ML19178A098

Restoration Project - Final Status Survey Release Record, Switchyard Survey Unit 10205, Final Report - Phase 1, Revision 1

ML19178A098
Person / Time
Site:	Zion  File:ZionSolutions icon.png
Issue date:	06/20/2019
From:	Yetter R ZionSolutions
To:	Office of Nuclear Material Safety and Safeguards
Shared Package
MML19178A106	List: ML19178A098 ML19178A100 ML19178A101 ML19178A102 ML19178A103 ML19178A104 ML19178A105 ML19178A107 ML19178A108 ZS-2019-0043, Transmittal of Revised Final Status Survey Report - Phase 1
References
ZS-2019-0043
Download: ML19178A098 (154)

Text

=11+++

()=1 1 3.630 ()+ 0.002 3.095 ()=3.622 / ()=1 1 1.091 ()+180.45914.458 ()=0.898 / ()=1 0.012 0.898 ()+0.00001 1.733+ 0.988 3.622 ()=3.494 /

3/29/2017 10:04:13AM

~§'~pe x-Gamma Analysis Report for 29-Mar-17-10012 L3-10205A-FRGC-OO 1 CV GAMMA SPECTRUM ANALYSIS Sample Identificatio n Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Descript i on Sample Number Fill Height Certificate Name Certificate Date : 29-Mar-17-10012

L3-10205A-FRGC-001CV

Sand 1.632E+03 grams : Default : 3/24/2017 8:55:00AM

3/29/2017 9:54:04AM

130G_Sand

Administrator

P11314 : 130G_Sand

600.0 seconds : 600.4 seconds : 0.06% : 3.00 : 120 -8192 : 120 -8192 : 1.000 keV : 11/10/2016

3/29/2017

i nitial 11/16/16 : 2617 : 1000.00 gram : Eu155-Na22

12/22/2008 12: 00: 00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2017 10:04:06AM Peak Analys i s From Channel Peak Analysis To Channel : 120 : 8192 Page 1 of6 3/29/2017 10:04: 13AM Page 2 of6 Analysis Report for 29-Mar-17-10012 L3-10205A-FRGC-001 CV Peak Energy ROI No. (keV) start 1 238.71 949 -2 250.69 999 -3 295.21 1177 -4 352.15 1402 -5 609.20 2430 -6 1461.06 5834 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma ROI end 959 1006 1185 1413 2439 5851 Peak Centroid 954.40 1002.26 1180 .11 1407 .. 60 2434.85 5842.19 No background subtract performed on this spectrum.

Net Peak Net Area Continuum Area Uncertainty Counts 3.16E+Ol 9.39 2.24E+Ol 8.00E+OO 4.01 4.00E+OO 1.54E+Ol 5.07 4.57E+OO 3.50E+Ol 7.75 9.98E+OO 1.36E+Ol 5.38 6.36E+OO 7.50E+Ol 9.00 2.00E+OO NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCi/grams)

Uncertainty K-40 0.99 1460.82

• 10.66 1.85E+OO 2.36E-01 Pb-212 0,99 115 .18 0.60 238.63

• 43.60 5.26E-02 1.62E-0 2 300.09 3.30 Bi-214 0.99 609.32

• 45.49 4.25E-02 1. 69E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1. 63 1238.12 5.83 FWHM (keV) 0.30 0.27 0.83 0.47 0.34 0.45 Analysis Report for 29-Mar-17-10012 L3-10205A-FRGC-OO 1 CV Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1280.98 1377. 67 1385. 31 1401.52 1407.99 1509.2 1 1661.2 7 1729.59 1764.49 1847.43 2 118.51 Pb-214 0.99 2 41.99 2 95.22 351.93 785.96 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000 keV Nuclide confidence index threshold

= 0.30 Errors quoted at 1.000sigma 3/29/2017 10:04:13AM Page3 of6 Yield(%) Activity Activity (pCilgrams)

Uncertainty

1. 43 3.99 0.79 1. 33 2.39 2.13 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 6.96E-02 2.36E-02 35.60 9.36E-02 2.20E-02 1. 06 INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Pb-21 2 Bi-214 Pb-214 Nuclide Id Confidence 0.991 0.999 0.999 0.996 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCi/grams) 1.85E+OO 5.26E-02 4.25E-02 8.24E-02 @ = nuclide c ontains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma Wt mean Comments Activity Uncertainty 2.36E-01 1.62E-02 1.69E-02 1.61E-02 3/29/2017 10:04:13AM Analysis Report for 29-Mar-17-10012

+ L3-10205A-FRGC-001 CV Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) 2 250.69 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : . 3/29/2017 10:04: 06AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 1.33333E-02 Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCUgrams) (pCi!grams)

BE-7 477.60 10.44 1.53E-01 3.33E-01 3.33E-01 K-40 1460.82

• 10.6 6 1.85E+OO 2.77E-01 2.77E-01 Co-60 1173.23 99.8 5 1.0lE-02 3.58E-02 4.05E-02 133'.::.49 99.98 1. 4 7E-02 3.58E-02 Nb-94 702. 65 99.81 -1.65E-02 2.2'7E-0 2 2.71E-0 2 871.09 99.89 -4.12E-02 2.27E-0 2 Ag-108m 79 .13 6.60 2.29E-01 2. 71E-02 6.15E-01 433.94 90.50 8.90E-03 2. 71E-02 614.28 89.80 -4.18E-02 3.60E-02 722. 94 90.80 -l.58E-03 3.18E-02 Sb-125 176.31 6.84 -2.37E-01 9.07E-0 2 2.59E-01 380.45 1. 52 5.17E-01 1.47E+OO 427.87 2 9.60 4.19E-02 9.07E-02 463.36 10.49 1.52E-01 2.52E-01 600.60 17.65 2.19E-02 1.56E-01 606.71 4.98 7.2 8E-01 8.55E-01 635.95 11. 22 1. llE-01 2.64E-01 671.44 1. '7 9 7.45E-02 1.77E+OO Page 4 of6 Tolerance Nuclide 3/29/2017 10:04:13AM Page 5 of6 Analysis Report for 29-Mar-17-10012 L3-10205A-FRGC-001 CV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCl!grams) (pCilgrams) (pCi/grams)

Ba-133 79.61 2.65 -2.64E-01 4.51E-02 l.42E+OO 81. 00 32.90 2.28E-02 l.09E-01 276.40 7.16 l.58E-01 3.44E-01 302.85 18.34 2.76E-02 l.07E-01 356.01 62.05 -2.61E-02

4. 51E-02 383.85 8.94 -5.66E-02

1. 96E-01 Cs-134 475.36 1. 48 8.65E-03 4.03E-02 2.28E+00 563.2 5 8.34 7.67E-02 3.36E-01 569.33 15.3 7 -l.08E-01 l.59E-01 604.72 97.62 3.65E-03 4.03E-02 795.86 85.46 1. 02E-02 4.31E-02 801.95 8.69 -2.07E-01 3.87E-01 1038.61 0.99 l.05E+OO 2.84E+OO 1167.97 1. 79 -l.15E-01 l.83E+OO 1365.19 3.0 2 -4.44E-0 2 l.29E+OO Cs-137 661.66 85.10 -l.77E-02 3.68E-02 3.68E-02 Eu-152 121. 78 28.67 -2.75E-03 7.22 E-02 7.22E-02 244.70 7.61 -1.62E-02 3.29E-01 295.94 0.45 2.05E+OO 5.74E+OO 344.2 8 26.60 3.34E-0 2 9.45E-02 367.79 0.86 8.22E-01 2.65E+OO 411.12 2.24 1.62E-01 1. 08E+00 443.96 2.83 l.48E-01 9.05E-01 488.68 0.42 2.40E-02 5.62E+OO 563.99 0.49 2.66E+OO 5.70E+OO 586.2 6 0.46 5.17E-Ol 6.97E+OO 678.62 0.47 l.87E+OO 6.09E+OO 688.67 0.86 l. llE+OO 3.51E+OO 719.35 0.28 -4.81E+OO 8.36E+OO 778.90 1 2. 96 -1. 2 2E-01 1. 90E-01 810.45 0.32 -9.31E+OO 8.87E+OO 867.37 4.2 6 3.55E-03 4.77E-01 919.33 0.43 -9.08E-01 9.50E+OO 964. 08 14.65 -l.84E-01 2.78E-01 1085.87 10.24 2.49E-01 4.05E-01 1089.74 1. 73 l.2 7E+OO 2. 72E+OO 1112.07 13. 69 -6.57E-0 2 2.72E-01 12 12.95 1. 43 1.77E+OO 3.02E+OO 1 2 49.94 0.19 1. 62E+OO 2.03E+Ol 1299.14 1. 63 -4.16E-02 2.43E+OO 1408.01 21. 07 3.63E-02 1.35E-01 1457.64 0.50 4.00E+Ol 2.3 8E+Ol 1528.10 0.2 8 l.93E+OO 9.32E+OO Eu-154 123.07 40.40 -2.05E-03 5.28E-02 5.28E-02 2 47.93 6.89 -l.84E-01 3.33E-01 591.76 4.95 1.25E-01 4.62E-Ol 692.4 2 1. 78 1.78E-01 l.76E+OO 723.30 2 0.06 2.25E-02 1.50E-01 756.80 4.52 2.12E-01 6.60E-01 873.18 12.08 -l.89E-03 l.88E-01 996.2 9 1 0.48 -l.39E-01 2.39E-01 3/29/2017 10:04:13AM Page 6 of6 Analysis Report for 29-Mar-17-10012 L3-10205A-FRGC-OO 1 CV Nuclide Energy Yield(%) Activity Nuclid e MDA LineMDA Name (keV) (pCl/grams) (pCilgrams) (pCi/grams)

Eu-154 1004.76 18.01 2.32E-02 5.2 8E-02 1.74E-01 1274.43 34.80 -4.19E-02 9.27E-02 1596.48 1. 80 -3.53E,...01 1.20E+OO Eu-155 45.30 1. 31 6.86E-02 1.05E-01 6.13E+OO 60.01 1. 22 1.70E+00 7.09E+OO 86.55 30.70 -2.63E-02 1.0SE-01 105.31 2 1.10 -1.83E-02

1. llE-01 Ra-22 6 186.21 3.64 1.65E-01 5.56E-01 5.56E-Ol Pa-231 2 7.36 10.30 O.OOE+OO 7.35E-02 7.35E-0 2 2 83.69 1. 70 4.15E-02 1. 33E+OO 3 00.07 2.47 -6.82E-02 8.llE-01 3 02.65 2.2 0 2.04E-01 8.95E-01 330.06 1. 40 3. 96E-01 1.77E+OO U-235 143.76 10.96 1.16E-01 3.66E-02 2.04E-01 163.33 5.08 1.38E-01 4.07E-01 185.71 57.2 0 3.06E-02 3.66E-0 2 2 02 .11 1. 08 -8.43E-01 1.70E+OO 2 05.3 1 5.01 1. 72E-01 4.00E-01 Am-241 59.54 35.90 7.18E-02 2.48E-01 2.48E-01 + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value Is Inconsistent with Currie MDA at 95% confidence level 60 55 50 45 1000 2000 3000 ROI Type: 1 0000002617 .CNF 4000 channel 5000 Live Tille :600.000 sec Real Ti11e :600.380 sec start: 1: -0.0(kev) stop : 8192: 2047 .8(kev) Acq. start :wed Mar 29 09: 54: 04 2017 6000 7000 8000 3/29/2017 10:16:42AM

~~~pex-Gamma Analysis Report for 29-Mar-17-10013 L3-10205A-FRGC-002CV GAMMA SPECTRUM ANAL YS/S Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Fill Height Certificate Name Certificate Date : 29-Mar-17-10013

L3-10205A-FRGC-002CV

Sand 1.594E+03 grams : Default : 3/24/2017 9:00:00AM

3/29/2017 10:06:34AM

130G_Sand

Administrator

P11314 : 130G_Sand

600.0 seconds : 600.4 seconds : 0.06% : 3.00 : 120 -8192 : 120 -8192 : 1.000 keV : 11/10/2016

3/29/2017

initial 11 /16/16 : 2619 : 1000.00 gram : Eu155-Na22

12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2017 10:16:36AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Pagel of6 3/29/2017 10:16:42AM Page 2 of6 Analysis Report for 29-Mar-17-10013 L3-10205A-FRGC-002CV Peak No. Energy (keV) ROI start ROI end 1 2 238.53 1461.19 947 -958 5833 -5851 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma Peak Centroid 953.72 5842. 72 No background subtract performed on this spectrum.

Net Peak Net Area Continuum Area Uncertainty Counts 4.36E+01 9.76E+Ol 8.34 10.59 1.04E+Ol 4.45E+OO NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) K-40 0.97 1460.8 2 Pb-212 0.99 115 .18 238.63 300.09 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000 keV Nuclide confidence index threshold

= 0.30* Errors quoted at 1.000sigma Yield(%) 10.66 0.60 43.60 3.30 Activity (pCilgrams) 2.46E+OO 7.44E-02 Activity Uncertainty 2.87E-01 1.54E-02 FWHM (keV) 0.59 0. 71 3/29/2017 10:16:42AM Analysis Report for 29-Mar-17-10013

+ L3-10205A-FRGC-002CV Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel PeakN~. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : 3/29/2017 10:16:36AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCUgrams) (pCi/grams) (pCi/grams)

BE-7 477.60 10.44 8.90E-02 3.03E-01 3.03E-01 K-40 1460.8 2

• 10.66 2.46E+OO 3.99E-01 3.99E-01 Co-60 1173.2 3 99.85 -1. 72E-03 3.12E-02 4.32E-02 1332.49 99.98 1.00E-0 2 3.12E-02 Nb-94 702. 65 99.81 -1.2 1E-03 2.73E-02 2.78E-02 871.09 99.89 O.OOE+OO 2.73E-0 2 Ag-108m 79.13 6.60 1.90E-01 2.07E-02 6.54E-01 433.94 90.50 -6.44E-03 2.07E-02 614.28 89.80 -1.84E-02 3.49E-02 722.94 90.80 8.07E-03 3.25E-02 Sb-125 176.31 6.84 -1.41E-01 8.19E-02 2.65E-01 380.45 1. 52 -1.13E+OO 1.18E+OO 427.87 29.60 1.05E-02 8.19E-02 463.36 10.49 -3.42E-01 2.38E-01 600.60 17.65 1. 43E-02 1. 54E-01 606.71 4.98 3.14E-01 7.40E-01 635.95 11. 22 2.28E-01 3.03E-01 671. 4 4 1. 79 1.13E+OO 1.76E+00 Ba-133 79.61 2.65 1.37E-01 4.76E-02 1.55E+OO Page4 of6 Tolerance Nuclide 3/29/2017 10:16:42AM Page 5 of6 Analysis Report for 29-Mar-17-10013 L3-10205A-FRGC-002CV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCl/grams) (pCUgrams) (pCl/grams)

Ba-133 81. 00 32.90 -4.26E-02 4.76E-02 1.04E-01 276.40 7.16 -4.0lE-02 2.47E-01 302.85 18.3 4 -8.38E-03 1.1 7E-01 356.01 62.05 -4.94E-0 2 4.76E-02 383.85 8.94 -5.05E-02 2.2 7E-01 Cs-134 475.36 1. 48 3.60E-01 3.54E-02 1. 87E+OO 563.25 8.34 -9.83E-02 2.86E-01 569.33 15.37 -8.59E-02 1.56E-01 604. 72 97.62 -2.21E-0 3 3.54E-0 2 795.86 85.46 -9.26E-03 4.54E-0 2 801.95 8.69 1. 06E-01 4.24E-01 1038.61 0.99 6.42E-01 2.39E+OO 1167.97 1. 79 -7.37E-01 l.88E+OO 1365.19 3.02 -3.82E-01 8.19E-01 Cs-137 661.66 85.10 l.16E-0 2 3.40E-02 3.40E-0 2 Eu-15 2 121.78 2 8.67 -4.22E-02 7.65E-0 2 7.65E-0 2 244.70 7.61 l.60E-01 3.38E-0 1 295.94 0.45 6.54E-01 6. llE+OO 344.2 8 2 6.60 4.06E-02 8.59E-02 367.79 0.86 4.27E-02 2.36E+OO 411.12 2.24 l.35E-0 1 9.20E-01 443.96 2.83 -7.53E-02 7.68E-01 488.68 0.42 -6.24E-01 5.55E+00 563.99 0.49 l.71E+OO 5.05E+OO 586.26 0.46 8.53E+OO 9.23E+OO 678.62 0.47 -2.18E+OO 5.99E+OO 688.67 0.86 -2.71E+OO 3.84E+OO 719.35 0.28 5.85E+OO 1.06E+Ol 778.90 12. 96 -l.66E-02 2.30E-01 810.45 0.32 -l.15E+Ol 9.97E+OO 867.37 4.26 -2.29E-Ol 5.94E-01 919.33 0.43 2.44E+OO 8.84E+OO 964.08 14.65 2.16E-01 3.68E-01 1085.87 10.2 4 l.49E-0 1 3.31E-01 1089.74 1. 73 4.73E-02 1. 84E+OO 1112.07 13.69 -l.67E-01 2.51E-0 1 1212.95 1.43 O.OOE+OO 2.56E+OO 1249.94 0.19 l.43E+Ol 2.94E+Ol 1 2 99.14 1. 63 -7.00E-01 1.46E+OO 1408.01 2 1. 07 -l.16E-02 l.55E-01 1457.64 0.50 5.65E+Ol 2.79E+Ol 1523.10 0.2 8 O.OOE+OO 2.84E+OO Eu-154 1 23.07 40.40 2.lOE-02 5.58E-02 5.58E-02 247.93 6.89 -7.lOE-02 3.42E-01 591.76 4.95 3.31E-0 2 3.91E-01 692.42 1. 78 2.2 4E-0 2 l.62E+OO 723.30 2 0.06 3.86E-02 1. 4 7E-01 756.80 4.52 9.57E-02 6.46E-01 873.18 12.08 3.2 6E-02 2.41E-01 996.29 10.48 -2.45E-02 3.54E-01 1004.76 18.01 9.17E-0 2 1. 89E-01 1 274.43 34.8 0 -4.07E-0 2 7.BOE-02 3/29/2017 10:16:42AM Page 6 of6 Analysis Report for 29-Mar-17-10013 L3-10205A-FRGC-002CV Nuclide Energy Yield(%) Activity Nuclid e MDA LineMDA Name (keV) (pCilgrams) (pCi/grams) (pCl/grams)

Eu-154 1596.48 1. 80 -3.25E+OO 5.58E-02 2.00E+OO Eu-155 45.30 1. 31 7.67E-01 1.0lE-01 6.19E+OO 60.01 1.22 3.28E+OO 6.42E+OO 86.55 30.70 1.54E-02 1.07E-0 1 105.31 21.10 -7.12E-02 1.0lE-01 Ra-226 186.21 3.64 5.89E-01 5.63E-01 5.63E-01 Pa-23 1 27.36 10.3 0 O.OOE+OO 7.53E-02 7.53E-02 2 83.69 1. 70 3.72E-01 1.28E+OO 300.07 2.47 -4.86E-01 8.59E-01 30 2.65 2.20 -1.lOE-01 9.49E-01 330.06 1. 40 4.33E-01 1.62E+OO U-23 5 143.76 10. 96 -1.06E-0 2 3.53E-02 1. 81E-01 1 63.33 5.08 7.45E-02 3.67E-01 185.71 57.2 0 2.89E-02 3.53E-02 202 .11 1. 08 -l.57E+OO 1.96E+OO 205.31 5.01 6.39E-02 4.58E-01 Am-241 59.54 35.90 1. 40E-02 2.05E-01 2.05E-01 + = Nuclide identified during the nuclide identification

.. = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level V} ..... C: 60 55 50 45 40 35 8 30 1000 2000 ROI Type: 1 3000 0000002619 .CNF 4000 channel 5000 Live Tine :600.000 sec Real Tine :600.350 sec Start: 1: -0.0(kev)

Stop : 8192:2047

.8(keV) Acq. start :wed Mar 29 10:06:34 2017 6000 7000 8000 3/29/2017 10:29:03AM

~~~pex-Gamma Analysis Report for 29-Mar-17-10016 L3-10205A-FRGC-003CV GAMMA SPECTRUM ANAL YS/S Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Fill Height Certificate Name Certificate Date : 29-Mar-17-10016

L3-10205A-FRGC-003CV

Sand 1.619E+03 grams : Default : 3/24/2017 9:05:00AM

3/29/2017 10: 18:55AM : 130G_Sand

Administrator

P11314 : 130G_Sand

600.0 seconds : 600.3 seconds : 0.05% : 3.00 : 120-8192 : 120 -8192 : 1.000 keV : 11/10/2016

3/29/2017

initial 11 /16/16 : 2620 : 1000.00 gram : Eu155-Na22

12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2017 10:28:58AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Page I of6 3/29/2017 10:29:03AM Page 2 of6 Analysis Report for 29-Mar-17-10016 L3-10205A-FRGC-003CV Peak Energy ROI No. (keV) start 1 2 38.51 948 -2 609.66 2432 -3 1460.88 5835 -M = First peak in a multiplet region m = other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma ROI end 958 2 441 5849 Peak Centroid 953.63 2 436.67 5841. 44 No background subtract performed on this spectrum.

Net Peak Net Area Continuum Area Uncertainty Counts 5.60E+O l 8.67 8.02E+OO 1.70E+Ol 5.80 6.96E+OO 5.42E+Ol 9.22 l.08E+Ol NUCLIDE /DENT/FICA T/ON REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams)

Uncertainty K-40 1. 00 1460.82

• 10.66 1.34E+OO 2.36E-01 Pb-212 0.99 115 .18 0.60 23 8.63

• 43.60 9.40E-02 1.64E-0 2 300.09 3.30 Bi-214 0.99 609.32

• 45.49 5.36E-02 1. 85E-02 768.36 4.89 806.18 1. 2 6 934.06 3 .11 1120.2 9 14.92 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 FWHM (keV) 0.82 0. 78 1. 26 Analysis Report for 29-Mar-17-10016 L3-10205A-FRGC-003CV Nuclide Name Bi-2 14 Id Confidence 0.99 Energy (keV) 1401.52 1407.99 1509.21 1661.27 1729.59 1764.49 1847.43 2118.51 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000 keV Nuclide confidence index threshold

= 0.30 Errors quoted at 1.000sigma Yield(%) 1. 33 2.39 2 .13 1. 05 2.88 1 5.30 2.03 1.16 3/29/2017 10:29:03AM Page 3 of6 Activity (pCilgrams)

Activity Uncertainty INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Pb-212 Bi-214 Nuclide Id Confidence

1. 000 0.998 0.993 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) l.34E+OO 9.40E-02 5.36E-02 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma wt mean Comments Activity Uncertainty 2.36E-01 1.64E-02 l.85E-02 3/29/2017 10:29:03AM Analysis Report for 29-Mar-17-10016

+ L3-10205A-FRGC-003CV Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : 3/29/2017 10:28:58AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCl/grams) (pCi/grams) (pCi!grams)

BE-7 477.60 10.44 6.61E-02 2.78E-01 2.78E-01 K-40 1460.82

• 10.66 1.34E+OO 5.39E-01 5.3 9E-01 Co-60 1173.23 99.85 5.01E-03 2.76E-02 4. 71E-02 1 332.49 99.98 -1.34E-0 2 2.76E-02 Nb-94 702.65 99.8 1 1. 51E-02 2.69E-02 3.30E-02 871.09 99.89 1.10E-02 2.69E-0 2 Ag-108m 79.13 6.60 l.57E-01 2.50E-02 6.14E-0 1 433.94 90.50 4.52E-03 2.50E-02 614.2 8 89.80 -4.64E-02 4.30E-02 722. 94 90.80 -l.90E-04 3.70E-02 Sb-125 176.31 6.84 -3.82E-0 2 7.33E-02 2. 96E-01 380.45 1. 52 -1.47E-02 1.49E+OO 427.87 2 9.60 -3.46E-02 7.33E-02 463.36 10.49 2.07E-02 2.48E-01 600.60 17.65 -4.42E-02

1. 62E-01 606.71 4.98 9.26E-01 9.75E-01 635.95 11. 22 8.40E-0 2 2.38E-01 671. 44 1. 79 2.14E-0 2 1. 55E+OO Ba-133 79.61 2.65 3.51E-01 4.12E-0 2 1.49E+OO Page 4 of6 Tolerance Nuclide 3/29/2017 10:29:03AM Page 5 of6 Analysis Report for 29-Mar-17-10016 L3-10205A-FRGC-003CV Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (keV) (pCi/grams) (pCilgrams) (pC//grams)

Ba-133 81. 00 3 2.90 -1. 4 7E-01 4.12E-02 9.40E-0 2 276. 40 7.16 -2.30E-0 1 2.50E-01 302.85 18.34 -1.18E-01 1.20E-01 356.01 62.05 -3.85E-03 4.12E-02 383.85 8.94 1.46E-01 2.85E-01 Cs-13 4 475.36 1. 48 3.93E-01 2. 96E-02 1.94E+OO 563.2 5 8.34 -5.29E-02 2.38E-0 1 569.33 15.37 3. 96E-0 2 1.61E-01 604. 72 97.6 2 -2.28E-0 2 4.00E-02 795.86 85.46 -1.60E-02

2. 96E-02 801.95 8.69 1.80E-01 3.46E-01 1038.61 0.99 -6.85E-01 3.47E+OO 1167.97 1. 79 1.21E-01 2.55E+OO 1 365.1 9 3.02 -5.0lE-01 8.07E-01 Cs-137 661.66 85.10 2.74E-0 2 4.87 E-02 4.87E-02 Eu-15 2 121.78 28.67 1.72E-02 8.00 E-02 8.00E-02 2 44.70 7.61 -9.0lE-02 3.14E-01 2 95.94 0.45 3.81E+OO 6.45E+00 344.2 8 26.60 3.83E-02 9.20E-0 2 367.79 0.86 -7. 77E-01 2.32E+OO 411.12 2.2 4 2.29E-01 9. 72E-01 443. 96 2.83 8.66E-02 9.80E-01 488.68 0.4 2 4.65E+OO 6.42E+OO 563.99 0.49 -3.45E+OO 4.03E+OO 586.26 0.46 5.3 0E-01 7.98E+OO 678.62 0.47 4.50E-01 5.3 8E+OO 688.67 0.86 -1.54E+OO 2.66E+OO 719. 35 0.28 2.84E+OO 1. 04E+Ol 778.90 1 2.96 -8.16E-0 2 2.26E-01 8 10.45 0.32 -5.27E+OO 6.78E+OO 867.37 4.2 6 -5.65E-01 5.85E-01 919.33 0.43 -2.36E+OO 6.95E+OO 964.0 8 14.65 1.34E-01 2.89E-01 1085.87 10.24 -2.70E-02 3.06E-01 1089.74 1. 73 1. 49E+00 2.42E+00 1112.0 7 13.69 -4.37E-0 2 2.75E-01 1 2 12.95 1. 43 1.18E-01 3.2 7E+OO 1249.94 0.19 -3.12E+OO 1.2 1E+Ol 1299.14 1. 63 8.94E-01 2.18E+OO 1408.01 21. 07 -8.24E-02

1. 78E-01 1457.64 0.50 3.89E+Ol 2.32E+01 15 2 8.1 0 0.2 8 -1.13E+OO 1.09E+Ol Eu-154 123.07 40.40 5.93E-03 5.61E-02 5.61E-02 247.93 6.89 5.24E-02 3.19E-01 591.76 4.95 1.29E-01 5. llE-01 692.42 1. 78 7.93E-01 1. 52E+OO 723. 30 2 0.06 -2.87E-03 1.68E-01 756.80 4.52 1. 4 7E-01 6.06E-01 873.1 8 12.08 1.07E-01 2.37E-01 996.2 9 10.48 O.OOE+OO 3.17E-01 1004.7 6 18.01 2.32E-0 2 1.95E-01 1274.43 34.80 4.12E-0 2 1.0 0E-01 3/29/2017 10:29:03AM Page 6 of6 Analysis Report for 29-Mar-17-10016 L3-10205A-FRGC-003CV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

Eu-154 1596.48 1. 80 6.32E-01 5.61E-02 1.97E+OO Eu-155 45.30 1. 31 2.73E+OO 1.13E-01 6.18E+OO 60.01 1. 22 l.34E+OO 5.45E+OO 86.55 30.70 1.02E-02 1.13E-01 105.31 2 1.10 -4.45E-0 3 1.18E-01 Ra-2 2 6 186.2 1 3.64 4.2 7E-01 6.50E-01 6.50E-01 Pa-231 27.36 10.3 0 O.OOE+OO 7.41E-02 7.41E-02 283.69 1. 70 4.14E-01 1.46E+OO 300.07 2.47 -3.03E-01 9.98E-01 302.65 2.20 -4.93E-01 1.0SE+OO 330.06 1. 40 l.09E-01 l.63E+OO U-23 5 143.76 10. 96 7.18E-0 2 4.17E-02 1. 95E-01 163.33 5.08 -1.33E-01 3.34E-01 185.71 57.2 0 2.26E-02 4.17E-02 202 .11 1. 08 -5.0lE-02 l.88E+OO 205.31 5.01 -l.20E-01 4.2 0E-01 Am-241 59.54 35.90 -4.29E-02 1.75 E-01 1. 75E-01 + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 60 55 50 45 40 1000 2000 3000 ROI Type: 1 0000002620 .CNF 4000 channel 5000 Live Time :600.000 sec Real Time :600.290 sec start: 1: -0.0(kev) stop : 8192: 2047 .8(kev) Acq. start :wed Mar 29 10:18:55 2017 6000 7000 8000 3/29/2017 10:41 : 03AM ~§/fff.~pe x-Gamma Analysis Report for 29-Mar-17-10017 L3-10205A-FRGC-004CV GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Fill Height Certificate Name Certificate Date : 29-Mar-17-10017

L3-10205A-FRGC-004CV

Sand 1.820E+03 grams : Default : 3/24/2017 9:10:00AM

3/29/2017 10:30:54AM

130G_Sand

Administrator

P11314 : 130G_Sand

600.0 seconds : 600.3 seconds : 0.06% : 3.00 : 120 -8192 : 120 -8192 : 1.000 keV : 11/10/2016

3/29/2017

ir:,itial 11/16/16 : 2621 : 1000.00 gram : Eu155-Na22

12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2017 10:40:57AM Peak Analysis From Channel Peak Analysis To Channel : 1 20 : 8192 Page I of6 3/29/2017 10:41 : 03AM Page 2 of6 Analysis Report for 29-Mar-17-10017 L3-10205A-FRGC-004CV Peak Energy ROI No. (keV) start 1 238.72 949 -2 351.94 1402 -3 1460.98 5833 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma ROI end 960 1413 5850 Peak Centroid 954.45 1406.77 5841.86 No background subtract performed on this spectrum.

Net Peak Net Area Continuum Area Uncertainty Counts 4.25E+Ol 10.27 2.45E+Ol 2.27E+Ol 6.97 1.03E+Ol 8.0BE+Ol 9.37 2.15E+OO NUCLIDE /DENT/FICA TIO/\! REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1460.82

• 10.66 1.78E+OO 2.21E-01 Bi-211 0.88 351.07

• 13.02 l.48E-01 4. 72E-02 Pb-212 0.99 115 .18 0.60 238.63

• 43.60 6.35E-02 1.62E-02 300.09 3.3 0 Pb-214 1. 00 241. 99 7.25 295.22 18.42 351.93

• 35.60 5.43E-02 1. 73E-0 2 785.96 1. 06 FWHM (keV) 0.99 0.44 0.95 Analysis Report for 29-Mar-17-10017 L 3-10205A-FRGC-004CV

• = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000 keV Nuclide confidence index threshold

= 0.30 Errors quoted at 1.000sigma 3/29/2017 10:41 :03AM INTERFERENCE CORRECTED REPORT ? ? Nuclide Name K-40 Bi-211 Pb-21 2 Pb-214 Nuclide Id Confidence 0.996 0.886 0.999 1. 000 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis wt mean Activity (pCilgrams) l.78E+OO 1. 48E-01 6.35E-02 5.43E-02 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma wt mean Activity Uncertainty 2.21E-Ol 4. 72E-02 1.62E-02 l. 73E-02 Page 3 of6 Comments 3/29/2017 10:41:03AM Analysis Report for 29-Mar-17-10017

+ L3-10205A-FRGC-004CV Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : 3/29/2017 10:40:57AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCl!grams) (pCi!grams) (pCi/grams)

BE-7 477.60 10.44 1.84E-01 2.99E-01 2.99E-01 K-40 1460.82

• 10.66 1. 78E+00 2.59E-Ol 2.59E-01 Co-60 1173.23 99.85 -1. 2 6E-02 2.12E-0 2 3.63E-02 1332.49 99.98 4.39E-03 2.12E-0 2 Nb-94 70 2.65 99.8 1 1.58E-02 2.69E-02 3.02E-0 2 871.09 99.89 4.39E-03 2.69E-02 Ag-108m 79.13 6.60 2.28E-01 2.62E-02 6.59E-01 433.94 90.50 1.60E-02 2.62E-02 614.28 89.80 l.98E-02 4.33E-02 72 2. 94 90.80 7.43E-03 3.08E-02 Sb-1 2 5 176.31 6.8 4 -8.53E-02 7.38E-02 2.70E-01 380.45 1. 52 7.48E-02 1.42E+OO 427.87 2 9.60 -4.98E-02 7.38E-02 463.36 10.49 5.65E-0 2 2.38E-Ol 600.60 1 7.65 -4.83E-02 l.34E-01 606.71 4.98 8.2 6E-01 7.98E-01 635.95 11. 22 l.08E-01 2.51E-01 671.44 1. 79 -5.57E-01 l.32E+OO Ba-133 79.61 2.65 2.87E-01 4.l:E-02 1.56E+OO Page 4 of6 Tolerance Nuclide 3/29/2017 10:41: 03AM Page 5 of6 Analysis Report for 29-Mar-17-10017 L3-10205A-FRGC-004CV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCVgrams) (pCi/grams) (pCi/grams)

Ba-133 81. 00 32.90 -6.0 8E-02 4.l:E-02 1.05E-01 276.40 7.16 1.12E-01 2.94E-01 302.35 18.34 -1.05E-01 8.73E-02 356.01 62.05 -1.44E-02 4.17E-0 2 383.85 8.94 1.37E-02 2.31E-01 Cs-13 4 47 5.36 1. 48 7.49E-01 2.71E-02 1.94E+OO 563.2 5 8.34 9.31E-02 3.52E-01 569.33 15.37 -1.00E-01 1.60E-01 60 4. 72 97.62 -9.57E-02 2.71E-02 795.86 85.46 -2.25E-02 2.96E-02 801. 95 8.69 1.78E-01 3.21E-01 1 038.61 0.99 -1.56E+OO 3.38E+OO 1 167.97 1. 79 7.27E-01 2.llE+OO 1365.19 3.0 2 -1.76E-01 7.17E-01 Cs-137 661. 66 85.10 1.13E-02 3.50E-02 3.50E-0 2 Eu-152 121. 78 2 8.67 2.35E-02 7.70E-02 7.70E-02 244.70 7.61 8.60E-02 3.12E-01 295.94 0.45 5.02E-01 5.35E+OO 344.28 2 6.60 1.19E-02 8.79E-0 2 367.79 0.86 1. lOE+OO 2.38E+OO 411.12 2.24 1.95E-02 1.09E+OO 443.96 2.8 3 3.94E-01 6.73E-01 488.68 0.4 2 -8. 92E-01 5.55E+OO 563.99 0.49 -1.llE+OO 5.70E+OO 586.26 0.46 -1.28E+OO 6.97E+OO 678.62 0.47 -2.82E+OO 4.25E+OO 688.67 0.86 3.63E-0 1 3.15E+OO 719.35 0.28 -8.12E+O O 6.97E+OO 778.90 12. 96 6.64E-02 2.lOE-01 810.45 0.32 -2.26E+OO 9.09E+OO 867.37 4.26 -4.39E-02 5.2 0E-01 919.3 3 0.43 2.45E+OO 8.99E+OO 964.08 14.65 -1.44E-0 1 2.85E-01 1085.87 10.2 4 4.19E-02 3.87E-01 10 89.74 1. 73 9.20E-02 2.37E+OO 1112.07 13.69 -3.25E-01 2.20E-01 121 2.95 1. 43 -7.95E-01 2.81E+OO 1249.94 0.19 1.44E+Ol 2.24E+Ol 1299.14 1. 63 9.55E-01 2.67E+OO 1408.01 2 1. 07 -1.17E-01

1. 05E-01 1457.64 0.50 4.06E+Ol 2.22E+Ol 1528.10 0.28 8.65E-01 6.63E+00 Eu-154 123.07 40.40 -2.15E-02 5.1 8E-02 5.18E-02 247.93 6.89 -7.43E-02 2.79E-01 591.76 4.95 1.13E-01 5.40E-01 692.42 1. 78 4. llE-01 1.68E+OO 723. 3 0 20.0 6 8.59E-02 1.39E-01 756.8 0 4.5 2 1.56E-01 7.03E-01 873.1 8 1 2.0 8 3.61E-02 2.34E-01 996.2 9 10.48 8.34E-0 2 2. 96E-01 1004.76 18.0 1 1. 76E-02 2.03E-01 1274.43 34.80 4.27E-02 9.51E-02 3/29/2017 10:41: 03AM Page 6 of6 Analysis Report for 29-Mar-17-10017 L3-10205A-FRGC-004CV Nuclide Energy Yield(%) Activity Nuclid e MDA LineMDA Name (keV) (pCilgrams) (pCl/grams) (pCilgrams)

Eu-154 1596.48 1. 80 1.41E-01 5.1 8E-02 l.08E+OO Eu-155 45.30 1. 31 7.48E-01 1.09E-01 5.64E+OO 60.0 1 1. 22 -4.22E+OO 4.84E+OO 86.55 30.70 5.70E-02 l.12E-01 105.31 21.10 4.39E-02 l.09E-01 Ra-22 6 186.21 3.64 4.20E-01 6 .13E-0 1 6.13E-01 Pa-231 2 7.36 10.30 O.OOE+OO 6.59E-02 6.59E-02 283.69 1. 70 1.37E-01 1.2 6E+OO 300.07 2.47 -2.05E-01 7.3 5E-01 302.65 2.2 0 -6.31E-01 7.70E-Ol 330.06 1. 40 1. 45E+OO 1.67E+OO U-2 35 143.76 10.96 5 .13E-02 3.83E-02 1. 96E-Ol 163.33 5.08 1.05E-01 4.llE-01 185.71 57.2 0 2.2 3E-0 2 3.83E-02 2 02 .11 1. 08 -1.45E+OO 1.65E+OO 2 05.31 5.01 2.54E-02 3.97E-01 Am-241 59.54 35.90 -1.53E-01 1.66E-0 1 l.66E-01 + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 60 55 50 45 1000 2000 3000 ROI Type: 1 0000002621.CNF 4000 channel 5000 Live Time :600.000 sec Real Ti re :600.340 sec Start: 1: -0.0(kev) stop : 8192:2047

.8(kev) Acq. start :wed Mar 29 10: 30: 54 2017 6000 7000 8000 3/29/2017 10:59:05AM Analysis Report for 29-Mar-17-10018 L3-10205A-FRGC-005CV GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Fill Height Certificate Name Certificate Date : 29-Mar-17-10018

L3-10205A-FRGC-005CV

Sand 1. 757E+03 grams : Default : 3/24/2017 9:22:00AM

3/29/2017 10:48:56AM

130G_Sand

Administrator

P11314 : 130G_Sand

600.0 seconds : 600.3 seconds : 0.05% : 3.00 : 120-8192 : 120 -8192 : 1.000 keV : 11/10/2016

3/29/2017

initial 11/16/16 : 2623 : 1000.00 gram : Eu155-Na22

12/22/2008 12: 00: 00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2017 10:58:59AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Page I of6 3/29/2017 10:59:0SAM Page 2 of6 Analysis Report for 29-Mar-17-10018 L3-10205A-FRGC-005CV Peak Energy ROI No. (keV) start 1 2 38.72 949 -2 609.70 2432 -3 14 61. 02 5832 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma ROI end 959 2441 5851 Peak Centroid 954.46 2436.83 5842.03 No background subtract performed an this spectrum.

Net Peak Net Area Continuum Area Uncertainty Counts 5.97E+Ol 9.36 l.13E+Ol l.79E+Ol 5.83 6.06E+OO 9.41E+Ol 10.55 4.88E+OO NUCLIDE /DENT/FICA T/ON REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1460.82

• 10.66 2.15E+OO 2.58E-01 Pb-212 0.99 115.18 0.60 2 3 8.63

• 43.60 9.2 4E-02 l.63E-02 3 00.09 3.30 Bi-2 14 0.99 609.32

• 45.49 5.20E-02 1. 72E-02 768.36 4.89 806.18 1. 26 934.06 3 .11 1120.29 14.92 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 FWHM (keV) 0.81 0.69 0.87 Analysis Report for 29-Mar-17-10018 L3-10205A-FRGC-005CV Nuclide Name Bi-214 Id Confidence 0.99 Energy (keV) 1401.52 1407.99 1509.21 1661.2 7 1729.59 1764.49 1847.43 2118.51 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000 keV Nuclide confidence index threshold

= 0.30 Errors quoted at 1.000sigma Yield(%) 1. 33 2.39 2.13 1. 05 2.88 15.30 2.03 1.16 3/29/2017 10:59:05AM Page 3 of6 Activity (pCilgrams)

Activity Uncertainty INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Pb-21 2 Bi-214 Nuclide Id Confidence 0.994 0.999 0.991 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCi!grams) 2.lSE+OO 9.24E-02 5.20E-02 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma wt mean Comments Activity Uncertainty 2.58E-01 1.63E-02 1. 72E-02 3/29/2017 10:59: 05AM Analysis Report for 29-Mar-17-10018

+ L3-10205A-FRGC-005CV Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : 3/29/2017 10:58:59AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCilgrams) (pCilgrams)

BE-7 477.60 10.44 2.53E-01 3.58E-01 3.58E-01 K-40 1460.82

• 1 0.66 2.15E+OO 3.86E-0 1 3.86E-01 Co-60 1173.23 99.85 -2.69E-02 2.54E-02 3.05E-02 1 332.49 99.98 -2.22E-02 2.54E-02 Nb-94 702.65 99.81 -5.54E-03 1.98E-02 1.98E-02 871.09 99.89 1.86E-0 2 3.18E-02 Ag-108m 79.13 6.60 6.04E-01 2.45E-02 7.23E-01 433.94 90.50 1.29E-03 2.45E-0 2 614.28 89.80 -2.54E-02 4.23E-0 2 7 22.94 90.80 -4.09E-04 2.95E-02 Sb-125 176.31 6.84 1.66E-01 8.97E-02 3.16E-01 380.45 1. 52 7.33E-01 1.67E+00 427.87 29.60 4.56E-02 8.97E-02 463.36 10.49 1.59E-02 2.22E-01 600.60 17.65 1.54E-02 1.44E-01 606. 71 4.98 1. llE+OO 8.99E-01 635.95 11. 22 -5.68E-02 2.19E-01 671.44 1. 79 -8.30E-01 1.36E+OO Ba-133 79.61 2.65 1.12E+OO 3.86E-02 l.73E+OO Page 4 of6 Tolerance Nuclide 3/29/2017 10:59:05AM Page 5 of6 Analysis Report for 29-Mar-17-10018 L3-10205A-FRGC-005CV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCl/grams) (pCilgrams) (pCilgrams)

Ba-1 33 81. 00 32.90 -1.48E-01 3.86E-02 1.06E-01 276.40 7.16 5.07E-02 3.22E-01 302.85 18.34 6.12E-02 l.23E-01 356.01 62.05 -4.65E-02 3.86E-02 383.85 8.94 1. llE-01 2.79E-01 Cs-134 4:5.36 1. 48 1.71E+OO 3.81E-02 2.34E+OO 563.25 8.34 -2.74E-01 3.03E-01 569.33 15.37 l.35E-02 l.95E-01 604. 72 97.62 -1.35E-02 3.81E-02 795.86 85.46 3.55E-02 4.44E-02 801.95 8.69 5.79E-0 2 3.72E-01 1038.6 1 0.99 -2.43E-01 3. 51E+OO 1167.97 1. 79 3.30E-01 2.27E+OO 1365.19 3.0 2 l.54E-01 7.43E-'01 Cs-137 6 61. 6 6 85.10 l.51E-03 3.62E-02 3.62E-02 Eu-152 12 1.78 28.67 2.64E-02 7.44E-02 7.44E-02 2 44.70 7.61 4.28E-02 3.13E-01 2 95.94 0.45 4.54E-02 4.79E+OO 344.28 2 6.60 6.77E-03 8.31E-02 367.79 0.86 -4.14E-01 2.69E+OO 411.12 2.2 4 -5.75E-01 9.25E-01 443.96 2.83 -l.21E-01 6.97E-01 488.68 0.42 2.36E+OO 5.22E+OO 563.99 0.49 1. 33E+OO 5.61E+OO 586.2 6 0.46 7.92E+00 8.60E+OO 678.62 0.47 4.04E+OO 7.00E+OO 688.67 0.86 -1. OlE+OO 2.75E+OO 719.35 0.28 5.84E+OO 9.97E+OO 778.90 12.96 -2. llE-02 2.44E-01 810.45 0.32 3.51E+OO 7.80E+OO 867.37 4.26 -4.95E-Ol 6.51E-01 919.33 0.43 6.46E-0 1 6.40E+OO 964.08 14.65 -1. 37E-01 2.51E-01 1085.87 10.2 4 -9.16E-02 3.00E-01 1089.74 1. 73 6.86E-01 l.67E+OO 11 12. 07 13. 69 l.32E-01 2.53E-01 1 2 12.95 1. 43 -1. llE+OO 2.80E+OO 1249.94 0.19 -9.36E+OO l.79E+Ol 1299.14 1. 63 3.35E-01 2.37E+OO 1408.01 2 1.07 3.37E-02 l.26E-01 1457.64 0.50 4.58E+Ol 2.51E+Ol 1528.10 0.2 8 -9.18E+OO

1. OOE+Ol Eu-154 123.07 40.40 1.63E-02 5.0lE-02 5.0lE-02 247.93 6.89 8.83E-0 2 3. llE-01 591.76 4.95 2.lOE-01 5.2 6E-01 692.42 1. 78 -3. llE-01 l.40E+OO 723.30 2 0.06 3.87E-02 l.34E-01 756.80 4.52 -1.06E-01 5.86E-0 1 873.18 12.08 -1.75E-02 2.53E-01 996.2 9 10.48 -l.07E-01 2.92E-01 1004.76 1 8.01 l.41E-0 2 l.62E-01 1 274.43 3 4.80 -6.57E-0 2 1.09E-Ol 3/29/2017 10:59: 05AM Page 6 of6 Analysis Report for 29-Mar-17-10018 L3-10205A-FRGC-005CV Nuclide Energy Yie/d{°/o)

Activity NuclideMDA LineMDA Name (keV) (pCl/grams) (pCilgrams) (pCi/grams)

Eu-154 1596.48 1. 80 -7.2 8E-01 5.0lE-02 1.41E+OO Eu-155 45.30 1. 31 -8.50E-01 1.lOE-01 5.771;:+00 60.01 1. 22 -1.llE+OO 5.39E+OO 86.55 30.70 7.02E-02 1.llE-01 105.31 21.10 5.56E-02 1.lOE-01 Ra-22 6 186.2 1 3.64 3.0lE-01 5.88E-01 5.88E-01 Pa-23 1 2 7.36 10.30 O.OOE+OO 6. 83E-02 6.83E-02 2 83.69 1. 70 9.70E-03 1. 30E+OO 3 00.07 2.47 -2.2 7E-01 8. '7 6:E;-01 3 02.65 2.2 0 5.37E-01 1. 04E+OO 330.06 1. 40 1. 7 9E-02 1.68E+OO U-235 143.76 10.96 -2.21E-04 3.74E-02 1.86E-01 163.33 5.08 2.26E-0 1 4.lBE-01 185.71 57.2 0 1.lBE-02 3.74E-02 2 02 .11 1. 08 1.14E-01 1.85E+OO 2 05.31 5.0 1 -2.91E-01 4.06E-01 Am-241 59.54 35.90 -2.16E-01 1. 69E-01 1.69E-01 + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 60 55 50 45 40 35 1000 2000 ROI Type: 1 3000 0000002623 .CNF 4000 channel 5000 Live Time :600.000 sec Real Time :600.300 sec start: 1: -0.0(kev) stop : 8192:2047.S(kev)

Acq. start :wed Mar 29 10: 48: 56 2017 6000 7000 8000 3/29/2017 11:10:36AM . ......:!§~

~pex-Gamma Analysis Report for 29-Mar-17-10019 L3-10205A-FRGC-006CV GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Fill Height Certificate Name Certificate Date : 29-Mar-17-10019

L3-10205A-FRGC-006CV

Sand 1.688E+03 grams : Default : 3/24/2017 9:18:00AM

3/29/2017 11 :00:27 AM : 130G_Sand

Administrator

P11314 : 130G_Sand

600.0 seconds : 600.4 seconds : 0.06% : 3.00 : 120-8192 : 120 -8192 : 1.000 keV : 11/10/2016

3/29/2017

initial 11 /16/16 : 2625 : 1000.00 gram : Eu155-Na22

12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2017 11 :10:30AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Page 1 of6 3/29/2017 11 :10:36AM Page 2 of6 Analysis Report for 29-Mar-17-10019 L3-10205A-FRGC-006CV Peak Energy ROI No. (keV) start 1 2 38.6 2 948 -2 3 51.77 1401 -3 583.29 232 7 -4 1460.88 5833 -M = First peak in a_ multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma ROI end 960 1412 2336 5851 Peak Centroid 954.07 1406.10 2 331. 28 5841.47 No background subtract performed on this spectrum.

Net Peak Net Area Continuum Area Uncertainty Counts 5.04E+Ol 10.76 2.46E+Ol 3.40E+Ol 7.68 9.95E+OO 1.77E+Ol 5.07 3.32E+OO 8.70E+Ol 9.33 O.OOE+OO NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDE$ Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams)

Uncertainty K-40 0.99 1460.82

• 10.66 2.07E+OO 2.39E-Ol Tl-208 0.99 583.19

• 85.00 2.77E-02 8.09E-03 Bi-211 0.92 351. 07

• 1 3.02 2.41E-01 5.76E-02 Pb-21 2 1. 00 115.18 0.60 2 38.63

• 43.60 8.12E-02 1.85E-02 300.09 3.30 Pb-214 0.99 2 41.99 7.25 2 95.2 2 13.42 351.93

• 35.60 8.80E-02 2. llE-02 785.96 1. 06 FWHM (keV) 0.94 0.36 0.43 1. 53 Analysis Report for 29-Mar-17-10019 L3-10205A-FRGC-006CV

• = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000 keV Nuclide confidence index threshold

= 0.30 Errors quoted at 1.000sigma 3/29/2017 11: 10:36AM INTERFERENCE CORRECTED REPORT ? ? ? = X = @ = Nuclide Name K-40 Tl-208 Bi-211 Pb-21 2 Pb-214 Nuclide Id Confidence 0.999 0.998 0.924 1.000 0.998 nuclide i s part of an undetermined solution nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 2.07E+OO 2.77E-02 2.41E-01 8.12E-02 8.80E-02 nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma Wt mean Activity Uncertainty 2.39E-01 8.09E-03 5.76E-02 l.85E-02 2. llE-02 Page 3 of6 Comments 3/29/2017 11: 10:36AM Analysis Report for 29-Mar-17-10019

+ L3-10205A-FRGC-006CV Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : 3/29/201 7 11:10:30AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCi/grams) (pCl/grams)

BE-7 477.60 10.44 1.47E-01 3.43E-01 3.43E-01 K-40 1460.8 2

• 10.66 2.07E+00 6.84E-02 6.84E-02 Co-60 1173.2 3 99.85 l.46E-02 4.23E-02 4.23E-02 1332.49 99.98 8.22E-03 4.44E-02 Nb-94 702.65 99.81 1.13E-02 2.85E-02 2.85E-02 871. 09 99.89 -3.lOE-02 3.31E-02 Ag-108m 79.13 6.60 1.29E-01 2.82E-02 6.76E-01 433.94 90.50 -3.50E-03 2.82E-0 2 614.28 89.80 -1.77E-02 4.05E-02 7 22.94 90.80 -7.73E-03 3.32E-02 Sb-125 176.31 6.84 -8.55E-02 8.77E-02 2.91E-01 380.45 1. 52 -3.54E-01 1.57E+OO 427.87 29.60 -2.25E-02 8.77E-02 463.3 6 10.49 -9.62E-04 2.24E-01 600.60 17.65 -1.74E-01 1.33E-01 606.71 4.98 1.02E+OO 8.83E-01 635.95 11. 22 6.88E-02 3.1 4E-01 671. 44 1. 79 2.06E-02 1.48E+OO Ba-13 3 79.61 2.65 3.37E-01 4.23E-02 1.66E+OO Page 4 of6 Tolerance Nuclide 3/29/2017 11:10:36AM Page 5 of6 Analysis Report for 29-Mar-17-10019 L3-10205A-FRGC-006CV Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (keV) (pCi/grams) (pCl/grams), (pCi/grams)

Ba-133 81. 00 32.90 -5.24E-02 4.23E-02 l.15E-01 2 76.40 7.16 1.60E-01 3.61E-01 3 02.85 18.34 -5.53E-0 2 1.0BE-01 356.01 62.05 -3.56E-02 4.23E-02 383.85 8.94 9.63E-02 2.49E-01 Cs-134 475.36 1. 48 6.32E-01 3.56E-02 2.24E+OO 563.2 5 8.34 l.50E-01 3.25E-Ol ,569.33 15.37 -1. 86E-02 1.60E-Ol 604. 72 97.62 -2.84E-0 2 3.56E-02 795.86 85.46 1.53E-02 4.05E-02 801. 95 8.69 -3.22E-01 3.32E-01 1038.61 0.99 -5.0SE-02 3.80E+OO 1167. 97 1. 79 -2.24E+00 1.88E+OO 1365.19 3.0 2 6.41E-01 1. 32E+OO Cs-137 661.66 85.10 -1.. 28E-02 3.33E-02 3.33E-02 Eu-152 121. 78 2 8.67 2.34E-02 7.45E-02 7.45E-02 244.70 7.61 1.30E-01 3.2GE-01 2 95. 94 0.45 -1.32E+OO 5.23E+OO 344.28 2 6.60 -3.0lE-02 8.47E-02 367.79 0.86 8.33E-01 2.57E+OO 411.12 2.24 -6.08E-01 9.63E-01 443.96 2.83 -8.58E-03 8.97E-01 488.68 0.4 2 -1.59E+OO 6.15E+OO 563.99 0.49 -3.36E+OO 4.97E+OO 586.26 0.46 4.42E+OO 8.07E+OO 678.62 0.47 -2.67E+OO 5.89E+OO 688.67 0.86 -3.05E-01 2.8oE+OO 719.35 0.28 -3.88E+OO 9.97E+OO 778.90 12. 96 -7.95E-03 2.85E-01 810.45 0.32 -1.83E+OO 8.12E+OO 867.37 4.2 6 -1. llE-01 8.31E-0 1 919. 33 0.43 -3.67E-01 6.66E+OO 964. 08 14.65 1.33E-01 3.00E-01 1085.87 10.2 4 -6.02E-02 3.12E-01 1089.74 1. 73 -4.38E-01 2.2 4E+OO 1112. 07 13.69 -1.75E-01 2.97E-01 1 2 12.95 1. 43 3.30E-01 2.55E+OO 1249.94 0.19 5.13E+OO 2.33E+Ol 1299.14 1. 63 1.14E+OO 2.35E+OO 1408.01 2 1.07 -l.14E-01 1.46E-Ol 1457.64 0.50 4.43E+Ol 2.41E+Ol 1528.10 0.28 4.66E+OO 1.27E+Ol Eu-154 123.07 40.40 -5.24E-03

5. llE-02 5. llE-0 2 247.93 6.89 1.15E-01 3.15E-01 591.76 4.95 2.34E-01 5.66E-01 692.42 1. 78 1.06E-01 1.59E+OO 723. 30 2 0.06 2.37E-03 1.56E-01 756.80 4.52 1.77E-01 4.81E-01 873.18 12.08 1.07E-0 2 3 .13E-01 996.29 10.48 -2.37E-01 3.97E-01 1004.76 18.01 9.89E-02 2.18E-01 1 2 74.43 34.80 2.17E-02 1.19E-01 3/29/2017 11:10: 36AM Page 6 of6 Analysis Report for 29-Mar-17-10019 L3-10205A-FRGC-006CV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCi!grams) (pCi!grams)

Eu-154 1 596.48 1. 80 -1.24E+OO 5. llE-02 1.70E+OO Eu-155 45.30 1. 31 2.21E+OO l.12E-01 6.61E+OO 60.0 1 1. 22 2.6 1 E-O l 6.47E+OO 86.55 3 0.70 -5.08E-0 2 1.12E-01 105.31 2 1.10 4.15E-02 1.19E-01 Ra-2 2 6 186.21 3.64 -8.55E-02 5.45E-0 1 5.45E-01 Pa-231 27.36 10.30 O.OOE+OO 7. llE-02 7. llE-0 2 283.69 1. 70 -6.99E-01 1.32E+OO 30 0.0 7 2.47 -2.98E-01 7.55E-01 302.65 2.2 0 -4.32E-01 8.75E-01 330.0 6 1. 40 -1.07E+OO 1. 80E+OO U-235 143.76 10.96 5.67E-02 3.38E-0 2 1. 95E-01 163.33 5.08 5.20E-02 3.94E-01 185.7 1 57.20 -8.27E-03 3.38E-02 20 2 .11 1. 08 -2.84E-01 l.90E+OO 205.31 5.01 8.41E-02 4.33E-01 Am-24 1 59.54 35.90 -6.9:3E-02 2.18E-01 2.18E-01 + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 60 55 50 45 40 GO I-1000 2000 ROI Type: 1 3000 0000002625 .CNF 4000 channel 5000 Live Tire :600.000 sec Real Tire :600.390 sec start: 1: -0.0(kev)

Stop : 8192: 2047. B(kev) Acq. start :wed Mar 29 11:00:27 2017 6000 7000 8000 3/29/2017 11 : 21 :38AM ~pex-Gamma Analysis Report for 29-Mar-17-10020 L3-10205A-FRGC-007CV GAMMA SPECTRUM ANAL YS/S Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Fill Height Certificate Name Certificate Date : 29-Mar-17-10020

L3-10205A-FRGC-007CV

Sand 1.634E+03 grams : Default : 3/24/2017 9:27:00AM

3/29/2017 11 :11 :30AM : 130G_Sand

Administrator

P11314 : 130G_Sand

600.0 seconds : 600.3 seconds : 0.05% : 3.00 : 120-8192 : 120 -8192 : 1.000 keV : 11/10/2016

3/29/2017

initial 11/16/16 : 2626 : 1000.00 gram : Eu155-Na22

12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2017 11 :21 :32AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 ' Page 1 of6 3/29/2017 11 :21 :38AM Page 2 of6 Analysis Report for 29-Mar-17-10020 L3-10205A-FRGC-007CV Peak Energy ROI No. (keV) start 1 238.72 949 -2 295.16 1176 -3 351.75 1400 -4 609.14 2430 -5 1461.16 5835 -M = First peak In a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma ROI end 959 1185 1411 2439 5851 Peak Centroid 954.44 1179.93 1406.03 2434.62 5842.60 No background subtract performed on this spectrum.

Net Peak NetArea Continuum Area Uncertainty Counts 4.20E+Ol 8. 71 1.40E+Ol 2.09E+Ol 5.88 6.07E+OO 3.58E+Ol 7.36 7.24E+OO 1.95E+Ol 6.12 7.50E+00 7.70E+Ol 9.88 7.04E+OO NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.98 1460.82

• 10.66 1.89E+OO 2.56E-Ol Pb-21 2 0.99 115 .18 0.60 2 38.63

• 4 3.60 7.00E-02 1.56E-02 300.09 3.30 Bi-214 0.99 609.32

• 45.49 6.07E-02 1.94E-0 2 768.36 4.89 806.18 1. 2 6 934.06 3.11 11 20.29 14.92 11 55.21 1. 63 1238.12 5.83 1280.98 1. 4 3 FWHM (keV) 0.60 1. 03 0. 96 0.52 0.42 Analysis Report for 29-Mar-17-10020 L3-10205A-FRGC-007CV Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1377. 67 13'85.31 1401.52 1407.99 1509.21 1661. 27 1 729.59 1764.49 1847.43 2118.51 Pb-214 0.99 2 4 1.99 2 95.22 351.93 785. 96 * "' Energy line found in the spectrum.

-"' Manually added nuclide. ? "' Manually edited nuclide. '~ * @ "' Energy line not used for Weighted Mean Activity Energy Tolerance

1.000 keV Nuclide confidence index threshold

= 0.30 Errors quoted at 1.000sigma 3/29/2017 11:21:38AM Page 3 of6 Yield(%) Activity Activity (pCilgrams)

Uncertainty 3.99 0.79 1. 33 2.39 2.13 1. 05 2.88 15.30 2.03 1.16 7.25 1 8.42 9.43E-02 2.76E-0 2 35.60 9.55E-02 2. llE-0 2 1. 06 INTERFERENCE CORRECTED REPORT Nuclide Name K-40 X Bi-211 Pb-21 2 Bi-214 Pb-214 Nuclide Id Confidence 0.981 0.928 0.999 0.998 0.997 ? = nuclide is part of an undetermined solution X "' nuclide rejected by the interference analysis Wt mean Activity (pCl/grams) 1.89E+OO 7.00E-02 6.0 7 E-02 9.50E-02 @ "' nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma Wt mean Comments Activity Uncertainty 2.56E-01 1.56E-02 1. 94E-02 1.67E-02 3/29/2017 11 :21 : 38AM Analysis Report for 29-Mar-17-10020

+ L3-10205A-FRGC-007CV Peak Locate Performed on Peak Locat e From Channel Peak Locat e To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : 3/29/2017 11 :21 :32AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (keV) (pCUgrams) (pCl/grams) (pCilgrams)

BE-7 477.60 10.44 1.66E-01 3.15E-01 3.15E-01 K-40 146 0.82

• 10.66 1.89E+OO 4.50E-01 4.50E-01 Co-60 11 73.23 99.85 3.57E-03 2.73E-02 3.69E-02 13 32. 49 99.98 -2.38E-02 2.73E-02 Nb-94 702.65 99.81 6.47E-03 3.06E-02 3.06E-02 871.09 99.89 1. 05E-02 3.55E-02 Ag-108m 79.1 3 6.60 1.50E-01 2.63E-02 6.09E-0 1 433.94 90.50 1.30E-02 2.63E-02 614.28 89.80 -2.04E-02 4.03E-02 722. 94 90.80 4.lOE-03 3.04E-02 Sb-125 176.31 6.84 1.22E-0 2 5.80E-02 2.90E-01 380.45 1. 52 -7.84E-01 1.35E+OO 427.87 29.60 -l.56E-01 5.80E-02 463.36 10.49 l.22E-0 1 2.09E-01 60 0.60 17.65 7.60E-02 2.06E-01 606. 71 4.98 3.91E-01 9.77E-01 635.95 11. 22 -l.41E-01 1.63E-01 671.44 1. 79 -2.76E-01 1.60E+OO Ba-133 79.61 2.65 2.19E-01 3.59E-02 1.45E+OO Page4 of6 Tolerance Nuclide 3/29/2017 11:21: 38AM Page 5 of6 Analys i s Report for 29-Mar-17-10020 L3-10205A-FRGC-007CV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCl/grams) (pCilgrams) (pCilgrams)

Ba-133 81.00 32.90 -8.52E-02 3.59E-02 1.04E-01 276.40 7.16 3.82E-02 3.20E-01 302.85 18.34 -2.42E-03 1.37E-01 356.01 62.05 -3.12E-0 2 3.59E-02 383.85 8.94 -2.84E-02 2.37E-01 Cs-134 475.36 1. 48 1. 31E+O O 3.77E-0 2 2.17E+OO 563.25 8.34 6.4 6E-02 3.15E-01 569.33 15.3 7 -1.2 0E-01 1.59E-01 604. 72 97.62 -1.35E-02 4.53E-0 2 795.86 85.46 2.55E-03 3.77E-02 80 1.95 8.69 1.35E-01 3.73E-01 1038.61 0.99 1. 2 5E+OO 3.06E+OO 1167. 97 1. 79 -2.31E+OO 1.70E+OO 1365.19 3.02 -1.70E+OO 9.2 6E-01 Cs-137 661.66 85.1 0 2.49E-03 3.32E-02 3.32E-02 Eu-152 121. 78 28.67 1.60E-02 6.68E-02 6.68E-02 244.70 7.6 1 -5.33E-02 3.15E-01 2 95. 94 0.45 2.33E+OO 6.52E+OO 344.2 8 2 6.60 -1.73E-02 8.56E-02 367.79 0.86 1.23E+OO 2.65E+OO 4 11.1 2 2.24 5 .13E-01 l.14E+OO 443. 96 2.83 3.66E-01 8.56E-01 488.68 0.42 2.95E+OO 6.85E+OO 563.99 0.49 2.03E+OO 5.13E+OO 586.2 6 0. 46 9.60E+OO 9.00E+OO 678.62 0.47 4.7 5 E-01 5.04E+OO 688.67 0.86 l.62E+O O 3.63E+OO 7 1 9.35 0.28 1.84E+O O 9.39E+OO 778. 9 0 12. 96 -2.92E-02 2.14E-01 810.45 0.32 1.62E+00 6.03E+OO 867.37 4.26 -5.68E-01 6.23E-01 919.33 0.43 3.98E+OO '.64E+OO 964.08 14.65 2.00E-02 2.69E-01 1085.87 10.24 -1.55E-0 2 3.03E-01 1089.74 1. 73 -2.92E-01 1.53E+OO 1112. 07 13. 69 l.58E-01 2.84E-01 1212.95 1. 43 1.20E-0 1 3.24E+OO 1249.94 0.19 -5.87E+OO 2.03E+Ol 1299.14 1. 63 3.62E-01 2.66E+OO 1408.01 21.07 1.21E-02 9.28E-02 1457.64 0.50 4.30E+01 2.54E+Ol 1528.10 0.28 2.89E+OO 1.08E+Ol Eu-15 4 123.07 40.40 -4.27E-02 4.46E-02 4.46E-02 247.93 6.89 1.15E-01 3.24E-01 591.76 4.95 -5.87E-02 5.27E-01 692.42 1. 78 -2.03E+OO

1. 28E+00 723. 30 2 0.06 -1.79E-02 1.31E-0 1 7 56.80 4.52 -1.34E-01 4.08E-01 873.18 12.08 2.2 6E-01 3.24E-01 996.2 9 10.48 1. 72E-01 3.30E-01 1 004.76 18.01 -3.64E-0 2 1.84E-01 1274.43 34.80 4.08E-02 9.95E-02 3/29/2017 11:21:38AM Page 6 of6 Analysis Report for 29-Mar-17-10020 L3-10205A-FRGC-007CV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCi/grams) (pCl/grams)

Eu-154 1596.48 1. 80 O.OOE+OO 4.46E-02 4.50E-01 E u-155 45.30 1. 31 1.99E+OO 1.13E-0 1 6.04E+OO 60.01 1. 22 -1.20E+00 5.60E+OO 86.55 30.70 6.46E-02 l.16E-01 1 05.31 2 1.10 8.05E-03 1.13E-01 Ra-22 6 186.2 1 3.64 8.67E-02 6.14E-01 6.14E-01 Pa-231 2 7.3 6 10.30 O.OOE+OO 7.34E-02 7.34E-02 283.69 1. 70 -1.12E+OO 1.26E+OO 300.07 2.47 -7.49E-01 9.47E-01 302.65 2.20 -4.90E-02 1.14E+OO 330.06 1. 40 5.76E-01 1.70E+OO U-235 143.76 10. 96 l.70E-02 3.82E-02 2.00E-01 163.33 5.08 l.47E-01 3.88E-01 185.7 1 57.2 0 2.78E-03 3.82E-02 202 .11 1. 08 1. 73E-01 1. 96E+OO 205.3 1 5.01 2.00E-02 4.37E-01 Am-24 1 59.54 35.90 8.48E-02 2.0 3E-0 1 2.03E-01 + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 60 55 50 45 1000 2000 3000 ROI Type: 1 0000002626.CNF 4000 channel 5000 Live Time :600.000 sec Real Time : 600 .320 sec start: 1: -0.0(kev)

Stop : 8192:2047.B(keV)

Acq. start :wed Mar 29 11:11:30 2017 6000 7000 8000 3/29/2017 11 :33:00AM ~~~pex-Gamma Analysis Report for 29-Mar-17-10021 L3-10205A-FRGC-008CV GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Fill Height Certificate Name Certificate .Date : 29-Mar-17-10021

L3-10205A-FRGC-008CV

Sand 1.649E+03 grams

Default : 3/24/2017 9:30:00AM

3/29/2017 11 :22:52AM : 130G_Sand

Administrator

P11314 : 130G_Sand

600.0 seconds : 600.3 seconds : 0.06% : 3.00 : 120-8192 : 120 -8192 : 1.000 keV : 11/10/2016

3/29/2017

initial 11/16/16 : 2627 : 1000.00 gram : Eu155-Na22

12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2017 11: 32: SSAM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Page 1 of6 3/29/2017 11 :33:00AM Page 2 0(6 Analysis Report for 29-Mar-17-10021 L3-10205A-FRGC-008CV Peak Energy ROI No. (keV) start 1 2 38.64 949 -2 3 51.5 3 1401 -3 1460.89 5833 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma ROI end 959 1409 5851 Peak Centroid 954.15 1405.14 5841.52 No background subtract performed on this spectrum.

NetPeak Net Area Continuum Area Uncertainty Counts 4.73E+O l 10.32 2.47E+Ol 1. 54E+O l 5.86 7.61E+OO 9.93E+O l 10.74 4.75E+OO NUCLIDE /DENT/FICA TJON REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\Z!ON LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams)

Uncertainty K-40 0.99 1460.82

• 10.66 2.42E+OO 2.82E-01 Bi-211 0.96 351.07

• 13.02 1. llE-01 4.33E-0 2 Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 7.79E-02 1. 81E-02 30 0.09 3.30 Pb-214 0.98 2 4 1.99 7.25 2 95.22 18.42 351.93

• 35.60 4.07E-02 1.58E-0 2 785.96 1. 06 FWHM (keV) 0.87 0.46 0.93 Analysis Report for 29-Mar-17-10021 L3-10205A-FRGC-008CV

• = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000 keV Nuclide confidence index threshold

= 0.30 Errors quoted at 1.000sigma 3/29/2017 11 :33:00AM INTERFERENCE CORRECTED REPORT Nuclide Name K-40 ? Bi-211 Pb-21 2 ? Pb-21 4 Nuclide Id Confidence 0.999 0. 967 1. 000 0.985 ? = nuclid e is part of an undetermined solution X = nuclid e rejected by the interference analysis Wt mean Activity (pCi/grams) 2.42E+OO l.llE-01 7.79E-02 4.07E-02 @ = nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma Wt mean Activity Uncertainty 2.82E-01 4.33E-02 1.81E-02 1.58E-02 Page 3 of6 Comments 3/29/2017 11 :33: 00AM Analysis Report for 29-Mar-17-10021

+ L3-10205A-FRGC-008CV Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : 3/29/2017 11 :32:54AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (keV) (pCl/grams) (pCi/grams) (pCilgrams)

BE-7 477.60 1 0.4 4 3.41E-02 3.30E-01 3.30E-01 K-40 1460.82

• 1 0.66 2.42E+OO 4.0 2E-01 4.02E-01 Co-60 1173.23 99.85 1. 56E-0 2 3.29E-02 3.46E-02 1332.49 99.98 1.21E-02 3.2 9E-02 Nb-94 702.65 99.8 1 -1.32E-02 2.45E-02 2.92E-02 871.09 99.89 -2.48E-02 2.45E-0 2 Ag-108m 79.13 6.60 -1.54E-01 3.02E-02 6.2 7E-0 1 433.94 90.50 1.45E-02 3.02E-02 614.2 8 89.80 -1.14E-02 4.15E-02 722.94 90.80 -6.03E-04 3.52E-02 Sl.J-125 176.31 6.84 4.39E-0 2 8.36E-02 2.98E-01 380.45 1. 52 -2.2 9E-01 1. 54E+OO 427.87 2 9.60 3.45E-0 2 8.36E-02 463.36 10.49 1.25E-03 2.80E-01 600.60 17.65 6.91E-02 1. 83E-01 606.71 4.98 6.89E-01 7.97E-01 635.95 11. 22 1.16E-01 2.78E-01 671. 44 1. 79 -7.18E-01

1. 45E+OO Ba-13 3 79.61 2.65 -9.74E-01 4.12E-02 1. 48E+OO Page 4 of6 Tolerance Nuclide 3/29/2017 1 1:33: 00AM Page 5 of6 Analysis Report for 29-Mar-17-10021 L3-10205A-FRGC-OOBCV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCl/grams) (pCilgrams) (pCi/grams)

Ba-133 81. 00 32.90 -1.07E-01 4.12E-02 1.0lE-01 2 76.40 7.16 7.09E-02 3.19E-01 302.85 18.34 5.99E-02 1.37E-0 1 356.0 1 62.05 -3.63E-02 4.12E-02 383.85 8.94 1. 71E-01 2.68E-01 Cs-134 475.36 1. 48 1.14E+O O 3.42E-02 2.18E+OO 563.25 8.34 -2.18E-02 3.23E-01 569.33 15.37 -4.53E-02 1.36E-01 604. 72 97.62 -3.2 3E-02 3.42E-02 795.86 85.46 7.46E-03 4.14E-0 2 801.95 8.69 -2.lOE-01 3.23E-01 1038.61 0.99 2.48E+OO 4.03E+OO 1167.97 1. 79 -8.36E-01 l.69E+OO 1365.1 9 3.02 2.46E-01 9.1 7E-01 Cs-137 661. 66 85.10 1.47E-02 3.53E-0 2 3.'j3E-02 Eu-152 121. 7 8 28.67 -::2.23E-02 7.55E-02 7.55E-0 2 244.70 7.61 -1.64E-01 2.97E-01 295.94 0.45 7.44E-01 5.52E+OO 344.2 8 2 6.6 0 7.88E-03 9.37E-02 367.79 0.86 -6.74E-01 3.19E+00 411.12 2.2 4 1.66E-01 1.15E+OO 443.96 2.8 3 1.49E-01 8.95E-01 488.68 0.42 1.64E+OO 5.36E+OO 563.99 0.49 1. 02E-01 5.64E+OO 586.26 0.46 -l.49E-01 7.07E+OO 678.62 0.47 -2.30E+OO 6.48E+OO 688.67 0.86 -2.90E-01 3.47E+OO 719.35 0.28 -5.llE+OO 8.27E+OO 778.90 12. 96 -2.93E-01 2.12E-01 810.45 0.32 1. 4 7E+OO 1.08E+Ol 867.37 4.26 5.lOE-02 6.17E-01 919.33 0.43 -7.0lE+OO 7.91E+OO 964.08 14.65 9.92E-03 2.58E-01 1 085.87 10.24 -3.25E-01 3.2 0E-01 1089.74 1. 73 -2.02E+OO 1.90E+OO 1112.0:' 1 3.69 2.65E-01 3.54E-01 1212.95 1. 43 -6.94E-01 3.2 1E+OO 1249.94 0.19 5.51E+OO 2. llE+Ol 12 99.1 4 1. 63 -1.16E-01 2.14E+OO 1408.01 21. 07 -3.14E-02 1.16E-01 1457.64 0.50 5.08E+Ol 2. 72E+Ol 1 528.10 0.28 1.91E+OO 9.22E+OO Eu-154 123.07 40.40 -9.34E-0 3 5.23E-02 5.23E-02 247.93 6.89 -3.80E-02 2.93E-01 591. 76 4.95 1.85E-01 5.22E-01 692.42 1. 78 -7.35E-01 1.63E+OO 723. 30 20.06 -4.71E-03 1.59E-01 756.80 4.52 -4.52E-03 5.2 9E-01 873.18 1 2.08 -1.49E-01 2.19E-01 996.29 10.48 -l.OlE-01 2.77E-01 1 004.76 18.01 -3.60E-0 2 2.00E-01 1274.4 3 3 4.80 4. 72E-0 2 1.05E-01 3/29/2017 11:33: 00AM Page 6 of6 Analysis Report for 29-Mar-17-10021 L3-10205A-FRGC-008CV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi!grams) (pCilgrams) (pCl!grams)

Eu-154 1 596.48 1. 80 3.lOE-01 5.2 3E-02 1. 50E+OO Eu-155 45.30 1. 31 -5.66E-01 1. llE-01 5.63E+00 60.01 1. 2 2 9.81E-01 6.70E+OO 86.55 3 0.70 7.2 4E-03 1. llE-01 105.31 2 1.10 8.64E-02 1.18E-01 Ra-22 6 186.21 3.64 6.18E-01 7.19E-0 1 7.19E-01 Pa-231 2 7.36 10.30 O.OOE+OO 7.2 7E-02 7. 27E-0:::'. 283.69 1. 70 -3.29E-01 1.05E+OO 300.07 2.47 3.31E-01 1.07E+OO 302.65 2.20 2.17E-01 1.14E+OO 330.0 6 1. 40 -7.38E-01 1.66E+OO U-23 5 1 43.76 10. 96 l.2 7E-01 4.44E-0 2 2.03E-01 163.33 5.08 2.00E-01 3.99E-01 185. 71 57: 2 0 2.22E-02 4.44E-0 2 202 .11 1. 08 -8.66E-01 1.94E+OO 205.31 5.01 8.36E-02 4.48E-01 Arn-241 59.54 35.90 -5.61E-02 2.2 6 E-01 2.26E-0 1 + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 60 55 50 45 40 35 1000 ROI Type: 1 ..-< 7 H .. 2000 3000 0000002627 .CNF 4000 channel 5000 Live Time :600.000 sec Real Time :600. 340 sec start: 1: -0.0(kev)

Stop : 8192: 2047. B(keV) Acq. start :wed Mar 29 11: 22: 52 2017 6000 7000 8000 3/29/2017 11:44:14AM ~F~pex-Gamma Analysis Report for 29-Mar-17-10022 L3-10205A-FRGC-009CV GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Fill Height Certificate Name Certificate Date : 29-Mar-17-10022

L3-10205A-FRGC-009CV

Sand 1.618E+03 grams : Default : 3/24/2017 9:35:00AM

3/29/2017 11 :34:06AM : 130G_Sand

Administrator

P11314 : 130G_Sand

600.0 seconds : 600.3 seconds : 0.05% : 3.00 : 120 -8192 : 120 -8192 : 1.000keV : 11/10/2016

3/29/2017

initial 11/16/16 : 2628 : 1000.00 gram : Eu 155-Na22 : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2017 11 :44:08AM Peak Analysis From Channel Peak Analysis To Channel : 1 20 : 8192 Page 1 of7 3/29/2017 11:44: 14AM Page 2 of? Analysis Report for 29-Mar-17-10022 L3-10205A-FRGC-009CV Peak Energy ROI No. (keV) start 1 238.66 949 -2 338 .13 1348 -3 351.91 1401 -4 583.00 2 325 -5 609.20 2430 -6 14 61. 00 5832 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma ROI end 960 1355 1411 2336 2 440 5850. Peak Centroid 954.22 1351.58 1406.64 2330.13 2434.83 5841.92 No background subtract performed on this spectrum.

Net Peak Net Area Continuum Area Uncertainty Counts 6.0lE+Ol 1 2.76 3.99E+Ol 1. 30E+Ol 5.39 8.00E+OO 1. 60E+Ol 6. 49 1.lOE+Ol 2.43E+Ol 6.67 7.66E+OO 2.33E+Ol 6.12 5.70E+OO 1.37E+02 12.38 4.75E+OO I\JUCLiDt:.

iDENTIF/CA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1460.82

• 10.66 3.41E+OO 3.41E-01 Tl-208 0.99 58 3.19

• 85.00 3.97E-02 1. llE-02 Bi-211 0.89 351.07

• 13. 02 1.18E-0 1 4.88E-02 Pb-21 2 1. 00 11 5 .18 0.60 238.63

• 43.60 1.0lE-01 2.2 9E-02 300.0 9 3.30 Bi-2 14 0.99 6 09.32

• 45.49 7.32E-02 1.97E-0 2 768.3 6 4.89 806.18 1. 26 93 4.06 3 .11 1120.2 9 14.92 FWHM (keV) 0.61 0. 72 0.67 1.17 1. 03 1. 24 Analysis Report for 29-Mar-17-10022 L3-10205A-FRGC-009CV Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1155.21 1238.12 1280.98 1377.67 1 385.31 1 401.52 1407.99 1509.2 1 166 1.27 1729.59 17 64.49 1 847.43 2118. 51 Pb-214 1. 00 241. 99 295.22 35 1.93 785.96 Ac-228 0.99 129.0 7 209.25 270.24 328.00 338.32 4 0 9.46 463.00 794.95 9 11.2 0 964. 77 968.97 1588.20 * = Energy line found in the spectrum.

• = Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000 keV Nuclide confidence index threshold

= 0.30 Errors quoted at 1.000sigma 3/29/2017 11: 44: 14AM Page 3 of7 Yield(%) Activity Activity (pCilgrams)

Uncertainty

1. 63 5.83 1. 43 3.99 0.79 1. 33 2.39 2.13 1. 05 2.88 15.30 2.03 1-.1 6 7.25 18.42 35.60 4.3 1E-02 1. 78E-02 1. 06 2.42 3.89 3.46 2.95 11. 27 1.07E-01 4.53E-0 2 1. 92 4.40 4.25 2 5.80 4.99 15.80 3.22 INTERFERENCE CORRECTED REPORT Analysis Report for 29-Mar-17-10022

? ? ? = X = L3-10205A-FRGC-009CV Nuclide Nuclide Name Id Confidence K-40 0.995 Tl-208 0.995 Bi-211 0.894 Pb-21 2 1. 000 Bi-2 1 4 0.999 Pb-21 4 1. 000 Ac-228 0.999 nuclide is part of an undetermined solution nuclide rejected by the interference analysis 3/29/2017 Wt mean Activity (pCilgrams) 3.41E+00 3.97E-02 1.lBE-01 1. OlE-01 7.32E-02 4.31E-02 1.07E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma 11:44:14AM Page 4 of7 Wt mean Comments Activity Uncertainty 3.41E-01 1. llE-02 4.BBE-02 2.2 9E-02 1.97E-02 1.78E-02 4.53E-02 3/29/2017 11 :44:14AM Analysis Report for 29-Mar-17-10022

+ L3-10205A-FRGC-009CV Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : 3/29/2017 11 :44:08AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (keV) (pCl/grams) (pCl/grams) (pCl/grams)

BE-7 477.60 10.44 2.21E-01 2.85E-01 2.85E-01 K-40 1 460.82

• 10.6 6 3.41E+00 4.0SE-01 4.08E-01 Co-60 1173.23 99.85 -1.78E-0 2 3.36E-02 5.00E-02 1 332.49 99.9 8 -3.2 3E-02 3.36E-02 Nb-94 702.65 99.8 1 1.16E-02 3.40E-02 3.40E-02 871.09 99.89 1.24E-02 4.16E-02 Ag-108m 79.13 6.60 2.93E-01 2.95E-02 6.56E-01 433.94 90.50 -2.12E-03 2.95E-0 2 614.28 89.80 -2.56E-02 4.67E-02 722. 94 90.80 -4.63E-02 4.60E-02 Sb-125 176.31 6.84 3.06E-03 8.30E-0 2 3.07E-01 380.45 1. 52 l.31E+OO 1.74E+OO 4 2 7.87 29.60 -9.52E-03 8.30E-0 2 463.36 10.49 8.53E-02 2.48E-01 600.60 17.65 -6.84E-02 l.45E-01 606.71 4.98 7.55E-01 9.43E-01 635.95 11. 22 -1.1 2E-01 2.48E-01 671.44 1. 79 -6.44E-02 1.48E+OO Ba-133 79.61 2.65 2.70E-01 4.2 7E-02 1.57E+00 Page 5 of7 Tolerance Nuclide 3/29/2017 11: 44: 14AM Page 6 of7 Analysis Report for 29-Mar-17-10022 L3-10205A-FRGC-009CV Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (keV) (pCl/grams) (pCilgrams) (pCilgrams)

Ba-133 81.00 32.90 -4.2 4E-02 4.27E-02 9.69E-02 2 76.40 7.16 1. 89E-01 3.54E-01 3 02.85 1 8.34 -3.39E-02 1.26E-01 356.01 62.05 -1.27E-02 4.27E-02 383.85 8.94 -3.85E-02 2.60E-01 Cs-134 475.36 1. 48 9.16E-01 4.0 0E-02 1.98E+OO 563.2 5 8.34 -8.73E-04 3.39E-01 569.33 1 5.37 -5.65E-03 1.80E-01 604. 72 97.62 -3.39E-0 2 4.0 0E~02 795.86 85.46 -3.33E-03 4.22E-02 801.95 8.69 -6.17E-02 4.04E-01 1 038.61 0.99 -5.75E+OO 3.8 1 E+OO 1167.97 1. 79 -4.04E+OO 2.37E+OO 1365.19 3.02 -5.43E-01 9.34E-01 Cs-13 7 661.66 85.10 1.65E-0 2 4.24E-02 4.2 4E-02 Eu-1 52 121. 78 2 8.67 -1.55E-02 8.64E-02 8.74E-02 244.70 7. 61 -4.92E-02 3.80E-01 295.94 0.45 2.13E+00 6.85E+OO 344.2 8 26.6 0 -2.20E-02 8.64E-0 2 367.79 0.86 1. OOE+OO 3.09E+OO 411.12 2.24 -5.98E-01 1.2 0E+OO 443. 96 2.83 2.07E-0 1 9.13E-01 488.68 0.4 2 3.55E+OO 6.59E+OO 563.99 0.49 3.17E-01 5.92E+OO 586.26 0.46 -4.94E+OO 1.07E+Ol 678.62 0.47 5.56E-01 4.45E+OO 688.67 0.86 2.44E-02 3.66E+OO 71 9. 35 0.2 8 -4.16E+OO 1.24E+Ol 778.9 0 1 2.96 1.97E-0 2 2.37E-01 810.45 0.3 2 9.52E-01 1.06E+Ol 867.37 4.26 -4.51E-01 7.76E-01 919.33 0.43 -2.70E+OO 8.39E+OO 964.08 14.65 2.52E-01 3.49E-01 1085.87 10.2 4 -3.77E-02 2.85E-01 1089.74 1. 73 8.69E-01 1.93E+OO 1112. 07 1 3.69 -7.56E-02 2.48E-01 1 2 12.95 1. 43 -7.65E-01 2.80E+OO 1249.94 0.19 -1.63E+Ol 2.90E+Ol 1299.14 1. 63 1.06E-0 1 2.32E+OO 1408.01 21. 07 -1.84E-0 1 1.6oE-01 1457.64 0.50 7.77E+Ol 3.22E+Ol 15 2 8.10 0.2 8 O.OOE+OO 2.80E+OO Eu-154 123.07 40.40 -4.07E-02 5.88E-02 5.88E-02 247.93 6.89 1.23E-01 3.50E-01 591. 7 6 4.95 2.32E-01 7.1 9E-01 692.42 1. 78 7.2 7E-01 2.05E+OO 723.30 2 0.06 -3.12E-02 2.12E-01 756.80 4.5 2 2.99E-01 7.68E-01 873.1 8 12.08 7.24E-02 3.36E-0 1 996.2 9 10.48 -2.80E-01 3.17E-0 1 10 04.76 18.01 1.60E-02 2.20E-01 1274.43 34.80 -2.99E-02 l.07E-01 3/29/2017 11:44: 14AM Page 7 of7 Analysis Report for 29-Mar-17-10022 L3-10205A-FRGC-009CV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCUgrams) (pCl/grams)

Eu-154 1596.48 1. 80 -2.02E+OO 5.88E-02 l.2 1E+OO Eu-155 45.30 1. 31 l.21E+OO 1.12E-01 6.97E+OO 60.01 1. 22 -8.42E-01 6.49E+OO 86.55 3 0.70 -3.31E-02 1.12E-01 105.3 1 2 1.10 6.59E-02 1.25E-01 Ra-2 2 6 186.21 3.64 5.0lE-02 6.38E-01 6.38E-01 Pa-231 2 7.36 10.30 O.OOE+OO 7.41E-02 7.41E-02 283.69 1. 70 -6.00E-01 1.2 1E+OO 300.07 2.47 -5.88E-01

1. OlE+OO 302.65 2.20 8.12E-02 1.llE+OO 330.06 1. 40 1.98E+OO 2.12E+OO U-235 143.76 10.96 -3.08£-02 4.05E-02 2.24E-01 163.33 5.08 4.2 6E-02 4.86E-01 185.71 57.20 1.23E-02 4.0SE-0 2 202 .11 1. 08 5.07E-01 2.17E+OO 205.31 5.01 -4.26E-01 4.14E-01 Am-241 59.54 35.90 2. llE-02 2.33E-01 2.33E-01 + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 60 55 50 45 40 ROI Type: 1 1000 2000 00~ 0"" ........... ' ' -' w I-X 3000 0000002628 .CNF 4000 Channel 5000 Live Time :600.000 sec Real Time :600.310 sec start: 1: -0.0(kev) stop : 8192: 2047 .8(kev) ACq. start :wed Mar 29 11:34:06 2017 6000 7000 8000 Analysis Report for 29-M ar-17-10024 L3-10205A-FRGC-010CV 3/29/2017 11 :55:33AM GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Fill Height Certificate Name Certificate Date : 29-Mar-17-10024

L3-10205A-FRGC-010CV

Sand

• 1.604E+03 grams Default

• 3/24/2017 10:10:00AM 3/29/2017 11 :45:25AM 130G_Sand Administrator P11314 130G_Sand 600.0 seconds

• 600.3 seconds : 0.06% : 3.00 : 120 -8192 : 120-8192 : 1.000 keV : 11/10/2016

3/29/2017

initial 11/16/16 : 2630 : 1000.00 gram : Eu155-Na22

12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2017 11 :55:27 AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Page 1 of6 Analysis Report for 29-Mar-17-10024 L3-10205A-FRGC-010CV Peak Energy ROI ROI No. (keV) start end 1 238.52 948 -961 2 351.85 1402 -1411 3 583.51 2328 -2337 4 911. 64 3639 -3649 5 1460.95 5833 -5850 M "" First peak in a multiplet region m "" Other peak in a multiplet reg ion F ""Fitted singlet Errors quoted at 1.000sigma 3/29/2017 11 :55:33AM Peak Net Peak Net Area Centroid Area Uncertainty 953.67 4.56E+Ol 9.98 1406.40 l.58E+Ol 6.17 2332.15 2.06E+Ol 5. 96 3644.00 1. 48E+Ol 4.21 5841.74 7.85E+Ol 9.65 No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLID ES Nuclide Id Energy Yield(%) Activity Page 2 of6 Continuum FWHM Counts (keV) l.94E+Ol 0. 92 9.20E+OO 0.55 6.44E+OO 0.40 1.23E+OO 0.36 4.50E+OO 0.90 Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1 460.82

• 10.66 l.97E+OO 2.56E-01 Tl-208 0.98 583.19

• 85.00 3.38E-02 1.00E-02 Bi-211 0.90 351.07

• 13. 02 1.17E-01 4.68E-02 Pb-212 0.99 115.18 0.60 238.63

• 43.60 7.73E-02 l.80E-02 300.09 3.30 Pb-214 0.99 241.99 7.25 295.22 18.42 351.93

• 35.60 4.30E-02 1. 71E-02 785.96 1. 06 Ac-228 0.99 129.07 2.42 209.25 3.89 Analysis Report for 29-Mar-17-10024 L3-10205A-FRGC-O 1 DCV Nuclide Id Energy Name Confidence (keV) Ac-228 0.99 270.24 328.00 338.32 409.46 463.00 794.95 911. 20 964.77 968. 97 1 588.20 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000 keV Nuclide confidence index threshold

= 0.30 Errors quoted at 1.000sigma 3/29/2017 11 :55:33AM Page 3 of6 Yield(%) Activity Activity (pCilgrams)

Uncertainty 3.46 2.95 11. 27 1. 9 2 4.40 4.25 25.80 1.l O E-01 3.1 6E-02 4.99 15.80 3.22 INTERFERENCE CORRECTED REPORT ? ? Nuclide Name K-40 Tl-208 Bi-211 Pb-212 Pb-214 Ac-228 Nuclide Id Confidence 0.997 0.984 0.908 0.998 0.999 0.991 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCi/grams) l.97E+OO 3*. 38E-02 1.17E-Ol 7.73E-02 4.30E-02 1.lOE-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma Wt mean Comments Activity Uncertainty 2.56E-01 1.00E-02 4.68E-02 1. 80E-02 1. 71E-02 3.16E-02 3/29/2017 11 :55:33AM Analysis Report for 29-Mar-17-10024

+ L3-10205A-FRGC-01 OCV Peak Locate Performed on Peak Locate From Chann el Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M "' First peak in a multiplet region m "' other peak in a multiplet region F "' Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : 3/29/2017 11:55:27AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (keV) (pCi!grams) (pCi/grams) (pCilgrams)

BE-7 477.60 10.44 8.99E-02 2.74E-01 2.74E-01 K-40 1460.82

• 10.66 1.97E+OO 3.97E-01 3.97E-Ol Co-60 1173.23 99.85 3.84E-03 3.39E-02 3.56E-02 1332.49 99.98 -l.93E-02 3.39E-02 Nb-94 702.65 99.81 9.59E-03 2.34E-02 2.34E-02 871.09 99.89 -4.33E-03

2. 71E-02 Ag-108m 79.13 6.60 3.81E-01 2.25E-02 6.85E-01 433.94 90.50 -2.03E-02 2.25E-02 614.28 89.80 -5.08E-02 3.57E-02 722. 94 90.80 5.46E-03 3.37E-D2 Sb-125 176.31 6.84 -1.45E-02 1.00E-01 2.87E-01 380.45 1. 52 -l.65E-01

1. 58E+OO 427.87 29.60 3.87E-02 1.00E-01 463.36 10.49 -1.61E-Ol 2.82E-01 600.60 17.65 8.84E-02 l.74E-01 606.71 4.98 6.44E-02 8.06E-01 635.95 11.1 2 1.66E-02 2.50E-01 671.4 4 1. 79 1.19E+OO 2. llE+OO Ba-133 79.61 2.65 9.64E-01 3.83E-02 1. 68E+OO Page4 of6 Tolerance Nuclide 3/29/2017 11:55:33AM Page 5 of6 Analysis Report for 29-Mar-17-10024 L3-10205A-FRGC-O 1 OCV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCilgrams) (pCi/grams)

Ba-133 81. 00 32.90 -8.05E-02 3.83E-02 1.15E-01 276.40 7.16 -1.61E-01 3.02E-Ol 302.85 18.34 5.82E-02 l.39E-01 356.01 62.05 -1. 09E-02 3.83E-02 383.85 8.94 -6.93E-02 2.55E-01 Cs-134 475.36 1. 48 3.38E-02 3 , 69E-02 1.86E+OO 563.25 8.34 3.82E-03 3.42E-01 569.33 15.37 5.68E-02 1.62E-01 604.72 97. 62 -1.0lE-02 3.90E-02 795.86 85.46 -5. llE-04 3.69E-02 801.95 8.69 O.OOE+OO 2.75E-01 1038.61 0.99 -7.49E-01 4.29E+OO 1167.97 1. 79 -2.87E-01 1.86E+OO 1365.19 3.02 3.37E-01 1.05E+OO Cs-137 661.66 85.10 8.35E-03 4.47E-02 4.47E-02 Eu-152 121. 78 28.67 -1.SSE-02 7.43E-02 7.43E-02 244.70 7.61 -6.65E-02 2.88E-01 295.94 0.45 2.lOE+OO 5.67E+OO 344.28 26.60 -l.48E-02

9. 28E-02 367.79 0.86 -4.98E-Ol 2.49E+OO 411.12 2.24 2.02E-01 l. lOE+OO 443.96 2.83 2.84E-01 7.64E-01 488.68 0.42 8.80E-01 5. 72E+OO 563.99 0.49 -5.69E+OO 5.43E+OO 586.26 0.46 6.88E+OO 9.67E+OO 678.62 0.47 -5.97E-01 6.66E+OO 688.67 0.86 -9.80E-01 3.70E+OO 719.35 0.28 -5.09E-01 9.56E+OO 778.90 12. 96 l.72E-01 2.67E-01 810.45 0.32 2.20E+OO 6.85E+OO 867.37 4.26 -l.84E-01 6.34E-01 919.33 0.43 9.0lE-01 4.35E+OO 964. 08 14.65 8.75E-02 2.83E-01 1085.87 10.24 4.87E-02 4.26E-01 1089.74 1. 73 1. 25E+OO 2.26E+OO 1112. 07 13.69 1. 44E-01 2.77E-01 1212. 95 1. 43 1.85E+OO 3.61E+OO 1249.94 0.19 1.0lE+Ol 2.07E+Ol 1299.14 1. 63 9.02E-01 2.20E+OO 1408.01 21.07 -5.23E-02

1. 38E-01 1457.64 0.50 3.79E+Ol 2.56E+01 1528.10 0.28 -9.57E+OO 7.53E+OO Eu-154 123.07 40.40 -6.94E-03 5.49E-02 5.49E-02 247.93 6.89 5.55E-02 3.12E-01 591. 76 4.95 1.47E-01 5.16E-Ol 692.42 1. 78 -2.30E-01 1.54E+OO 723.30 20.06 -4.BOE-02 1.53E-01 756.80 4.52 2.02E-Ol 6. 71E-01 873.18 12.08 -7.99E-02 2.09E-01 996.29 10.48 6.55E-02 3.66E-01 1004.76 18.01 1.14E-01 2.06E-01 1274.43 34.80 1.17E-02 l.14E-Ol 3/29/2017 11:55:33AM Page 6 of6 Analysis Report for 29-Mar-17-10024 L3-10205A-FRGC-O 1 OCV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCi!grams) (pCi!grams)

Eu-154 1596.48 1. 80 -1.25E+OO 5.49E-02 1.78E+OO Eu-155 45.30 1. 31 -1.69E+OO 1.16E-01 6.15E+OO 60.01 1. 22 -1.75E+OO 6.81E+OO 86. 55 30.70 2.61E-02 1.16E-01 105.31 21.10 6.46E-02 1. 25E-Ol Ra-226 186.21 3.64 2.19E-Ol 6.S2E-01 6.62E-Ol Pa-231 27.36 10.30 O.OOE+OO 7.48E-02 7.48E-02 283.69 1. 70 5 .13E-02 1.24E+OO 300.07 2.47 -1.75E-01 9.26E-01 302.65 2.20 -1.90E-01 1.lOE+OO 330.06 1. 40 5.61E-02 1.87E+OO U-235 143.76 10.96 3.74E-02 4 .13E-02 1. 78E-01 163.33 5.08 -1.22E-01 4.00E-01 185.71 57.20 -4.lOE-03 4.13E-02 202 .11 1. 08 -7.29E-01

1. 84E+OO 205.31 5.01 -2.91E-02 3.95E-01 Am-241 59.54 35.90 3. 72E-03 2.44E-01 2.44E-01 + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Vl .f-J C: 60-= 55-45 40 35 8 30 25 20 15 10 5 ROI Type: 1 1000 2000 3000 0000002630.CNF 4000 channel 5000 Live Time 600.000 sec Rea 1 Time 600. 340 sec start: 1 -0.0(kev)

Stop : 8192 2047. 8(kev) Acq. start wed Mar 29 11: 45: 2 S 2017 6000 7000 8000 3/29/2017 12:06:31PM

~pex-Gamma Analysis Report for 29-Mar-17-10025 L3-10205A-FRGC-O 11 CV GAMMA SPECTRUM ANAL YS/S Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Fill Height Certificate Name Certificate Date : 29-Mar-17-10025

L3-10205A-FRGC-011CV

Sand 1.536E+03 grams : Default : 3/24/2017 9:45:00AM

3/29/2017 11 :56:22AM : 130G_Sand

Administrator

P11314 ; 130G_Sand

600.0 seconds : 600.3 seconds : 0.05 % : 3.00 : 120-8192 : 120 -8192 : 1.000 keV : 11/10/2016

3/29/2017

initial 11 /16/16 : 2631 : 1000.00 gram : Eu155-Na22

12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2017 12:06:25PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Page I of6 3/29/2017 12:06:31PM Page 2 of6 Analysis Report for 29-Mar-17-10025 L3-10205A-FRGC-011CV Peak Energy ROI No. (keV) start 1 2 38.63 948 -2 3 38.28 1349 -3 583.43 2 327 -4 1460.94 5831 -M = First peak in a multiplet region m = other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma ROI end 960 1358 2336 5851 Peak Centroid 954 .11 1352.20 2331. 8 6 5841.68 No background subtract performed on this spectrum.

NetPeak Net Area Continuum Area Uncertainty Counts 6.63E+Ol 1 2.07 2.97E+Ol 2.16E+Ol 6.05 6.39E+OO l.12E+Ol 5.58 8.77E+OO 1. 08E+02 12.07 1. 05E+Ol NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams)

Uncertainty K-40 0.99 1460.82

• 10.66 2.81E+OO 3.38E-01 Tl-208 0.99 583.19

• 85.00 l.93E-02 9.66E-03 Pb-21 2 1. 00 11 5 .18 0.60 2 38.63

• 43.60 1.17E-01 2.34E-0 2 300.09 3.30 Ac-228 1. 00 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.3 2

• 11. 27 l.88E-01 5.48E-02 409.46 1. 92 463.00 4.40 7 94.95 4.2 5 FWHM (keV) 0.80 0.52 0.89 1. 77 Analysis Report for 29-Mar-17-10025 L3-10205A-FRGC-011 CV Nuclide Name Ac-2 2 8 Id Confidence

1. 00 Energy (keV) 911.2 0 964. 77 968.97 1588.2 0 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000 keV Nuclide confidence index threshold=

0.30 Errors quoted at 1.000sigma Yield(%) 25.80 4.99 15.80 3.22 3/29/2017 12:06:31PM Page 3 of6 Activity (pCilgrams)

Activity Uncertainty INTERFERENCE CORRECTED REPORT ? = X = Nuclide Name K-40 Tl-208 Pb-21 2 Ac-228 Nuclide Id Confidence 0.998 0.990 1. 000 1. 000 nuclide i s part of an undetermined solution nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 2.81E+OO 1. 93E.,..02 1.1 7E-01 1.88E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma Wt mean Comments Activity Uncertainty 3.38E-01 9.66E-03 2.34E-02 5.48E-02 3/29/2017 12:06:31PM Analysis Report for 29-Mar-17-10025

+ L3-10205A-FRGC-011 CV Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (ke V) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : 3/29/2017 12:06:24PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCUgrams) (pCl/grams)

BE-7 477.60 10.44 6.68E-02 3.60E-01 3.60E-01 K-40 1460.82

• 10.66 2.81E+OO 6.23E-01 6.23E-01 Co-60 1173.23 99.85 2.2 7E-0 2 3.24E-02 5.40E-02 1332.49 99.98 -2. llE-0 3 3.24E-02 Nb-94 702.65 99.81 6.lSE-04 3.34E-02 3.97E-0 2 871.09 99.89 -1.2 0E-02 3.34E-0 2 Ag-108m 79.13 6.60 3.76E-01 3.44E-0 2 7.03E-01 433.94 90.50 1.SlE-03 3.44E-02 614.2 8 89.80 -2.40E-02 4.19E-02 7 22.94 90.80 9.35E-04 4.0lE-02 Sb-125 176.31 6.84 -4.03E-02 9.42E-02 3.34E-01 380.45 1. 52 3.19E-01 1.76E+OO 427.87 2 9.60 1.82E-03 9.42E-0 2 463.36 10.49 -1.98E-01 2.54E-01 600.60 17.65 9.71E-02 1.82E-01 606. 71 4.98 4.62E-01 8.13E-01 635.95 11. 2 2 7.29E-02 3.2 3E-01 671. 44 1. 79 9.94E-01 1.70E+OO Ba-133 79.61 2.65 6.46E-01 4.87E-02 1. 66E+OO Page 4 of6 Tolerance Nuclide 3/29/2017 12:06:31PM Page 5 of6 Analysis Report for 29-Mar-17-10025 L3-10205A-FRGC-011 CV Nuclide Energy Yield(%) Activity Nuclid e MDA LineMDA Name (keV) (pCi!grams) (pCilgrams) (pCilgrams)

Ba-133 81. 00 32.90 -6.62E-02 4.87E-02 1.02E-01 2 76.40 7.16 1.51E-01 3.68E-01 3 02.85 1 8.34 1. 05E-01 1.49E-01 3 5f;.0 1 62.05 -4.72E-02 4.87E-02 383.85 8.94 -1.49E-01 2.44E-01 Cs-134 475.36 1. 48 1. 52E+OO 3.49E-02 2.26E+OO 563.25 8.34 7.32E-02 3.99E-01 569.33 15.37 -8.77E-0 2 2.0lE-01 604. 72 97.6 2 -3.45E-0 2 3.49E-0 2 795.86 85.46 6.54E-0 3 4.58E-0 2 801.95 8.69 1.23E-01 4.66E-01 1 038.61 0.99 2.67E+OO 4.33E+OO 1167.97 1. 79 -2.43E+00 3.0lE+OO 1365.19 3.0 2 2.64E-01 9.84E-01 Cs-1 3 7 661.66 85.10 5.41E-03 5.04E-02 5.04E-02 Eu-1 52 121. 78 2 8.67 2.1 7E-02 7.84E-02 7.84E-0 2 244.70 7.61 l.53E-01 4.00E-0 1 295.94 0.45 7.49E-01 6.64E+OO 344.28 26.60 3.84E-02 9.86E-02 367.79 0.86 1.73E+OO 3.08E+OO 411.12 2.2 4 -7.51E-01 1.31E+OO 443. 96 2.83 2.19E-01 1.0lE+OO 488.68 0.4 2 3.63E+OO 6.76E+OO 563.99 0.49 -3.41E+OO 6. 41E+OO 586.26 0.46 4.88E+OO 9.84E+OO 678.62 0.47 -9.48E-01 5.36E+OO 688.67 0.86 -2.00E+OO 2.80E+OO 719.35 0.28 l.19E+OO 1.18E+Ol 778.90 12. 96 -5.37E-02 2.38E-01 810.45 0.32 -2.56E+OO l.03E+Ol 867.37 4.26 -8.71E-01 7.05E-01 919.3 3 0.43 -9.14E-01 8.12E+OO 964.0 8 1 4.65 -2 .13E-0 2 3.53E-01 10 85.87 1 0.24 -3.86E-0 2 3.98E-01 10 89.74 1. 73 -6.02E-01 2.36E+OO 1112.07 13.69 1.51E-01 2.89E-01 1212.95 1. 43 -1.07E+OO 3.08E+OO 12 4 9.94 0.19 -3.83E+00

~.82E+Ol 1 2 99.14 1. 63 -2.90E+OO 1. 96E+OO 1 408.01 2 1. 07 5.14E-0 2 1.60E-01 1 457.64 0.50 6.62E+Ol 3.l OE+Ol 1528.10 0.2 8 -1.79E+OO 7.86E+OO Eu-154 123.07 40.40 -1. llE-02 5.61E-02 5.61E-02 2 47.93 6.89 -4.67E-02 3.20E-01 591.7 6 4.95 -:.65E-02 5.82E-01 692.42 1. 78 -1.44E+OO 1.1 6E+OO 723.30 2 0.06 1. 27E-0 2 1.82E-01 756.80 4.52 -2.81E-01 8.09E-Ol 873.18 12.08 -4.0 lE-03 3.0lE-01 996.2 9 10.4 8 -2.85E-02 3.67E-01 1004.7 6 18.01 -5.80E-02 l.48E-01 1 2 74.4 3 34.80 9.72E-03 l.1 9E-01 3/29/2017 12:06:31PM Page 6 of6 Analysis Report for 29-Mar-17-10025 L3-10205A-FRGC-011 CV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCl/grams) (pCUgrams) (pCilgrams)

Eu-154 1596.48 1. 80 4.99E-01 5.61E-02 1.86E+OO Eu-155 45.30 1. 31 2. 72E-01 1.1 6E-0 1 7.18E+OO 60.0 1 1. 22 -1.33E+OO 7.61E+OO 86.55 30.70 7.32E-03 l.18E-01 105.31 2 1.10 -2.68E-02 1.16E-01 Ra-226 186.2 1 3.64 -8.95E-02 6.72E-01 6. 72E-01 Pa-23 1 27.36 10.30 O.OOE+OO 7.BlE-02 7.BlE-02 283.69 1. 70 -2.34E-01 1.44E+OO 300.0 7 2.47 -6.28E-01

1. 02E+OO 302.65 2.20 4.91E-01 1.20E+OO 330.0 6 1. 40 1.40E+OO 2.12E+OO U-235 143.76 i0.96 1.2 2E-0 2 4.31E-02 2.34E-01 1 63.33 5.08 -3.0 lE-02 4.61E-01 185. 71 57.2 0 1.BlE-02 4.31E-02 202 .11 1. 08 7.2 1E-01 2.23E+OO 2 05.31 5.0 1 -1.61E-01 4.65E-01 Am-241 59.54 35.90 1.75E-02 2. 72E-01 2. 72E-01 + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 60 55 50 45 40 35 1000 2000 ROI Type: 1 3000 0000002631.CNF 4000 channel 5000 Live Time :600.000 sec Real Tire :600.330 sec Start: 1: -0.0(kev)

Stop : 8192:2047 .S(kev) Acq. start :wed Mar 29 11:56:22 2017 6000 7000 8000 3/29/2017 12:17: 34PM ~pex-Gamma Analysis Report for 29-Mar-17-10026 L3-10205C-FRGC-012CV GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample S i ze Facility Sample Taken On Acqu i sition Started Procedure Operator Detector Name Geometry Live T i me Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Fill Height Certificate Name Certificate Date : 29-Mar-17-10026

L3-10205C-FRGC-012CV

Sand 1.600E+03 grams : Default : 3/24/2017 9:50:00AM

3/29/2017 12:07:25PM

130G_Sand

Administrator

P11314 : 130G_Sand

600.0 seconds : 600.4 seconds : 0.06% : 3.00 : 120 -8192 : 120 -8192 : 1.000 keV : 11/10/2016

3/29/2017

initial 11/16/16 : 2633 : 1000.00 gram : Eu155-Na22

12/22/2008 12:00: 00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2017 12:17:28PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Page 1 of6 3/29/2017 12:17: 34PM Page 2 of6 Analysis Report for 29-Mar-17-10026 L3-10205C-FRGC-O 12CV Peak No. Energy (keV) ROI start ROI end 1 2 238.67 1461.22 948-959 5834 -5850 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma Peak Centroid 954.24 5842.83 No background subtract performed on this spectrum.

Net Peak Area 4.55E+Ol 7.88E+Ol Net Area Uncertainty 8.90 9.92 Continuum Counts l.35E+Ol 6.20E+OO NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) K-40 0.97 1460.82 Pb-212 1. 00 115 .18 238.63 300.09 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000 keV Nuclide confidence index threshold

= 0.30 Errors quoted at 1.000sigma Yield(%) 10.66 0.60 43.60 3.30 Activity (pCi/grams) 1.98E+OO 7.73E-02 Activity Uncertainty 2.63E-Ol l.64E-02 FWHM (keV) 0.86 0.54 3/29/2017 12:17:34PM Analysis-Report for 29-Mar-17-10026 L3-10205C-FRGC-O 12CV INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Pb-212 Nuclide Id Confidence 0.975 1. 000 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCi/grams) l.98E+OO 7.73E-02 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma Wt mean Activity Uncertainty 2.63E-01 1.64E-02 Page3 of6 Comments 3/29/2017 12:17:34PM Analysis Report for 29-Mar-17-10026

+ L3-10205C-FRGC-O 12CV Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : 3/29/2017 12:17: 28PM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL. NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCl/grams) (pCi/grams)

BE-7 477.60 10.44 5.2 0E-02 3.40E-01 3.40E-01 K-40 1460.82

• 10.6 6 1.98E+OO 4.49E-01 4.49E-01 Co-60 1173.23 99.85 -7.73E-03 2.79E-02 4.77E-02 1332. 49 99.98 7.48E-0 3 2.79E-02 Nb-94 702.65 99.8 1 -2.00E-0 2 2.49E-02 2.49E-02 871. 09 99.89 1. 73E-02 3.99E-0 2 Ag-1 08m 79 .13 6.60 3.85E-01 2.98E-0 2 6.75E-01 433.94 90.50 -9.33E-03 2.98E-02 614.28 89.80 -1. 72E-03 3.57E-02 72 2.94 90.80 -1.80E-03 3.74E-02 Sb-125 1 76.31 6.84 1.02E-01 9.84E-02 3.14E-01 380.45 1. 52 1. 87E-01 1.2 8E+OO 427.87 29.60 3.93E-03 9.84E-02 463.36 10.49 -4.22E-02 2.37E-01 600.60 17.65 2.51E-02 1.59E-01 606. 71 4.98 3.27E-01 7.2 2E-01 635.95 11. 22 -7.42E-02 2.19E-01 671.44 1. 79 3.62E-02 1.2 7E+OO Ba-133 79.61 2.65 2.64E-01 4.67E-02 1.57E+OO Page 4 of6 Tolerance Nuclide 3/29/2017 12: 17: 34PM Page 5 of6 Analysis Report for 29-Mar-17-10026 L3-10205C-FRGC-O 12CV Nuclide Energy Yield(%) Activity Nuc/id e MDA LineMDA Name (keV) (pCi/grams) (pCl/grams) (pCi/grams)

Ba-1 33 81. 00 32.90 -2.0lE-02 4.67E-02 9.95E-0 2 276.40 7.16 l.78E-01 3. 72E-01 30 2.85 18.34 2.28E-02 l.39E-01 356.01 62.05 -4.35E-0 2 4.67E-02 383.85 8.94 -2.08E-01 2.42E-01 Cs-13 4 475.36 1. 48 1.17E+OO 3.18E-02 2.21E+OO 563.25 8.34 -3.19E-01 2.97E-Ol 569.33 15.37 5.52E-02 1.99E-01 604. 72 97.6 2 -3.31E-02 3.18E-02 795.86 85.46 -4.79E-02 3.19E-02 801.95 8.69 9.63E-0 2 4.35E-01 1038.61 0.99 1. 3 3E+OO 4.0lE+OO 1167. 97 1. 79 -1. 73E+OO 2.49E+OO 1365.19 3.02 2.53E-01 9.45E-01 Cs-137 661. 66 85.10 3.42E-02 4.2 9E-0 2 4.29E-02 Eu-152 121. 78 28.67 -1.31E-02 7.94E-02 7.94E-0 2 244.70 7.61 -9.37E-02 3.lOE-01 295.94 0.45 l.69E+OO 6.3 1E+OO 344.2 8 2 6.60 l.44E-0 2 9.48E-02 367.79 0.86 -1.41E+OO 2.64E+OO 411.12 2.2 4 6.34E-01 9.84E-01 443.96 2.83 -2.65E-01 7.65E-01 488.68 0.42 3.98E+OO 6.83E+OO 563.99 0.49 -3.65E+OO 5.2 4E+OO 586.26 0.46 7.50E+OO 9.06E+OO 6?8.62 0.47 -1.57E+OO 4.50E+OO 688.67 0.86 -1.40E+OO 2.86E+OO 719.35 0.2 8 -9.74E+OO 1.09E+Ol 778.90 12.96 -1. 59E-02 1.80E-01 810.45 0.32 -3.47E+OO 9.93E+00 867.37 4. 26 -3.lOE-01

7. 51E-01 919.33 0.43 3.2 9E+OO 8.80E+OO 964. 08 14.65 -1.15E-01 2.46E-01 10 85.87 10.24 4.76E-02 4.41E-01 1089.74 1. 73 1.63E+OO 2.53E+OO 1112. 07 13.69 3.93E-0 2 2.78E-01 1212.95 1. 43 -1.3 0E+OO 2.69E+OO 1249.94 0.19 2.79E+OO 1. 85E+Ol 1299.1 4 1. 63 5.65E-02 2.48E+OO 1408.01 2 1. 07 3.70E-02 1. 38E-01 1457.64 0.50 4.78E+Ol 2.57E+Ol 1528.10 0.28 O.OOE+OO 2.83E+OO Eu-154 123.07 40.40 7.53E-0 3 5.56E-02 5.56E-02 247.93 6.89 -1.88E-01 3.36E-01 591.76 4.95 2 .-3 1E-01 5.38E-01 692.42 1. 78 -3.12E-0 1 1.61E+OO 723. 3 0 2 0.06 9.44E-02 1.80E-01 756.80 4.52 3.73E-Ol 6.73E-01 873.1 8 12.08 -4.02E-02 3.2 1E-01 996.29 10.48 -3.17E-02 2.43E-01 1004.76 18.0 1 -4.85E-02 l.78E-01 1274.43 34.80 1.04E-02 1.08E-01 3/29/2017 12:17: 34PM Page 6 of6 Analysis Report for 29-Mar-17-10026 L3-10205C-FRGC-O 12CV Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (keV) (pCi!grams) (pCi/grams) (pCl/grams)

Eu-154 1596.48 1. 80 3.2 0E-01 5.56E-02 1. 54E+OO Eu-155 45.30 1. 31 4.06E-01 9.57E-02 6.25E+OO 60.01 1.22 2.89E+OO 6.66E+OO 86.55 3 0.70 6.2 5E-0 3 9.57E-02 105.31 2 1.1 0 4.93E-03 1.16E-01 Ra-226 186.21 3.64 3.94E-01 6.51E-01 6.51E-01 Pa-231 27.36 10.30 O.OOE+OO 7.50E-02 7.50E-0 2 283.69 1. 70 -7.73E-01 1.30E+OO 300.07 2.47 -5.45E-01 9.2 8E-01 302.65 2.20 -7.54E-01 1.07E+OO 330.06 1. 40 -1.66E-02 L 72E+OO U-2 3 5 143.76 10.96 -3.2 0E-02 3.98E-02 2.00E-01 163.33 5.08 2.21E-01 4.42E-01 185.71 57.2 0 6.49E-03 3.98E-0 2 202 .11 1. 08 -7.34E-01 1.88E+OO 205.31 5.01 -7.59E-02 4.36E-01 Am-2 41 59.54 35.90 4.27E-02 2.30E-01 2.30E-01 + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 60 55 50 45 1000 2000 3000 ROI Type: 1 0000002633 .CNF 4000 channel 5000 Live Time :600.000 sec Real Tire :600.350 sec Start: 1: -0.0(kev) stop : 8192: 2047. S(kev) Acq. start :wed Mar 29 12:07:25 2017 6000 7000 8000 3/29/2017 12:33:49PM Analysis Report for 29-Mar-17-10029 L3-10205S-FRGC-013CV GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Fill Height Certificate Name Certificate Date : 29-Mar-17-10029

L3-10205S-FRGC-013CV

Sand 1.606E+03 grams : Default : 3/24/2017 10:02:00AM

3/29/2017 12:23:41PM

130G_Sand

Administrator

P11314 : 130G_Sand

600.0 seconds : 600.4 seconds : 0.06 % : 3.00 : 120 -8192 : 120 -8192 : 1.000 keV : 11/10/2016

3/29/2017

initial 11/16/16 : 2635 : 1000.00 gram : Eu155-Na22

12/22/2008 12: 00: 00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2017 12:33:43PM Peak Analysis From Channel Peak Analysis To Channel : 1 20 : 8192 Page 1 of6 3/29/2017 12:33:49PM Page 2 of6 Analysis Report for 29-Mar-17-10029 L3-10205S-FRGC-O 13CV Peak Energy ROI No. (keV) start 1 238.56 949 -2 910.87 3 636 -3 1461.01 5835 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma ROI end 959 3645 5849 Peak Centroid 953.81 3640.93 5841.97 No background subtract performed on this spectrum.

NetPeak Net Area Continuum Area Uncertainty Counts 4.86E+Ol 8.8 2 1.14E+Ol 1. 35E+Ol 4.43 2.50E+OO 6.09E+Ol 9.17 8 .13E+OO NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defau!t\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams)

Uncertainty K-40 0.99 1460.8 2

• 10.66 1. 52E+OO 2.39E-01 Pb-21 2 0.99 115 .18 0.60 238.63

• 43.60 8.23E-0 2 1. 63E-0 2 300.09 3.30 Ac-228 0.99 129.07 2.4 2 209.25 3.89 2 1 0.2 4 3.46 328.00 2.95 338.3 2 11.27 409.46 1. 92 463.0 0 4.40 794.95 4.2 5 9 11. 20

• 2 5.80 1.00E-0 1 3.31E-02 964. 77 4.99 FWHM (keV) 0.69 0.97 0.50 Analysis Report for 29-Mar-17-10029 L3-10205S-FRGC-O 13CV Nuclide Name Ac-2 28 Id Confidence 0.99 Energy (keV) 968. 97 1588.20 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000 keV Nuclide confidence index threshold

= 0.30 Errors quoted at 1.000sigma Yield(%) 15.80 3.22 3/29/2017 12:33:49PM Page 3 of6 Activity (pCilgrams)

Activity Uncertainty INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Pb-212 Ac-228 Nuclide Id Confidence 0.995 0.999 0.995 ? = nuclide i s part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCl/grams) 1.52E+OO 8.23E-02 1.00E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma wt mean Comments Activity Uncertainty 2.39E-01 1.63E-02 3.31E-02 3/29/2017 12:33:49PM Analysis Report for 29-Mar-17-10029

+ L3-10205S-FRGC-013CV Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : 3/29/2017 12:33:43PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCl!grams) (pCilgrams) (pCl/grams)

BE-7 477.60 10.44 1.56E-01 2.81E-01 2.81E-01 K-40 1460.82

• 10.66 1. 52E+OO 4.80E-01 4.80E-01 Co-60 1173.23 99.85 4.37E-03 3.34E-02 3.34E-02 1332.49 99.98 1.74E-02 3.87E-02 Nb-94 702.65 99.81 1.02E-02 2.88E-0 2 3.00E-02 871.09 99.89 -1.96E-02 2.88E-0 2 Ag-108m 79.13 6.60 1. 62E-01 2.97E-02 6.61E-01 433.94 90.50 1.59E-03 2.97E-02 614.28 89.80 -7.28E-0 2 4.0lE-02 722.94 90.80 l.35E-0 2 3.61E-02 Sb-125 176.31 6.84 -1.30E-01 9.22E-02 2.83E-01 380.45 1. 5 2 8.51E-01 1. 50E+OO 4 2 7.87 29.60 2.47E-02 9.22E-0 2 463.36 10.49 -5.66E-03 2.57E-01 600.60 17.65 -4.35E-02 1.40E-01 606.71 4.98 7.90E-01 8.93E-01 635.95 11. 22 4.86E-0 2 2.93E-01 671.44 1. '7 9 5.40E-01 1.91E+OO Ba-133 79.61 2.65 -2.14E-02 4.52E-02 1.61E+OO Page 4 of6 Tolerance Nuclide 3/29/2017 12:33: 49PM Page 5 of6 Analys i s Report for 29-Mar-17-10029 L3-10205S-FRGC-013CV Nuclide Energy Yield(%) Activity Nuclld e MDA LineMDA Name (keV) (pCilgrams) (pCilgrams) (pCi/grams)

Ba-13 3 81.00 32.90 -2.60E-02 4.52E-0 2 1.15E-01 2 76.40 7.16 -1.70E-01 3.07E-01 3 02.85 18.34 -8.63E-02 1.18E-0 1 356.01 62.05 -5.69E-02 4.52E-02 383.85 8.94 7.14E-02 2.09E-01 Cs-134 475.3 6 1. 48 -2.87E-01 3.74E-02 1. 71E+OO 563.25 8.34 -6.28E-0 2 2. 96E-01 569.33 15.37 -3.59E-03 l.93E-01 604.72 97.62 -2.75E-02 3.74E-02 795.86 85.46 -4.79E-03 4.12E-02 801.95 8.69 -1.87E-01 3.32E-01 1038.61 0.99 5.05E-01 3. llE+OO 1167.97 1. 79 2.15E-01 2.09E+OO 1365.19 3.0 2 5.05E-01 l.23E+OO Cs-137 661. 66 85.10 2.2 0E-02 4.99E-0 2 4.99E-02 Eu-152 12 1. 78 28.67 3. 91E-03 7.59E-02 7.59E-02 244.70 7.61 1.21E-02 3.1 7E-01 295.94 0.45 1.57E+00 6.14E+OO 344.2 8 2 6.60 2.08E-0 2 8.12E-0 2 367.79 0.86 1.77E+00 3.00E+OO 4 11.12 2.2 4 -7.07E-02 9.13E-01 44 3. 96 2.83 6.90E-01 9.19E-01 488.68 0.42 -7.33E-02 5.91E+OO 563.99 0.49 2.03E+OO 5.42E+OO 586.2 6 0.46 -2.58E-01 8.34E+OO 678.62 0.47 -6.32E+OO 6.19E+OO 688.67 0.86 l.06E+OO 3.30E+OO 7 19.35 0.28 -l.2 0E+Ol 7.90E+OO 778.90 12.96 7. 72E-02 2.48E-Ol 810.45 0.3 2 3.84E+OO 8.54E+OO 867.37 4.2 6 -4.62E-01 7.12E-01 919.33 0.4 3 2.09E+00 7.77E+OO 964. 08 14.6 5 -2.04E-02 2.65E-01 1085.87 10.2 4 3.34E-02 3.08E-01 1089.74 1. 73 -1.93E+OO 1.56E+OO 1112.07 13.69 1.54E-01 3.54E-01 1212.95 1. 43 -1.44E+OO 3.29E+OO 1 2 49.94 0.19 3.37E+OO 2.62E+Ol 1 2 99.14 1. 63 1.05E+OO 2.34E+OO 1408.01 2 1.07 -2.77E-02 1.67E-01 1457.64 0.50 4 .13E+Ol 2.39E+Ol 1528.10 0.2 8 4.90E+OO 1. 33E+Ol Eu-154 1 23.07 40.40 1.42E-02 5.48E-0 2 5.48E-0 2 2 47.93 6.89 6.74E-03 3.16E-01 591. 76 4.95 2.60E-01 5.76E-0 1 692.42 1. 78 8.88E-0 1 1.60E+00 723. 30 2 0.06 9.lOE-02 1. 69E-01 756.80 4.5 2 4.46E-01 7.24E-01 873.18 12.08 1. 54E-01 2.77E-01 996.2 9 10.48 -1.51E-02 3.36E-0 1 1 004.76 18.01 -l.88E-02 1.55E-01 1 2 74.4 3 34.8 0 -2.08E-03 9.42E-02 3/29/2017 12:33:49PM Page 6 of6 Analysis Report for 29-Mar-17

-10029 L3-10205S-FRGC-013CV Nuclide Energy Yield(%) Activity Nuclid e MDA LineMDA Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

Eu-154 1596.48 1. 80 3.18E-01 5.48E-02 1. 54E+OO Eu-155 45.30 1. 31 -2.20E+OO 1. llE-01 5.49E+OO 60.01 1. 22 -2.29E+OO 6.80E+OO 86.55 30.70 5.41E-02 1. llE-01 105.31 2 1.10 -3.87E-02 1.19E-01 Ra-226 186.2 1 3.64 3.56E-01 6.61E-01 6.61E-01 Pa-23 1 2 7.36 1 0.30 O.OOE+OO 7.47E-02 7.47E-02 2 83.69 1. 7 0 l.67E-01 1. 38E+00 300.07 2.47 -9.06E-01 9.41E-01 30 2.65 2.20 -2.38E-01 l.OOE+OO 330.06 1. 40 -3.50E-01 1.74E+OO U-235 143.76 10.96 -5.96E-02 4.16E-02 l.89E-01 1 63.33 5.08 -1.2 7E-01 4.05E-01 1 85.71 57.2 0 2.56E-0 2 4.16E-02 2 02 .11 1. 08 -1.48E-01 1.87E+OO 205.31 5.01 1. 33E-01 4.29E-01 Am-2 4 1 59.54 35.90 -1.18E-01 2.41E-01 2.41E-01 + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 60 55 50 45 1000 2000 3000 ROI Type: 1 0000002635.CNF 4000 channel 5000 Live Time :600.000 sec Real Tille :600.350 sec start: 1: -0.0(kev) stop : 8192: 2047 .8(kev) Acq. start :wed Mar 29 12:23:41 2017 6000 7000 8000 3/29/2017 1: 01: 14PM ~pex-Gamma Analysis Report for 29-Mar-17-10031 L3-10205A-FRGC 014CV GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample S i ze Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live lime Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Fill Height Certificate Name Certificate Date : 29-Mar-17-10031

L3-10205A-FRGC 014CV

Sand 1.652E+03 grams : Default : 3/24/2017 10:10:00AM

3/29/2017 12:51:03PM

130G_Sand

Administrator

P11314 : 130G_Sand

60.0.0 seconds : 600.3 seconds : 0.04 % : 3.00 : 120 -8192 : 120 -8192 : 1.000 keV : 11/10/2016

3/29/2017

initial 11/16/16 : 2637 : 1000.00 gram : Eu155-Na22

12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2017 1:01: 06PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Page 1 of6 3/29/2017 1:01:14PM Page 2 of6 Analysis Report for 29-Mar-17-10031 L3-10205A-FRGC 014CV Peak Energy ROI No. (keV) start 1 2 38.83 949 -2 3 51.95 1402 -3 609.27 2431 -4 1460.92 5834 -M a: First peak in a multiplet region m a: Other peak in a multiplet region F a: Fitted singlet Errors quoted at 1.000sigma ROI end 959 1410 2441 5849 Peak Centroid 954.90 1406.80 2435.12 5841.61 No background subtract performed on this spectrum.

Net Peak Net Area Continuum Area Uncertainty Counts 3.08E+Ol 9.65 2.62E+Ol 2.17E+Ol 6.78 1.13E+Ol 1.94E+Ol 5.93 6.56E+OO 6.92E+Ol 8.62 1. 81E+OO NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams)

Uncertainty K-40 0.99 1460.8 2

• 10.66 1.68E+OO 2.2 2E-01 Bi-211 0.88 351.07

• 13. 02 1.57E-01 5.0 6E-02 Pb-212 0.99 115 .18 0.60 238.63

• 43.60 5.07E-02 1.64E-02 300.09 3.30 Bi-2 1 4 1. 00 609.32

• 45.49 5.98E-02 1. 8 6E-02 768.36 4.89 8 0 6.18 1. 2 6 934.06 3.11 112 0.29 1 4.92 1 155.2 1 1. 63 1238.12 5.83 128 0.98 1. 43 FWHM (keV) 0.37 0.69 0.29 0.31 Analysis Report for 29-Mar-17-10031 L3-10205A-FRGC 014CV Nuclide Id Energy Name Confidence (keV) Bi-214 1. 00 1377. 67 1385.31 1401.52 1407.99 1509.2 1 1661. 2 7 1729.59 1764.49 1847.43 2 118.51 Pb-214 1. 00 241.99 295.22 351.9 3 785. 96 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000 keV Nuclide confidence index threshold

= 0.30 Errors quoted at 1.000sigma 3/29/2017 1:01: 14PM Page3 of6 Yield(%) Activity Activity (pCi/grams)

Uncertainty 3.99 0.79 1. 33 2.39 2 .13 1. 05 2.88 15.30 2.03 1.16 7.2 5 18.42 35.60 5.73E-02 1.85E-02 1. 06 INTERFERENCE CORRECTED REPORT Nuclide Name K-40 ? Bi-2 11 Pb-21 2 Bi-214 ? Pb-214 Nuclide Id Confidence 0.999 0.884 0.994 1. 000 1.000 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 1.68E+OO 1.57E-01 5.0':'E-02 5.98E-02 5.73E-02 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma Wt mean Comments Activity Uncertainty 2.22E-01 5.06E-02 1.64E-02 1.86E-02 1. 85E-02 3/29/2017 1 :01: 14PM Analysis Report for 29-Mar-17-10031

+ L3-10205A-FRGC 014CV Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : 3/29/2017 1 :01 :06PM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide

• Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCl/grams) (pCi/grams)

BE-7 477.60 10.44 1.97E-01 2.99E-01 2.99E-01 K-40 1460.82

• 10.6 6 l.68E+00 2.5":'E-01 2.57E-01 Co-60 1173.2 3 99.85 5.61E-03 3.53E-02 3.83E-02 1332.49 99.98 1.45E-0 2 3.53E-02 Nb-94 702.65 99.81 l.70E-02 2.45E-02 3.42E-02 871.09 99.89 2.2 5E-03 2.45E-0 2 Ag-108m 79.13 6.60 -4.2 0E-02 2.68E-0 2 6.37E-01 433.94 90.50 8.79E-03 2.68E-02 614.28 89.80 8.02E-03 3. 98E....:02 722.94 90.80 8.18E-03 3.27E-02 Sb-125 176.31 6.84 -9. 71E-03 7.90E-02 2.79E-01 380.45 1. 52 -3.33E-01 1.46E+OO 427.87 2 9.60 2.3 0E-02 7.90E-02 463.36 10.49 -2.0lE-01 2.49E-01 600.60 17.65 -1.63E-02 1.54E-01 606.71 4.98 7.39E-Ol 8.91E-01 635.95 11. 22 -2.65E-02 2.23E-01 671. 44 1. 79 -3. 96E-01 l.75E+OO Ba-133 79.61 2.65 -9.56E-02 4.46E-02 l.56E+OO Page 4 of6 Tolerance Nuclide 3/29/2017 1:01:14PM Page 5 of6 Analysis Report for 29-Mar-17-10031 L3-10205A-FRGC 014CV Nuclide Energy Yield(%) Activity Nuclid e MDA LineMDA Name (keV) (pCl/grams) (pCi!grams) (pCilgrams)

B a-1 3 3 81. 00 32.90 2.45E-03 4.46E-02 1.07E-01 2 76.40 7.16 -5. llE-02 3.14E-01 302.85 18.34 4.1 6E-02 1.15E-01 356.01 62.0 5 -4.43E-02 4.46E-02 383.85 8.94 -2.0 0E-02 2.48E-01 Cs-134 475.36 1. 48 7.18E-01 3.43E-02 1.98E+OO 563.25 8.34 2.23E-01 3.32E-01 569.33 15.37 -4.82E-02

1. 51E-01 604.72 97.62 -2.97E-02 4.24E-02 795.86 85.46 -1.15E-0 2 3.43E-02 8 01.95 8.69 -2.45E-0 2 3.39E-01 1038.61 0.99 -5.16E-02 3.22E+OO 1167. 97 1. 79 5.57E-01 2.23E+OO 1365.19 3.0 2 1.64E-01 7.91E-01 Cs-137 661.66 85.10 -2.55E-03 4.15E-02 4.15E-02 Eu-15 2 121. 78 28.67 5.45E-0 2 8.0 6E-02 8.06E-0 2 244.70 7. 61 -9.5 6E-02 3.12E-01 295.94 0.45 2.81E-01 5.82E+OO 344.2 8 2 6.60 2.5 6E-02 8.66E-02 367.79 0.86 -6.49E-01 2.49E+OO 411.12 2.24 9.92E-01 1.1 7E+OO 443. 96 2.83 -5.05E-01

7. 96E-01 488.68 0.4 2 4.48E-0 1 5.93E+OO 563.99 0.49 1.llE+OO 5.27E+OO 586.26 0.46 4.92E+OO 8.38E+OO 678.62 0.47 3.42E+OO 7.07E+OO 688.67 0.86 -1.16E+OO 3.59E+OO 719.35 0.28 -8.18E-01

1. 02E+Ol 778.9 0 1 2. 96 1.05E-01 2.50E-01 810.45 0.32 4.2 6E+OO 8.76E+OO 867.37 4.26 3.58E-02 5.73E-01 919.33 0.43 -1.06E+OO 6.81E+OO 964.0 8 14.65 -1.12E-01 2.75E-01 1085.87 10.24 8.88E-02 3.54E-01 1089.7 4 1. 73 6.95E-02 1.89E+OO 1112.0 7 13. 69 3.90E-0 3 3.04E-01 1 2 12.95 1. 43 -3.40E+OO 2.86E+OO 1249.94 0.19 -5.1 9E+OO 2.0lE+Ol 1299.14 1. 63 8.76E-01 2 .13E+OO 1408.01 21.07 -1. 2 9E-01 1.15E-01 1457.64 0.50 3.81E+Ol 2.2 7E+Ol 15 2 8.1 0 0.2 8 -7.15E+OO 9.20E+OO Eu-154 123.0 7 40.40 -2.91E-03 5.44E-02 5.44E-02 247.93 6.89 -l.96E-0 1 3.07E-01 591.76 4.95 -6.94E-03 4.79E-01 692.42 1. 78 -6.48E-02 1.49E+OO 72 3.30 2 0.06 3.51E-02 l.48E-Ol 756.80 4.52 1.75E-01 6.2 3E-01 873.1 8 12.08 -l.18E-01 2.03E-01 996. 2 9 10.48 -2.46E-02 2.57E-01 1004.76 18.01 8.85E-0 2 1.82E-01 1274.43 34.80 -1. llE-01 1.16E-01 3/29/2017 1 :01 :14PM Page 6 of6 Analysis Report for 29-Mar-17-10031 L3-10205A-FRGC 014CV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCi/grams) (pCi!grams)

Eu-154 1596.48 1. 80 1.55E-0 1 5.44E-02 l.19E+OO Eu-155 45.30 1. 31 6.08E-01 9.38E-02 6.53E+OO 60.01 1. 22 -8.70E-01 5.34E+OO 86.55 30.70 -l.72E-02 9.38E-02 105.31 2 1.10 3.39E-03 l. lOE-01 Ra-226 186.2 1 3.64 2.38E-01 5.00E-01 5.00E-01 Pa-231 27.36 10.30 O.OOE+OO 7.2 6E-02 7.2 6E-02 283.69 1. 70 -5.40E-01 l.2 3E+00 300.07 2.47 -3.85E-0 1 9.47E-01 302.65 2.2 0 3.76E-O: 9.56E-01 330.06 1. 40 -5.30E-01 1.38E+OO U-235 143.76 10.96 1. 42E-02 3.08E-02 l.77E-01 163.33 5.08 -7.78E-0 2 3.54E-01 185. 71 57.2 0 -7.08E-0 3 3.0 8E-0 2 2 02 .11 1. 08 -4.76E-01 1.94E+OO 205.31 5.01 -1.40E-01 4.06E....:01 Am-241 59.54 35.90 -7.61E-02

1. 80E-01

• 1.80E-01 + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perfomi the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 60 55 50 45 40 35 1000 2000 3000 ROI Type: 1 0000002637.CNF 4000 channel 5000 Live Time :600.000 sec Real Tire :600.260 sec start: 1: -0.0(kev)

Stop : 8192: 2047 .S(keV) Acq, Start :wed Mar 29 12: 51: 03 2017 6000 7000 8000 3/29/2017 12:49: 59PM ~pex Gamma Analysis Report for 29-Mar-17-10030 L3-10205A-FRQC-O 13CV GAMMA SPECTRUM ANAL YS/S Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Fill Height Certificate Name Certificate Date : 29-Mar-17-10030

L3-10205A-FRQC-013CV

Sand 1.614E+03 grams : Default : 3/24/2017 10:02:00AM

3/29/2017 12:39:SOPM

130G_Sand

Administrator

P11314 : 130G_Sand

600.0 seconds : 600.4 seconds : 0.06% : 3.00 : 120 -8192 : 120-8192 : 1.000 keV : 11/10/2016

3/29/2017

initial 11 /16/16 : 2636 : 1000.00 gram : Eu155-Na22

12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 3/29/2017 12:49:53PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Page 1 of6 3/29/2017 12:49:59PM Page 2 of6 Analysis Report for 29-Mar-17-10030 L3-10205A-FRQC-013CV Peak No. Energy (keV) ROI start ROI end 1 2 238.60 1460.71 948 -960 5832 -5850 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma Peak Centroid 953.97 5840.76 No background subtract performed on this spectrum.

Net Peak Area 5.93E+O l 8.90E+O l Net Area Continuum Uncertainty Counts 9.91 9.43 1. 4 7E+Ol O.OOE+OO NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) K-40 0.99 1460.82 Pb-212 1. 00 115 .18 238.63 300.09 * = Energy line found In the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000 keV Nuclide confidence index threshold

= 0.30 Errors quoted at 1.000sigma Yield(%) 10.66 0.60 4 3.60 3.30 Activity (pCilgrams) 2.2 1E+OO 9.99E-02 Activity Uncertainty 2.54E-01 1.85E-02 FWHM (keV) 0.94 0.80 3/29/2017 12:49:59PM Analysis Report for 29-Mar-17-10030 L3-10205A-FRQC-013CV INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Pb-212 Nuclide Id Confidence 0.998 1. 000 ? = nuclid e is part of an undetermined solution X = nuclid e rejected by the interference analysis Wt mean Activity (pCl!grams) 2.21E+OO 9.99E-02 @ = nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma Wt mean Activity Uncertainty 2.54E-01 1.85E-02 Page 3 of6 Comments 3/29/2017 12:49:59PM Analysis Report for 29-M_ar-17-10030

+ L3-10205A-FRQC-O 13CV Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : 3/29/2017 12:49:53PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCl/grams) (pCilgrams) (pCl/grams)

BE-7 477.60 10.44 4.31E-02 3.06E-01 3.06E-01 K-40 1460.8 2

• 10.66 2.21E+OO 7.1 5E-02 7.15E-0 2 Co-60 1173.23 99.85 -1.42E-04 3.73E-02 3.73E-02 1 332.49 99.98 -1.68E-0 2 3.85E-02 Nb-94 702.65 99.81 -l.61E-02 2.87E-02 2.87E-02 871.09 99.89 -1.13E-02 3.46E-02 Ag-108m 79 .13 6.60 2.73E-03 2.50E-0 2 6.46E-01 433.94 90.50 -l.67E-04 2.50E-0 2 614.2 8 89.80 -5.73E-02 4.24E-02 722.94 90.80 -1.09E-0 2 3.82E-02 Sb-125 176 . .?l 6.84 9.2 6E-02 7.85E-02 2.89E-01 380.45 1. 52 3.19E-01 1.68E+OO 427.87 2 9.60 8.75E-04 7.85E-02 463.36 10.49 l.97E-02 2.42E-01 600.60 17.65 -4.44E-02 l.63E-01 606.71 4.98 9. llE-01 9.00E-01 635.95 11.22 -2.53E-0 2 2.2 8E-01 671.44 1. 79 1.53E-Ol l.90E+OO Ba-133 79.61 2.65 4.0 SE-01 3.72E-02 1.60E+OO Page 4 of6 Tolerance Nuclide 3/29/2017 12:49:59PM Page 5 of6 Analys i s Report for 29-Mar-17-10030 L3-10205A-FRQC~013CV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCUgrams) (pCilgrams) (pCi/grams)

Ba-133 81. 00 32.90 -5.38E-02

3. 72E-02 1.08E-01 276.40 7.16 3.07E-03 3.05E-01 302.85 18.34 -1.0lE-02 1.13E-01 356.0 1 62.05 -3.66E-02

3. 72E-0 2 383.85 8.94 1. 4 9E-01 2.92E-01 Cs-134 475.36 1. 48 5.25E-01 3.82E-02 2.19E+OO 563.25 8.34 -6.60E-03 3.30E-01 569.33 1 5.37 -l.44E-02 1.54E-01 6 04. 72 97.62 2.81E-03 3.87E-02 795.86 85.46 -6.46E-04 3.82E-02 801.95 8.69 2.41E-01 3.92E-0 1 1 038.61 0.99 2. llE+OO 3.82E+OO 1167.97 1. 79 -2.53E+OO 1.58E+OO 1365.19 3.02 -9.00E-01 8.09E-01 Cs-137 661.66 85.10 4.34E-03 4.15E-02 4.15E-02 Eu-15 2 121. 78 2 8.67 4.lOE-02 8.33E-02 8.33E-02 244.70 7.61 1.14E-01 3.48E-01 295.94 0.45 3.75E+OO 6.40E+OO 344.28 26.60 -5.77E-02 8.67E-0 2 367.79 0.86 -1.07E+OO 2.41E+OO 411.12 2.24 -5.05E-0 2 1.lOE+OO 443. 96 2.83 2.90E-01 9.83E-01 488.68 0.42 -2.08E+OO 6.61E+OO 563.99 0.49 2.46E+OO 5.58E+OO 586.26 0.46 4.lOE+OO 9.llE+OO 678.62 0.47 -7.JBE-01 6.83E+OO 688.67 0.86 -2.59E+OO 3.14E+OO 71 9. 35 0.28 4.33E-01 1.09E+Ol 778.90 12.96 -8.22E-02 1.64E-01 810.45 0.32 -2.32E+OO 7.98E+OO 867.37 4.2 6 -2.37E-01 8.97E-01 919.33 0.43 -7.09E-01 6.55E+OO 964.0 8 14.65 9 .13E-02 2.82E-01 1085.87 10.24 1.89E-01 3.62E-01 1089.74 1. 73 -9.86E-01 2.15E+OO 11 12.07 13. 69 8.90E-0 2 3.22E-01 1 2 12.95 1. 43 5.54E-01 3.05E+00 1249.94 0.19 3.34E+OO 2.16E+Ol 1299.14 1. 63 8. 96E-01 2.19E+OO 1408.01 21.07 3.67E-02 1. 37E-01 1457.64 0.50 3.75E+Ol 2.55E+Ol 1528.10 0.28 -5.61E+OO 9.42E+OO Eu-154 123.07 40.40 -7.02E-03 5.68E-02 5.68E-0 2 247.93 6.89 -5.75E-0 2 3.24E-01 591. 7 6 4.95 -9.94E-0 2 6.lOE-01 692.4 2 1. 78 -3.65E-0 1 1. 72E+OO 723. 3 0 20.06 1.16E-02 1.73E-01 756.8 0 4.52 -3.47E-01 6.67E-01 873.1 8 12.08 -1.76E-01 2.87E-0 1 996.29 10.48 9.67E-02 2.63E-0 1 1004.76 18.01 2.83E-03 1.66E-01 1 2 74.43 34.80 7.58E-0 2 1.2 9E-01 3/29/2017 12:49:59PM Page 6 of6 Analysis Report for 29-Mar-17-10030 L3-10205A-FRQC-013CV Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCUgrams) (pCi/grams)

Eu-154 1596.48 1. 80 4.75E-01 5.68E-02 1.77E+OO Eu-155 45.30 1. 31 -2.1 4E+OO 1.04E-0 1 6.52E+OO 60.01 1.22 -4.89E-01 6.15E+OO 86.55 30.70 -2.91E-02 1.04E-01 105.31 2 1.10 -2.00E-02 1.23E-01 Ra-226 186.2 1 3.64 -3.55E-01 6.1 5E-01 6.15E-01 Pa-231 2 7.36 10.30 O.OOE+O O 7.43E-02 7.43E-02 283.69 1. '7 0 -2.78E-0 2 1. 31E+OO 300.07 2.47 -8.85E-01 9.20E-01 302.65 2.20 4.14E-01 9.79E-01 330.06 1. 40 -6.21E-01 1.80E+OO U-235 143.76 10. 96 1. 27E-02 3.99E-02 2.00E-01 163.33 5.08 -8.62E-0 2 3.57E-01 185. 71 57.20 4.99E-03 3.99E-02 2 02 .11 1. 08 5.42E-02 1.81E+OO 2 05.31 5.01 -3.59E-01 4.21E-01 Am-2 4 1 59.54 35.90 -2.83E-02 2.06E-0 1 2.06E-01 + = Nuclide identified during the nuclide identification = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level

• 60 55 50 45 40 35 1000 2000 ROI Type: 1 3000 0000002636.CNF 4000 channel 5000 Live Time :600.000 sec Real Ti11e : 600 .390 sec Start: 1: -0.0(keV)

Stop : 8192:2047

.S(keV) Acq. start :wed Mar 29 12: 39: 50 2017 6000 7000 8000

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