ML14143A269

Transmittal of Letter from David R. Vasbinder Responding to Letter Dated 05/22/2014 and Complete Enercon Survey Packages for Survey Unit BBC-200-1 and ADM-000-5

ML14143A269
Person / Time
Site:	University of Buffalo
Issue date:	05/22/2014
From:	Vasbinder D University of Buffalo
To:	Document Control Desk, NRC/FSME
References
Download: ML14143A269 (52)

Text

Umnhvuuh at ESeifl.The State University of New York Environment, Health & Safety Services May 22, 2014 Docket 50-57 License R-77 U.S. Nuclear Regulatory Commission ATTN: Document Control Desk Washington, D.C. 20555 -0001

Dear Sir or Madam:

Enclosed please find the following documents: " Letter dated May 22, 2014 from The University's Decommissioning Management Contractor Enercon to Mr. Dave Vasbinder detailing supplemental information and data to address comments provided by ORISE and the N.R.C. regarding building release surveys performed at the University at Buffalo's Buffalo Materials Research Center to prepare the building for demolition." Complete Enercon Survey Packages for Survey Unit RBC-200-1 and ADM-000-5.

We have also provided courtesy copies of this information to our Project Manager, Ted Smith and Region 1 Inspector, Steve Hammann as well as to ORISE.If you have any questions or wish further information, please contact me at (716) 829-3301.SincerelYQfja David A bZnder Director, Buffalo Materials Research Center Cc: Ted Smith, U.S.N.R.C.

Project Manager Steve Hammann, NRC Region 1 Nick Altic, ORISE OENERCON Excellence-Every project. Every day.May 22, 2014 GEW-P14-005 Mr. Dave Vasbinder Associate Director Environment, Health, and Safety Services BMRC The State University of New York University at Buffalo 220 Winspear Avenue Buffalo, NY 14215-1034 Re: BMRC Demolition Surveys Mr. Vasbinder; This letter provides additional documentation to address specific comments provided by ORISE and NRC to the University at Buffalo (SUNY) regarding the building release surveys performed at the BMRC to prepare the building for demolition.

This information supplements the data submitted by letter on May 16, 2014. Based on the results provided with this letter, it is concluded that the building has met the release criteria in the Final Status Survey (FSS) Plan, the Decommissioning Plan, and MARSSIM guidelines.

Remediation of Areas Identified by ORISE ORISE questions on further remediation are focused on two specific locations.

These two locations, identified by ORISE at the time of their site visit, were remediated immediately upon being identified to ENERCON and LVI.MARSSIM Statistical Assessment of Survey Units Three survey units were assessed during scans and surveys using the release criteria of 1,000 dpm/100cm 2.These survey package units are RBC-200-1, RBC-201-1, and ADM-000-5.

This release criteria is the appropriate selection for areas impacted with a beta-emitting radionuclide (Sr-90). Two of these survey package units have individual readings that exceed 1,000 dpm/100cm 2 (two measurements for RBC-200-1 and four measurements for ADM-000-5).

The third survey unit (RBC-201-I) has no individual readings that exceed 1,000 dpm/l00cm2.

Statistical analysis for RBC-200-1 and ADM-000-5 is based on the Sign Test, since the radionuclide in question is not present in the background.

Statistical analysis documentation has been added to each survey package unit immediately behind the radiological survey report. The Sign Test statistical analysis confirms that both survey package units pass the criteria.

As stated to ORISE in our discussion, measurements are based on the use of the Co-60 efficiency rather than the Sr-90 efficiency to provide conservatism.

GEW-PI 4-005 May 22, 2014 Page 2 of 2 Conclusion ENERCON's actions have addressed the items noted by ORISE. Revised data packages are attached as verification of this process. Based on the results in these attached MARSSIM survey packages, we have concluded that the building has met the FSS release criteria in the FSS plan, the decommissioning plan, and the methodology specified in MARSSIM.Sincerely, Gerald E. Williams, P.E.Manager, Environmental Services Group Frank Brown Project Manager Enclosures cc: Robert Weller 4490 Old William Penn Highway Murrysville, PA 15668 phone 724.733.8711 fax 724.325.6383 enercon.com Enercon Services Inc.Survey Package Building:

Administration Survey Unit #: ADM-000-5

[ Page 1 of 5 Classification:

S Class I -Impacted E3 Class 2- Impacted El Class 3 -Impacted Survey Type: El Characterization

[ Demolition 13 Final Status Survey 3 Applicable Nuclides of Concern: Nuclide SEE SPECIAL SURVEY INSTRUCTIONS SECTION Release Limit 1,000 (dpm/1OOcm 2)Investigation 750 (dpm/100cm 2)Level Applicable Survey Unit Surfaces:

% of Surface Requiring Scan Surveys" Floors El10% []50% [100% o EN/A" Lower walls El 10% [1 50% Z100% E] N/A[E Upper walls E3 10% E150% [] 100% ZN/A Z Ceilings E1 10% E150% 100% E- N/A E3 Structures (Permanent Furnishings)

Interior and Exterior Surfaces 13 10% E3 50% [1 100% [D N/A Required Survey Measurement Static Scan Rate Instrument Typical Instrumentation Type Count Time Efficiencies Based on: MDA(dpm)I probe EL-2360/43-93 Beta/Gamma 1 Minute width Tc-99 N/A 612 per/sec ZASC 950 Alpha/Beta 1 Minute N/A Th-230 Tc-99 Alpha- 25 Beta- 150 A Planchet Counter shall be used for analysis of any required removal contamination measurements.

See General Survey Instructions Item #7.Since this instrumentation is non-nuclide specific (gross measurements), the applicable efficiency and DCGLI values have been selected based on the most limiting nuclides of concern for the survey unit.ADM-000-5

/ Page 1 of 25 Enercon Services Inc.Survey Package General Survey Instructions:

ADM-000-5 I Page 2 of 5 1. Perform scan surveys of the required surface area at the prescribed scan rates. If less than a 100% scan is required, use professional judgment to select the areas scan surveyed.

Select areas with the highest probability to contain residual activity (i.e., areas of known radionuclide usage, floor traffic pathways, cracks and/or crevices not easily cleaned, countertop workspaces, storage locations, stained or water spotted areas, or areas with a known history of contamination).

2. If elevated activity is detected during the scan surveys, then establish the extent (size) of the contaminated area(s) and mark the affected area(s) and quantify the activity by taking static measurements of the affected area(s). Notify the Project Manager or designee of the type, amount, and extent of any contamination.

3. Document all scan survey results on the applicable survey maps and data results sheets.4. The established number of static measurement locations needed for the statistical evaluation of this survey unit is 14. However, due to statistical and geometrical considerations, the actual number of locations may vary. In this case, collect the actual locations provided on the survey map whether this number is greater than or less than 14.5. Locate and mark the required static measurements locations using the survey map(s). Survey maps with sufficient detail to measure and locate all of these locations have been provided.6. Collect all required static measurements and document the results on the associated data results sheets.Additional static measurements may be taken in suspect areas at the discretion of the Project Manager or survey technician.

However, these additional locations are not included in the analysis of the statistical sample set.7. Removable contamination measurements (swipes) shall be performed at the established measurement locations and counted on a planchet counter accounting for alpha/beta contamination.

8. Notify the Project Manager or designee if elevated activity is detected by any of the static measurements or applicable removable contamination measurements.

9. Ensure that all package information is completed and signed prior to turning in this Survey Package to the RSO or designee for review.Special Survey Instructions:

NUCLIDES:

Co-60; Cs-137; Ag-108; Eu-152; Eu-154; Ni-63; Sr-90 Floor and wall data from the post-decontamination survey will be used in place of the computer generated points resulting in 16 wall points and 12 floor points. These 28 points replace the 14 points on the list.ADM-000-5

/ Page 2 of 25 Enercon Services Inc.Survey Package Location Code Description ADM-000-5 I Page 3 of 5 A unique location code shall be assigned to each individual survey location to ensure proper data management of the survey results. The following format shall be used to ensure consistency throughout the final status survey process: BBB-RRRR-SS-M-LLL Where: BBB = Building or area code. This field represents the facility area. This will be the building number of an assigned area number. (3 characters)

RRRR = Survey unit ID code. This field represents the survey unit i.e. 2-01, 2-02 etc. (up to 4 characters).

Building system survey units (i.e. ventilation systems, drain systems, or vacuum systems) are assigned unique 4-digit numbers that are consistent with the building section and floor. (up to 4 characters)

SS = Structural surface code. This field represents the structural surface such as floor, wall, ceiling, etc. and the surface division code. For example, if a room has a very large floor area, it may be divided into two or more divisions and each section would be assigned unique codes such as Fl, F2, and so on. Walls may be divided on a frequent basis. If only one surface area is identified for a particular survey area, then the default number will be "I" (e.g., WI, Fl, etc.). (2 characters)

M = Structural material code. This field represents the type of structural material on which a particular measurement is taken. This field is usually used to track and assign specific material natural background levels. If not material background value is to be assigned, the default character shall be"M." (I character)

LLL = Numerical identification number. This field represents the survey point assigned numerical identifier.

The field "001" means survey point location number 1. Numerical identifiers shall not be duplicated within the same survey unit. (3 characters) 1)4 Prepared By: Reviewed By: Date: e__W__Name/Signature Frank Brown Date: /1/' +5 Package Complete: Printed Name" ignature ADM-000-5

/ Page 3 of 25 Enercon Services Inc.Survey Package Building:

Administration Survey Unit #: ADM-000-5 Page 4 of 5 Before Beginning Surveys Examine the area to ensure no hazards are present. Verify that all radiological instrumentation intended for use is source checked, in calibration, and operating properly.Identify any area within a given survey unit where contamination has been measured, even if less than the release guidelines.

Survey Technician(s):

R Boczar Floor Survey -Completed in accordance with the survey package EN/A[ Beta Scan Date Completed 10/1/13 Initials RB Step #1 E] Alpha Scan Date Completed N/A Initials N/A (D Beta Static Date Completed 10/1/13 Initials RB El Alpha Static Date Completed N/A Initials N/A[ Smears Date Completed 10/1/13 Initials RB Lower Wall Survey -Completed in accordance with the survey package EN/A[ Beta Scan Date Completed 10/1/13 Initials RB Step #2 El Alpha Scan Date Completed N/A Initials N/A[D Beta Static Date Completed 10/1/13 Initials RB E] Alpha Static Date Completed N/A Initials N/A[ Smears Date Completed 10/1/13 Initials RB Upper Wall Survey -Completed in accordance with the survey package E N/A El Beta Scan Date Completed Initials Step #3 El Alpha Scan Date Completed Initials El Beta Static Date Completed Initials[] Alpha Static Date Completed Initials 0I Smears Date Completed Initials ADM-000-5

/ Page 4 of 25 Enercon Services Inc.Survey Package Building:

Administration Survey Unit #: ADM-000-5 Page 5 of 5 Ceiling Survey -Completed in accordance with the survey package EN/A[ Beta Scan Date Completed 10/1/13 Initials RB Step #4 E] Alpha Scan Date Completed N/A Initials N/A Z Beta Static Date Completed 10/1/13 Initials RB El Alpha Static Date Completed N/A Initials N/A[ Smears Date Completed 10/1/13 Initials RB RAM Use and Storage Areas -Completed in accordance with the survey package (benches, countertops, sinks, and hoods)Z N/A El Beta Scan Date Completed Initials Step #5 El Alpha Scan Date Completed Initials El Beta Static Date Completed Initials El Alpha Static Date Completed Initials El Smears Date Completed Initials Penetrations, Drains, and Openings Survey -Completed in accordance with the survey package Step #6 [ N/A El Smears Date Completed Initials ADM-000-5

/ Page 5 of 25

AL SUIRVEY REPORT n..ma. ofo£y oOtlf u35I , olomA140114 LOW", lo NyLe mbm, 11 au. fw Des "Goo. W,.h As m I loop "" goa lietjw ftas~m mmEt"osf ilk" f ~ GK 111113 S .. 1 LL M L4 2m 43-" 125 a 1 4.6% 134 102 4AI%_ _ A 100......JU~in........

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Page 6 of 25 RADIOLOGICAL SURVEY REPORT 38pwlowDomtmeW FeM A911460- tWWW lomww, tol 3mmbm011101-

• • 03 no 1!0"" sillow */A4. VIA 1 1______ 8&1% 24 so 2&% 13n lo&%i=123114211 -ts 1 1 44% 134 in3 4A% 3*3 3hml 100-~dps UpUI w DPUI om um P D Gým -, aml mAp 0. not% 8______________________________

n ~ CPU IS0SmS (11 0 CPU lO0mS 41 100=3 m 0. GI3. 2O.2 CPU love" ml Wm 1. cmU 1. inCPU b 3m n 0D-3t.41 .1m___ __ 3___ _ 9_A_4__yA:7___

-2 "A 7510 ANK44mikU463 0 mD -3 72 mm 704 MA 7 ] 7-S 0n~~~ _ _ _210 104 16 IA 7-5 I£su-oops-v U-earn _____ __3_ __ __ 43_ __ log HD_12__o MI 3..0"44 0U ounl .3 57 mm -1 W&im AUDA x .i.*SItoasý AM COWst 4WSl ý I M- -.tmk roate4.2042 ADM-000-5

/ Page 7 of 25 Survey Package ADM-000 Unit 5 Surface Sign Test Summary Survey Package: ADM-000 Survey Unit: 05 Evaluator:

Todd Brautigam DCGLw: 1,000 DCGLemc: 2,000 Assumes AF of 2 LBGR: 500 Sigma: 160 Type I error:, 0.05 Type II error: 0.05 Total Instrument Efficiency:

4.3%Detector Area (cm 2): 125 Choosing 'N/A' sets material Material Type:I N/A background to "0" Sign p: 0.96 Calculated Relative Shift: _3.1_Relative Shift Used: 3.0 Uses 3.0 if Relative Shift >3 N-Value: 1 N-Value+20%:

Number of Samples: 28 Median: 104 Mean: 250.Net Static Data Standard Deviation:

612 Total Standard Deviation:

612 Sum of samples and all background Maximum] 1,l618 Adjusted N Value: 28 S+ Value: ........_...._24 Critical Value: 18 Sufficient samples collected:

Pass Maximum value <DCGLw: Max value <DCGLemc Median value <DCGLw: Pass Mean value <DCGLw: Pass Maximum value <DCGLm: Pass Total Standard Deviation

<=Sigma: Due to use of calculated numbers Sign test results: Pass The survey unit passes all conditions:l In Investigations OK -PASS Copy of ADM-000-5 Sign.xis 5/2212014 7:35 AM ADM-000-5

/ Page 8 of 25 A 10 (, R J 1 3 2 4 14 13 Tritium Sample Locations Neutron Level -Admin Bldg 1 K Pit Sample Locations North is Left ADM-000-5

/ Page 9 of 25 I --mmoli O-' ENERCON Excellence-Every projecr. Every day.Radiological Survey Form (Continuation Sheet)Surveyed By: R Boczar Log Number: 01/10/2013-007 I K Tank Room Pit Static/Removeable Locations ADM-000-5

/ Page 10 of 25

.V6 TELEDYNE 01 BROWN ENGINEERING, INC.A Teledyne Technlogies Company 2508 Quality Lane Knoxville, TN 37931-3133 865-690-6819 Frank Brown Enercon 4490 Old William Penn Highway Murrysville, PA 15668 Report of Analysis/Certificate of Conformance 09/23/2013 LIMS #: L56078 Project ID#: EN005-3EUOFB-10 Received:

09118/2013 Delivery Date: 09/25/2013 P.O.#: SUNYUB022 Release #: SDG#: This is to certify that Teledyne Brown Engineering

-Environmental Services located at 2508 Quality Lane, Knoxville, Tennessee, 37931, has analyzed, tested and documented samples, as received by the laboratory, as specified in the applicable purchase order.This also certifies that requirements of applicable codes, standards and specifications have been fully met and that any quality assurance documentation which verified conformance to the purchase order is on file and may be examined upon request.I hereby ce that the above statements are true and correct.Keith Jeter (/7 Operations Manager Cross Reference Table Client ID Laboratory ID Station ID (if applicable) 1 L56078-1 2 L56078-2 3' L56078-3 4 L56078-4 5 L56078-5 6 L56078-6 7 L56078-7 8 L56078-8 Page I of 9 ADM-000-5

/ Page 11 of 25 Afh TELEDYNE P* BROWN ENGINEERING, INC.A Teledyna Technologies Company 2508 Quality Lane Knoxville, TN 37931-3133 865-690-6819 Cross Reference Table Client ID Laboratory ID Station ID (if applicable) 9 L56078-9 10 L56078-10 II L56078-11 12 L56078-12 13 L56078-13 14 L56078-14 15 L56078-15 16 L56078-16 17 L56078-17 18 L56078-18 19 L56078-19 20 L56078-20 21 L56078-21 22 L56078-22 23 L56078-23 24 L56078-24 25 L56078-25 26 L56078-26 27 L56078-27 28 L56078-28 This report shall not be reproduced or distributed except in its entirety.Page 2 of 9 ADM-000-5

/ Page 12 of 25 Report of Analysis TELEDYNE 02114BROWN ENGINEERING, INC.09/23/13 13:47 ATdedyno Technolovles Company L56078 Enercon EN005-3EUOFB-10 Sample ID: I Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number. L56078-1 0PV Activity FUncertainty IRun Aliquot fAliquot Reference Count Count Count FlgVue Radionuclide SOP# Cone 2 Sigma MDC Units # Volume Units Date j Date f Time Units Flag Values H-3 [ 2010 4.78E+00_( 6.56E--+00 9.44E+00 DPM/TOTAL I 1 100 1 % 1 09/20/131 5 R M -Sample ID: 2 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/1812013

% Moisture: LIMS Number: L56078-2 Activity *Uncertainty MC Ran rAliquot I Allquot 1 Reference Count Count Count Rainuld SO# Coe 2Cim Units # I Volume IUnits I Date Date Time Units Flag Values H-3 72010] 9.31E+00 7.23E+00 [ 9.38E+00 1DPM/IOTAL 1_ 100 I _ _ __ 9/2o0 / 3l jJI _M l 1 ]I I Sample ID: 3 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Dale: 09/18/2013

% Moisture: LIMS Number: L56078-3 S Activity Uncertainty Run Aliquot Aliquot Reference 1 Count Count Count Radionuclide SOP# Cone 2 Sigma MDC Units J #n Volume Units Date Date Time j Units j Flag Values H-3 2010 ] 1.62E+01 8.27E+00 9.52E+00 [DPM/TOTAL]

100 J % ] ]09/20/13F 5J M Sample ID: 4 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-4 IActivity

• Uncertainty

{Ruin Aliquot Aliquot 1 Reference Counts Count Count Radionuclide SOP# Cone 2 Sigma MDC Units a Volume Units Date Date I Time Units Flag Values H-3 I 2010] 1.04E+01 7.42E+00 9.42E+00 IDPM/TOTAL_

[ 100 % ] I-09/20/13 1 5 [ M Iu[ Z Flag Values U = Compound/Analyte not detected (< MDC) or less than 3 sigma No = Peak not identified in gamma spectrum+ = Activity concentration exceeds MDC and 3 sigma; peak identified(gamma only) Yes = Peak identified in gamma spcctrum U* = Compound/Analyte not detected.

Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High = Activity concentration exceeds customer reporting value **** Unless otherwise noted, the analytical results reported Spec = MDC exceeds customer technical specification are related only to the samples tested in the condition they L -Low recovery are received by the laboratory.

H = lHigh recovery MDC -Minimum Detectable Concentration Bolded text indicates reportable value.Page 3 of 9 ADM-000-5

/ Page 13 of 25 Report of Analysis TELEDYNE 09/23/13 13:47 BROWN ENGINEERING, INC.Aeledy'no Technologies Company L56078 Enercon Frank Brown EN005-3EUOFB-1 0 Sample ID: 5 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMIS Number: L56078-5 Activity Uncertainty Run Aliquot [ Aliquot Reference I Count Count Count Radionuclide

]SOP# Conc 2 Sigma MDC Units I 1 Volume Units Date Date Time Units I Flag Values 11-3 2010 3.07E+00 6.25E+0 9.39E+00 DPM0TOTAL

.[ 100 _ 7 %1 /7_ 09/20/13_

5 [ M _Ui Sample ID: 6 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-6 Activity Uncertainty i Run Aliquot Aliquot Reference Count Count Count Radionuclide SOP# Cone 2 Sigma MIDC Units # Volume Units Date Date Time j Units Flag Values H-3 7 2010" -2.81E+00[

5.17E+00 9.43E+00 IDPMr/TOTAL

]J Ioloj % 1_, ,109/20/13]

5 M I --I--Sample ID: 7 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

-Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-7 Activity Uncertainty S 1Run Aliquot Aliquot Reference Count Count Count Radionuclide SOP Conc 2 Sigma MDC Units # Volume Units Date Date Time J Units Flag Values H-3 2010 5.60E+00 9A3E+00 DPM/TOTALI i 1 I 09/20/13 5 M U Sample ID: 8 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-8 SP1 Activity Uncertainty Run Aliquot Aliquot Reference count Count count Radionuclide SOPS Conc 2 Sigma MDC Units # Volume Units Date Date j Time Units Flag Values H-3 2010 3.49E+00 6.35E+00 9.44E+00 IDPMiTOTAL

[ 100 [% j 09/20/131 5 [ M [U " Flag Values U = Compound/Analytc not detected (< MDC) or less than 3 sigma No = Peak not identified in gamma spectrum+ = Activity concentration exceeds MDC and 3 sigma; peak identified(gamma only) Yes = Peak identified in gamma spectrum U* = Compound/Analyte not detected.

Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High = Activity concentration exceeds customer reporting value **** Unless otherwise noted, the analytical result reported Spec = MDC exceeds customer teclmical specification are related only to the samples tested in the condition they L = Low recovery are received by the laboralory.

H = High recovery Bolded text indicates reportable value. MDC -Minimum Detectable Concentration Page 4 ot 9 ADM-000-5

/ Page 14 of 25 Report of Analysis brqbh TELEDYNE 09/23/13 13:47 BROWN ENGINEERING, INC.A Teledcne Technoigias Company L56078 Enercon Frank Brown EN005-3EUOFB-10 Sample ID: 9 Collect Start 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number:. L56078-9 So# Activity Uncertainty jRun] Aliquot ] liquot Reference

[Countj Count fCount Radionuclide SOI Cone 2 Sigma MDC Units N Volume j Units Date Date I Time Units Flag Values H-3 ]2010 -2.73E+00 5.18E-+00 9.42-to- [DPMITOTAL

[ 100 % % [ 09/20/13_

5 M I ZUI Sample ID: 10 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-10 ISOPF Activity Uncertainty i I Run Aliquot I AliquotI Reference Count Count r Count Radionuclide SOP Conc 2 Sigma MDC Units I Volume IUnits Date I Date Time Units Flag Values H-3 ,_2010

• 3.60E1+00_]

633E+00 I 9.38E+00 [DPMITO'TALX

ý 100 1 %7 __ __9o/131 -5 _M 1 U I i I I Sample ID: 11 Collect Start- 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-11 T Activity Uncertainty Run Aliquot Aliquot Reference Count[ Count Count Radionuclide SOP# Cone 2 Sigma XDC Units U Volume units j Date Date T Time Units Flag Values H-3 2010 1_3.75E*00 6.398+o00 9.44E+00 DPIrTAl 1 -_ 09/20/13_....

5 [I M lU[ [Sample ID: 12 Collect Start 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number. L56078-12 I I Activity Uncertainty

[rRun Aliquot [Aliquot 1 Reference Count Count Count1 Radionuclide SOP# Cone 2 Sigma MDC Units # Volume Units j Date Date Time. Units Flag Values H-3 T 20101 -6.68E-01 5.58E+00 ( 9.40E+00 DPM/TOTAL I 100 _ _% _ [09/20/131 5 1 M I U I Flag Values U = Compound/Analyte not detected (< MDC) or less than 3 sigma No = Peak not identified in gamma spectrum+ = Activity concentration exceeds MDC and 3 sigma; peak identified(gamma only) Yes = Peak identified in gamma spectrum U* = Compound/Analyte not detected.

Peak not identified, hut forced activity concentration exceeds MDC and 3 sigma High = Activity concentration exceeds customer reporting value **** Unless otherwise noted, the analytical results reported Spec = MDC exceeds customer technical specification are related only to the samples tested in the condition they L = Lov recovery ar received by the laboratory.

H = High recovery Bolded text indicates reportable value. MDC -Minimum Detectable Concentration Page 5 ot 9 ADM-000-5

/ Page 15 of 25 Report of Analysis TELEDYNE 09/23/13 13:47 BROWN ENGINEERING, INC.A Teledyne Technolooies Company L56078 Enercon Frank Brown EN005-3EUOFB-10 Sample ID: 13 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number-. L56078-13 I I Activity Uncertainty ffRunj Aliquot 1Aliquot Reference ICount ICount count1 Radionuclide SOPn Cone 2 Sigma MDC Units Volume Units Date Date Time Units Flag Values H-3 82010 3.0E+00 6.28E+00 9.44E+00 [DPM/TOTAL

[ 100 % 09/20/131 5 1 U IU I Sample ID: 14 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-14 Activity o Uncertainty

[ Run Aliquot Aliquot Reference Count Count Count Radionuclide Son Cone 2 Sg MDC [ Units Volume Units Date Date Time Units Flag Values H-3 32010! 1.54E+00 6.04E+00 9.48E+00 LDP__TOTALI..

100 _ -% _ I09/20/13j 5 [ M I Uj j I Sample ID: 15 Collect Start 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-15 Sn Activity jUncertainty j D Run I Aliquot Aliquot Reference Count Count Count Radionuelide Conc 2 Sigma MDC Units Volume Units Date Date Time Units Flag Values H-3 t2010[ -6.16E-01 5.60E+00 [ 9.42E+00 DPMITOTAL 100 T- [ _ 1 09/20/131 5 [ M I U I I I Sample ID: 16 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-16 Son Activity Uncertainty Run[ Aliquot Aliquot Reference I Count Count Count Radionuclide SOP// Cone 2 Sigma I MDC I Units # Volume Units Date Date Time Units Flag Values H-3 [ 2010 [ -3.25E-01 5.73E+00 [ 9.54E+00 JDPM/TOTAL 100 [ % I I]O/20/ 3 5 [ M [i-i1II I Flag Values U = Compound/Analyte not detected (< MDC) or less than 3 sigma No = Peak not identified in gamma spectrum+ = Activity concentration exceeds MDC and 3 sigma; peak identified(gamma only) Yes = Peak identified in gamma spectrum U* = Compound/Analyte not detected.

Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High = Activity concentration exceeds customer reporting value **** Unless otherse noted, the analytical results reported Spec = MDC exceeds customer technical specification are related only to the samples tested in the condition they L = Low recovery are received by the laboratory.

H = High recovery MDC -Minimum Detectable Concentration Bolded text indicates reportable value.Page 6 of 9 ADM-000-5

/ Page 16 of 25 Report of Analysis TELEDYNE I0/331: BROWN ENGINEERING, INC.09/23/13 13:47 AT Trhthbies Cmpanv L56078 Enercon Frank Brown EN005-3EUOFB-10 Sample ID: 17 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

%Moisture:

LIMS Number: L56078-17 Activity Uncertainty fRun Aliquot Aliquot Reference Count Count Count Radionuclide SOP# Cone 2 Sigma MDC Units 7 Volume Units Date Date Time Units Flag Values 11-3 2010 1.23E+00 I 6.04E+00 9.58E+-00 DPM1TOTAL 100 % 1 1o 9/20131 5 F M n !Sample ID: 18 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-18 ISOPI Activity jUncertainty 1 C I Units RunI Aliquot Aliquot I Reference Count Count Count 1 Radionuclide I Cone 2 Sigma MDU # Volume Units Date Date Time Units Flag Values H-3 J 2010 I -9.43E-01

] 5.57E+00 1 9.48E+00 IDPMITOTALI 1 100 ] % I[ =90_ 131 .5 1 M Ur ITO Sample ID: 19 Collect Stait 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

-% Moisture: LIMS Number: L56078-19 Activity Uncertainty Run Aliquot Aliquot Reference 1 Count f Count Count Radionuclide 2Sigma j MDC Units # Volume j Units Date Date Time Units Flag Values H-3 ] 2010 [ 1.88E-01 5.76E+00 9.43E+00 DPMITOTAL

] 100 % I 09/20/13F 5 L M [U[ [I Z Sample ID: 20 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-20 S Activity Uncertainty MDC Run Aliquot , Aliquot Reference

ý Count Count Count Radionuclide Coe Units Date Date Time Units Flag Values_H-3 I2010 1 2.2613+00

[ 6.28E+00 T 9.68E+00 IDPM(TOTALI 1 100 % 109/20/13[

5 M I U Flag Values U = Compound/Analyte not detected (< MDC) or less than 3 sigma No =Peak not identified in gamma spectrum+ = Activity concentration exceeds MDC and 3 sigma; peak identified(gamma only) Yes ý Peak identified in gamma spectrum U* = Compound/Analyte not detected.

Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High = Activity concentration exceeds customer reporting value **** Unless otherwise noted, the analytical results reported Spec = MDC exceeds customer technical specification arc related only to the samples tested in the condition they L = Low recovery are received by the laboratory.

H = High recovery Bolded text indicates reportable value. C -Minimum Detectable Concenuation Page 7 of 9 ADM-000-5

/ Page 17 of 25 Report of Analysis TELEDYNE 0 3 3 BROWN ENGINEERING.

INC.09/23/13 13:47 ATeledyne Company L56078 Enercon Frank Brown EN005-3EUOFB-10 Sample ID: 21 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture:*LIMS Numnber: L56078-21 F Activity Uncertaintycn 2 iga Ru Aliquot Aliquoti Reference ICount l Count Count'Dt Radionuclide SOP# Con 2 Sigma MDC Units i# Volume Units Date Time' Units Flag Values H-3 2010 -2.78E+o0 5.27E+00 9.sE+oo IDPMTOTAL I 100 % 1 09120/131 5 M U Sample ID: 22 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L,56078-22 Activity Uncertainty 1 u Aliquot Aliquot Reference Count Count Count Radionuclide SOPN Cone 2 Sigma MDC Units u#n Volume Units Date Date Time Units Flag Values H-3 120101 3.79E+00 6.4E49+00 09.51"0 ]DPM/TOTALI 1 100 1 % I _ 09/20/131

-5 ] M I U I l [Sample ID: 23 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09118/2013

% Moisture: LIMS Number. L56078-23 I Activity Uncertainty 1 1 Run Aliquot Aliquot Reference

[ Count Count Count Radionuclide SOPN Cone MDC Units i Date Date Time Units Flag Values Sml-3 I 2010 -3.06E+00 6.23E00 9.37E1+00 1DPMwrOTAL

--.I [ 1300 I % 109120/13-5

] M UI I I Sample ID: 24 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-24 SOP Activity 1 Uncertainty 1 1 n Rus i Aliquot Aliquot Reference

[ Count Count CountI Radionuclide Cone 2 Sigma MDC Units Volume Units Date Date Time Units Flag Values H-3 ] 2010 ] -1.22E+00 I 5.55E+00 ] 9.53E+00 IDPM/rOTAL I -10 I--.l 109/20/131 5[ M 10I 0 ]Flag Values U -Compound/Analyte not detected (< MC) or less than 3 sigma No = Peak not identified in gamma spectrum+ = Activity concentration exceeds MDC and 3 sigma; peak identified(gamma only) Yes = Peak identified in gamma spectrum U* = Compound/Analyte not detected.

Peak not identified, but forced activity concentration exceeds MEDC and 3 sigma High = Activity concentration exceeds customer reporting value *** Unless otherwise noted, the analytical results reported Spec = MDC exceeds customer technical specification are related only to the samples tested in the condition they L = Low recovery are received by the laboratory.

H = High recovery H = 1ligh=ver MDC- Minimum Delectable Concentration Bolded text indicates reportable value. Pag 8 Minmum Detectable Concentrotio5 Page 8 of 9 ADM-O00-5

/ Page 18 of 25 Report of Analysis TELEDYNE 09/23/13 ayis'r o BROWN ENGINEERING, INC.09/23/13 13:47 A Teledvie Ta che.l.es L56078 Enercon Frank Brown EN005-3EUOFB-10 Sample ID: 25 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-25 Activity Uncertainty Run Aliquot Aliquot Reference Count Count Count F Radionuclide SOP# Cone 2 Sigma MDC Units # Volume Units Date Date Time f Units Flag Values H-3 2010 -7.OOE-01 5.85E+00 9.85E+00 DPMtTOTAL I 100 1 % 69712/1 5 m Sample ID: 26 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-26 1 Activity IUncertainty 11-Rn Aliquo Aliquot Reference Count 1Ion on Radionuclide SOP# Cone 2 Sigma MDC Units { Volume Units Date Date Time Uni Flag Values H-3 1 2010 5.0E-1 591E+00 9.61E+00 ]DPM/OTALI 100 ] % 1 _09/20/131 5 1 K M j U IZ Sample ID: 27 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number-. L56078-27 1 Activiy lUncertainty]

Run Aliquot Aliquot Reference CountT Count Count F Radionuclide SOP] Cone 2 Sigma] MDC Units N n Volume Units Date [ Date Time Units Flag Values H-3 ]2010 5.431-01 J 5.90E+00 J 9.55E+00 TDPM/TOTALI 100 ] 09/_20/13 5 M U Sample ID: 28 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-28 Actviy Uneraity ~ 41n Aliquot Aliquot 1 Reference ICountT Count [Count Radionuclide SOP# Cone 2 Sigma MDC Units Volume Units. Date Date Time Units Flag Values H-3 ] 2010 ] 1.03E+00 J 5.98E+00 ] 9.54%1+00 jDPM/TOTALJ 100 ] % [ 09/20/131 M U Flag Valucs U = Compound/Analyte not detected (< MDC) or less than 3 sigma No = Peak not identified in gamma spectrum+ = Activity concentration exceeds MDC and 3 sigma; peak identified(gamma only) Yes = Peak identified in gamma spectrum U* = Compound/Analyte not detected.

Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High = Activity concentration exceeds customer reporting value **** Unless otherwise noted, the analytical results reported Spec = MDC exceeds customer technical specification are related only to the samples tested in the condition they L = Low recovery are reecived by the laboratory.

H = High recovery MDC -Minimum Detectable Concentration Bolded text indicates reportable value.Page 9 of 9 ADM-O00-5

/ Page "19 of 25 QC Summary Report for EN005-3EUOFB-10 09/23/2013 13:47 L56078 ,I. bTELEDYNE:

F- BROWNGI,,NE l ING-A Teledyne rTchna{olloe Company H1-3 Method Blank Summary TBE Sample ID Radionuclide Matrix Count Date/Time Blank Result Units Qualifier P/F WG16294-1 H-3 WO 09/20/2013 14:45 <4.250E+00 pCi/Total U P WG16299-1 H-3 WO 09/20/2013 19:36 < 4.240E+00 pCi/Total U P LCS Sample Summary TBE Sample ID Radionuclide Matrix Count Date/Time Spike Value LCS Result Units Spike Recovery Range Oualifier P/F WG16294-2 H-3 WO 09/20/2013 14:54 5.05E+02 5.050E+02 pCi/Total 100.0 70-130 + P Spike ID: 311-041706-1 Spike Conc: 5.05E+02 Spike Vol: 1.00E+00 WG16299-2 H-3 WO 09/20/2013 19:45 5.05E+02 4.830E+02 pCi/Total 95.7 70-130 + P Spike ID: 3H-041706-1 Spike Conc: 5.05E+02 Spike Vol: 1.OOE+00 U P F NE Positive Result Compound/analyte was analyzed, peak not identified and/or not detected above MDC< 5 times the MDC are not evaluated Nuclide not detected Spiking level < 5 times activity Pass Fail Not evaluated Page I ADM-000-5

/ Page 20 of 25 QC Summary Report for EN005-3EUOFB-10 09/23/2013 13:47 L56078 AWI&T-EL WYNNE BROWN. EfNG(NEEfRING A Teledyne Teiihnalo~es Caom"pany U-3 LCSD Sample Summary TBE Sample ID Radionuclide Matrix Count Date/Time Spike Value LCSD Result LCSD Recovery Units RPD Oualifier P/F WG16294-3 H-3 WO 09/20/2013 15:03 5.05E+02 4.940E+02 97.9 pCi/Total 2.1 + P WGI 6294-2 Spike ID: 3H-041706-I Spike Conc: 5.05E+02 Spike Vol: 1.00E+00 WG16299-3 H-3 WO 09/20/2013 19:55 5.05E+02 4.950E+02 98.1 pCi/Total 2.5 + P WG 16299-2 Spike ID: 3H-041706-1 Spike Cone: 5.05E+02 Spike Vol: I.OOE+O0 U F NE Positive Result Compound/analyte was analyzed, peak not identified and/or not detected above MDC< 5 times the MDC are not evaluated Nuclide not detected Spiking level < 5 times activity Pass Fail Not evaluated Page 2 ADM-000-5

/ Page 21 of 25 W t TELEDYNE-QC Summary Report for L56078 BROVV.N ENG!NEERING EN005-3EUOFB-10 A Tale dyne Thehnotfofes Company 09/23/2013 13:47 H-3 H-3 Associated Samples for WG16294 Sample Client ID L56078-1 I L56078-2 2 L56078-3 3 L56078-4 4 L56078-5 5 L56078-6 6 L56078-7 7 L56078-8 8 L56078-9 9 L56078-10 10 L56078-11 11 L56078-12 12 L56078-13 13 L56078-14 14 L56078-15 15 L56078-16 16 L56078-17 17 L56078-18 18 L56078-19 19 L56078-20 20+ Positive Result U Compound/analyte was analyzed, peak not identified and/or not detected above MDC* < 5 times the MDC are not evaluated Nuclide not detected*** Spiking level < 5 times activity P Pass F Fail Page 3 NE Not evaluated ADM-000-51 Page 22 of 25 QC Summary Report for ENOO5-3EUOFB-10 0912Y32013 13:47 L56078 W.TELEDYNE.

SBROWN .E.ENGINEERING:

A Teledyne Technotagles Company H-3 H-3 Associated Samples for Sample Client ED L56078-21 21 L56078-22 22 L56078-23 23 L56078-24 24 L56078-25 25 L56078-26 26 L56078-27 27 L56078-28 28 WG16299+U P F NE Positive Result Compoundlanalyte was analyzed, peak not identified and/or not detected above MDC< 5 times the MDC are not evaluated Nuclide not detected Spiking level < 5 times activity Pass Fail Not evaluated Page 4 ADM-000-5

/ Page 23 of 25 L 56o I?Page: I of I Laboratory Information Project #: SUNYUB027 Name: Teledyne Brown Eng COC Number "): SUNYUB027-09162013 Street: 2508 Quality Lane City/State/Zip:

Knoxville.

TN 37931-3133 Excellence-Every project Every day Phone: 865-934-0379 ENERCON P.O.C: Frank Brown Phone: 814-599-0677 e-mail: fbwwnr)enercon,com Sample Analysis Requested (Fill in the number of containers for each test)Project/Site Name: SUY BMRC Z= revaveT (3 Address: Buffalo, NY J;e , .-ZCommnts ci Collected by (print/sign):

T J Keane Note: extra sample isrequired for sample Sample ID sabry) QC"Code t , -o .' specific QC Far cemposites

-indicate star and stop date/time (m12dd-yy) (Idemo)BM11RC-Snsear Sam lea 09-16-13 1300 N P Y N 28 X TATRequested:

Normal: Rush: ASAP speci: Fax ResultS: Yes No Circle Deliverable:

CofA / QC Sunmasy / Lcvel I I Level 2 / Level 3 / Level 4 Remarks: Are there any known hazards applicable to these samples? If so, list the hazards. samole Collection Time Zone Eastern Pacific Central Other Chain of Custody Signatures Sample Shipping and Delivery Details Relinquisbed BY(Siwed Date Time a c -ed by (signed) Date Time 1 ,, VLaboratory PM: Rebecca Charles 2 ,1010,b Metbod ofShipment Fed-X Date Shipped: 09/17/2013 2 2 Airbil M:_3 Airbill #: 1.) fCh t ody Nmber=Seep V For Lab Receiving Use Only 2.) QC Codes N -Nw.nl Sample. Tat -Tri Blamk. FD -Field Duplicate ED -Equipment Blank. MS Metrix Spike Svipk MSD) Matrix Spike Duplicate SampK G = Cmrb. C = Composite 3.) Preservative Type. HA -Hydraxlilc Acid. NI = Nitric Aci SH -Sodium HFydrrtid.

SA -Sufic Add AA ý Ascorbic Acid. FiX -Hee, ST -Sodium Thinsulfatim, a preservatve is oad leave field Custody Seal Intact?4.) Matrcc Code- DW-DciabtdWiae.

GW-Ocewundaatc.

SW-Sorface Watw. WW-Waste Water. W-Wee.. J.,,-Mbc Liquaid. SO-Sa. SD-Sedimen t.SLSludze..

SS-Slid Wase..O OiL-Fiter.

P-We t.ULine..

F-F.4m, YES NO N-Nanal Cooler Temp: 5.) Sataplk Analds Reqemsted:

Analytical me"-d reqaested L e. 80260,60OB7470A) and oonaines 6at each (Le. 82608 .3. 6010/7474A

-I).wtA21-Zi ADM-000-5

/ Page 24 of 25 09/18/13 14:04 Teledyne Brown Engineering Sample Receipt Verification/Variance Report SR #: SR36574 Client: Enercon Services, Inc. Project #: EN005-3EUOFB-10 LIMS #L56078 Initiated By: JSIMMONS Init Date: 09/18/13 Receive Date: 09/18/13 Notification of Variance Person Notified:

Contacted By: Notify Date: Notify Method: Notify Comment: Client Response Person Responding:

Response Date: Response Method: Response Comment Criteria Yes No NA Comment I Shipping container custody seals present NA and intact.2 Sample container custody seals present NA and intact.3 Sample containers received in good Y condition 4 Chain of custody, received with samples Y 5 All samples listed on chain of custody Y received 6 Sample container labels present and Y legible.7 Information on container labels Y correspond with chain of custody 8 Sample(s) properly preserved and in NA appropriate container(s) 9 Other (Describe)

NA For Hazardous Materials Only: 10 Paperwork shows TBE and shippers name, NA address and phone number 11 Paperwork shows sample quantity NA information ADM-000-5

/ Page 25 of 25 Enercon Services Inc.Survey Package Building:

Reactor Building Survey Unit #: RBC-200-1 I Page 1 of 5 Classification:

Z Class I -Impacted Li Class 2- Impacted El Class 3 -Impacted Survey Type: Li Characterization Z Demolition El Final Status Survey Applicable Nuclides of Concern: Nuclide SEE SPECIAL SURVEY INSTRUCTIONS SECTION Release Limit 1,000 (dpm/1OOcm 2)Investigation 750 (dpm/100cm 2)Level Applicable Survey Unit Surfaces:

% of Surface Requiring Scan Surveys[] Floors El 10% [_ 50% Z 100% LiN/A Z] Lowerwalls EL 10% [_ 50% Z 100% [] N/A[ Upper walls [:] 10% [-150% [L 100% Z N/A Li Ceilings 0i 10% Ei 50% [L 100% Z N/A EL Structures (Permanent Furnishings)

Interior and Exterior Surfaces El 10% Li 50% [L 100% Z N/A Required Survey Measurement Static Scan Rate Instrument Typical Instrumentation Type Count Time Efficiencies Based on: MDA(dpm)ZL-2360/43-93 Beta/Gamma 1 Minute I probeN width/sec Tc9N/61[ASC 950 Alpha/Beta iMinute N/A Th-230 Tc-99 Alpha- 25~ASC950Beta

-150 Z A Planchet Counter shall be used for analysis of any required removable contamination measurements.

See General Survey Instructions Item #7.Since this instrumentation is non-nuclide specific (gross measurements), the applicable efficiency and DCGL, values have been selected based on the most limiting nuclides of concern for the survey unit.RBC-200-1

/ Page 1 of 24 Enercon Services Inc.Survey Package General Survey Instructions:

RBC-200-1 I Page 2 of 5 1. Perform scan surveys of the required surface area at the prescribed scan rates. If less than a 100% scan is required, use professional judgment to select the areas scan surveyed.

Select areas with the highest probability to contain residual activity (i.e., areas of known radionuclide usage, floor traffic pathways, cracks and/or crevices not easily cleaned, countertop workspaces, storage locations, stained or water spotted areas, or areas with a known history of contamination).

2. If elevated activity is detected during the scan surveys, then establish the extent (size) of the contaminated area(s) and mark the affected area(s) and quantify the activity by taking static measurements of the affected area(s). Notify the Project Manager or designee of the type, amount, and extent of any contamination.

3. Document all scan survey results on the applicable survey maps and data results sheets.4. The established number of static measurement locations needed for the statistical evaluation of this survey unit is 14. However, due to statistical and geometrical considerations, the actual number of locations may vary. In this case, collect the actual locations provided on the survey map whether this number is greater than or less than 14 5. Locate and mark the required static measurements locations using the survey map(s). Survey maps with sufficient detail to measure and locate all of these locations have been provided.6. Collect all required static measurements and document the results on the associated data results sheets.Additional static measurements may be taken in suspect areas at the discretion of the Project Manager or survey technician.

However, these additional locations are not included in the analysis of the statistical sample set.7. Removable contamination measurements (swipes) shall be performed at the established measurement locations and counted on a planchet counter accounting for alpha/beta contamination.

8. Notify the Project Manager or designee if elevated activity is detected by any of the static measurements or applicable removable contamination measurements.

9. Ensure that all package information is completed and signed prior to turning in this Survey Package to the RSO or designee for review.Special Survey Instructions:

NUCLIDES:

Co-60; Cs-137; Ag-108; Eu-152; Eu-154; Ni-63; Sr-90 Additional Samples:.14 Tritium Smears RBC-200-1

/ Page 2 o0 24 Enercon Services Inc.Survey Package Location Code Description RBC-200-1 I Page 3 of 5 A unique location code shall be assigned to each individual survey location to ensure proper data management of the survey results. The following format shall be used to ensure consistency throughout the final status survey process: BBB-RRRR-SS-M-LLL Where: BBB = Building or area code. This field represents the facility area. This will be the building number of an assigned area number. (3 characters)

RRRR = Survey unit ID code. This field represents the survey unit i.e. 2-01, 2-02 etc. (up to 4 characters).

Building system survey units (i.e. ventilation systems, drain systems, or vacuum systems) are assigned unique 4-digit numbers that are consistent with the building section and floor. (up to 4 characters)

SS = Structural surface code. This field represents the structural surface such as floor, wall, ceiling, etc. and the surface division code. For example, if a room has a very large floor area, it may be divided into two or more divisions and each section would be assigned unique codes such as FI, F2, and so on. Walls may be divided on a frequent basis. If only one surface area is identified for a particular survey area, then the default number will be "I" (e.g., WI, Fl, etc.). (2 characters)

M = Structural material code. This field represents the type of structural material on which a particular measurement is taken. This field is usually used to track and assign specific material natural background levels. If not material background value is to be assigned, the default character shall be"M." (1 character)

LLL = Numerical identification number. This field represents the survey point assigned numerical identifier.

The field "001" means survey point location number I. Numerical identifiers shall not be duplicated within the same survey unit. (3 characters)

Prepared By: Kurt Myers Reviewed By: T J Keane Package Complete:

Frank Brown Date: //J//Date: Date: A 3 Pr* W~NamcISignature i -IrName/Signmure Pri~i~cd Name/Signature RBC-200-1 I Page 3 of 24 Enercon Services Inc.Survey Package Building:

Reactor Building Survey Unit : RBC-200-1 Page 4 of 5 Before Beginning Surveys Examine the area to ensure no hazards are present. Verify that all radiological instrumentation intended for use is source checked, in calibration, and operating properly.Identify any area within a given survey unit where contamination has been measured, even if less than the release guidelines.

R Boczar Survey Technician(s):

K Myers R Shank Floor Survey -Completed in accordance with the survey package 0 N/A Z Beta Scan Date Completed 03/26/14 Initials RS Step #1 E] Alpha Scan Date Completed N/A Initials N/A Z Beta Static Date Completed 09/30/2013 Initials RB E] Alpha Static Date Completed N/A Initials N/A 0 Smears Date Completed 09/30/2013 Initials RB Lower Wall Survey -Completed in accordance with the survey package[JN/A[ Beta Scan Date Completed 03/26/14 Initials RS Step #2 []Alpha Scan Date Completed N/A Initials N/A Z Beta Static Date Completed 09/30/2013 Initials KM U Alpha Static Date Completed N/A Initials N/A[ Smears Date Completed 09/30/2013 Initials KM Upper Wall Survey -Completed in accordance with the survey package ZN/A El Beta Scan Date Completed Initials Step #3 El Alpha Scan Date Completed Initials El Beta Static Date Completed Initials El Alpha Static Date Completed Initials El Smears Date Completed Initials RBC-200-1

/ Page 4 of 24 Enercon Services Inc.Survey Package Building:

Reactor Building Survey Unit #: RBC-200-1 Page 5 of 5 Ceiling Survey -Completed in accordance with the survey package EN/A E[ Beta Scan Date Completed Initials Step #4 [] Alpha Scan Date Completed Initials El Beta Static Date Completed Initials E] Alpha Static Date Completed Initials EL Smears Date Completed Initials RAM Use and Storage Areas -Completed in accordance with the survey package (benches, countertops, sinks, and hoods)0 N/A E] Beta Scan Date Completed Initials Step #5 El Alpha Scan Date Completed Initials Ei Beta Static Date Completed Initials E] Alpha Static Date Completed Initials 0l Smears Date Completed Initials Penetrations, Drains, and Openings Survey -Completed in accordance with the survey package Step #6 [D N/A El Smears Date Completed Initials RBC-200-1

/ Page 5 of 24 RADIOLOIAL SURVEY REPORT-wm or pamutb aIw suven II.,.. mu I24D1LW am LK 1119126 A bvuýKHWI&I~

h T_ _ J_ ..ý. CAAC 4ef11 jmmn.... 1 LO :UZI= MIA NIA 1 10 52.1% 24 25.1% 352 Tb.. I"*1,00 "0 31512 81183Mj 4VO 129......

1 1 lit 4.V%

• m sno zoo Gým CPU .io:::M XDMS GýC cv. .2 lebis'0 m loe'e cm. 100sgSi 106.ewUI.

1 Rmt mftDwRf XNC-200-1.U4PA4

______ Om____ 6____ 76 km 62 *A RUC-250&4-7.49 4 m 9 MD 4 I 19 1DA 27 IAMA I 33C-S.01.W.404M I_____ .1m____ 0 b 12=3 mm 742VIAMI ca4~W*lW4M I _& 1 JM 4 1 PM W -i. /VMC-2W5.1.W4141

___DA-_6_DA2_11____l IAMA I mmcNw-m.1wu4"1 Rtm____ 142 _____14- 14rM 0dh Rm -3b 15.M14em.W HAVI RD4l.44 050 -Mrn ..43. 81211 mmui 195 IN 35752 -101 w34 A.b lM...4.1A s.AMN&W An 0~t *0*90m i 1* I mim Nm"h Of.1.4.="'-ftamtw Wl 0....1. wafts "Wow to Uam exVwmu~. v.1..lo0t RBC-200-1 I Page 6 of 24 Survey Package RBC-200 Unit I Surface Sign Test Summary Survey Package: RBC-200 Survey Unit: 01 Evaluator:

Todd Brautigam_

DCGLw.: 1,000 DCGLrr.: 2,000 Assumes AF of 2 LBGR: 500 Sigma: 160 Type I error: 0.0 Type II error: 0.05 Total Instrument Efficiency:

4.9%Detector Area (cm 2: 2125 Choosing 'N/A' sets materialT-J== KI/A *ý "w" Maximum value <DCGL,:I to use of calculated numbers Copy of RBC-200-1 Sign.xls 5122/2014 7:36 AM RBC-200-1

/ Page 7 of 24 REACTOR-CTL-SR 90-Lower Surfaces Area: Room 202 Floor Label Type Surface South of A East of A Local Z 1 Systematic Floor 4.2 13.8 -2 Systematic Floor 4.2 7.4 -3 Systematic Floor 4.2 1.0 4 Systematic Floor 9.7 10.6 5 Systematic Floor 9.7 4.2 Area: Room 202 Walls Label I Type Surface Distance from B Local Z S 6-Label 7 I Label Label 9 Label 10 Label 11 Label 12 Label 13 Label I Systematic Type Systematic S Type Systematic S Type Systematic I Type Systematic Type Systematic Type Systematic S Type Systematic Type Wall 1.4 Surface Distance from C Wall 5.4 Surface Distance from C Wall 1.0 Surface Distance from A Wall 0.8 Surface Distance from D Wall 2.7 Surface Distance from D Wall 3.7 Surface Distance from E Wall 1.5 Surface Distance from E Wall 4.9 Surface I Distance from B I E J--E 5.4 Local Z 5.4 Local Z 5.4 Local Z 5.4 LocalI Z 5.4 Local Z 5.4 Local Zý2.51 Lo=al =Z I 5.4 Local Z I i I I I Surface Ditac from.......

14 Systematic Wall 1 0.7 1 5.4 1 Notes: Distances are measured in feet from Reference Point as seen on floor plan drawing.RBC-200-1

/ Page 8 of 24 12 11 D 9 7 Level -SR 90 Lab"urface Sample Locations North is Down RBC-200-1 I Page 9 of 24 AINNO TELEDYNE BROWN ENGINEERING, INC.A Teledyne Technologies Company 2508 Quality Lane Knoxville, TN 37931-3133 865-690-6819 Frank Brown Enercon 4490 Old William Penn Highway Murrysville, PA 15668 Report of Analysis/Certificate of Conformance 09/23/2013 LIMS #: L56078 Project ID#: EN005-3EUOFB-10 Received:

0911812013 Delivery Date: 09/25/2013 P.O.#: SUNYUB022 Release #: SDG#: This is to certify that Teledyne Brown Engineering

-Environmental Services located at 2508 Quality Lane, Knoxville, Tennessee, 37931, has analyzed, tested and documented samples, as received by the laboratory, as specified in the applicable purchase order.This also certifies that requirements of applicable codes, standards and specifications have been fully met and that any quality assurance documentation which verified conformance to the purchase order is on file and may be examined upon request.l that the above statements are true and correct.Keith Jeter 67 Operations Manager Cross Reference Table Client ID Laboratory ID Station ID (if applicable)

I L56078-1 2 L56078-2 3 L56078-3 4 L56078-4 5 L56078-5 6 L56078-6 7 L56078-7 8 L56078-8 Page I of 9 RBC-200-1

/ Page 10 of 24 lVb, TELEDYNE 7* BROWN ENGINEERING, INC.A Teledyne Technologies Company 2508 Quality Lane Knoxville, TN 37931-3133 865-690-6819 Cross Reference Table Client ID Laboratory ID Station ID(ifapplicable).

9 L56078-9 10 L56078-10 11 L56078-11 12 L56078-12 13 L56078-13 14 L56078-14 15 L56078-15 16 L56078-16 17 L56078-17 18 L56078-18 19 L56078-19 20 L56078-20 21 L56078-21 22 L56078-22 23 L56078-23 24 L56078-24 25 L56078-25 26 L56078-26 27 L56078-27 28 L56078-28 This report shall not be reproduced or distributed except in its entirety.Page 2 of 9 RBC-200-1

/ Page 11 of 24 Report of Analysis 7! TELEDYNE 09/23/13 13:47 BROWN ENGINEERING, INC.A Teledyne Technalolies Company L56078 Enercon EN005-3EUOFB-10 Sample IH: I Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number L56078-1 Activity UncertaintyoF Run [ Aliquot [ Aliquot Reference 1 Count Count Count Radionuclid SOP# Cone 2 Sigma LUiVolume Units Date Date Time Units H-3 2010 J 4.78E+00 r 6.56E+00 [ 9.44E+00 jDPMrrOTAL 1 00 ! %_09/20/1_

_ 5 ] M 0U9 ! I Sample ID: 2 Collet Start: 09116/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-2 LMNubrL5082Activity IUncertainty I Run FAiot Aliquot Reference Count [Count1Con Radionuclide SOPN Cone 2 Sigma j MDC Units j # Volume IUnits Date Date Time Units I Flag Values H-3 12010J 9.31E4-00

[ 7.23E+00 [ 9.38E+00 jDPI /TOTAL i O % _ _ _ 09120/13J 5 K4M i 1 U i Sample ID: 3 Collect Start: 09(1612013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

%Moistum: LIMS Number L56078-3 S Activity Uncertainty I Run Aliquot Aliquot Reference Count Count Count Radionuclide SI P# Cone 2 Sigma MDC Units j Volume Units Date Date Time Units Flag Values H-3 12010 l.62E+01 [ 8.27E+00 9.52E+00 DPM OTAL , 100 % 09/201131 5 M ..I +Sample ID: 4 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-4 0# Activity Uncertainty Run Aliquot [Aliquot 1 Reference Count ICount 1Count Radionuclide SOP# Cone 2 Siga MDC Units Volume Units Date Date Time Units Flag Values H-3 J2010 [ 1.04E+0l 7.42E+00 [9.42E+00 IDPM/rOTAL.

_ 100 [ % _ _ _ 09/20/13 5 M U Flag Values U = Compound/Analyte not detected (< MDC) or less than 3 sigma No = Peak not identified in gamma spectrum+ = Activity concentration exceeds MDC and 3 sigma; peak identified(gamma only) Yes = Peak identified in gamma spectrum U4 = Compound/Analyte not detected.

Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High = Activity concentration exceeds customer reporting value **** Unless otherwise noted, the analytical results reported Spec = MDC exceeds customer technical specification are related only to the samples tested in the condition they L = Low recovery are received by the laboratory.

H h igh recoveay H tt inicatesre l vMDC -Minimum Detectable Concentration Bolded text indicates reportable value.Page 3 of 9 RBC-200-1

/ Page 12 of 24 Report of Analysis TELEDYNE 09/23/13 13:47 BROWN ENGINEERING, INC.A Teledyne Techntaiaies Conpany L56078 Enercon Frank Brown EN005-3EUOFB-1 0 Sample ID: 5 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-5 A y a U R Aliquot Aliquot Reference Count Count Count Radionuclide SOP# Cone 2 Sigma MDC Units Volume Units Date Date Time Units Flag Values H-3 2010 i 3.07E+00 J 6.25E+00 5 9.39E'O0 DPM/TOTAL

[ 1 100 % _. ...09/20/131 5 _M [ U Sample ID: 6 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-6 Activity Uncertainty 1 Run Aliquot Aliquot Reference Count Count Count Radionuclide Cone 2 Sigma MDC Units # Volume Units Date Date Time Units Flag Values I _ M_____ _ -I I___ T ___ 1 1 I__ [____ __1 1_H-3 j2010I -2.81E+00 1 5.17E+00 9.43E+00 IDPMWTOTAL1 100 1 % _6 09/20/13[

5 M I U ] " [IJ Sample ID: 7 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-7 I f Activity Uncertainty T2SgRun Aliquot Aliquot Reference " Count Count Count Radionulide SOP# Coc 2SMDC Units # Volume Units Date Date Time { Units Flag Values H-3 2010 -6.70E-01 3 5.60E+00 j9.43E+00 DPM/TOTAL 100 ] % 3 [09/20/13[

5 [ M U SamplelID:

8 Collect Start: 09/1612013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-8 Activity1 Uncertainty

~Run Aiqo Aliquot Reference Count Count Jcount Radionuclide SOP# Conc 2 Sigma MJDC Units # Volume Units Date Date Time Units Flag Values H-3 [ 2010 [ 3.49E+00 ] 6.35E+00 9.44E+00 [DPWITOTAL I 100 3 % ! j09/20/13 5 [ M U -i Flag Values U = Compowid/Analyte not detected (< MDC) or less than 3 sigma No = Peak not identified in gamma spectrum+ = Activity concentration exceeds MDC and 3 sigma; peak idcntificd(gamma only) Yes -Peak identified in gamma spectrum U* = CompoundlAnalyte not detected.

Peak not identified, but forced activity concentration exceeds MDC and 3 sigma n High = Activity concentration exceeds customer reporting value **** Unless otherwise noted, the analytical results reported Spec = MDC exceeds customer technical specification are related only to the samples tested in the condition they L = Low recovery are received by the laboratory.

H = High recovery Bolded text indicates reportable value. MDC -Minimum Detectable Concentraton Page 4 of 9 RBC-200-1 I Page 13 of 24 Report of Analysis TELEDYNE 09/23/13 13:47 BROWN ENGINEERING, INC.A Teledyne Technologies Company L56078 FEnercon Frank Brown EN005-3EUOFB-10 Sample ID: 9 Collect Start 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-9 I I [ e I. n Activity Uncertainty Run Aliquot Aliquot Reference Count Count Count Radionuclide SOP# Cone 2 Sigma #DC Units Volume Units Date Date Time Units Flag Values H-3 ] 2010 5 -2.73E+00 5.18E+00[

9.42i+_00 DPMITOTAL

[ 100 0920/1 5 M u Sample ID: 10 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-10 ISop# Activity Uncertainty j7 Run Aliquot Aliquot 1 Reference i Cunt Count Count 1 RaIdsulid Flag Values Radionuclide I O#j Cone -Sigma j MODC J Units #t Volume UisJ DateDt Time jUnits FlgVue H-3 ]2010 3.60E1+00 6.33E+00 9-38E+00 ]DPMTOTAL

] [h 100 % 10[9/20/131 5 l M 7 TrlI Sample ID: 11 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-11 1 Activity Uncertainty Run Aliquot Aliquot Reference Count Count Count Radionuclide SOP# Conc 2 Sigma MDC Units j # Volume Units Date Date Time Units Flag Values H-3 ] 20Y10 3.75E+00 j 6.39E+00 9.44E+00 ]DPM/TOTALI j 100 _ % _ 109/2011¶ 5 M U Sample ID: 12 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-12 1 1 Activity Uncertainty 11Run Aliquot Aliquot [ Reference Count count Count Radionuclide SOP# Cone 2 Sigma MDC Units Volume Units Date Date Time Units Flag Values H-3 _ 200 ___6E _ ] 5.58E+00 J 9.40E+00 IDPM/TOTAL1

-100 ] % __o________-M I_ ijj [Flag Values U = Compound/Analyte not detected (< MDC) or less than 3 sigma No = Peak not identified in gamma spectrum+ = Activity concentration exceeds MDC and 3 sigma; peak identified(gamma only) Yes = Peak identified in gamma spectrum U* -Compound/Analyte not detected.

Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High = Activity concentration exceeds customer reporting value **** Unless otherwise noted, the analytical results reported Spec = MDC exceeds customer tchlmical specification are related only to the samples tested in the condition they L = Low recovery arc received by the laboratory.

H = High recovery MDC -Minimum Detectable Concentration Bolded text indicates reportable value.Page 5 of 9 RBC-200-1

/ Page 14 of 24 Report of Analysis TELEDYNE 09/23/13 13:47 BROWN ENGINEERING, INC.A TetedynTeTchnotagies Campany L56078 Enercon Frank Brown EN005-3EUOFB-10 Sample ID: 13 Collect Start 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number:. L56078-13 SActivity 1 Uncertainty 1 f Run Aliquot Aliquot Reference Count Count Count Radionuclide SOP# Cone [ 2 Sigma MDC J Units I #I Volume Units Date j Date Time Units Flag Values H-3 I2010 3.08E+00J 6.28E+00 I 9.44E+00 ]DPM/rOTALI 1 100 ] % _ _ _ 09/20/131 5 1 M IUI I I Sample ID: 14 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-14 Ac ncrait Run Aliquot Aliquot Reference Count Count Count Radionuclide SOP# Cone MI2 Sigma MDC Units # Volume Units Date Date Time Units I Flag Values H-3 _ _2010 _ _1.5413+00

_6.0413+00_

9.48E+00 1DPM/TOTAL i _ 00 3 o"_ _ _ 09/20/13 100 1 1_U___Sample ID: 15 Collect Start: 09116/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-15 T i Activity 1Uncertainty 1Run] Aliquot 1 Aliquot Reference 1 Count Count Count Radionuclide Cone 2 Sigma MDC Units Volume Units j Date Date Time Units Flag Values H-3 I 2010 -6.16E1-01]

5.60E+00 9.42E+00 DPM/TOTAL

-10O6 [7' i 09/20/4131

-5 [ M -[ U Sample ID: 16 Collect Start 09/16/2013 13:00 Marix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-16 Activity Uncertainty1 I Run] Aliquot Aliquot Reference 1 Count Count Count Radionuclide SOP# Cone 2 Sigma Units Volume Units Date Date Time Units Flag Values'1-3 [ 2010 -3.25E-01

] 5.73E+00 ] 9.54E+00 JDPMJTOTAI.

-__[ 100 % "( _0-9/20/131 5 M I u I Flag Values U = Compound/Analyte not detected (< MM) or less than 3 sigma No = Peak not identified in gamma spectrum+ = Activity concentration exceeds MDC and 3 sigma; peak identified(gamma only) -Yes = Peak identified in gamma spectrum U* = Compound/Analyte not detected.

Peak not identified, but forced activity concentration exceeds NM and 3 sigma High = Activity concentration exceeds customer reporting value **** Unless otherwise noted, the analytical results reported Spec = MDC exceeds customer technical specification are related only to the samples tested in the condition they L = Low recovery are received by the laboratory.

H = High recovery MDC -Minimum Detectable Concentration Bolded text indicates reportable value.Page 6 of 9 RBC-200-1

/ Page 15 of 24 Report of Analysis A TELEDYNE 09/23/13 13:47 Jr BROWN ENGINEERING, INC.A Teledyne Technologies Company L56078 Enercon Frank Brown EN005-3EUOFB-10 Sample ID: 17 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-17 Activity Uncertainty Run Aliquot Aliquot Reference Count Count Count1 Radionuclide SOP# Conc 2 Sigma MDC Units N VolumeI Units Date ate Time Units I Flag Values 1-1-3 2010 1 =.23E+00 I 6.04E+00 9.SSE+00 ] DPM/TOTAL 1 100 1 % f _ 09/20/131 5 [M I Sample 1D: 18 Collect Start 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-18 1civt Uncertainty 71Run T Aliquot Aliquot Reference rCount Count rCount Radionuaclide SOP#__ Cone 2 Sim I DC Units # I Volume Units Date Date I Time IUnits Flag Values H-3 D 2010 --9.43E-01 5.57E+00 I 9.48E+00 §DP'r' 1 100 0% 0_131 5 1 M I U_ I I I Sample ID: 19 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-19 SOP# Activity Uncertainty 1 Ut Aliquot1 Aliquot Reference Count Count Count RaincieCone 2 Sigma #n U Volume Units Date Date Time Units Flag Vle H-3 [ 2010 1.88E-01 5.76E+00 1 9.43E+00rj DPM/TTAL I 100 % I T09 =0/13[ 5 [M IU I Sample ID: 20 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-20 Sop I Activity Uncertainty -D Un ts Runj Aliqunot Aliquot1 Reference ICount Count Count FlgVue Radionuclide SOP Cone 2 Sigma MDC Units Volume Units Date Date Time Units Flag Values H-3 i2010_[ 2.26E+00 6.28E+00 1 9.68E&00 DPfIOTALLZ 100 _1./To113 5 I_ _ M I u , I I --Flag Values U = Compound/Analyte not detected (< MDC) or less than 3 sigma No = Peak not identified in gamma spectrum+ = Activity concentration exceeds MDC and 3 sigma; peak identified(gamma only) Yes = Peak identified in gamma spectrum U* = Compound/Analyte not detected.

Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High = Activity concentration exceeds customer reporting value **** Unless otherse noted, the analytical results reported Spec = MDC exceeds customer technical specification are related only to the samples tested in the condition they L = Low recovery are received by the laboratory.

H = High recovery Bolded text indicates reportable value. MDC -Minimum Detectable Concentration Page 7 of 9 RBC-200-1

/ Page 16 of 24 Report of Analysis Ai TELEDYNE 09123113 13:47 BROWN ENGINEERING, INC.A Teledyne Technologios Company L56078 Enercon Frank Brown EN005-3EUOFB-10 Sample ID: 21 Collect Start: 09116/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09118/2013

% Moisture: LIMS Number. L56078-21 S Activity Uncertainty jRun Alquot Aliquot Reference Count Count Count Radionuclide SOP# Cone 2 Sigma MDC Units # Volume Units Date Date Time Units Flag Values H-3 12010 -2.78E+00 I 5.27E+00 j 9.58E+00 IDPM/TOTAL_

100 67 % [09/20/131 5 M ] u Sample ID: 22 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

%Moisture:

LIMS Number: L56078-22 S I Activity IUncertainty 1 Run AliquotR Alquot Reference Count1 Count Count Radionuclide SOP# Cone 2 Sigma MDC Units Volume Units Date 7 Date Time Units Flag Values H-3 12010t 3-79E+00 6.44E+00 I 9.51E+00 ]DPM/TOTAL

[I 100 i % I [ 09/20/131 5 [ NM U]I I Z Sample ID: 23 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 0911812013

% Moisture: LIMS Numnber- L56078-23 SOP# Activity Uncertainty1a n Run Aliquot J Aliquot Reference Count Count Count Radionulide Cone 2 SigM C Units I Volume Units Date Date Time Units Flag Values H-3 1 2010 3.06E+00 6.23E+00 j9.37E+00 jDPM/TOTAL]

1 100 1 % J _ 09/'20/13F 5 -M U[I Ii [Sample ID: 24 Collect Start: 09/16/'2013

[3:00 Matrix: Swipcs (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-24 1 Ctivtye Uncertainty 1 1 Run Aliquot Aliquot Reference Count Cunt [Count Radionuclide SOP# Cone 2 Sigma MDC Units # Volume Units Date Date Time Units Flag Values H-3 I 2010 -i.22E+00

] 5.55E3+00 J 9.53E+-00

]DPM/TOTAL

] 100 I % iOU09/20/13 5 M U Flag Values U = Compound/Analyte not detected (< MDC) or less than 3 sigma No = Peak not identified in gamma spectrum+ = Activity concentration exceeds MDC and 3 sigma; peak idcntificd(gamma only) Yes = Peak identified in gamma spectnum U' = Compound/Analyte not detected.

Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High = Activity concentration exceeds customer reporting value **** Unless otherwise noted, the analytical results reported Spec = MDC exceeds customer technical specification are related only to the samples tested in the condition they L = Low recovery are received by the laboratory.

H = Hfigh recoveny Bolded text indicates reportable value. MDC -Minimum Detectable Concentration Page 8 of`9 RBC-200-1

/ Page 17 of 24 Report of Analysis TELEDYNE Repo1rt/of 137 BROWN ENGINEERING, INC.09123113 13:47 ATeledyne Technologies Comparri L56078 Enercon Frank Brown EN005-3EUOFB-10 Sample [1: 25 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-25 RaincieSp Activity j Uncertainty I I Run Aliquot Aliquot Reference ICount fCount Count1 Radionuclide Cone 2 Sigma MDC Units # Volume Units Date Date Time Units Flag Values H-3 2010 -7.00E-01 1 5.85E+00 9.85E+00 DPMDTOTAL]

J 100 [ % ! 109/2o/13

[ 5 ! M ilU iZ I i Sample ID: 26 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-26 Sop Activity Uncertainty 1_ts 1R 1 Aliquot Aliquot Reference I Count Count Count Radionuclide S Cone 2 Sigma MDC Units # Volume Units Date Date Time Units Flag Values H-3_ _ 2!1J 4.10E-01 ] 5.91E+400 9 0 1DPMnTOTAL]

100 M % _ _ _ 09/20/i3.

MIi Ui [ " ]Sample ID: 27 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number. L56078-27 SI Aliquot Aliqu Count Count Count Radionuclide SOP# Cone 2 Sigma J MDC Units # Volume Units Date Date Time Units Flag Values H-3 ]20.10 5.43E-0F 5.90E+00 9.55E+00 TDPMroTAL. ) 100 __% j09013! 5 [M U Sample ID: 28 Collect Start: 09/16/2013 13:00 Matrix: Swipes (SW)Station: Collect Stop: Volume:

Description:

Receive Date: 09/18/2013

% Moisture: LIMS Number: L56078-28 Activity Uncertainty Run Aliquot Aliquot Reference Count Count Count Radionuclide SOPH Cone 2 Sigma NDC units # I Volume Units Date DteI Time Units Flag Values H-3 2010 [ 1.03E+O0 5.98E+00 9.54E+00 DPM/TOTAL

] 100 ] % 1_ _ 09/20113 5 j M JI L JI Flag Values U = Compound/Analyte not detected (< MDC) or less than 3 sigma No =Peak not identified in gamma spectrum+ = Activity concentration exceeds MDC and 3 sigma; peak identified(gamma only) Yes = Peak identified in gamma spectrum U* = Compoumd/Analyte not detected.

Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High = Activity concentration exceeds customer reporting value =*** Unless otherwise noted, the analytical results reported Spec = MDC exceeds customer technical specification art related only to the samples tested in the condition they L = Low recovery are received by the laboratory.

H = High recovery MDC -Minimum Detectable Concentration Bolded text indicates reportable value. Page 9 of 9 RBC-200-1

/ Page 18 of 24 QC Summary Report for EN005-3EUOFB-10 09/23/2013 13:47 L56078 AI", TELEDYNE BROWN _ NGNEERING A Telidyne 7-rchnofogles Company H-3 Method Blank Summary TBE Sample ID Radionuclide Matrix Count Date/Time Blank Result Units Qualifier P/F WG16294-1 H-3 WO 09/20/2013 14:45 < 4.250E+00 pCi/Total U P WG16299-1 H-3 WO 09/20/2013 19:36 <4.240E+00 pCi/Total U P LCS Sample Summary TBE Sample ID Radionuclide Matrix Count Date/Time Spike Value LCS Result Units Spike Recovery Ranne oualifler P/F WG16294-2 H-3 WO 09/20/2013 14:54 5.05E+02 5.050E+02 pCi/Tota!

100.0 70-130 + P Spike ID: 3H-041706-1 Spike Conc: 5.05E+02 Spike Vol: 1.00E+00 WG16299-2 H-3 WO 09/20/2013 19:45 5.05E+02 4.830E+02 pCi/Total 95.7 70-130 + P Spike ID: 311-041706-1 Spike Conc: 5.05E+02 Spike Vol: 1.00E+00 U F NE Positive Result Compound/analyte was analyzed, peak not identified and/or not detected above MDC< 5 times the MDC are not evaluated Nuclide not detected Spiking level < 5 times activity Pass Fail Not evaluated Page 1 RBC-200-1

/ Page 19 of 24 QC Summary Report for ENOO5-3EUOFB-10 09/23/2013 13:47 L56078 BROW ENI RIN~G A .reledyne Thcthnoto~les Company H-3 LCSD Sample Summary TBE Sample ID Radionuclide Matrix Count Date/Time Spike Value LCSD Result LCSD Recovery Units RPD Oualifier P/F WG16294-3 H-3 WO 09/20/2013 15:03 5.05E+02 4.940E+02 97.9 pCi/Total 2.1 + P WG16294-2 Spike ID: 3H-041706-1 Spike Conc: 5.05E+02 Spike Vol: 1.OOE+00 WG16299-3 H-3 WO 09/20/2013 19:55 5.05E+02 4.950E+02 98.1 pCi/Total 2.5 + P WG16299-2 Spike ID: 3H-041706-1 Spike Conc: 5.05E+02 Spike Vol: I.OOE+00+U P F NE Positive Result Compound/analyte was analyzed, peak not identified and/or not detected above MDC< 5 times the MDC are not evaluated Nuclidc not detected Spiking level < 5 times activity Pass Fail Not evaluated Page 2 RBC-200-1

/ Page 20 of 24 Aw mLTELEDYVNES QC Summary Report for L56078 BTRE N.!EDNGYNEERING EN005-3EUOFB-10 A erde befnotoyfes 09/23/2013 13:47 H-3 H-3 Associated Samples for WG16294 Sample Client ID L56078-1 I L56078-2 2 L56078-3 3 L56078-4 4 L56078-5 5 L56078-6 6 L56078-7 7 L56078-8 8 L56078-9 9 L56078-10 10 L56078-11 1I L56078-12 12 L56078-13 13 L56078-14 14 L56078-15 15 L56078-16 16 L56078-17 17 L56078-18 18 L56078-19 19 L56078-20 20+ Positive Result U Compound/analyte was analyzed, peak not identified and/or not detected above MDC* < 5 times the MDC are not evaluated** Nuclide not detected** Spiking level < 5 times activity p Pass F Fail Page 3 NE Not evaluated RBC-200-1

/ Page 21 of 24 QC Summary Report for EN005-3EUOFB-10 09/23/2013 13:47 L56078 TELEDYN W-BROWN-ýEý

~NINEERINGý A Tletdyne Technologiet Compaeny H-3 H1-3 Associated Samples for Sample Client ID L56078-21 21 L56078-22 22 L56078-23 23 L56078-24 24 L56078-25 25 L56078-26 26 L56078-27 27 L56078-28 28 WG16299 U P F NE Positive Result Compound/analyte was analyzed, peak not identified and/or not detected above MDC< 5 times the MDC are not evaluated Nuclide not detected Spiking level < 5 times activity Pass Fail Not evaluated Page 4 RBC-200-1

/ Page 22 of 24 L 5ýo7?page I of I LEN E Project #: SUNYUB027 Name: Teledyne Brown Eng COC Number "): SUNYUB027-09162013 E Street: 2508 Quality Lane City/State/Zip:

Knoxville, TN 37931-3133 Excellence-Every project Every day Phone: 865-934-0379 ENERCON P.O.C: Frank Brown Phone: 814-599-0677 e-mail: fbm1thenerconcom Sample Analysis Requested t5 (Fill in the number of containers for each test)Project/Site Name: sUNY BMRC ~-Preservattive Type (3)Address: Buffalo, NY Comments Collected by (printlsign):

T J Kcane Note: extra sample is* 4i,,,c teid. required for sam ple Sample ID IMltr) QCc code ) specific QC Fo. composites

-indicate Mart and stop datetime (t-dd-Tyl (1i 14) ie TAT Requested:

Normal: Rush: ASAP Specify: ]IF.Results:

Yes I No Circle Deliverable:

CofA / QCSummary

/ Level I Level2 1 Level,3 / Level4 Remarks: Are there any known hazards applicable to these samples? If so, list the hazards. Sample Colleclion Time Zone Eastern Pacific Central Other -y Chain ofCustady Signatures Sample Shipping and Delivery Details Relinquished By (s Date Time ved by(simed)

[/ Date Time LabortoryPW RebeccaCharles 3 I M e oofShipm ent :ed-X D ate Ship ped: 0 9/17/20 13 22 Aiebill M: 3 Airbil 6'.WOUA-ý2 j.) Chain of~mady Nuebe, -See Procedure VFor Lab Receiving Use Only 2.) QC Cedw. N = Noralen Seacipl.TB Trip Blank. FD -Field Duplieate.

EB -EquimentBlnk MS = Matiex Spike Sampie. VISt) -bauix Spike Diiplieese Snmispk G -Ceob. C -Composite 3.) Presevaive Tym F HA=lyriochlede Acid. NI = Nitric Acdd. 511- Sediumi Hydrnodde, SA -Sulfluic Acid, AA =Ascmbde Ackid, -Z fieuse, ST = Sodiumi TtdoesaLfoe, Wone presaevdve is addted -]caw field blank Cstody Seal Intact?4.) Manicti Codes: DW-Dtobieg Wcait. GW-0roicdwce.

SW dareca Wtec. WW-Weot.Wne..

W-Waern. ML-Misc.iUqsid SO-St.0 STY-edimicat.

SL.Siudse, 354o.Id Wwce.-OOil.O F.Fg.f ae VPIhpa. U-Jim F-F" YES IHO rd-Need Coaler Temp.5..) istieAnlyismepmel.Anltialietbdrepine (c. 566.6tOflba) a cceic iceiniei eeidd cceds(L. 208-3 6t -?473A-.)RBC-200-1

/ Page 23 of 24 09/18/13 14:04 Teledyne Brown Engineering Sample Receipt Verification/Variance Report SR #: SR36574 Client: Enercon Services, Inc. Project #: EN005-3EUOFB-10 LIMS #L56078 Initiated By: JSIMMONS Init Date: 09/18/13 Receive Date: 09/18/13 Notification of Variance Person Notified:

Contacted By: Notify Date: Notify Method: Notify Comment: Client Response Person Responding:

Response Date: Response Method: Response Comment Criteria Yes No NA Comment 1 Shipping container custody seals present NA and intact.2 Sample container custody seals present NA and intact.3 Sample containers received in good y condition 4 Chain of custody received with samples y 5 All samples listed on chain of custody y received 6 Sample container labels present and y legible.7 Information on container labels y correspond with chain of custody 8 Sample(s) properly preserved and in NA appropriate container(s) 9 Other (Describe)

NA For Hazardous Materials Only: 10 Paperwork shows TBE and shippers name, NA address and phone number 11 Paperwork shows sample quantity NA information RBC-200-1

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