ML18331A027

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Enclosure 4 - Letter from Haley Aldrich to Wisconsin Department of Natural Resources Proposed Long Term Sampling of Supply Wells 3, 5, and 7
ML18331A027
Person / Time
Site: La Crosse  File:Dairyland Power Cooperative icon.png
Issue date: 11/06/2018
From: Glucksberg N
Haley & Aldrich
To: Zeichert T
Office of Nuclear Material Safety and Safeguards, State of WI, Dept of Natural Resources
References
File No. 128924, LC-2018-0075
Download: ML18331A027 (32)
v • d • e


Text

{{#Wiki_filter:www.haleyaldrich.com 6 November 2018 File No. 128924 Mr. Tim Zeichert Hydrogeologist Remediation & Redevelopment Program Wisconsin Department of Natural Resources 101 Webster Street P.O. Box 7921 Madison, WI 53707 -7921

Subject:

Proposed Long Term Sampling of Supply Wells 3, 5, and 7 LaCrosse Boiling Water Reactor, Genoa , Wisconsin WDNR BRRTS Activity #02 581112 DNR FID# 663020930

Dear Mr. Zeichert:

LaCros seSolutions, LLC, is in the final stages of safely completing the Decontamination & Decommissioning (D&D) of the LaCros se Boiling Water Reactor (LACBWR) Site located on at S4601 on State Highway 35 in Genoa, Wisconsin. As you are aware, during the dismantlement of the reactor building, the ventilation system released tritium to the ground surface directly outside of the south east side of the structure and impacted ice/snow. The impacted ice/snow was then inadvertently transported via storm water to the former Reactor Plant/Generator Plant Area (RGPGA) sump. Once identified, the ventilation system was modified and condensate/ice/snow melt/surface water collected to prevent future releases. Once in the RPGPA sump, the tritium was then detected in the downgradient monitoring well MW -203A and eventually at MW -202A. Upon discovery of the tritium in groundwater, the site notified DNR on 14 March 2018

1. In response, DNR issued the requirement 2 for LaCrosseSolutions to complete an additional site investigation under Section 292.11 of the Wisconsin Statutes. The proposed site investigation included completing a groundwater model to better evaluate the potential fate and transport of this release as well as a dye tracer study, to both confirm the release mechanism and source of tritium to groundwater as well as calibrate the groundwater model.

1 14 March 2018 Notification from Joe Nowak of La Crosse Solutions to Wisconsin Department of Natural Resources, Form 4400 -225, Notification For Hazardous Substance Discharge (Non -Emergency Only). 2 30 March 2018 Letter from Tim Zeichert of the State of Wisconsin Department of Natural Resources to Mr. Joseph Nowak of La Crosse Solutions,

Subject:

Reported Contamination at La Crosse Boiling Water Reactor Facility, 4601 S tate Highway 35, Genoa, WI. HALEY & ALDRICH, INC . 75 Washington Avenue Suite 1A Portland, ME 04101 207.482.4600

Wisconsin Department of Natural Resources 6 November 2018 Page 2 Approval to introduce Rhodamine WT (RWT) was issued by DNR on 28 June 2018 3 and the dye was then introduced 12 July 2018. As part of the dye introduction activities, 1 pound of RWT was poured into the former RPGPA sump area followed by the addition of approximately 230 gallons of unchlorinated water. The groundwater monitoring wells, river and supply wells were then monitored weekly for five weeks, and then on a monthly schedule. The laboratory data is summarized on Table 1 and the laboratory data is provided in Attachment A. It should be noted that RWT has only been detected at monitoring well MW-203A; no dye has been detected in the deeper wells or in the supply wells; and no detections are anticipated. Per Item 13 or your approval letter (dated 28 June 2018), we understand that DNR will require monthly samples to be collected until such time that the trailing edge of the RWT plume has migrated past the most downgradient supply well (i.e. #5 or WUWN: AK187). Based on the data collected to date, we believe that the leading edge of the dye has migrated past supply well #5 (AK187) as have the peak concentration

s. The remaining trailing edge will likely continue for some time, as the sump area is still visibly colored from the RWT introduction.

We have collected the data required to calibrate the groundwater model and are now requesting your approval for proposed long term groundwater monitoring of the supply wells.

Item #13 of your letter also indicates that supply wells #3 (AK168), #5 (AK187) and #7 (WQ177) must be sampled during the study and that DNR will provide written approval for terminating the sampling effort. Based on the data collected to date, we recommend collecting monthly samples through December 2018 from supply wells 

#3 (AK168), #5 (AK187), and #7 (WQ177). If RWT is not detected as anticipated through December 2018, that will mark six consecutive monthly samples as required under Item 13. If any RWT is detected in these rounds from the supply wells, we will extend the sampling until we have six months of non

-detect results. We have already collected the data needed to assess the tritium detected in groundwater, and the tritium levels have decreased to below the drinking water Maximum Contamination Levels (MCLs) in all monitoring wells. Furthermore, tritium has never been detected in any of the supply wells onsite or any of the monitoring wells in the deeper aquifer. Therefore, we are also confident that the RWT will not be detected in these supply wells. However, we also understand the need for documentation and to provide this data via our communication plan to Dairy land Power. Please note that we will also continue to provide bottled water to Dairy land Power until we receive written notice from your department that the Dye Study may be terminated.

3 28 June 2018 Letter from Tim Zeichert of the State of Wisconsin Department of Natural Resources to Mr. Joseph Nowak of La Crosse Solutions,

Subject:

Infiltration/Injection Temporary Exemption Request for La Crosse Boiling Water Reactor Facility, S4651 STH 35, Genoa, WI.

Wisconsin Department of Natural Resources 6 November 2018 Page 3 We are respectfully requesting your approval for this proposed groundwater sampling plan for supply wells #3 (AK168), #5 (AK187), and #7 (WQ177). If you would like to discuss any aspect of this project, please feel free to call Gerard van Noordennen at 860-462-9707. Sincerely yours, HALEY & ALDRICH, INC.

Nadia S. Glucksberg, PG Senior Associate l Hydrogeologist

CC: Joseph Nowak, EnergySolutions Kim Martinson, LaCrosseSolutions (electronic copy) Bob Busch, Wisconsin Department of Public Health (electronic copy) Rhex Edwards, Nuclear Regulatory Commission, Region III (electronic copy)

Marlayna Vaaler, Nuclear Regulatory Commission, Headquarters (electronic copy)

Page1of1 TABLE1

SUMMARY

OFDYERESULTS LACROSSEBOILINGWATERREACTOR(LACBWR)GENOA,WISCONSIN StationNumber DatePlaced03/08/1807/12/1807/19/1807/26/1808/02/1808/09/1808/16/18 09/11/1809/12/1803/08/1807/12/1807/19/1807/26/1808/02/1808/09/1808/16/18 09/11/1809/12/18 DateCollected03/16/187/10/201807/19/1807/26/1808/02/1808/09/1808/16/18 09/10/1809/12/18 10/09/1810/10/1803/16/187/10/201807/19/1807/26/1808/02/1808/09/1808/16/18 09/10/1809/12/18 10/09/1810/10/18201 A202 B202 AR203 A54.452984.112.35439407.7775.5712.011.7620.8832.41203 B204 B204 AWell 5*Well 7*Well 3*RiverNotes:1poundofRWTwasintroducedon07/12/2018andflushedwithapproximately230gallonsofnon chlorinatedwaterppb/daycalculatedbydividingtheconcentrationdetectedbythelabinppbbythenumberofdaysthepacketwassubmerged*Watersamplessubmitted.Sampleswerecollectedconcurrentlywithsamplepackets.ppb:indicatespartsperbillion RhodamineWTConcentration(ppb)RhodamineWTConcentration(ppb/day)"":indicatesnon detect"":indicatesnotsampled Haley&Aldrich Z:\128924LACBWR\Deliverables\DyeStudy\TerminationLetter\Table1SummaryofDyeResults.xlsx October2018 A Dye Laboratory Da ta Ozark UNDERGROUND LABORATORY 1572 A l ey Lan e* Protem, MO 65733 * (4 17) 7 85-4 289

  • fax (417) 785-4290
  • contact@ozarktmdergrounclJab

.com Certificate of Analysis Date of certificate: March 2 0 , 2 0 1 8 Client: Ha l ey & A l d r ich I 00 Co r porate P l ace, Suite 1 05 Rocky H ill , CT 06067 Project name/l ocat i o n: LACBWR , Genoa, WI Cl i ent project#: 1 28924-004 Contact pe r son: Mile s van Noo r denn e n (mvannoo r dennen@ha l eya l drich.c om) Samples collected by: M. van Noordennan Date samples sh i pped: March 1 6, 2018 Date samp l es rec'd at OUL: Ma r ch 1 9, 2018 Date ana l yzed by OUL: Mar c h 20, 2 018 Incl u ded with certificate of analysis! Tab l e of resu l ts and copy of sa mpl e co l lectio n data s h ee t Results for backg.-o u nd charcoa l samp l ers ana l yzed for the presence of tl u orescein , eosine, rhodam i ne WT (RWT) and su l fo r hodamine B (SRB) dyes. p k ea wave e ngt 1s are r eporte ( ) d in nanomete r s n m ; 1ye concentrat i ons a r e reporte d' 111 part s per b'II' ( b) I 1011 .PP OUL Stat i on Number Date/Time Date/Time Fluorescei n Results Eosine Results RWT Resu l ts SRB Results Number P l aced Collected Peak (nm) Cone. (ppb) Peak (nm) Cone. (nob) Peak (nm) Cone. (ppb) Peak (nm) Cone. (ppb) C9 1 IO MW-20 28 3/8/18 1 1 51 3/1 6/18 0755 ND ND ND ND C9 1 I I MW-2 0 3A 3/8/1811 37 3/16/18 0745 516.4 0.964 ND ND ND C9 11 2 MW-20 3 8 3/8/1 8 11 42 3/16/1 8 0740 ND ND ND ND Note: D ye concentrations are bas e d upon standards u se d at the OUL. The sta ndard co n centrations a r e ba sed u pon the as so l d we i ght of the dy e t h at the OUL use s. l ft h e c li ent is not u si ng OUL dyes , the c li ent shou l d provide t h e OUL with a sa mp l e of the dy e to compa r e to t he OUL dyes. Footnotes: ND= No dye dete c t ed Thomas J. A l ey, PHG and RG F:\doc s\COA \Ha l ey A l drich\Haley A l dric h_ LA CB WR_ 0 I I of I OZARK UNDERGROUND LABORATORY, INC. 1572 Aley Lane Protem, MO 65733 (417) 785-4289 fnx (417) 785-4290 emn il: co11tnct@oz11rkun d ergrou n dlab.com SAMPLE COLLECTION DATA SHEET for FLUORESCENCE ANALYSIS Project (_,q Gt)v.J{L . Week No: 6k..5d Samples Collected By: M. y.:;oNc>oden/\Q,(\ Samples Shipped By: M. YBot\JoaaknYVo. Samples Received By: }Q..LL Date Samples Shipped: 3

  • lb-I'&' Date Samples Received:

,2 \ \ q J18' Time Samples Received: \;l$O 1 Return Cooler? Ye~ No D Bill to: Ha.I 9-l Send Resu l ts to: ~-..1..*(\11......:....;.' ..,._V4;;:;,,o........_ /\ .... L .... a ..... a.ud...:e::..:n:.u&~'.".\...,__ ________ ~----Analyze for: Rhoda mine WT D Other Ship coo ler to:

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N N "-(<()(,/,_1 t-1: 11 OUL Please indicate stations where d',!.e was visible in the {leld OUL use 011/y for field technician use -use black ink on l v u se only #CHA R LAD STAT I ON STATlON NAME l'LACED COLLECTED u REC'D N U M B ER NUMBER WATER QhQ.~a.1 DATE TIME DATE TIME llEC'D . I c_q l lO rn IA.) *-o.l R J. a-, I d' I J S) ~-/&*18 0)5$' 0 I r.~\I I MW* J-o 1/.\ s .£-*,$-// 3) 3 *16*1~ (1) '-I~' () I e,q \1 2. (V)~\ -Jo<-~ 3 * , 8' J)'./2 3*/£-/'l t))</0 0 . COMMENTS --;){\-rt) --r-J-J~-k. ,v , . vv Th i s sheet fil l ed out by OUL staff? Yes_ NoL OULProjectNo .1 11'::l: DateAnalyzed: o ji.011& Charts for samples on this page proofed by OUL: _____ .._ __________ _ Ana l yzed By: USo.. G.i \(Y-e,o.St_ Certificate of Analysis Date of certificate: July 1 3, 20 18 Client: H a l ey & Aldrich l 00 Corporate P l ace, S u i t e I 05 Rocky Hill , CT 06067 Project name/location: LACBWR, Genoa, Wl Client project#: 1289 24-0 04 Contact person: Miles van Noordennen (mvannoordennen @h a l eya l drich.com) Samples collected by: M. van Noordennan Date samples shipped: Ju l y 11 , 2 018 Date samples rec'd at OUL: Ju l y 1 2, 20 18 Date analyzed by OUL: Ju l y 13 , 2 0 1 8 Included with certificate of analysis: Tab l e of re s u l ts and co py of sam pl e co ll ec tion dat a s h ee t Results for week O water samples analyzed for the presence of rhodamine WT (RWT) dye. Peak wavelengths are reported in nanom e t ers (nm)* dye concentrations are reported in parts per b i lli o n (ppb). ' OUL Station Number Dateffime RWT Results Number Collected Peak (nm) Cone. (ppb) D0943 We ll-3-071018 7/10/1 8 1 345 ND D0944 W e ll-5-071018 7/10/18 1 235 ND D0945 Well-7-07 1 0 1 8 7/1 0/18 1255 ND Note: Dye concentrations are b ased upon s tand a r ds u sed at the OUL. The s tand a rd concentrations are based upon the as so l d weight of t h e dye that the OUL u ses. If th e c li ent i s not u s in g OUL dy es, th e c l i e nt s hould provide the OUL w i th a sa mp l e of the dye to compare to the OUL d yes. Footnotes: ND= No dy e detected Thomas J. Aley, PHG and RG F:\docs\COA \Hal e y A l dr i c h\Hal ey Aldrich_ LACS WR_ 02 I of l OZARK UNDERGROUND LABORATORY, INC. 1572 Aley Lane Protem, MO 65733 (417) 785-4289 fax (417) 785-4290 email: contact@ozarkundergroundlab .com SAMPLE COLLECTION DATA SHEET for FLUORESCENCE ANALYSIS Project L Ac \S L, J .a_ &w Week No: 0 Samples Collected By: M , v C.r-. r0 dook n rt.h Samples Shipped By: fYt, vc.r-.. oo kn~ 0. Samples Received By: __.~~:;,-/-=ou:..='--=--

Date Samples Shipped: )

  • I I * / '¥ Date Samples Received:

1' 1'2.-'2.Dl8' Time Samples Received: I 500 Bill to: N~I~+ Aldc~ Send Results to: M-,Jc,-.. rJdC.>aJe11y\.D,'r\ Analyze for: D Fluorescein D Eosine ~hodamine WT D Other Ship cooler to: {Y). Vea {Vl!"oJe./l"lf..u-.. -Return Cooler? Yes~ NoO Geno" l.,J-;._ l o c.A.J..,~ OUL Please indicate stations where dye was visible in the field OUL u s e only for field technician use -use black ink only use onl y #CHAR LAB STATION STATION NAME PLACED C OLL E CTED # REC'D N UMBER NUMBER WA T ER DATE TIME DATE TIME R EC'D 0 DOC\4~ We,\\-1::.

  • o)/Di~* --),)D*\? I si./ S' l 0 ~Y4 W.V.,l,~ -OJID/8' --).)[)*)? ,:xss I 0 1Xft~ W-vJ., ") -cf) 16 I~ --), JD*)? JJS<; I COMMENTS----------------------------------------------

This sheet filled out by OUL staff? Yes_~o Charts for samples on this page proofed by OUL: L0, _ OUL Project No. l t-\4 Date Analyzed: ~ot~ Analyzed By: K,e)ouk ~~+-, ~""----------Page/ of~/ (Jl)L, Certificate of Analysis Date of certificate: J u l y 25, 2 0 1 8 C lient: H a l ey & A l dri c h I 00 Corporate P l ace, Suite I 05 R oc ky Hi ll , CT 06067 Project name/location: LACBWR, Genoa, WT Client project#: 1 28924-004 Contact peop l e: Mi l es van Noorde nn e n (mvannoord e nn e n@h a l eya l drich.com) Samples collected by: S. Kaney Date samples shipped: Ju l y 1 9, 20 l 8 Date sampl es rec'd at O U L: Ju l y 2 0 , 2 018 Date analyzed by OUL: July 24, 20 1 8 Included with c e rtificate of ana l ysis: Tab l e of re s u l t s a nd co pi es of s a m p l e c o ll ec t i on d a t a sheet Na d i a G lu cksberg (N g l u c k s b e r g.haleyaldr i c h.c om) Res u lts for charcoal and water samples analyzed for the presence of rhodamine W T (RWT) dye. P eak wavel e ngt h s are reported i n n a nom e ter s (n m); dye co nc e ntrati o n s are reported in pa rts p e r bi lli o n (ppb). A ll r esu l t s are for c harcoa l u nl ess otherwise ind i cated. OUL Station Date/Time Date/Time RWT Results Number Number P l aced Collected Peak (nm) Cone. (ppb) DI07 3 202-AR 7/1 2/18 l 1 37 7/1 9/18 1 055 ND D l 074 2 02-8 7/1 2/1 8 1 204 7/1 9/18 1 045 N D D I 075 2 0 1-A 7/1 2/1 8 1 2 1 5 7/19/1 8 1 0 33 ND D I 076 203-A 7/12/18 1 227 7/1 9/1 8 11 07 ND D1077 2 03-8 7/1 2/1 8 1 244 7/19/18 11 16 ND D I 078 204-8 7/1 2/1 8 130 1 7/19/1 8 1 1 3 0 ND D 1 079 204-A 7/1 2/1 8 1 3 08 7/l 9/l8 1140 ND D l 080 L a bo r a t ory contro l charcoa l b l a n k D I 08 1 Riv e r 7/ 12/1 8 1 337 7/1 9/1 8 1 0 1 4 ND D l 08 2 W e ll-3 Water 7/1 9/1 8 1 2 48 ND D I 08 3 We ll-5 Water 7/1 9/l8 1 400 ND D I 084 We ll-7 Water 7/19/18 1 4 1 0 ND Note: Dye concen t rat i ons are ba se d upon s ta n dard s u se d at t h e OUL. T h e standard concentrat i o n s a r e b ase d upon th e as so l d we i g ht of th e dy e t h at t h e OUL u ses. lfthe c lient i s n ot u si n g OUL d yes, t h e c li e n t s h o ul d provide t he OUL w i th a sa mp l e of t h e dy e t o compare to the OUL dye s. Footnotes: ND= No dy e d e t ec t e d Thomas J. Aley, PHG and RG F:\docs\COA\ Ha l eyA l drich\H a l ey A l dr i c h_LA CB WR_0 3 I of I OZARK UNDERGROUND LABORATORY , INC. 1572 Aley Lane Protem, MO 65733 (417) 785-4289 ra,. (417) 785-4290 emai l: contact@ozarkundergroundl a b.com SAMPLE COLLECTION DATA SHEET for FLUORESCENCE ANALYSIS Project ( Pr(,,6vJ '2-' 6 W Week No: Samples Collected By: ..;;: S::;..;..:;. 1;;::: 4>,....,..~-"""":a;i,...----------- -Samples Shipped By: ~-i£,, Samples Received By: {J.fk~ I ouu ........ D Date Samples Shipped: 1/ 1zj1;J ~ate Samples Received: 1-;}.-(), -1"8' T im e Samples R;;v1d: I i..o u Return Cooler? Yes D No(Sl:'_ Bill to: r\ni:e1:qS.A:1dckb _ Send Results to: rov4.nooo<'d..:?>::lo:£.:n@bal:t"(B 14:ric..k

  • l Cfo Rhodamine WT O Other Ship coo ler to: -----------------

OUL Please indicate stations where d'f.e was visible in the fl.eld use only #CHAR LAB STATION REC'D NUMBER c:.roxc.ocv\ NUMBE R 1 1)\0l-3 Joa-A{l.. I D1014 J{);)., s l l'b10 15 J-OI-Ai I (:)\O~ .0.0'6-,:\ l 1)\011-~~3-B \ t)l(Jti Jo£.1-.t3 l Dlol'l .'.2cy-A I T)\~l iZi J-(,(" 0 \Nt'.11 3 0 1 , ue 11-c:; D IWT'll-7 COMMENTS nto~o ()UL.-Q,'t\a.vrg.,..\ }?lo..(\~ This sheet filled out by OUL staff? Yes_ N~ OUL Project No. l'l f L{ Date Analyzed: i 2. J ' for field te chnic.ian use -use black ink only STATION NAME PLACED DATE TIME 7/, a./1? i137 _ -7' ld/11 J~O"I 7/,a.!18 Id. l J ' 7/ ,J. /t'a I JJ"'J 7/1.i/if 1.;2 YY 7/ui )1'8 , ac.:i , . 7}1~)1<1 l~og-1 7/1.:i ,,~ /3.3 t 7/i~J ,i 13.4"8 ,) '° Js 1400 *. ""?ft'1} I~ lulu Charts for samp::St~age proofed by OUL: A.q!l ly zcd By:__, M..:..u£:=t-- -'~ ...... =-.-------. ' Page/ of / t) I.kt.-OUL use only COLLECTED fl WATER DATE TIME REC'D 7 /,c, )1'8 10,S'"S-b -i},c,J,:r / OY S"' 0 1l1'l Ii~ Jt:,~3 0 7 Jiq I i'iS' /1 c, 0 'J,q J,s 1 11"1 0 t1 J 1q It i 1131::> a 1"'7/ ,q I, i' 1 i 4D 0 -,Jiq Ii~ {011...l D --I --' -\ - OZARK UNDERGROUND LABORATORY, INC. 1 572 Aley Lan~ Pro t em, MO 65733 {417) 78S-4289 fe>. {417) 78S-4290 email: con tact@ozarkundergroundleb.com SAMPLE COLLECTION DATA SHEET for FLUORESCENCE ANALYSIS Project L 8;c,.6v,[

a. -6 W Week No: Samples Collected By: ...;::: 5=*=JL.o.==h:,,,/l"""":A;t----

Samples Shipped By: S.. Samples Received By: ~~-~.-...1.D.fk.:::::sil!l:t::;;.....(..:: 6lM..:-==::.: D;__ ____________ _ Date Samples Shipped: 7/ J9}a§ Date Samples Received: 1-.;2..C -f 'g' Time Samples R;;;:,1d: / l-u" Return Cooler? Yes O No C5l::. Bill to: J*ln £:e,q M:1 d deb . Send Results to: rov 4'..t::>O OP(d , v,o:e.n@)oq 1-c,,,. A 14::ri c,,h, ., !rmr ~Rhodamine WT O Other Ship cooler to: ----------------- OUL Please indicate stations where dr,e was visible in the fl.eld OUL ast only for field technic}an use -use black ink only use only #CHAR LAB ST A TION STATION NAME PLACED COLLECTED

  1. REC'D I~ NUMBER WATER DATE TIME DATE T IME REC'D l aot1-A~ 7/,a./1"8' 113 7 _ 7/re,},! I OS-S-() I J<).;2 -6 7/ ,~/1&' 1~01.j ..,},'} kl /OY~ 0 ' J.OI-Ai 7/,~/,g ,a ,s-7Jiq ,,~ lt:>33 0 I ,9.01>-I\ , 7/ ,.2 /1-a r:2.1-, 7J,ql14K /1 0, 0 I c:}c.3 -B 7/Ja/ii i o'l'iY 7 /,q/,s 111 0 ~1-.6 7/1;,/1"8 13<::i, i7J l'l Iii 11 :'le (J l .'.lcy-A . 7)1~}148 *):SO%' 17J,q l,f I I YD 0 I a. jJ'(,< *. 71,:i I,~ /?...3, "'h'il1~ /01~ 0 0 T)l('\l'( 2.. :wrn 3 7/,qj.'fs I ;3.y'g -....., I () T\l()S(~ ,lcJ~\1-~

7/ 1DJI rs 11~ro --' 0 ntoit.\-W-e/1-7 *. --:,h~ltt I< II C) -\ -COMMENTS--------------------....;--------------------------This sheet filled out by OUL staff? Yes No~ / OUL Project No. Ii ,'( Date Analyzed: '/, ~rJ t Charts for s~c page proofed by OUL: AQ~lyzed By: Mte M . . -c.........:...,.. Page/ of/ t)/.U._.. Certificate of Analysis Date of certificate: Aug u st 2, 2 018 Client: Haley & A l drich 100 Co rporat e P l ace, S uit e 105 Rocky H ill , CT 06067 Project name/location: LACBWR, Ge n oa, Wl Client project#: 1 28924-004 Contact people: M il es va n Noordennen (mva nn oo r dennen@h a l eya ldri ch.com) Samples collected by: S. Kaney Date samples sh i pped: Jul y 26, 2 018 Date samp l es rec'd at OUL: July 27, 20 1 8 Date ana l yz ed by OU L: Augu s t 2, 2018 Included w i th certificate of ana l ysis: Tab l e of resu lt s , co pi es of sample co ll ect i on da t a s h eet and di screpa ncy sheet Na dia G lu c k s berg (Ng l ucksberg.ha l eya ldr ic h.com) Results for charcoal and water samp l es analyzed for t h e presence of rbodamine WT (RWT) dye. Peak wave l en g t h s a r e reported in n a n omete r s (nm); dye concentrat i o n s a r e reported in part s p er b illi on (ppb). A ll re s ul ts are for c h a r coa l u n l ess ot h e r w i se i ndicated. OUL Station Date/Time Date/Time RWT Resu lt s Number Number Placed Collected Peak (nm) Cone. (ppb) D 1 2 1 3 River 7/1 9/18 10 2 0 7/26/1 8 0950 ND 01 2 1 4 2 01-A 7/1 9/1 8 1 041 7/26/1 8 101 5 ND D1215 202-B 7/1 9/1 8 10 53 7/26/1 8 10 24 ND 012 1 6 202-AR 7/1 9/1 8 I 10 2 7/2 6/18 1 032 ND 01217 203-A 7/19/1811 1 4 7/26/18 I 048 568.6 54.4 01218 203-B 7/1 9/1 8 11 24 7/26/1 8 1058 ND 0 1 219 204-B 7/1 9/1 8 11 36 7/26/1 8 111 0 ND 01220 Laboratory contro l c h arcoa l b l ank 012 2 1 2 04-A 7/1 9/1 8 11 45 7/2 6/181118 ND 01222 Well-3 Water 7/2 6/1 8 11 55 ND 0 1 223 Well-5 Water 7/26/1 8 1 2 1 5 ND 0 1 224 Well-7 Water 7/26/1 8 1 226 ND Note: Dye conce nt rat i o n s are based u po n s tandard s u se d at the OUL. The sta ndard conce nt ra ti ons are ba se d u pon th e as so l d we i ght of the dye t hat the OUL u ses. I f th e cl i e nt is not u si ng OUL dye s, t h e c li ent s h ou ld provide t h e OUL w ith a sa mple of th e dye to com p a r e t o t h e OUL dyes. Footnotes: ND= No dy e detected Thomas J. Aley, PHG and RC F:\do cs\C OA \Ha l ey A ld ric h\Hal ey Ald ri c h_ LACB WR_ 04 I of I OZARK UNDERGROUND LABORATORY, INC. 1572 Aley Lane Protem, MO 65733 (417) 785-4289 fax (417) 785-4290 email: contact@ozarkundergroundlab.com SAMPLE COLLECTION DATA SHEET for FLUORESCENCE ANALYSIS Project LA L{:)w62.

  • 6 l.}.J WeekNo: -=----Samples Shipped By: 3' -1~ Samples Received By: __,, ... <......._*

.........,, a-ry=="'f-7 .... , ... c , .... u ... ,__.~-------------,. Date Samples Shipped: 1}:i!okiJ Date Samples Received: 7-;2.'1-/ 8 Time Samples Received: /3 SO Return Cooler? Yes D No :..i Bill to: \.b1JZ..,..t~ A:1 <:k-i d.._ Send Results to: TV\v a..,b O O iv J_p n 0-RK' Q la lft4 c,. I d,.,,* G: h. , cer,.,.. D Eosine ~Rhodamine Wf O Other Ship cooler to: ------------------ OUL Please indicate stations where dve was visible in. the field OUL USI! only for field technician use -use black ink only use only #CHAR LAB STATION STATION NAME PLACED COLLECTED

  1. REC'D NUMBER NUMBER WATER c,,!* ---I DATE TIME DATE TIME REC'D \ 1111.l~ Q,vU'. ?}JCIJ*l Jcae> 7/JID)t'i, 9S-c 0 I D\'Ll't .;201-P, , } I Cf Jt~ /OL.f1 7Ja1olt'if 101'5' 0 l t').l?t< dDa-6 7J,q hi' *~~3 7}~"'"~ to..2.'-1 0 -I b\1 \LD Jb~-A~ ,J,<;).~ IIOd. 7/;;lw Ii~ I~ 3.;> 0 \ 11)\'2. l1-Jo~-*A 17J,~ 1,~ I \\ '-i 7J;;1t..l 1'is jc 'i'is o* \ t)l'2.JCS' J.o'3-:-.8 7 l,.,,118' II 3'-f 7}~~1,i ( t;;;,S8 0 I Dt'2..\~ 2,.cr-\-.B 7}1'71 ,s , .. b 7 / f).IP},~ /1 /0 0 I D\1.'Z.\ ::1.Ci'-1,-A

~h~I,! .,~s-7/ J<P}1& I II 'i?' 0 0 1.:-1 e11-.3 7/dr;J,;, i '.s-s--.-\ 0 w~\\ *S' 7/J~lfif I~\ j --' *O \N{ ti-, -,t ::h,,I ,'6 \,'.l~~. --t COMMENTS Dl22D ~out-~l'coo...l b\oJ\~ This sheet filled out by OUL staff? Yes_ No. OUL Project No. 1r11y Date Analyzed: S(z.[ 1e, Charts* for samples on this page proofed by OUL: __ Analyzed By: \.J~a.. (;j le.re.a. $L Page /of/ O LU._ OZARK UNDERGROUND LABORATORY, INC. 1572 Aley Lane Protem, MO 65733 (417) 785-4289 fax (417) 785-4290 email: co11tact@ozarkundergroundlab.com SAMPLE COLLECTION DATA SHEET for FLUORESCENCE ANALYSIS Project LA C....f>U,}62,.

  • 6 w Week No:....,/).""". __ _ Samples Shipped By: )' .)~ Samples Received By: __,l ... ct",:;..,,;.'

_._., 4'"'8!7=~-""""""u;""'-"";:;._-----------~ Date Samples Shipped: 7Jhlii Date Samples Received: '1-;1.'1-/ 8 Time Samples Received: ?~30 Return Cooler? Yes O No .:Z Bill to: u,,J /Z .. *H Al d-n lL....... Send-Results to:-l"f"va..,,~0-0-"-caw,::rg,N':: iQ la Je .. ,{ q. J cL:,* d, , l'.C!:M D E-Osine ~Rhodamine WT O Other Ship cooler to: ------------------ I OUL Please indicate stations where dve was visible in the field OUL ust only for field technician use -use black ink only use only RCHAR LAB STATION STATION NAME PLACED COLLEcn:D

  1. REC'D NllMBER NUMBER WATER WtLt~ DATE TIME DATE TIME RECD \ ~,vll. 7},Cf]>'J 1031) 7/aeo ), 'is 9$"°C 0 I JOJ-A, ,},qJ,~ toy, ) Jd.1#/1% / 0 IS° 0 I ~ca-6 7},q h~ ,~~3 7 };itD)\'y

/o..2.'-1 C I :l~~-1\~ 7J,4h&' IJO~ t7/J1Dj1f; lt::.3.;J 0 \' 1:103-*A '7J,qJ1-r 11\ "1 71.~~l*'is jc"i~ o*. \ J..o'3-:--8 .., I, ..,,,s-113'1 7)~1o1,i { '*1-8 0 I ~-e, 711'1) ,g 113b 7 /3. IP),'* / II 0 I ~c.'-1 ... A i7J1~l1S II US'"° 7/ !}.CJ,}, b (II~ 0 0 011,7? IN ell-.3 7/:i~l,i' I I .S'S--.-l 0 n,12~ W,t\\ *S' 7/al4>/~ (~\ j --. ' *O 11) 1"2..., _q \f\/{11-, ,b1ol,~ \;J~\O. --' COMMENTS ____________________________________________ _ This sheet OUed out by OUL staff? Yes_ No. OUL Project No. l'Jll.f Date Analyzed: g

  • 2-10 Cbarts*ror samples on this page proofed by Analyzed By: \J.5o.. Q,..\ut:c,..S.t...

Page/ of/ OlU-OZARK UNDERGROUND LABORATORY, INC. "-DISCREPANCIES BETWEEN CHAIN-OF-CUSTODY SHEETS AND ACTUAL SAMPLES RECEIVED Page/ of J Company & Project Name: +I /:.Je'4 A -L ;4 I An cL Date Rec'd by OUL: 7-.;;, 7-/B Wk# ( lAcBuJtc.. -C1-W Lab# Sta# Station Name Date Problem Solution Pulled 1) /J.,').,'J.. We.l\ -:2, ';f /'UII Wo..~M ",:,_\ i s rx-12,1,,,,.t. !he<, .£ ( * * "' \I -h?..n< ~*h=r r,MAllll.1;:.,.. '" @,U~b . 1 .J ' <. a 0:: 1'\'\A \' ,~ ...... l!... ~ftAnl.. 1*1"\~ r.:i V\1, , VIA. , /)tJI_ \i .. ~t.,_A \J;D. l 1t 1l,4..\,, ,~fut~tW\ -fmM r rlll,1,.....l. v,"n .. \. -',!.c./ 6V I,.. Comments: flolt.--hJ dth,/-h~~c ~i" lAtl\'ti!r M,-... u,IY~-4-.wlf\

  • ,Yl ..._\,.,,J 11,..l,1.M_y\

' ' f:\shared\fo nn s\dscrpsht.doc rev. 12/28/9 9 Certificate of Analysis Date of ce rtificate: A u g u st 8 , 2018 C lient: Ha l ey & A ldr ich I 00 Cor p o r a t e P l ace, Suite I 0 5 Rocky H ill , CT 06067 Project name/location: LAC8WR , Genoa, WI Client project #: 1 28924-004 Contact people: M il es van N oor d en n e n (mvannoord e nn e n@h a l eya ldri c h.com) Samples collected by: S. Kaney Date samples sh ipped: Augu s t 2, 2018 Date samples rec'd at OUL: August 6 , 2018 Date ana lyzed by OUL: August 8, 20 18 Included with certificate of analysis: Tab l e of r esu lt s, cop i es of sa mple co ll ection dat a s heet Nad i a Glucksberg (Ng lu cksbe r g.h a l eya l drich.com) Results for charcoal and water samples analyzed for the pres e nce of rhodamine WT (RWT) dye. Peak wave l engt h s are reported in n a nom eters (nm); d ye concentrat i ons are r e ported in parts per billion (ppb ). A ll resu l ts are for c har coa l unless otherwise indicated. OUL Station Dateffime Dateffime RWT Results Number Number Placed Collected Peak (nm) Cone. (ppb) Dl289 River 7/26/18 0956 8/2/18 0842 ND Dl290 MW-201A 7/2 6/18 1018 8/2/1 8 0908 ND D1 29 1 MW-2028 7/26/1 8 I 029 8/2/18 0918 ND 01292 202-AR 7/26/18 10 37 8/2/18 09 25 ND D l 293 2 0 3-A 7/2 6/18 1055 8/2/1 8 0935 568.1 529 Dl294 203-8 7/2 6/1 8 1104 8/2/1 8 0941 ND Dl295 204-8 7/26/1 8 111 6 8/2/18 0952 ND 01296 204-A 7/26/1 8 112 3 8/2/18 09 58 ND D l 297 W e ll-3 Water 8/2/1 8 I 035 ND 01298 Well-5 Water 8/2/1 8 1 247 ND Dl 299 Well-7 Water 8/2/1 8 1 300 ND 01300 Laboratory control water blank Note: Dye concentrations are based upon sta ndard s u sed at th e OUL. The sta nd a rd co ncentration s are based up o n the as so l d we i g ht of the dye th a t the OUL u ses. If the cl i e nt i s not u s in g OUL dye s, th e c li e nt s hould provide the OUL with a sa mple of th e dye to compare to the OUL dyes. Footnotes: ND= No dye d etec t ed Thomas J. Aley, PHG and RG F:\docs\COA \Ha l ey A ldri ch\Hal ey A l d ri c h_ LAC8 WR_ 05 l o f I

, OZARK UNDERGROUND LABORATORY, INC. 1572 Aley Lane Protem, MO 65733 (417) 785-4289 fax (417) 785-4290 email: contact@ozarkundergroundlab.com SAMPLE COLLECTION DATA SHEET for FLUORESCENCE ANALYSIS Project I ft<.,..<7>uJl1.

-6 w Week No: 3 Samples Collected By: ..i..'.3:~. Y-ia...,r....c::.~..i....

  • od--------------

Samples Shipped By: S' a n-8~

  • Samples Received By: ....L.!.M;.i......., R~<<C'Ji.a.:.~~~~

oZZ-==~-----------

Date Samples Shipped: SJ;). JI'? 0 Date Samples Received: i4,11i Time Samples Received: /c3o6 Return Cooler? Yes D No~ 1 l /L ' Bill to: l+ti.l:g:r .4'14::r*iob.

  • SendResultsto:

d'::£a.n<1cC>n:~.e. ..... o~"'Q ha k-tald.,,-

, 1-, -ro ........ Analyze for
D Fluorescein D Eosine .@ Rhodamine WT D Other Ship cooler to: -------'-----------

OUL Please indicate stations where dve was visible in the field OUL use only for field technician use -use black ink only u se only #CHAR LAB STATION STATION NAME PLACED COLLECTED

  1. REC'D /'JUMBER NUMBER WATER IU'n,d. DATE TIME DATE TIME REC'D ( f)/;:>9,?

0..*,-..1e/ 7) ~1u}1y ft S"<o '!J~/J"8 o~~'-1~ D t 0/'2-'fD l'--\W' a t>lt 7)11:,/18 lb)b' '6};)} ,i :,G)o& 0 l J)/2. q I !'-,\.1.J

  • J~o£, 7):Ju/ I~ to JC} j;> /ti p'l 1 'S' j) I V 12.. '12-J. C, (:) -A?-, }aro},~ 103 7 ~Ja/,i @.;2~ 0 ( PJ'l 13 ;}00-A 7/J.,J<lf I oS-S-'?°{~ } I<( D°l "s-S-D I DJ2.CJ1 J.03 -£ rJ )t1-lo} Ii 11oy 3 }:9) l"S° OC14-1 i) I D12-9~ d-e)<-{-_6 17/Jl£1/ ,& i \ \(o gJJ }Ii 00,<;-;;>

0 ( {)12-1~ oloy -A 7/c)eo}, g 1,;;3 ~/J/1~ D<=i-S-~ () 0 *.uell-3 Y/d/1~ IC °3 '.:)---( {) wen -) 25/J.)1'6' a.y, --I 0 'i5/;)} I'( 1 '3<lw --11e11-7 ( COMMENTS---------------------------------------------- This sheet filled out by OUL staff? Yes_ No~ OUL Project No. L 1L 'f Date Analyzed: 8 J i/t f' 7 Charts for samples on this page proofed by OUL:_.....:..o::::...1,.,...,.:. ___________ _ Analyzed By: )1 e / O f.JL 1 Page / of / \, OZARK UNDERGROUND LABORATORY, INC. 1572 Aley Lane Protem, MO 65733 (417) 785-4289 fax (417) 785-4290 email: contact@ozarkundergroundlab .com SAMPLE COLLECTION DATA SHEET for FLUORESCENCE ANALYSIS Project I K<1>v , n2.. -6 w Week No: 3 Samples Collected By: ~3'""-!..' ~e:-.:Ai...r-..i;;::~......,~

Samples Shipped By: S' 0 r,. R"°1: , Samples Received By: -L.!M~. ,..t(.,_ic\""'-"~<.:..!..!~('.--~-==-=------------ Date Samples Shipped: SJ~) I? 0 Date Samples Received: ?40? Time Samples Received: Jc&>t:> Return Cooler? Yes D No~ Bill to: !+ti.I!:=( ll. A1d-x,uk

  • SendResultsto:

d'YOxb ,,....Dcn}e.. ..... a~""Q be l~~ta)d.,,--ic , h -ro,...., Analyze for: D Fluorescein D Eosine Rhodamine WT D Other Ship cooler to: _______ ' ----------- OUL Please indicate stations where dy_e was visible in the fleld O UL use only for field technician use -use black ink only use o n ly #CHAR LAB STATION STATION NAME PLACED CO LLECTED # REC'D ~rR NUMBER WATER l,J,r, tX' DATE TIME DATE TIME RE C'D I (L.Je/ 7 J ;}lo J ,y ftSl<> '3' I~/ 1"8 lo'?~ ~;? 0 ( 1\-\W' Jt:>lt 7)-a.r:,J,g t b1% '6/cJ) ,& b'J o'g c) ( li'-,\JJ . J ~c12> 7):;u/ ,rs loJC.:, ~j)/1~ 10'1 t '8" .:> ' J.0. !)-Af_ 17 }a10J , a /IJ 3 7 a I a J,1 c:ft.J s-0 f ;)c-:3-A 7/Jb/<ls' /O S-~ I , 1 O°l '3-S-. 0 { Jo3 -.B 17)J,~) Ii 110y '& J 9 ) 1"3' OC!y. I D I J..oy-_6 tJ/Jtt,/ 1% t \ \ \o ?;jJ ,,~ 0 0,<;"",;) I) l oloy -A 7fo eo),K 1,;;3 ,g-J J. },cf 0'1 s-8" 0 () .D11 '11 li.uell-3 '8' );1 ),-s IC'3:f" --' 0 J) /2 '18 we 1\-) 175 / )Jir;, a. I..{-, --I r) ID 12-qq 1,e11-7 <;;/J)l<i 13\}u --I : 7) / C) /) :: oUL e,,.) d-"1.r J, / .-:u I k.._ This sheet filled out by OUL staff? Yes_ No_6_ Charts for samples on this page proofed by OUL:_-+-.,.:-;._;:,------------- OUL Project No. [71 'f Date Analyzed: (?-9 -/ 8 Analyzed By:_.L.;vt....:...L.R....::,,,-/-=o=ic...:"-=----

Page f of/

Certificate of Analysis Date of certificate: A u gust 1 6, 20 1 8 Client: Ha l ey & A l dric h I 00 Corporate P l ace, S ui te I 05 Rocky Hi ll , CT 06067 Project name/location: LACBWR, Genoa, WI Client project#: 128924-004 Contact people: M il es va n Noorde nn en (mvannoordennen @h aleya l dric h.com) Samp l es collected by: S. Ka n ey Date samples shipped: A u gust 9, 2018 Date samples rec'd at OUL: Aug u st 1 3 , 20 1 8 Date analyzed by OUL: Augus t 1 5 , 20 1 8 Included with certificate of ana l ysis: Tab l e of r esu l ts , copies of samp l e co ll ection data s h eet Nadia G lu cksberg (Ng lu cksberg.h aleya l drich.com) Results fo1* charcoal and water samples analyzed for the presence of rhodamine WT (RWT) dye. Peak wavele n gt h s are reported in nanomete r s (n m); dye concentrations are reported in parts per b illi on (ppb). A ll res ul ts a r e fo r c h arcoa l un l ess ot h erwise ind i cated. OUL Station Date/T i me Date/Time RWT Results N u mber Number P l aced Collected Peak (nm) Cone. (ppb) D l 422 River 8/2/18 0852 8/9/18 0823 ND D l 423 201-A 8/2/1 8 09 1 3 8/9/ 1 8 0838 ND Dl424 202-B 8/2/1 8 0923 8/9/1 8 0846 ND D l 425 202-AR 8/2/18 0930 8/9/1 8 0853 ND D 1 426 203-A 8/2/1 8 0940 8/9/1 8 0903 567.2 84.1 0 1 427 203-8 8/2/18 0947 8/9/18 0908 ND D l 428 204-8 8/2/1 8 0957 8/9/1 8 09 1 8 ND D l 429 204-A 8/2/18 1 003 8/9/1 8 0953 ND 01430 We ll-5 Water 8/9/18 0932 ND 0 1 43 1 We ll-7 Water 8/9/1 8 0943 ND 01432 We ll-3 Water 8/9/1 8 1 022 ND Note: Dye concentrations are base d u pon sta n dards used a t the OUL. T h e standa r d co n centrat i ons a r e based upon th e as so l d we i g ht of t h e dye t h at the OUL uses. If t h e c li ent i s n ot us i ng OUL dyes, the cl i ent s h o ul d provide t h e OUL w i th a samp l e of the dye to co m pare to t h e OUL dyes. Footnotes: ND= No dye de t ected Thomas J. A l ey, PHG a n d RG F:\doc s\COA \Ha l ey A l d ri ch\Ha l ey A l dric h_ LACS WR_ 06 I of I OZARK UNDERGROUND LABORATORY, INC. 1572 Aley Lane Protem, MO 65733 (417) 785-4289 fax (417) 785-4290 email: contact@o zarkunde rgroundlab.com .*, SAMPLE COLLECTION DArA SHEE'F for FLUORESCENCE ANALYSIS ProjectL e~t. Week No: 1 Samples Col~ed B1: S...:.i-La...,...~....,._-.,._ __ ~----------Samples S~ipped By: . Samples Received By: {~ C}l,l,( ____. . Date Samples Shipped: Date Samples Received: \ Time Samples Received: l '3 3o Return Cooler? Yes O No Bill to: t. A:t <6:;;cfl:: Send Results to: vYyJo ,.n C_! o c de on£.., @ ~-I th(O Id n* r to . c c.A::> Analyze for: 0 Fluorescein O Eosine ~Rhodamine WT O Other Shi~ler-to:

  • -----_:___:_ ____ -:--_ OUL Please indicate stations where dr.e was visible in the fl.eld OUL use only for field technician use -use black ink only use only #CHAR LAB STATION STATION NAME l PLACED COLLECTED
  1. REC'D ltMBER NUMBER WATER --IJ DATE TIME DATE TIME REC'D I D 1L1 2 2-Q~v e,/ 'i }~ ), g-~rol* S-)1 /1%' ai a,3 0 .. l Diu....:J ,. dol*A <?;)a), B" D~l.'.3 '( }cy J 18 0-?31 0 I f)/L/~4. [}\\~-6 "3 }s ),? o'L13 'if)"' ),'i' OS"t{ b r<) I Dt l.fZ w; /).of)-~ *-~loJ,i 6Gt 3i:) }Cf}fi? 0¥~3 0 I N4Zlo Jo~-A 'i }a. )1 'g , D'l4u . 'tS) C,L,"t. e>Cfc:3 eJ I D i'-/-2 1 .?.u~ -6 g )a},~ 0'1Ll7 8 )q J,g-oqn'b 19 I Cr 4J. 9" c) uY-8 s-/a},~ OC!S-7 g/9 )18 cc,,, e) I Ct'-1 2 9 ~L\-.4-<l'/J../*'f

)'(l03 ~, <t/,'4' 09S3 n D well *5 --5f )9 / ,'t D43,,;1. J f) we II-, --3' fl ),'i' c,qy 3 I 0 I.Pe 11-3 -¥}ci}1Y /Of)~ I -~St. COMMENTS*-----------------------

,---------------This sheet filled out by OUL staff? Yes_ No. OUL Project No. I 114 Date Analyzed:

~-I 5=j8, Charts for samples on this page proofed by Analyzed By: L\50-G,\ ltre.a.SL.- Page\ of\ f\G\ ov\ V -~ OZARK UNDERGROUND LABORATORY, INC. 1571 Aley Lane Protem, MO 65733 (417) 785-4289 fax (417) 78S-4:290 email: contad@ozarkundergrouodlab.com SAMPLE COLLECTION DArt: SHEET, for FLUORESCENCE ANALYSIS ProjectL e~l;. WeekNo: SamplesCo~...,-~~~..i:l,,,.l,lj

  • ~,__,...,..-,1----------

~.,.,.,._-:i------------+-SamplesReceivedBy: ~~LU '.=: Date Sampies Shipped: Date Samples Receiv~: \ Thne Samples Received: \? 00 Return Cooler? Yes D No i.at*

  • Bill ~:_\.k..t ,, \ tA:1<k;)d1::

_ _ Send Results to: Yb\{P...ro

  • o*o c d*eo2_-§_@ ~} t1::,<o tdri c to. .. rc......,-----A-n-aly.r.e-for:-g_'...Fluoresceln-E)

-Eoslne-f2tRh~amlne WT E] QUi~r .. Ship-cooler-to: , .*, OUL Please indicate stations where df..e was visible in the [zeld OUL Ultonly for field technician use -use black ink onlv Ultonly OCHAJl LAB STATION STATION NAME ,'.f PLACED COLLECTED

  • REC'D NUMBER NUMBER. WATER W\J~ I>ATE TIME DATE TIME REC'D I Q~" e,/ ,* irJ~J,r-Di'S-~-g.Je,J,~ oi a-3 0 --I ~ol-A ~,~J*R-b913 i'l~l,8 O'ir?,~ 0 ' .90~-e "$)8),y oGt~ cg' J "I J,'l oSl{b ,.., { ,9.o~-A'!t

-S-1 a. J*i 6G! o-:> }'ilfif O<jS3 0 I dO~-A ~,~,,~-0~40 ~}Cji,"j' o'°ltlS © I ~<); -& 11" )a /,-a 0'1'-17 8 )q J,tr oqc:.~ Ii) I d04-8 ~/aJ,Cj ,, t!) ( .;2oy-,4. I'?' I ~J, er 1~03 a-J,/,f' o,sa n D 'Dl&.f 30 UJell-S----i)"IJ,?' C><'J 3a. 1 (') INLJ~I we 11--; --8' Jci },~ 6'i<.f 3 I 0 T)1L/.~1-U,)e 11-3 -s,JqJ,~ lo&J~ I - This sheet filled out by OUL staff? Yes_ No Z: OUL Project No. 1114

  • Date Analyzed:

R-15-1B Charts for samples on this page proofed by OUL:-4,Q--J. a~~~-===:__ ________ _ Analy.r.ed By: Ll':.o. Gi 1o::epS(:..- Page\ of\ f\v\o\AV Certificate of Analysis Date of certificate

Aug u st 22 , 2 0 1 8 Client: Ha l e y & A l d ri ch I 00 Co r porate P l ace , Suite I 05 Rocky H ill , CT 06067 Project name/location:

LACBWR , Genoa , Wl Client project#: 1 28924-004 Contact people: Mi l e s van Noorde n ne n ( mvannoord e n ne n@ha l eya l d r i c h.com) Samp l es collected by: S. Ka n ey Date samples shipped: Aug u s t 1 6 , 20 1 8 Date samples rec'd at OUL: A u gust 20, 20 I 8 Date analyzed by OUL: A u gu s t 22, 20 1 8 Included with certificate of ana l ysis: Tab l e of res u l t s , cop i es of s am.p l e co ll ect i on data s h eet Nad i a G lu ck s ber g (Ng l ucks b erg.h a l eya l dr i c h.com) Resu l ts for charcoal and water samples analyzed for the presence of rhodam i ne WT (RWT) dye. Peak wave l engt h s are r e ported i n na n ometers (nm); dy e concentrat i on s a r e r e ported i n part s pe r b illi on (ppb). A ll re s ul t s a r e fo r cha r coal u nl ess ot h erwise in d i cated OUL Station Dateffime Dateff i me RWT Results Number Number Placed Collected Peak (nm) Cone. (ppb) D l 462 R i ver 8/9/1 8 083 1 8/16/18 0748 ND D1463 20 1-A 8/9/1 8 0844 8/16/18 0807 ND D 1 464 202-B 8/9/1 8 0852 8/1 6/1 8 08 1 5 ND 01465 202-AR 8/9/1 8 0856 8/1 6/1 8 082 1 ND D l 466 203-A 8/9/1 8 0908 8/16/18 0830 566.0 1 2.3 D l 467 20 3-B 8/9/18 09 1 4 8/1 6/1 8 0836 ND 0 1 468 204-8 8/9/18 0922 8/1 6/18 0847 ND 0 1 469 204-A 8/9/1 8 0957 8/16/1 8 0852 ND 0 1 470 We ll-3 Water 8/1 5/1 8 1 055 ND D 1 471 We ll-5 Water 8/1 5/1 8 1 305 ND 0 1 472 We ll-7 Water 8/15/1 8 1 320 ND Note: Dye co n ce n trat i o n s are based u pon s ta n dard s u s ed at t h e OUL. T h e standard co n centrat i ons are based up on t h e as sold we i g h t of t h e dye that the OUL uses. If t h e c l ient i s n ot u s ing OUL dye s , t h e c li e n t s h ould provide the OUL wit h a samp l e of the dy e to compa r e to the OUL dye s. Foot n otes: ND= No dye d e tected Thomas J. Aley, PHG and RG F:\doc s\COA \Ha l e y A l dr i ch\Ha l eyA l d ri ch_ LACB WR_ 07 I of I OZARK UNDERGROUND LABORATORY, INC. 1572 Aley Lane Protem , MO 65733 (417) 785-4289 fax (417) 785-4290 email: contact@ozarkundergroundlab.com SAMPLE COLLECTION DATA SHEET for FLUORESCENCE ANALYSIS Project f,~~u~-P;1.e ?>~= Week No: c:;-Sa~ples Collected By: s~~:1: Samples Shipped By: '.j . )~ .... 2...6!:, Samples Received By: {) 06-,--t/ Cl./.k.. Date Samples Shipped: ts:I I l,t J 1 't O Date Samples RKeived: f, .:2<J -/ 8 Time Samples Received: 13 tJ O Return Cooler? Yes O No Bill to: '\-\ct,l-c-1 1\:1~~-_ _ Send Results to: m va...boouCMneeo@ha-l;;pys-1 de,","-*,o"::\ -------iQlRhodamine WT O Other Ship cooler to: ------------------- OUL -Please indicate stations where d1t.e was visible in the (leld OUL use only . for field technician use -use black ink only use only #CHAR LAB STATION STATION NAME PLACED COLLECTED

  1. REC'D NUMBER NUMBER WATER /\ 1"10. yroa..\ DAT£ TIME DATE TIME REC'D \ D141pi. Q* >li 8' Jc,),~ o~.~\ '8' }l1s, J 18 074.l" n I t)L\ t, ..;Z.ol-A

~/q /cfr Wt/4 /11.,118 Un>7 () I DI I.\ ltY .;l...¢.;i -,0 <i}qfiq OfiS.;) ~)Ito I, i 08't) 0 I DtL\i,5 ~o;;. ,A{l. ~Jtt lit D~'$""1o ~/1v./11 0%.;I I 0 I D\4~\o J..t> '::> -A q' Jc, /I 8' oC/0~ i 'B"J I \JI I,'"{ o&-;,o n I Dl4\,1 .;I\'>;.-($ '?r J <:i },~ O&f1i..J 'i },i; /,t 0~3b> () I DtL\ 1.R au~ , d" }c,}1f DC,~~ 'Z/tLP / tf 08'47 ri I 1)1L\lo'\ c9o*-t.-A -s /o,)rr oa,~-7 J11o/6( o& S-d 0 () v>~\I -.3 '8 J ;S" },~ JoS-S --I {} ~11-S-o/1 , 5'/Jfj Ibo$"" --I ~11-7 r),<Jf6 13J..O --I n COMMENTS ~Sr:ce 1 I A&-*p ....... .,e C,k e:£ ut?lbn r£::b:i::41o.J? Weo fL :,xr, ' ..; This sheet filled out by OUL staff! Yes_ No__b OUL Project No. 11/'f Date Analyzed: ~~'*2,-(~ Charts for samples on this page proofed by OUL:~=...:.;:=- Analyzed By: { Qu.! ' S/17/JR 9/J P age / of / d' UJ._ OZARK UNDERGROUND LABORATORY, INC. 1572 Aley Lane Protem, MO 65733 (417) 785-4289 fax (417) 785-4290 email: contad@ozarkundergrouadlab.com SAMPLE COLLECTION DATA SHEET for FLUORESCENCE ANALYSIS Project (,kc~ ,W,. -Oj& Tu-L Week No: Sa~p l es Collected By: S-.J/~~~::4' Samples Shipped By: _}~_n Samples Received By: __./2r....-_..1o C2:S&'f,i!!l~il=ifL..,-fl-{. ..S.'(2.L1ti-"~1C-------------- Date Samples Shipped: Kl llf I I J Date Samples Received: g -.fJ.cJ -/ 8 Time Samples Received: 13 tJ O Return Cooler? Yes O No~ Bill to: J_:tQ,\"C>J ft\ .Lri cb,. _ _ . . __ . . ~n~-Results-to:.-yn va:15 c-o i\*£di*noen@~'nal1:q:0-1*&: d,. *c 01':'.) ***-0 Eosine @Gihodamine WT D Other

  • Ship cooler to: -----------------

OUL . Please indicate stations where dJ!..e was visible in the fl.eld OUL use only . forfield technician use -use black ink onlv use only ~CHAR LAB STATION STATION NAME PLACED COLLECTED

  1. REC'D NUM B ER NlJM BER ' WATER D ATE TIME D A TE TIME REC'D ' rJ.: Ill Jci),'3 0'&'.~ I 48" )i~ J ,s fl o7l.fi n I l~ol-A ¥"/q /*8 ~"' s-1,~1ig Qn, n I .sl-eol-J)

?Rl1<t oi;s d '8)11# ft 'g 08"1$' n I 1:ro;;. -A(l ~Jq/,t t)~~ ~1,~1,r Ot~ I n I d-b:> -It: . <r lct/1~ q<qo'ir I 'zfl,"'li~ o&;P I'> I ;)-!1-:;-e, o/ I c:t Ji ,g, oq >'1 'J) I~ /1'! 0~31::> n I ~4-_f., ~Jc,J,r ll~~,::i <$/ tu/ ,f o~-, . ,., I ~o**kA f-alq.Jrr 00,~~7 ~,,,ft,,,, 08)d n () Dtt.\10 ~-ell -.3 '3) ;S" ,,~ Jo~S---I I) Dt411 (.)j,,e ll -o/16'/1S IOO) --I !)1412. w-eli-7 rh~/6 13J.O --f ('\ COMMENTS ~Sne::e 11 ),u, 3 s ...... ee fl(... ,,, de:,,,. '(:f':tri:::"'1eJl fr:,;>,..,* f2. iJ?C, i . This sheet filled out by OUL staff? Yes_ Nr/J2 OULProjectNo. 1]14 Date Analyzed: Charts for samples_ on this page proofed by OUL:.__,.:~'--;;::-=-

Analyzed By: lf#!,Jot-R 8/17/JR 9/J Page / of / ft" w.__ Certificate of Analysis Date of cert i ficate: September 19 , 2 0 18 Client: Haley & Aldrich I 00 Cor p orate P l ace , S uite 10 5 Rocky Hi ll , CT 06067 Project name/location: LACBWR , Genoa , WI C l ient project#: 1 2 8924-004 Contact people: M il e s van Noorden n en (mva nn oordennen@h aleyaldric h.co m) Samples collected by: S. Kaney Date samples shipped: September 12 , 2018 Date samp l es rec'd at OUL: September 1 3 , 20 l 8 Date analyzed by OUL: September 18 , 20 1 8 Included with certificate of analysis: Nad i a G l uck s berg (Ng lu ck s berg.h a l eya l dric h.c om) Tab l e of r e s u l ts, copies of s amp l e co ll ection data s heet Results for charcoal and water samples analyzed for the presence of rhodamine WT (RWT) dye. Peak wave l e n gth s are reported in na n ometers (n m); dye concentrations a r e r epo r ted in parts per bi lli o n (p p b ). A ll resu l ts a r e fo r charcoa l un l es s otherwise ind i cated. OUL Station Date/Time Date/Time RWT Res ult s Numbe r N u mber Placed Collected Peak (nm) Cone. (opb) Dl888 R i ver 8/16/18 0756 9/12/18 11 36 ND Dl889 20 1-A 8/16/1 8 08 1 2 9/11/18 0800 ND Dl890 202-B 8/1 6/18 0820 9/1 1/1 8 0955 ND Dl89 1 202-AR 8/1 6/18 0825 9/1 1/18 0959 ND 0 1 892 2 03-A 8/16/1 8 0834 9/11/1 81330 567.6 543 Dl89 3 203-B 8/1 6/1 8 0843 9/11/1 81335 ND Dl894 204-B 8/1 6/1 8 0850 9/12/18 0902 ND D1895 204-A 8/16/18 0856 9/1 2/18 0906 ND D l 896 Well-3 Water 9/10/1 8 1 5 1 5 ND 0 1 897 We ll-5 Water 9/1 1/181240 ND 0 1 898 We ll-7 Water 9/1 1/18 1255 ND Note: Dye concentratio n s a r e ba s ed u po n standards used at t h e OUL. The standa r d concentrations are base d u po n t h e a s so l d weigh t of the dye t h at t h e OUL u ses. If the cl i e n t i s n ot u s i ng OUL dyes, the clie nt sho ul d prov i de t h e OUL wi t h a sa m p l e of t he dye to compare to t h e OUL dyes. Footnotes: ND= No d ye detected Thomas J. Aley, PHG a n d RG F:\docs\COA \Haley A l dri c h\Haley A l drich_ LA CB WR_ 08 I of 1 \I OZARK UND RGROUND LABORATORY, INC. 1572 Ale~~i,i~;~~;~TIC::J 7 1 ~-;: s:ii:~i ;:~;{~~~~~~~ti~~~~;;~lab.com Project b A-{, £;) u , s-(/ -~'i, e 7:-e > b Week No\ (a -CJ Samples Collected By: _S'L...-:...l!L,,....t:l..:c::o..11*~<,,{,f,. ,------------- Samples Shipped By: d Samples Received By: A{ a -(). Ou...L Date Samples Shipped: q / 1 a JI Y Date Samples Received: Time Samples Received: <)ic;,3c;:) Return Cooler? Yes O No~ Bill to: 1-\a..te.x i A--u;, elk. Send Results to: (b'14-t:Jnb,,,.d_g C'Ofc1?0 ha leu,a/d:xJ'c £.., 1 Oll'/'Y"\ I::::" ' Rhodamine WT D Other Ship cooler to: ------------,..,....------ OUL Please indicate stations where dy_e was visible in the (leld OUL use only use only for field technician use -use black ink onlv #CHAR LAB STATION STATION NAME PLACED COLLECTED

  1. REC'D NUMBER WATER ' ~o DATE TIME DATE TIME REC'D I bJt&g (lJ,\IC f r;n,~ /1'? D'1S1., 4/,a),'8 ii 31.o 0 I lot8g9 Ja 1 -A 8") I lo) c'g os, d' 9) 11 \1%' D%i5D CJ I D1~CfD ~~;)-,& }11o),~ C>~:J. D 'f/ ,,,, 'Ir C>C, S'S-(j I D1&9 t J uJ'Ar;,. ~)Iii>}, g 0 g-.;> S" q /11 I ,s--dr.scr I 1'l!Pi92-J.~1-A '81 1 j (p /, i OS3'--I .ql,,/,<c

,*-:,,~o () I D//113 ~os-6 I ? }11.. J, 8 t::,!?'U fq I '" \:, ,"33~-0 I .1>189'1-;;Lo t-f -A '1?), ro I c v a~D lq/, a/,i oqnt:) D I IJJ;fftS )ts'-\,, .A :r )1 t,p/ 'y o~~., Cf/ , r;_ I 1<1' Oiu(t; 0 0 W()\-3 --1 0 IC I I b° ID'S'" J I q',,1,'8 I 0 Llf\1-5" --ra'-l o 0 *ue 11-7 --or) II /iir 1;l..'S;) l I l COMMENTS------------------------

This sheet filled out by OUL staff? Yes_ N~ OUL Project No. l?f:IL\ Date Analyzed:~ Charts for samples on this page proofed by OUL:__._.......,+-=~ Analyzed By: ¢/ OVI.--__._~,'-=--"--------- ---Page { of / Project~ OZARK UND!RGROUND LABORATORY, INC. 1 S72 A~ey Lane Protem, MO 6S733 (417) 7 S-4289 fax (417) 785-4290 email: contact@ozarkundergroundlab.com

SAMPLE COLLECTION ATA SHEET for FLUORESCENCE ANALYSIS I t:te :Z::r: sb: WeekN Samples Shipped By: Date Samples Shipped: q) ,~a, I y\ Bill to: 1-\a.A.LX i Jir: IJ..c; c/t-[ (.)J,4_ Date Samples Received:

.,,.,., 9 F I Time Samples Received: 'f'<<.;3c) Return Cooler? Yes 0 ,Se nd Results to: fbV4'::l 6b o c d,g c o&:>9 ha 1.-'L,q I d:::o

  • c b,, , C2>rc No~ Df>sine '<:!1"' r Rhodamine WT O Other Ship cooler to: ------------------

i OUL I Please indi cate stations where dye was visible in the field OUL use only l use only I for field technician use -use black ink onlv #CHAR. LAB STATION l STATION NAME PLACED COLLECTED

  1. REC'D NUM;E.R NUMBER I WATER Wti ('" DATE TIME DATE TIME REC'D I a_,,Jt' ( ~lb J1'? C>7$1, .!j/1 a I 1 'B i13~ 0 I JO I -.A ~)11o)t'g O~lol 9111 \1%' ()%ts'Q a I Jl~;)-{:;, I )p'OJii o"ir::l D "f/ 11/, f-DC,S'S-(j I cli:>ol-~

I r:?)11.o }, g 0S'o7 $"" Cf /11/ ,~ dlst:r I I '8'}1~/1'/i ~i-/Jr Q'a-54 .:, /11 I,~ 1-?i~O 0 I ii9os-f> i i In,/, 8 r-.8'f./. ~' 1 1 1 \ 1 '732-.... -0 I !2..ri v{ -()... I R'J11ol19 a~() lqJ , a /t'& Oqn-9 D I ~~'-\., A I )')11g/ ,9 O<i<-t"i.,, c,/,i),~ OjOltJ 0 b,~q~ we.11-3 I --lq flt) Iii IS1" I 0 httf/7 l if>l\-" I 0 --lq 1,, I, i ta40 I 0 :n1f(ie:, : ue11-7 ! -cr/11 lt~ '~'S"'S""" ' -' l l I COMMENTS------....------------------------------------~ ' -This sheet filled out by OUL staff? Yes N 1-0UL Project No. l:J-14 Date Anatr,ed: 4 U>!K' Charts for samples on this page proofed by OUL: tK'.d { )J. L-Analyzed By: t'C,/OUL----""t, __ .....__ ________ _

  • Page ( o f (

Certificate of Analysis Date of certificate: O c tob e r 1 8, 20 18 C lient: Ha l ey & Ald ri c h I 00 Co r porate Pl ace, S uit e I 0 5 Rock y Hi ll , C T 06067 Pro j ect name/location: LACBWR, Ge n oa , W I C li ent project#: 1 2 89 2 4-004 Contact people: M il es van Noo rd e nn e n (mvann oo rd e nn en@h a l eya l dri c h.co m) Samples collected by: S. Kan ey Date samples shipped: October 1 2, 20 1 8 Date samples rec'd at OUL: O c tober 1 5, 2 0l8 Date analyzed by OUL: October 1 7, 2 0 1 8 [ncluded with certificate of analysis: Nadi a G lu cksberg (Ng lu cks b erg.h a l eya l dri c h.com) Tab l e o f r es u l t s, co pies of sa mp l e co ll ec tion data s h eet Results for charcoal and water samples ana lyz ed for the presence of rhodamine WT (RWT) d ye. P eak wave l e n g th s a r e repo r t e d i n n a n o m e t ers (n m); d ye concentrat i ons a r e r eported in part s per billi on (ppb ). A ll result s a r e for c h arcoa l unl ess ot h erw i se in d i ca ted. OUL Station Date/Time Dat e/Time RWT Results Number Number Placed Co llected Peak (nm) Cone. (ppb) D 2 47 3 2 0 l-A 9/l 1/18 09 3 9 10/10/[8 10 35 ND D 2 474 2 0 2-8 9/11/1 8 11 44 10/1 0/18 1 335 ND D2475 2 02-AR 9/11/1 8 11 47 1 0/10/18 1 337 ND D 2 476 2 0 3-A 9/11/18 1520 1 0/1 0/1 8 0829 567.2 940 D2477 203-8 9/11/181524 10/10/1 808 33 ND D 2 478 204-A 9/12/1 8 1 0 55 I 0/9/18 1 3 1 2 ND D 2 4 79 2 04-8 9/1 2/[8 10 58 10/9/18 1308 ND D 2 480 L a boratory co n trol charcoa l b l ank D2481 W e ll-3 Wate1* 1 0/10/1 8 1600 ND D2482 We ll-5 Water 1 0/10/18 1 235 ND D248 3 Well-7 Water I 0/10/18 1 2 4 5 ND Note: D ye co nc e ntration s a r e ba se d upon s tandard s u se d at th e OUL. Th e s tandard concentratio n s are ba se d upon th e a s sold w e i g ht of th e dy e that the OUL u ses. If the client i s not u s ing OUL d yes , the c li ent s h o uld prov i d e th e OUL with a sa mp l e of th e dye to co mpar e to the OUL dye s. Footnotes: ND= No dy e d e t ected Thomas J. Ale y, PHG and RC F:\do cs\CO A \Ha l ey A l drich\Hal ey A l d ri c h_ LA C B WR_ 09 I o f I OZARK UNDERGROUND LABORATORY, INC. 1572 Aley Lane Protem, MO 65733 (417) 785-4289 fax (417) 785-4290 email: contact@oza rkundergroundlab.com SAMPLE COLLECTION DATA SHEET for FLUORESCENCE ANALYSIS WeekN~: JO -/3 Sa~plesCollected:: -: VA:~:: , * , &<<6 V6r1 Samples Received By: ___ e=--, .... t'M--"7--./ '-_-t2 ... (,'"'"',!:(_.._.{l ......_ _____________ _ ,-; .* ,. 11 "-Date Samples Received: /tJ-/5:-(f::; Time Samples Received; /'fttd Return Cooler? YesO No~ Bill to: i:+aA~ & A I cko' r l-..

  • Send Results to: 'fV'0a..."'

0 PD c 4£:!> Q..R o@ kA-1~':f q I d..,i.-; c. L-.. . C6 Analyze for: O'Ftuorescein D Eosine J::0 Rhodamine WT D Other Ship cooler to: ------------------ OUL Please indicate stations where dye was visible in the field OUL use only use onl y for field technician use -use black ink only #CHAR LAB STATION STATION NAME PLACED COLLECTED

  1. REC'D NUM BER NUMBER WATER ~vc.ooJ DATE TlME DATE TIME REC'D \ D2413 ao1 -/), 'l}11Jrr Oi13CJ 10) ,~),'8 t0'2>5' n l qJ1ili'?-f v/t aJ /8' D2.y1i..t J.c.?-6 l i L-1 LJ 133~ /J l D2-~1S" ;2.c;>-k(L . ~/till,~ \1~/ 1cj,c/,<g-1'637 0 l D2-41t., JD3 -A 1) (I }1 i JS-,;io 10/JO) f6 o<?~ 0 l D2'-l11 ;>03 -.Bi ~)11) 18 L),;2W ie1e}1% .-b~-~ n I D2'-llH 2,ol..\-A q J 1).J ,y' !OS~ I olCf )1g 131d () I \);z_tn,'1

!:l.N..1-{) q),~)1'? iO~ to)q},'l I soi 0 0 -a *,, r e/ q/,,;1\~ llU -t: 0 a \.µe 11-3 --,.,{ ,vl('r I ~01J I 0 wtll-~ --Jo/ ,o/1'i, 13, 3-S-I 0 ~,1-7 --,o},o/rf"' I ~'-'\S-\ \ '~11 ~"'-,., h\ 11 -tl) rt> i I\ v:>r [)r., D +--( ,'\n<,; n \<;;:\A * (\/).L) ,...I

  • O.t J -0.iA0t1flMc&

R/~ -. D&48D This sheet filled out b y OUL.starr? Yes_ No~_, OUL Project No. / 7/1-( Date Analyzed:_J_Qfl.1/1.X Charts for samples pn this page proofed by OUL:___.,{£=--~~..::...... ---Analyzed By: IU/!.J{Jut Page ( of/ (J I,){/ OZARK UNDERGROUND LABORATORY, INC. 1572 Aley Lane Protem, MO 65733 (417) 78S-4289 fax (417) 78S-4290 email: contact@ozarkunderg roundlab.com SAMPLE COLLECTION DATA SHEET for FLUORESCENCE ANALYSIS Project (_ Week N9: JO -13 Samples Collected ~~:-:VA:*&:": Samples Shipped By: Samples Received By: _e_::.....o.., /1/.._._-.,~11,1_v.-4-/_.t1_...,(,""g_"""-'{l......_ ____________ _ Date Samples Shipped: /0 11 Date Samples Received: / 0-/5:/ t:J Time Samples Received~ / 'f:t1 d Return Cooler? Yes D No~ Bill to: l::!o~& Ar~rk

  • SendResultst o:yV'\.Ja..noPDCO:&!>N Oo@ lo..e.*!~'fK 14:: r;i ck. .cl) ...... Analyze for: D Fluorescein O Eosine ]i;'J Rhodamine WT D Other Ship cooler to: -----------~-----

OUL Please indicate stations where dve was visible in the [u!ld use only for field technician use -use black ink onlv #CHAR LAB STATION STATION NAME REC'D NUMBER NUMBER wo.-kf \ ;JO\,/). I ).cJ-B ' .7t>~ -AfL . l .103 -A l Jo3-B1 I .2..-ol.\,A I !lN1'8 .. 0 -Q~rt>,.{ 0 'D'2.Y~I l>.llll--3 0 b2-482 we11-~ 0 \J2ye; well-7 *s-/1;, ......... h\ I t, rf'; (\ .Dr /)r, r J r,-'--( ,'\.n\ n ,..,1. '"'"A . A/)_D ,.J

  • This sheet filled out by OUL.stam Yes_ No-.£_ OUL Project No. d I 1./ Date Analyzed:

l O {IJ/ {8 t . Charts for samples 01 this page proofed by OUL: Analyzed By: ~.I t ( J..J \ Page / of/ () ti,{/ PLACED DATE TIME }11 lit oq3q c:il II li'?-) j l.gJ 'l I II k'? \I\.\ 7 "I J" kl ~.;io f7111 )18 iS-d~ CJ Ill,?' 10~$"' [q ,~}r~ ;o'rir qi J;,1 \ \Ill~ ------' -, '(,.,,, < OUL use only COLLECTED

  1. WATER DATE TIME REC'D 1oi10J1<'t ti37 0 1011 Q) o'l o!.-Cj 0 relt,J,i .~N~ ... n 10JqJ, g 131d () 1oj "1]1'i. I 80~ 0 -s: D 10( l<J It}-t loOU I Jo/,o/'1; ,a. BS-l 10/10/tf--

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