B 0.0118 RCA -SO IL-16-B 7.06 RCA-SOIL-16-B 0.626 RCA-SOIL-16-B 4.89 RCA -SOI L-19-B 0.005 8 RCA -SOI L-19 -B 6. 77 RCA-SOIL-19-B 0.636 RCA-SOIL-19-B 4. 5 1 Maxi mum 0.0118 Maximum 7.65 Maximum 0.636 Max imum 5.51
- Sr-90 Positively identified in analysis
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Technical Basis Document No. 24-01-12-2888 R0 Dose Contribution from Insignificant Radionuclides in the Oyster Creek Site-Specific Suite of Radiological Nuclides
4.0 CALCULATIONS Calculation of Potential Dose from Insignificant Nuclides The dose from the postulated insignificant radionuclides was calculated using the HTD maximum MDC radionuclide values provided in Table 4-1. The individual radionuclide doses were calculated by multiplying the ratio of the MDC to DCGL by the release criterion (25 mrem/y). The total potential dose from all HTD radionuclides is 7.50E-02 mrem/y using the maximum MDC values and following equation:
HTD mrem/y = ((MDC, pCi/g)/(DCGL, pCi/g))* 25 mrem/y
The aggregate dose is the summation of the individual HTD doses.
Table 4-1: Calculation of Aggregate HTD Dose
Soil DCGL Max MDC HTD Dose ROC (IU) (pCi/g) (mrem/y)
(pCi/g)
Am-241 7.30E+02 1.52E-01 5.21E-03 C-14 2.07E+03 6.36E-01 7.68E-03 Cm-243 1.81E+02 2.53E-01 3.49E-02 Cm-244 1.82E+03 2.53E-01 3.48E-03 Fe-55 8.39E+06 9.06E+01 2.70E-04 H-3 5.02E+04 4.55E+00 2.27E-03 Ni-63 7.75E+06 5.04E+00 1.63E-05 Np-237 5.75E+01 1.18E-02 5.13E-03 Pu-238 1.14E+03 1.98E-02 4.34E-04 Pu-239 2.37E+02 3.47E-02 3.66E-03 Pu-240 1.08E+03 3.47E-02 8.03E-04 Pu-241 2.50E+04 7.65E+00 7.65E-03 Sr-90 4.24E+03 6.97E-02 4.11E-04 Tc-99 1.37E+04 1.46E+00 2.66E-03 Aggregate dose 7.46E-02
5.0 CONCLUSION
As shown in Table 4-1, the total dose contribution of the OCNGS HTD radionuclides is less than 10% of the dose criteria and therefore it is appropriate to consider them as insignificant.
6.0 RECOMMENDATIONS Survey Unit QC offsite sample analyses should include analysis of the postulated
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Technical Basis Document No. 24-01-12-2888 R0 Dose Contribution from Insignificant Radionuclides in the Oyster Creek Site-Specific Suite of Radiological Nuclides
insignificant radionuclides to address the potential for dose from the postulated insignificant radionuclides and exposure pathways.
A dose contribution of 0.075 mrem/y should be added to the FSS survey unit total dose whereby accounting for the potential dose contribution for postulated insignificant radionuclides.
If additional information regarding the presence of insignificant radionuclides become available during remediation activities or FSS, the potential dose contribution/analysis frequency will be reevaluated and adjusted, as appropriate.
The approach used for determining the insignificant status of HTD nuclides in soil should be applied to other volumetric site media, such as concrete in basement remaining below grade and buried pipe.
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Technical Basis Document No. 24-01-12-2888 R0 Dose Contribution from Insignificant Radionuclides in the Oyster Creek Site-Specific Suite of Radiological Nuclides
Attachment A Off-Site Results
Page 10
m ~ II Laboratories LLC
a member of The GEL Group INC
November 09, 2023
Chris Messier BHI Energy 97 Libbey Industrial Parkway 4th Floor Weymouth, Massachusetts 02189
Re: Oyster Creek Soil Analysis Work Order: 642226
Dear Chris Messier:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on October 20, 2023. This original data report has been prepared and reviewed in accordance with GELs standard operating procedures.
The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt.
Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory.
Copies of GELs accreditations and certifications can be found on our website at www.gel.com.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4504.
Sincerely,
Amanda Turner forPM_SIGN_HERE Erin Trent Project Manager
Purchase Order: ENG-P2023-98002888-01 Enclosures
Page 1 of 30 SDG: 642226 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for HBHI001 Holtec BHI Client SDG: 642226 GEL Work Order: 642226
The Qualifiers in this report are defined as follows:
- A quality control analyte recovery is outside of specified acceptance criteria
- Analyte is a Tracer compound
Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
The designation ND, if present, appears in the result column when the analyte concentration is not detected above the limit as defined in the 'U' qualifier above.
This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Erin Trent.
Reviewed by USER_SIGN_HERE
Page 2 of 30 SDG: 642226 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
Certificate of Analysis Report Date: November 9, 2023 Company : BHI Energy Address : 97 Libbey Industrial Parkway 4th Floor Weymouth, Massachusetts 02189
Contact:
Chris Messier Project: Oyster Creek Soil Analysis Client Sample ID: RCA-SOIL-16-B HBHI00222Project:
Sample ID: 642226001 Client ID: HBHI001 Matrix: Soil Collect Date: 12-OCT-23 10:59 Receive Date: 20-OCT-23 Collector: Client
Parameter Result UnitsQualifier Analyst Date TimeUncertaintyMDC PFRLDFBatchMethod Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid "Dry Weight Corrected" Americium-241 U 0.0131 +/-0.0291 0.0510 0.261 pCi/g EJ1 10/31/23 0837 2513350 1 Curium-243/244 U -0.00598 +/-0.0139 0.0411 0.488 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 U -0.00365 +/-0.00516 0.0118 0.0110 pCi/g EJ1 10/28/23 1433 2513355 2 Alphaspec Pu, Solid "Dry Weight Corrected" Plutonium-238 U 0.00676 +/-0.0133 0.0184 0.219 pCi/g EJ1 10/28/23 1045 2513351 3 Plutonium-239/240 U 0.0144 +/-0.0170 0.0184 0.281 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 U 1.22 +/-4.08 7.06 8.83 pCi/g EJ1 10/30/23 1718 2513353 4 Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 0.0697 +/-0.0121 0.0161 0.0177 pCi/g ST2 11/02/23 1833 2512641 5 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "As Received" Tritium U 1.29 +/-2.54 4.38 5.05 pCi/g KXA1 10/25/23 2026 2512884 6 Liquid Scint C14, Solid "As Received" Carbon-14 U 0.131 +/-0.366 0.626 0.0284 pCi/g KXA1 10/31/23 0931 2512921 7 Liquid Scint Tc99, Solid "As Received" Technetium-99 U 0.0416 +/-0.412 0.703 0.157 pCi/g AG2 10/30/23 2233 2512495 8 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 U -24.9 +/-55.9 87.5 516 pCi/g TXJ1 10/30/23 1012 2512806 9 Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U 2.00 +/-2.89 4.89 7.24 pCi/g TXJ1 11/01/23 0758 2512838 10 The following Prep Methods were performed:
Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 10/23/23 2512302WGR1152
Page 3 of 30 SDG: 642226 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
Certificate of Analysis Report Date: November 9, 2023 Company : BHI Energy Address : 97 Libbey Industrial Parkway 4th Floor Weymouth, Massachusetts 02189
Contact:
Chris Messier Project: Oyster Creek Soil Analysis Client Sample ID: RCA-SOIL-16-B HBHI00222Project:
Sample ID: 642226001 Client ID: HBHI001
Parameter Result UnitsQualifier Analyst Date TimeUncertaintyMDC PFRLDFBatchMethod The following Analytical Methods were performed:
Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 6 EPA 906.0 Modified 7 EPA EERF C-01 Modified 8 DOE EML HASL-300, Tc-02-RC Modified 9 DOE RESL Fe-1, Modified 10 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Acceptable LimitsResultNominalRecovery%
Americium-243 Tracer Alphaspec Am241, Cm, Solid "Dry Weight 46.2 (15%-125%)
Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 78.5 (15%-125%)
Plutonium-242 Tracer Alphaspec Pu, Solid "Dry Weight Corrected" 69.9 (15%-125%)
Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 69.9 (15%-125%)
Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 65.9 (25%-125%)
Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 1.30E+06 CPM 1.38E+06 93.9 (15%-125%)
Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 101 (15%-125%)
Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 88.8 (25%-125%)
Notes:
Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
Column headers are defined as follows:
DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
Page 4 of 30 SDG: 642226 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
Certificate of Analysis Report Date: November 9, 2023 Company : BHI Energy Address : 97 Libbey Industrial Parkway 4th Floor Weymouth, Massachusetts 02189
Contact:
Chris Messier Project: Oyster Creek Soil Analysis Client Sample ID: RCA-SOIL-19-B HBHI00222Project:
Sample ID: 642226002 Client ID: HBHI001 Matrix: Soil Collect Date: 12-OCT-23 10:41 Receive Date: 20-OCT-23 Collector: Client
Parameter Result UnitsQualifier Analyst Date TimeUncertaintyMDC PFRLDFBatchMethod Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid "Dry Weight Corrected" Americium-241 U 0.0727 +/-0.0831 0.104 0.261 pCi/g EJ1 10/28/23 1104 2513350 1 Curium-243/244 U 0.0215 +/-0.0591 0.102 0.488 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 U 0.00305 +/-0.00422 0.00583 0.0110 pCi/g EJ1 10/28/23 1433 2513355 2 Alphaspec Pu, Solid "Dry Weight Corrected" Plutonium-238 U -0.000960 +/-0.00828 0.0192 0.219 pCi/g EJ1 10/28/23 1045 2513351 3 Plutonium-239/240 U 0.00911 +/-0.0161 0.0244 0.281 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 U 0.543 +/-3.88 6.77 8.83 pCi/g EJ1 10/30/23 1734 2513353 4 Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0173 +/-0.0115 0.0176 0.0177 pCi/g ST2 11/01/23 1220 2512641 5 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "As Received" Tritium U 0.269 +/-2.57 4.55 5.05 pCi/g KXA1 10/25/23 2103 2512884 6 Liquid Scint C14, Solid "As Received" Carbon-14 U 0.111 +/-0.372 0.636 0.0284 pCi/g KXA1 10/31/23 1007 2512921 7 Liquid Scint Tc99, Solid "As Received" Technetium-99 U 0.633 +/-0.489 0.814 0.157 pCi/g AG2 10/30/23 2336 2512495 8 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 U -13.1 +/-51.0 79.5 516 pCi/g TXJ1 10/30/23 1027 2512806 9 Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U -1.10 +/-2.54 4.51 7.24 pCi/g TXJ1 11/01/23 0815 2512838 10 The following Prep Methods were performed:
Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 10/23/23 2512302WGR1152
Page 5 of 30 SDG: 642226 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
Certificate of Analysis Report Date: November 9, 2023 Company : BHI Energy Address : 97 Libbey Industrial Parkway 4th Floor Weymouth, Massachusetts 02189
Contact:
Chris Messier Project: Oyster Creek Soil Analysis Client Sample ID: RCA-SOIL-19-B HBHI00222Project:
Sample ID: 642226002 Client ID: HBHI001
Parameter Result UnitsQualifier Analyst Date TimeUncertaintyMDC PFRLDFBatchMethod The following Analytical Methods were performed:
Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 6 EPA 906.0 Modified 7 EPA EERF C-01 Modified 8 DOE EML HASL-300, Tc-02-RC Modified 9 DOE RESL Fe-1, Modified 10 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Acceptable LimitsResultNominalRecovery%
Americium-243 Tracer Alphaspec Am241, Cm, Solid "Dry Weight 21.3 (15%-125%)
Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 73.4 (15%-125%)
Plutonium-242 Tracer Alphaspec Pu, Solid "Dry Weight Corrected" 74.4 (15%-125%)
Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 74.4 (15%-125%)
Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 72.7 (25%-125%)
Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 1.26E+06 CPM 1.38E+06 90.8 (15%-125%)
Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 100 (15%-125%)
Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 95 (25%-125%)
Notes:
Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
Column headers are defined as follows:
DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
Page 6 of 30 SDG: 642226 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
Certificate of Analysis Report Date: November 9, 2023 Company : BHI Energy Address : 97 Libbey Industrial Parkway 4th Floor Weymouth, Massachusetts 02189
Contact:
Chris Messier Project: Oyster Creek Soil Analysis Client Sample ID: RCA-SOIL-15-B HBHI00222Project:
Sample ID: 642226003 Client ID: HBHI001 Matrix: Soil Collect Date: 12-OCT-23 10:58 Receive Date: 20-OCT-23 Collector: Client
Parameter Result UnitsQualifier Analyst Date TimeUncertaintyMDC PFRLDFBatchMethod Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid "Dry Weight Corrected" Americium-241 U -0.00435 +/-0.0653 0.152 0.261 pCi/g EJ1 10/28/23 1104 2513350 1 Curium-243/244 U -0.0592 +/-0.0981 0.253 0.488 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 U 0.00819 +/-0.00729 0.0107 0.0110 pCi/g EJ1 10/28/23 1433 2513355 2 Alphaspec Pu, Solid "Dry Weight Corrected" Plutonium-238 U 0.00314 +/-0.0118 0.0198 0.219 pCi/g EJ1 10/28/23 1050 2513351 3 Plutonium-239/240 U -0.00479 +/-0.0130 0.0347 0.281 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 U 0.463 +/-3.94 6.87 8.83 pCi/g EJ1 10/30/23 1751 2513353 4 Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.0160 +/-0.0110 0.0171 0.0177 pCi/g ST2 10/31/23 1717 2512641 5 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "As Received" Tritium U 1.92 +/-2.63 4.47 5.05 pCi/g KXA1 10/25/23 2140 2512884 6 Liquid Scint C14, Solid "As Received" Carbon-14 U 0.287 +/-0.376 0.634 0.0284 pCi/g KXA1 10/31/23 1042 2512921 7 Liquid Scint Tc99, Solid "As Received" Technetium-99 U 0.538 +/-0.549 0.921 0.157 pCi/g AG2 10/31/23 0038 2512495 8 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 U 4.01 +/-58.5 90.6 516 pCi/g TXJ1 10/30/23 1043 2512806 9 Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U 0.629 +/-2.91 5.03 7.24 pCi/g TXJ1 11/01/23 0832 2512838 10 The following Prep Methods were performed:
Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 10/23/23 2512302WGR1152
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Certificate of Analysis Report Date: November 9, 2023 Company : BHI Energy Address : 97 Libbey Industrial Parkway 4th Floor Weymouth, Massachusetts 02189
Contact:
Chris Messier Project: Oyster Creek Soil Analysis Client Sample ID: RCA-SOIL-15-B HBHI00222Project:
Sample ID: 642226003 Client ID: HBHI001
Parameter Result UnitsQualifier Analyst Date TimeUncertaintyMDC PFRLDFBatchMethod The following Analytical Methods were performed:
Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 6 EPA 906.0 Modified 7 EPA EERF C-01 Modified 8 DOE EML HASL-300, Tc-02-RC Modified 9 DOE RESL Fe-1, Modified 10 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Acceptable LimitsResultNominalRecovery%
Americium-243 Tracer Alphaspec Am241, Cm, Solid "Dry Weight 17.5 (15%-125%)
Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 74 (15%-125%)
Plutonium-242 Tracer Alphaspec Pu, Solid "Dry Weight Corrected" 71.6 (15%-125%)
Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 71.6 (15%-125%)
Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 90.9 (25%-125%)
Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 1.22E+06 CPM 1.38E+06 88.5 (15%-125%)
Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 94 (15%-125%)
Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 85.1 (25%-125%)
Notes:
Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
Column headers are defined as follows:
DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
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Certificate of Analysis Report Date: November 9, 2023 Company : BHI Energy Address : 97 Libbey Industrial Parkway 4th Floor Weymouth, Massachusetts 02189
Contact:
Chris Messier Project: Oyster Creek Soil Analysis Client Sample ID: RCA-SOIL-10-B HBHI00222Project:
Sample ID: 642226004 Client ID: HBHI001 Matrix: Soil Collect Date: 12-OCT-23 11:05 Receive Date: 20-OCT-23 Collector: Client
Parameter Result UnitsQualifier Analyst Date TimeUncertaintyMDC PFRLDFBatchMethod Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid "Dry Weight Corrected" Americium-241 U 0.0109 +/-0.0215 0.0298 0.261 pCi/g EJ1 10/28/23 1104 2513350 1 Curium-243/244 U 0.00931 +/-0.0214 0.0339 0.488 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 U 0.00205 +/-0.00403 0.00656 0.0110 pCi/g EJ1 10/28/23 1433 2513355 2 Alphaspec Pu, Solid "Dry Weight Corrected" Plutonium-238 U -0.000949 +/-0.00818 0.0190 0.219 pCi/g EJ1 10/28/23 1050 2513351 3 Plutonium-239/240 U -0.00285 +/-0.00859 0.0241 0.281 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 U -0.255 +/-4.34 7.65 8.83 pCi/g EJ1 10/30/23 1807 2513353 4 Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 U 0.00683 +/-0.0102 0.0176 0.0177 pCi/g ST2 10/31/23 1717 2512641 5 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "As Received" Tritium U 2.31 +/-2.69 4.54 5.05 pCi/g KXA1 10/25/23 2217 2512884 6 Liquid Scint C14, Solid "As Received" Carbon-14 U 0.253 +/-0.365 0.618 0.0284 pCi/g KXA1 10/31/23 1118 2512921 7 Liquid Scint Tc99, Solid "As Received" Technetium-99 U 0.211 +/-0.633 1.08 0.157 pCi/g AG2 10/31/23 0141 2512495 8 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 U -28.7 +/-56.6 88.9 516 pCi/g TXJ1 10/30/23 1059 2512806 9 Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U 3.57 +/-3.16 5.26 7.24 pCi/g TXJ1 11/01/23 0848 2512838 10 The following Prep Methods were performed:
Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 10/23/23 2512302WGR1152
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Certificate of Analysis Report Date: November 9, 2023 Company : BHI Energy Address : 97 Libbey Industrial Parkway 4th Floor Weymouth, Massachusetts 02189
Contact:
Chris Messier Project: Oyster Creek Soil Analysis Client Sample ID: RCA-SOIL-10-B HBHI00222Project:
Sample ID: 642226004 Client ID: HBHI001
Parameter Result UnitsQualifier Analyst Date TimeUncertaintyMDC PFRLDFBatchMethod The following Analytical Methods were performed:
Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 6 EPA 906.0 Modified 7 EPA EERF C-01 Modified 8 DOE EML HASL-300, Tc-02-RC Modified 9 DOE RESL Fe-1, Modified 10 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Acceptable LimitsResultNominalRecovery%
Americium-243 Tracer Alphaspec Am241, Cm, Solid "Dry Weight 57.8 (15%-125%)
Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 85.3 (15%-125%)
Plutonium-242 Tracer Alphaspec Pu, Solid "Dry Weight Corrected" 64.5 (15%-125%)
Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 64.5 (15%-125%)
Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 61.4 (25%-125%)
Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 8.79E+05 CPM 1.38E+06 63.6 (15%-125%)
Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 101 (15%-125%)
Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 81.4 (25%-125%)
Notes:
Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
Column headers are defined as follows:
DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
Page 10 of 30 SDG: 642226 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
Certificate of Analysis Report Date: November 9, 2023 Company : BHI Energy Address : 97 Libbey Industrial Parkway 4th Floor Weymouth, Massachusetts 02189
Contact:
Chris Messier Project: Oyster Creek Soil Analysis Client Sample ID: RCA-SOIL-04-B HBHI00222Project:
Sample ID: 642226005 Client ID: HBHI001 Matrix: Soil Collect Date: 12-OCT-23 10:48 Receive Date: 20-OCT-23 Collector: Client
Parameter Result UnitsQualifier Analyst Date TimeUncertaintyMDC PFRLDFBatchMethod Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid "Dry Weight Corrected" Americium-241 U 0.0474 +/-0.0459 0.0622 0.261 pCi/g EJ1 10/31/23 0837 2513350 1 Curium-243/244 U -0.00142 +/-0.0213 0.0497 0.488 pCi/g Alphaspec Np, Solid "Dry Weight Corrected" Neptunium-237 U 0.00202 +/-0.00475 0.00828 0.0110 pCi/g EJ1 10/28/23 1433 2513355 2 Alphaspec Pu, Solid "Dry Weight Corrected" Plutonium-238 U 0.00832 +/-0.0143 0.0125 0.219 pCi/g EJ1 10/28/23 1050 2513351 3 Plutonium-239/240 U 0.00432 +/-0.0148 0.0274 0.281 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 U -0.724 +/-4.23 7.49 8.83 pCi/g EJ1 10/30/23 1823 2513353 4 Rad Gas Flow Proportional Counting GFPC, Sr90, Solid "Dry Weight Corrected" Strontium-90 0.0436 +/-0.0115 0.0167 0.0177 pCi/g ST2 11/02/23 1833 2512641 5 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "As Received" Tritium U 2.64 +/-2.70 4.51 5.05 pCi/g KXA1 10/25/23 2254 2512884 6 Liquid Scint C14, Solid "As Received" Carbon-14 U 0.272 +/-0.367 0.620 0.0284 pCi/g KXA1 10/31/23 1154 2512921 7 Liquid Scint Tc99, Solid "As Received" Technetium-99 U 0.820 +/-0.869 1.46 0.157 pCi/g AG2 10/31/23 0647 2512495 8 Liquid Scint Fe55, Solid "Dry Weight Corrected" Iron-55 U 71.1 +/-50.5 75.1 516 pCi/g TXJ1 10/30/23 1114 2512806 9 Liquid Scint Ni63, Solid "Dry Weight Corrected" Nickel-63 U 0.856 +/-3.19 5.51 7.24 pCi/g TXJ1 11/01/23 0905 2512838 10 The following Prep Methods were performed:
Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 10/23/23 2512302WGR1152
Page 11 of 30 SDG: 642226 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
Certificate of Analysis Report Date: November 9, 2023 Company : BHI Energy Address : 97 Libbey Industrial Parkway 4th Floor Weymouth, Massachusetts 02189
Contact:
Chris Messier Project: Oyster Creek Soil Analysis Client Sample ID: RCA-SOIL-04-B HBHI00222Project:
Sample ID: 642226005 Client ID: HBHI001
Parameter Result UnitsQualifier Analyst Date TimeUncertaintyMDC PFRLDFBatchMethod The following Analytical Methods were performed:
Method Description Analyst Comments 1 DOE EML HASL-300, Am-05-RC Modified 2 ASTM C 1475-00 Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 EPA 905.0 Modified/DOE RP501 Rev. 1 Modified 6 EPA 906.0 Modified 7 EPA EERF C-01 Modified 8 DOE EML HASL-300, Tc-02-RC Modified 9 DOE RESL Fe-1, Modified 10 DOE RESL Ni-1, Modified Surrogate/Tracer Recovery Test Acceptable LimitsResultNominalRecovery%
Americium-243 Tracer Alphaspec Am241, Cm, Solid "Dry Weight 40.7 (15%-125%)
Corrected" Americium-243 Tracer Alphaspec Np, Solid "Dry Weight Corrected" 84.5 (15%-125%)
Plutonium-242 Tracer Alphaspec Pu, Solid "Dry Weight Corrected" 64.9 (15%-125%)
Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" 64.9 (15%-125%)
Strontium Carrier GFPC, Sr90, Solid "Dry Weight Corrected" 59.1 (25%-125%)
Technetium-99m Tracer Liquid Scint Tc99, Solid "As Received" 7.33E+05 CPM 1.38E+06 53 (15%-125%)
Iron-59 Tracer Liquid Scint Fe55, Solid "Dry Weight Corrected" 91.8 (15%-125%)
Nickel Carrier Liquid Scint Ni63, Solid "Dry Weight Corrected" 78.9 (25%-125%)
Notes:
Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
Column headers are defined as follows:
DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
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QC Summary Report Date:November 9, 2023 BHI Energy Page 1 of 5 97 Libbey Industrial Parkway 4th Floor Weymouth, Massachusetts
Contact:
Chris Messier Workorder: 642226
Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 2513350 QC1205555385 642226001DUP Americium-241 U 0.0131 U 0.0227 pCi/g N/A N/A E-1 10/28/23 11:04
Curium-243/244 U -0.00598 U 0.00265 pCi/g N/A N/A
QC1205555386 LCS Americium-241 0.950 0.837 pCi/g 88.1 (75%-125%) 10/28/23 11:04
Curium-243/244 0.965 0.906 pCi/g 93.9 (75%-125%)
QC1205555384 MB Americium-241 U -0.00103 pCi/g 10/28/23 11:04
Curium-243/244 U -0.00611 pCi/g
Batch 2513351 QC1205555388 642226001DUP Plutonium-238 U 0.00676 U 0.00748 pCi/g N/A N/A E-1 10/28/23 10:50
Plutonium-239/240 U 0.0144 U 0.00278 pCi/g N/A N/A
QC1205555389 LCS Plutonium-238 0.0145 pCi/g 10/28/23 10:50
Plutonium-239/240 0.984 0.975 pCi/g 99.1 (75%-125%)
QC1205555387 MB Plutonium-238 U -0.00429 pCi/g 10/28/23 10:50
Plutonium-239/240 U -0.00429 pCi/g
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QC Summary Workorder: 642226 Page 2 of 5
Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 2513353
QC1205555391 642226001DUP Plutonium-241 U 1.22 U -0.00766 pCi/g N/A N/A E-1 10/30/23 18:56
QC1205555392 LCS Plutonium-241 64.7 64.9 pCi/g 100 (75%-125%) 10/30/23 19:12
QC1205555390 MB Plutonium-241 U -1.55 pCi/g 10/30/23 18:40
Batch 2513355 QC1205555394 642226001DUP Neptunium-237 U -0.00365 U -0.00521 pCi/g N/A N/A E-1 10/28/23 14:33
QC1205555395 LCS Neptunium-237 1.23 1.36 pCi/g 111 (75%-125%) 10/28/23 15:34
QC1205555393 MB Neptunium-237 U 0.00106 pCi/g 10/28/23 14:33
Rad Gas Flow Batch 2512641 QC1205553829 642226001DUP Strontium-90 0.0697 0.0444 pCi/g 44.3 (0% - 100%) ST2 11/08/23 18:15
QC1205553830 LCS Strontium-90 1.61 1.69 pCi/g 105 (75%-125%) 10/30/23 17:40
QC1205553828 MB Strontium-90 U 0.00695 pCi/g 10/31/23 17:17
Rad Liquid Scintillation Batch 2512495
QC1205553510 642226001DUP Technetium-99 U 0.0416 U 0.417 pCi/g N/A N/A AG2 10/31/23 08:52
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QC Summary Workorder: 642226 Page 3 of 5
Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 2512495
- Technetium-99m Tracer 1.38E 06 1.30E 06 1.28E 06 CPM 92.5 (15%-125%) AG2 10/31/23 08:52
QC1205553511 LCS Technetium-99 16.1 15.0 pCi/g 93 (75%-125%) 10/31/23 10:00
- Technetium-99m Tracer 1.38E 06 1.30E 06 CPM 94.3 (15%-125%)
QC1205553509 MB Technetium-99 U -0.0783 pCi/g 10/31/23 07:49
- Technetium-99m Tracer 1.38E 06 1.29E 06 CPM 93.3 (15%-125%)
Batch 2512806 QC1205554207 642226001DUP Iron-55 U -24.9 U -45.3 pCi/g N/A N/A T;-1 10/30/23 11:46
QC1205554208 LCS Iron-55 596 562 pCi/g 94.3 (75%-125%) 10/30/23 12:01
QC1205554206 MB Iron-55 U 6.77 pCi/g 10/30/23 11:30
Batch 2512838 QC1205554285 642226001DUP Nickel-63 U 2.00 U 1.62 pCi/g N/A N/A T;-1 11/01/23 09:39
QC1205554286 LCS Nickel-63 137 144 pCi/g 106 (75%-125%) 11/01/23 09:56
QC1205554284 MB Nickel-63 U -0.270 pCi/g 11/01/23 09:22
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QC Summary Workorder: 642226 Page 4 of 5
Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 2512884
QC1205554433 642226001DUP Tritium U 1.29 U 1.30 pCi/g N/A N/A K;A1 10/26/23 00:07
QC1205554435 LCS Tritium 47.7 43.9 pCi/g 92.2 (75%-125%) 10/26/23 01:21
QC1205554432 MB Tritium U 0.442 pCi/g 10/25/23 23:30
QC1205554434 642226001MS Tritium 139 U 1.29 118 pCi/g 85 (75%-125%) 10/26/23 00:44
Batch 2512921 QC1205554553 642226001DUP Carbon-14 U 0.131 U 0.184 pCi/g N/A N/A K;A1 10/31/23 13:06
QC1205554555 LCS Carbon-14 24.0 22.5 pCi/g 93.7 (75%-125%) 10/31/23 14:17
QC1205554552 MB Carbon-14 U 0.168 pCi/g 10/31/23 12:30
QC1205554554 642226001MS Carbon-14 69.1 U 0.131 65.7 pCi/g 95 (75%-125%) 10/31/23 13:41
Notes:
The Qualifiers in this report are defined as follows:
U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
J Value is estimated X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier H Analytical holding time was exceeded
< Result is less than value reported
> Result is greater than value reported UI Gamma Spectroscopy--Uncertain identification
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QC Summary Workorder: 642226 Page 5 of 5
Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time BD Results are either below the MDC or tracer recovery is low h Preparation or preservation holding time was exceeded R Sample results are rejected
^ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
N/A RPD or %Recovery limits do not apply.
ND Analyte concentration is not detected above the detection limit M M if above MDC and less than LLD NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier FA Failed analysis.
UJ Gamma Spectroscopy--Uncertain identification Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
K Analyte present. Reported value may be biased high. Actual value is expected to be lower.
UL Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
L Analyte present. Reported value may be biased low. Actual value is expected to be higher.
N1 See case narrative Y Other specific qualifiers were required to properly define the results. Consult case narrative.
- Analyte is a Tracer compound M REMP Result > MDC/CL and < RDL J See case narrative for an explanation N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable.
^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.
- Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.
Page 17 of 30 SDG: 642226 Radiochemistry Technical Case Narrative Holtec BHI SDG #: 642226
Product: Alphaspec Am241, Cm, Solid Analytical Method: DOE EML HASL-300, Am-05-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 28 Analytical Batch: 2513350
Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 24 Preparation Batch: 2512302
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID# Client Sample Identification 642226001 RCA-SOIL-16-B 642226002 RCA-SOIL-19-B 642226003 RCA-SOIL-15-B 642226004 RCA-SOIL-10-B 642226005 RCA-SOIL-04-B 1205555384 Method Blank (MB) 1205555385 642226001(RCA-SOIL-16-B) Sample Duplicate (DUP) 1205555386 Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on a "dry weight" basis.
Data Summary:
All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
Technical Information
Recounts Sample 642226001 (RCA-SOIL-16-B) was recounted due to a peak shift. The recount is reported. Sample 642226005 (RCA-SOIL-04-B) was recounted due to a suspected false positive. The recount is reported.
Miscellaneous Information
Additional Comments The tracer peak centroid for sample 642226001 (RCA-SOIL-16-B) is greater than 50 keV from the expected library energy value for the tracer; however, the tracer yield requirement was met and the tracer peak is within the tracer region of interest.
Page 18 of 30 SDG: 642226 Product: Alphaspec Pu, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 28 Analytical Batch: 2513351
Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 24 Preparation Batch: 2512302
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID# Client Sample Identification 642226001 RCA-SOIL-16-B 642226002 RCA-SOIL-19-B 642226003 RCA-SOIL-15-B 642226004 RCA-SOIL-10-B 642226005 RCA-SOIL-04-B 1205555387 Method Blank (MB) 1205555388 642226001(RCA-SOIL-16-B) Sample Duplicate (DUP) 1205555389 Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on a "dry weight" basis.
Data Summary:
There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
Product: Alphaspec Np, Solid Analytical Method: ASTM C 1475-00 Modified Analytical Procedure: GL-RAD-A-069 REV# 1 Analytical Batch: 2513355
Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 24 Preparation Batch: 2512302
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID# Client Sample Identification 642226001 RCA-SOIL-16-B 642226002 RCA-SOIL-19-B 642226003 RCA-SOIL-15-B 642226004 RCA-SOIL-10-B 642226005 RCA-SOIL-04-B 1205555393 Method Blank (MB) 1205555394 642226001(RCA-SOIL-16-B) Sample Duplicate (DUP) 1205555395 Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on a "dry weight" basis.
Page 19 of 30 SDG: 642226 Data Summary:
All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
Quality Control (QC) Information
RDL Met Samples did not meet the detection limits. The samples were counted the maximum count time in order to achieve the lowest possible MDAs.
Sample Analyte Value 1205555394 (RCA-SOIL-16-BDUP) Neptunium-237 Result -0.00521 < MDA 0.0114 > RDL 0.011 pCi/g 642226001 (RCA-SOIL-16-B) Neptunium-237 Result -0.00365 < MDA 0.0118 > RDL 0.011 pCi/g
Product: Dry Weight Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 24 Preparation Batch: 2512302
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID# Client Sample Identification 642226001 RCA-SOIL-16-B 642226002 RCA-SOIL-19-B 642226003 RCA-SOIL-15-B 642226004 RCA-SOIL-10-B 642226005 RCA-SOIL-04-B
The samples in this SDG were analyzed on an "as received" basis.
Data Summary:
There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
Product: GFPC, Sr90, Solid Analytical Method: EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Analytical Procedure: GL-RAD-A-004 REV# 22 Analytical Batch: 2512641
Preparation Method: Dry Soil Prep
Page 20 of 30 SDG: 642226 Preparation Procedure: GL-RAD-A-021 REV# 24 Preparation Batch: 2512302
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID# Client Sample Identification 642226001 RCA-SOIL-16-B 642226002 RCA-SOIL-19-B 642226003 RCA-SOIL-15-B 642226004 RCA-SOIL-10-B 642226005 RCA-SOIL-04-B 1205553828 Method Blank (MB) 1205553829 642226001(RCA-SOIL-16-B) Sample Duplicate (DUP) 1205553830 Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on a "dry weight" basis.
Data Summary:
All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
Technical Information
Recounts Sample 1205553828 (MB) was recounted due to a suspected blank false positive. The recount is reported.
Samples 642226001 (RCA-SOIL-16-B) and 642226005 (RCA-SOIL-04-B) were taken through additional clean-up steps and recounted to confirm the results. The recounts are reported. Sample 1205553829 (RCA-SOIL-16-BDUP) was recounted due to high relative percent difference/relative error ratio. The recount is reported. Samples 642226002 (RCA-SOIL-19-B), 642226003 (RCA-SOIL-15-B) and 642226004 (RCA-SOIL-10-B) were recounted due to a suspected false positive. The recounts are reported.
Product: Liquid Scint Pu241, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-035 REV# 24 Analytical Batch: 2513353
Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 24 Preparation Batch: 2512302
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID# Client Sample Identification 642226001 RCA-SOIL-16-B 642226002 RCA-SOIL-19-B 642226003 RCA-SOIL-15-B 642226004 RCA-SOIL-10-B 642226005 RCA-SOIL-04-B 1205555390 Method Blank (MB)
Page 21 of 30 SDG: 642226 1205555391 642226001(RCA-SOIL-16-B) Sample Duplicate (DUP) 1205555392 Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on a "dry weight" basis.
Data Summary:
There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
Product: Liquid Scint Tc99, Solid Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Procedure: GL-RAD-A-059 REV# 5 Analytical Batch: 2512495
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID# Client Sample Identification 642226001 RCA-SOIL-16-B 642226002 RCA-SOIL-19-B 642226003 RCA-SOIL-15-B 642226004 RCA-SOIL-10-B 642226005 RCA-SOIL-04-B 1205553509 Method Blank (MB) 1205553510 642226001(RCA-SOIL-16-B) Sample Duplicate (DUP) 1205553511 Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
Data Summary:
All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
Quality Control (QC) Information
RDL Met Samples (See Below) did not meet the detection limits. Samples were counted the maximum count time in order to achieve the lowest MDAs possible.
Sample Analyte Value 1205553509 (MB) Technetium-99 Result -0.0783 < MDA 0.62 > RDL 0.157 pCi/g 1205553510 (RCA-SOIL-16-BDUP) Technetium-99 Result 0.417 < MDA 0.676 > RDL 0.157 pCi/g 642226001 (RCA-SOIL-16-B) Technetium-99 Result 0.0416 < MDA 0.703 > RDL 0.157 pCi/g 642226002 (RCA-SOIL-19-B) Technetium-99 Result 0.633 < MDA 0.814 > RDL 0.157 pCi/g 642226003 (RCA-SOIL-15-B) Technetium-99 Result 0.538 < MDA 0.921 > RDL 0.157 pCi/g 642226004 (RCA-SOIL-10-B) Technetium-99 Result 0.211 < MDA 1.08 > RDL 0.157 pCi/g
Page 22 of 30 SDG: 642226 642226005 (RCA-SOIL-04-B) Technetium-99 Result 0.82 < MDA 1.46 > RDL 0.157 pCi/g
Product: Liquid Scint Fe55, Solid Analytical Method: DOE RESL Fe-1, Modified Analytical Procedure: GL-RAD-A-064 REV# 1 Analytical Batch: 2512806
Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 24 Preparation Batch: 2512302
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID# Client Sample Identification 642226001 RCA-SOIL-16-B 642226002 RCA-SOIL-19-B 642226003 RCA-SOIL-15-B 642226004 RCA-SOIL-10-B 642226005 RCA-SOIL-04-B 1205554206 Method Blank (MB) 1205554207 642226001(RCA-SOIL-16-B) Sample Duplicate (DUP) 1205554208 Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on a "dry weight" basis.
Data Summary:
There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
Product: Liquid Scint Ni63, Solid Analytical Method: DOE RESL Ni-1, Modified Analytical Procedure: GL-RAD-A-022 REV# 19 Analytical Batch: 2512838
Preparation Method: Dry Soil Prep Preparation Procedure: GL-RAD-A-021 REV# 24 Preparation Batch: 2512302
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID# Client Sample Identification 642226001 RCA-SOIL-16-B
Page 23 of 30 SDG: 642226 642226002 RCA-SOIL-19-B 642226003 RCA-SOIL-15-B 642226004 RCA-SOIL-10-B 642226005 RCA-SOIL-04-B 1205554284 Method Blank (MB) 1205554285 642226001(RCA-SOIL-16-B) Sample Duplicate (DUP) 1205554286 Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on a "dry weight" basis.
Data Summary:
There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
Product: LSC, Tritium Dist, Solid Analytical Method: EPA 906.0 Modified Analytical Procedure: GL-RAD-A-002 REV# 24 Analytical Batch: 2512884
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID# Client Sample Identification 642226001 RCA-SOIL-16-B 642226002 RCA-SOIL-19-B 642226003 RCA-SOIL-15-B 642226004 RCA-SOIL-10-B 642226005 RCA-SOIL-04-B 1205554432 Method Blank (MB) 1205554433 642226001(RCA-SOIL-16-B) Sample Duplicate (DUP) 1205554434 642226001(RCA-SOIL-16-B) Matrix Spike (MS) 1205554435 Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
Data Summary:
All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
Miscellaneous Information
Additional Comments The matrix spike, 1205554434 (RCA-SOIL-16-BMS), aliquot was reduced to conserve sample volume.
Product: Liquid Scint C14, Solid
Page 24 of 30 SDG: 642226 Analytical Method: EPA EERF C-01 Modified Analytical Procedure: GL-RAD-A-003 REV# 17 Analytical Batch: 2512921
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID# Client Sample Identification 642226001 RCA-SOIL-16-B 642226002 RCA-SOIL-19-B 642226003 RCA-SOIL-15-B 642226004 RCA-SOIL-10-B 642226005 RCA-SOIL-04-B 1205554552 Method Blank (MB) 1205554553 642226001(RCA-SOIL-16-B) Sample Duplicate (DUP) 1205554554 642226001(RCA-SOIL-16-B) Matrix Spike (MS) 1205554555 Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
Data Summary:
All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions.
Quality Control (QC) Information
RDL Met Samples (See Below) did not meet the detection limits due to the small sample aliquots used. The aliquots were reduced due to the matrix of the samples.
Sample Analyte Value 1205554552 (MB) Carbon-14 Result 0.168 < MDA 0.617 > RDL 0.0284 pCi/g 1205554553 (RCA-SOIL-16-BDUP) Carbon-14 Result 0.184 < MDA 0.635 > RDL 0.0284 pCi/g 642226001 (RCA-SOIL-16-B) Carbon-14 Result 0.131 < MDA 0.626 > RDL 0.0284 pCi/g 642226002 (RCA-SOIL-19-B) Carbon-14 Result 0.111 < MDA 0.636 > RDL 0.0284 pCi/g 642226003 (RCA-SOIL-15-B) Carbon-14 Result 0.287 < MDA 0.634 > RDL 0.0284 pCi/g 642226004 (RCA-SOIL-10-B) Carbon-14 Result 0.253 < MDA 0.618 > RDL 0.0284 pCi/g 642226005 (RCA-SOIL-04-B) Carbon-14 Result 0.272 < MDA 0.62 > RDL 0.0284 pCi/g
Miscellaneous Information
Additional Comments The matrix spike, 1205554554 (RCA-SOIL-16-BMS), aliquot was reduced to conserve sample volume.
Certification Statement
Page 25 of 30 SDG: 642226 Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
Page 26 of 30 SDG: 642226 Page : ___ I of 2 GEL Laborato ries, L LC Project# 2040 Savage Road 8 GEL Quote# ; Cha rleston, SC 29407 [ij :ti I ~§.£~~~!g~ YRal ~y I Specrti~ d--?--(o COC Numb e r ' 11: Chain of Custodv and Analvtical Reauest Ph one: ( 843) 556 -8 17 1 PO Num ber : GEL Work Order Numb er: GEL Project Ma nage r: Fax: (8 4 3) 766-1178 Client N am e : BHI Ene rgy, Inc. Pho ne # : 339 -44 0- 1043 Sampl e A nalysis Requested <5l (Fill in the num be r o f cont a iner s for e ac h test)
I Fax# Should this <- Pre servative Type (6)
Project/S ite Name : O yster C ree k sample be.e £ A ddr ess: 741 Ro ui e 9, S o u th, For ked Rive r, NJ 0873 1 considered: s ~
,._ ~ "'. e UJ 0 UJ UJ UJ N + Comments ~ 0 N ~
Collected B y: P a u l L e a v itt S end Res u lts To: C hri s M ess ie r c.g: ~ ",-... co + UJ UJ UJ CJ) C")
<D '": ~ co UJ co,-... Note : ext ra sam p le is
~ = li <:'! V CX) - CC! N ~ I'-: ~..
~ ime -.;; e ~ i,-i st' r--: ~ ~ req ui red for s ampl e
- Date Co ll ected Collected ~ ~ :s. ~ - = V N V V,-... 00 ~ N st' N N i,-i C") C") V 0 c'ri Samp le JD.(M ilit ary) QC Field Swi,ple l2 i a. a ".!!. :a ~ 6. :!, u N N "l' CJ) CJ) s p ecili c QC
- For comrxmtes - 111d1cote.iart and stoo dote,t,me Codtn, ( mon-dd-yy) (hbmm) Filtered I.II M mrix <*> ~ :s 0 (.) z 11 lf ~ " E E E '9 <( (J (J z (l_ (l_ I-:l c'Ji a: >,, * - -C. !--
RCA-SOIL-16 -B I 0 /1 212023 10:5 9 N NIA so Yes NIA I X X X X X X X X X X Please co u nt 10 RCA-SOlL-19-B I 1011212023 10:41 N NIA so Yes NIA I X )( X X X X X X X X values give n above
RCA-SO IL-15-B 101 1212023 10 5 8 N NIA so Yes NIA I )( X X )( X X X X X X and lo the left representing
RCA-S OLL-I 0 -B I 10/12/2023 1 1:05 N NIA so Yes NIA I X )( )( X X X X )( )( )( 1%DCGLL LD.
RC A-SO IL-04-B I 10/121202 3 10 :4 8 N NIA so Yes NIA I X )( )( X X )( X X X X I
I
I
C~ain of Custo dy S ignatures TAT Requ ested : No rmal : -- Ru s h : -:x __ S p ecify : (Suhj ecl t o S urch :irgc)
Relinquished By (Signed) Dale.,.. A Ti mb Received by (signed) Da1e Time Fax Results : r ] Yes rx l No
I ~~,/ lo/Jq/:}3 10710 1 J-.L/1, J - /J - /1) - /Cj. _:;i:Z, 1.'t/0 Se lec t Delive ra ble: [XI C of A [ l QC S u mmary [ l level I [ ] Level 2 I I Level 3 [ l Leve l 4 2 ( -I h J,; ll~.,IJ,,. - le ~,~-:)~ 12--v< 2 C' \\.. J I A I ?\\ L, J,,. Addirio 11a/ Remarks:
3 ( 3 ll~ etr1~~ I '-'/ /' 9 3, For Lab Rec ei 11i11g Use Only: Custody Seal Intact? [ ] Yes [ ]No Cooler Temp: oc
> For sa mple sMppi11g am/ delfrery details, see S 4mp/e Receipt & Review form (SRR.) Sample Co /lectio11 Tim e Zo11e ; [ ] Eas tern [ J Pacific ( ] Centra l [ ] Mountai n [ ] Other:
I ) C ham of Custody Number
- Client Dctcnmned 2 ) QC Codes N
- Nonna! Sample. TB
- Trip Blank, FD - Field Duplicaie, Ell
- Equipment Blank. MS
- Matrix Spike Sample. MSD
- Mamx Spike Duplicate Snmplc. G
- Grnb. C - Composite
3 ) field Filtered For liquid matnces. md1C3lC with a - V - for yes 1he sample was field filtered or - N - for sample W3S not field filtered
4 ) M;:Hn x Codes OWc Onnkmg Water, C\\V* Groundwaicr, S '*Surface Water, \\V\\V-Wostc Water. \\V* Water. M L
- M i sc Liquid. SO==Soil. SD =-Sedi mcnt, S1..- Sludye. SS= Soild Waste, 0 1110 11. F'- F1hcr. p;;c\\Vipe. U* Urinc. F'* Fccal, N.aNnsal
5 ) Sample,lnalysis Reques1ed Analytical mc1hod requcSled (1.e 8260B. 60 101l/7HOA) :md number of contamers prondcd for each (1
- 81608 - 3. 60/08 7./70A - I )
- 6) Preservat ive Type HA - H ydrochloric Acid, N I
- N 11ric Ac ct. S I-I
- Sodi um Hydrox ide. SA
- Sulfuric Acid, AA
- Ascorbic Acid, HX
- Hexane.ST
- Sodium T hiosul fatc, lfn o prcserva11 ve is added
- leave field bl an k
7 l K NOW N OR POSS IBL E HAZ A RDS C har acter is ti c Hazard s I Lis ted Waste Ot h er Please provide a11y additio11al details FL = Fla mm a ble/Ign itable LW = List ed W aste OT= O th e r I Un kno w n below regarding lta11dlillg a111Jlor disposal RCRA Me tal s I C O = Corros ive (F. K.P and U-listed wastes.) (i.e.: Higlt/10 111 p l-I. asbestos, bery ffium. irritan ts. other concems. (i.e.: Origin of sample(s), type As= Arsen ic H g= Merc u ry R E = Reactive Wast e code(s): misc. health ha=ards. etc.) of site collected from. odd matrices. ere.)
Ba = B ari u m Se= Seleniu m Des cription:
C d = Cadmi u m Ag= S il ver TSC A R c i:utatcd '
C r = C h rom ium MR= M isc. RCRA melals P C B = Polych lo rinat ed Pb = Lead bip h enyls
I I
Page: 2 of 2 - - -', l GEL Laboratories, LLC
~
Project# ' 2040 Savage Road Lab oratori es LLc GEL Q u o te#: m~1 1 gal com Chem istry I Radiochemistry I Rad1ob1oassay I Spec,alt y AoalyUcs Charl eston, SC 294 07
COC N um ber <1>: Chain of Custodv and Analvtical Reauest Phone: ( 843) 556-8171 PO Numbe r: GEL Work Order Number: GEL Project A1a11ager: Fax: (843) 766-1178 C lient Name : B H I Energy, Inc. Phone# : 339-440- 1043 Sample A nalysis Requested <5> (Fill in the number of con tainers for each test)
Project/Site Name : Oyster Creek I Fax# Sh ould this <- Preser vative Type (6)
Address: 741 Route 9, South, Forked Ri ver, NJ 08f 31 sample be.:
con sidered: c w N w Collected By: Paul Leavitt Send R esults To: Chr i s Messie r a2:- ~ UJ ~ + 0 Comments
Q, lo] 0 ex:> co +
Note: extra sample i s
- Tim e ~.s,0 N.,; l{') N CJ i-; ~ ~ UJ required fo r sample
~ ! :s ~ 6i 0 0 ~ - II)
'Date Collected Collected.i 0..a_ 0 ~.Q -;; N l{') <"i N C (") ti'i "<I' (Militn ry) QC Field Sample C :,: *:;; ::, (l) ::, specific QC
- For comnosites ~,~fil~, a~nd stop daiJ/ime (mm-dd-yy) (hhmm ) Code"' Filteredm Matrix<-'> ;::-a ci +/-. ~ t ~
a:: >, * - ~ C. f-a.. LL a..
RCA-SO IL-I6 -B I 1011212023 10:59 N NIA so Yes NIA I X X X X Please count l o
I RCA - SOlL-I9 -B ]011212023 10:4 1 N NIA so Yes NIA J X X X X val ues g i ven above
RCA-SO IL-I 5-B I 01 1212023 10:58 N NIA so Yes NIA I X X X X and t o the left represen ti ng
I RCA-SOIL-I0-B 10/1212023 11 :05 N NIA so Yes NIA I X X X X 1% DCGL LLD.
RCA-SO I L-04 - B 10 /12 12023 10:48 N NIA so Yes NIA I X X X X
I I
I
I C~ai n of Custody Signatures TAT Requ es ted: N ormal: Rush : X Specify : ( Su bj cl*t to S urchar ge)
Re linquished By (Si gned) Date T i me Recei ved by I.1. (si1aied) Date Time Fax Resul ts: [ l Yes [X] No I. ~~ I0/1'1/) 3 10710 I ~ju, M j} Ju - 1q - :25 11/6 Sel ect Deli verable : [X 1 C of A [ 1 QC Summary [ ] level I f l Level 2 f ] Level 3 r 1 L evel 4
-+h1u ;_:, ~~ J/) -Jej_ ;:i~ /Z'I<.. --. \\.t.o-1 2 ~ *-........._,...- - \\, n~.hM~ JfJ)o/25, Additiona l Remarks:
3 3 For '( I '-1~~ Lub Receiving Use Only: C ustody Seal Intact ? [ ] Yes [ ]No Cooler Temp: oc
l
> For sampl e shippin g and delivery details, see Samp l e R eceipt & R eview fo rm (SRR.) Sample Col/ectio11 Time Zo11e : [ ] Eastern [ ] Pacific [ J Cent ral [ J Mountain [ J Othe r :
I ) Cha in o f Custo dy Number= Cl ie nt Determined J
2 ) QC Codes: N = Nom,al Sample, TB = Tnp Blank. FD
- Fi Id Duplicate. EB = Equipmen1 Blank. M S= Matrix Spike Sample, M SD = Matrix Spike Dupl icate Sample, G = Grab, C = Composite
3 ) Fie ld Filte red, For liquid matrices, ind icate with a - Y - for J s 1hc sample was field filte red or - N - for sample was not field fi ltered.
- 4. ) Ma1nx Codes. D\\V= Drmkmg Water. G\\V =Gro undwat er. S \\: ll=Surface Water. \\ VW =Waste Water, \\ \\'= Water. ML= M isc Liquid. SO=Soil, SD=Sediment. S L,.Sl udge. SS=Solid Wast e. O =Oil, F= Filter, P=Wipe. U""'Urin e. F= Fecal, N=N asal
- 5) Sample Analysis Requested: Analytical method requested (i.~. 82608. 60 I0B/7470A) and number of containers provided for each (i.e. 8 1 60B
- 3, 60/0B 74 70A - I)
- 6) Preservative Type : HA = Hydrochl o nc Ac id. N I = Nitric Acib, S H = Sodiu m Hydroxide, SA = Sul furic Acid. AA = Ascorbic Acid. HX = Hexa ne. S T =- Sodium T hiosulfate, Ifno preservative is added = leave field blank 7.) KNOWN OR POSSIBLE HAZARDS C harac teris tic Hazards I Lis ted Wa s te I I Other I Pleas e provide auy addition a l deta ils FL= F lamm able/Ignitab l e LW= Listed W aste OT= Other I Unknown b elow regardi ng J,a11d li11g a 11dlor disposa l R C RA Metals I C O = Corrosive (F. K, P and U-listed wast es.) (i.e.: High/lo w pH. asbes tos, be1ylli11m, irritants, other co ncems. (i.e.: Origin ofsample(s), type As= Arsenic H g= Mercu ry RE = Reactive Waste code(s): misc. heollh ha=ards, etc.) of site collec tedfi-0111, odd ma/rices. etc.)
Ba = Barium Se= Selenium D escriptio11:
C d =Cadmium Ag= Silver TSCA Re!!ulatcd C r = Chromi um M R= Misc. RCRA metals P C B = Polych l orinated Pb = Lead biphenyl s I
lml!I J Laboratories LLC
Client:
Date Received: 0 Circle Applkoble:
FedEx Ground UPS Field Services Courier Other
Carrier and Tracking Number
Suspected Hamrd Information ;! l *If Net Counts> IOOcpm on s11mp]es not marked "radioactive", contact lhe Radiation Safety Group for further investigntion.
Haz.ard Class Shipped: UN#:
A)Shl ed as a DOT Hazardous? IfUN2910, Is the Radioactive Shipment Survey Compliant? YeL-No_
B) Did the client designate the: samples are to be received as radioactive?
C) Did the RSO dassify lhe sam~es 11&
radioactive?
D) Old the client desi ate sam Jes are haznnlous?
E) Did the RSO identif ossible hazards? RCRA Asbestos Beryllhun Other:
Snmple Receipt C:ritedn CmnmenWQunliOcl's (Required for Non-Conforming Items)
Shipping containers received intact and Cil'cle Applicnblc: Senls broken Damaged comainer Leaking container Olhcl' (desci*ibc) sooled?
Circle Applicable: Clicm contacted am! pl'Ovidcd COC COC created upon receipt 2 Chain of custody documents included with shipment?
Preservation Method: Wet lee Ice Packs Dry ice on Olher:
3 Samples requiring cold preservation *all temperatures are recorded in Celsius TEMP:;~--"'---
within (0 < 6 de. C)?*
Temperature Device Scrla1 #:cl0R,c*'e'~----
4 Daily check pe1formed and passed on IR temperature gun? Scco11daryTempemturc Device Serial# (If Applicable):
Circle Applicable: Seals broken Damaged confllincr Leaking container Other (descl'ilie) 5 Sample containers intact and sealed?
Samples requiring chemical preservation Sample 10'3 and Container.< Affected:
6 at proper pH?
If Prcsciw!lon added, Lotil:
fYes, are Encores or Soil Kits present for solids? Yes_ No_ NA __ (Ifyes, take to VOA Freezer)
Do liquid VOA vials conlai11 acid presc1vation? Yes_ No_ NA_(Ifunknown, select No) 7 Do any samples require Volatile Analysis? Arc liquid VOA vials f1ee ofheadspoce? Yes_ No_ NA __
8 Samples received within holding time? ID's and tests affected:
Sample ID's on COC match ID's on !D's and containers affected:
9 bottles?
Circle Applicable: No dates on containers No limes on conlainern COC missing info Other (describe)
Circle Applicable: No container count on COC Other (describe)
12 Arc sample containers identifiable as GEL rovided b use ofGELlabels? L 13 COC form is properly signed in
__________ -~ rclinquishe.d/n::ceived.scctions'1-----. -
Comments (Use Continuation Forni if needed):
Gl-CHL-SA-001 Rev 7
Page 29 of 30 SDG: 642226 List of current GEL Certifications as of 09 November 2023 State Certification Alabama 42200 Alaska 17-018 Alaska Drinking Water SC00012 Arkansas 88-00651 CLIA 42D0904046 California 2940 Colorado SC00012 Connecticut PH-0169 DoD ELAP/ ISO17025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-15-00283, P330-15-00253 Georgia SC00012 Georgia SDWA 967 Hawaii SC00012 Idaho SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky SDWA KY90129 Kentucky Wastewater KY90129 Louisiana Drinking Water LA024 Louisiana NELAP 03046 (AI33904)
Maine 2023019 Maryland 270 Massachusetts M-SC012 Massachusetts PFAS Approv Letter Michigan 9976 Mississippi SC00012 Nebraska NE-OS-26-13 Nevada SC000122024-04 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R-158 Oklahoma 2023-152 Pennsylvania NELAP 68-00485 Puerto Rico SC00012 S. Carolina Radiochem 10120002 Sanitation Districts of L 9255651 South Carolina Chemistry 10120001 Tennessee TN 02934 Texas NELAP T104704235-23-21 Utah NELAP SC000122023-38 Vermont VT87156 Virginia NELAP 460202 Washington C780
Page 30 of 30 SDG: 642226